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DOE OSTI2025

Freestanding VO 2 membranes on epidermal nanomesh for ultra-sensitive correlated breathable sensors

The interest in highly sensitive sensors is rapidly increasing for detecting very tiny signals for Internet of Things devices. Here, we achieve ultra-sensitive correlated breathable sensors based on freestanding VO 2 membranes. We fabricate the membranes by growing VO 2 films onto sacrificial Sr 3 Al 2 O 6 layer grown on SrTiO 3 , selectively dissolving the Sr 3 Al 2 O 6 in water, and then rendering freestanding VO 2 membrane on nanomesh. The nanomeshes are extremely flexible, sweat permeable, and readily skin-adhesive. The resistance of the VO 2 membranes is reversibly tuned by human’s tiny mechanical stimuli and breath stimuli. The stimuli modulate the Peierls dimerization of one-dimensional V-V chains in the VO 2 lattice which concomitantly controls the electron correlation and hence resistivity. Since our breathable sensors operate based on quantum-mechanical correlation effects, their sensitivity is 1-2 orders of magnitude higher than conventional tactile and respiratory sensors based on other materials. Thus, the freestanding membranes of correlated oxides on epidermal nanomeshes are multifunctional platforms for developing ultra-sensitive correlated breathable sensors.

36 MATERIALS SCIENCE↗

DOE OSTI2023

Smart Manufacturing Pathways for Industrial Decarbonization and Thermal Process Intensification

Rapid decarbonization is fast becoming the primary environmental and sustainability initiative for many economic sectors. Industry consumes more than 30 % of all primary energy in the United States and accounts for nearly 25 % of all greenhouse gas (GHG) emissions. More than 70 % of energy consumed by the industrial sector is related to thermal processes, which are also the largest contributors of carbon emissions, overwhelmingly due to the combustion of fossil fuels. Thermal process intensification (TPI) seeks to dramatically improve the energy performance of thermal systems through technology pillars focusing on alternative energy sources and processes, supplemental technologies, and waste heat management. The impacts of TPI have significant overlap with the goals of industrial decarbonization (ID) that seeks to phase out all GHG emissions from industrial activities. Emerging supplemental technologies such as smart manufacturing (SM) and the industrial internet of things (IoT) enable significant opportunities for the optimization of manufacturing processes. Combining strategies for TPI and ID with SM and IoT can open and enhance existing opportunities for saving time and energy via approaches such as tighter control of temperature zones, better adjustment of thermal systems for variations in production levels and feedstock properties, and increased process throughput. Data collected by smart processes will also enable new advanced solutions such as digital twins and machine learning algorithms to further improve thermal system savings. Herein, this paper examines the individual pathways of TPI, ID, and SM and how the combination of all three can accelerate energy and GHG reductions.

42 ENGINEERING↗

DOE OSTI2020

Self-assembly for electronics

Self-assembly, a process in which molecules, polymers, and particles are driven by local interactions to organize into patterns and functional structures, is being exploited in advancing silicon electronics and in emerging, unconventional electronics. Additionally, silicon electronics has relied on lithographic patterning of polymer resists at progressively smaller lengths to scale down device dimensions. Yet, this has become increasingly difficult and costly. Assembly of block copolymers and colloidal nanoparticles allows resolution enhancement and the definition of essential shapes to pattern circuits and memory devices. As we look to a future in which electronics are integrated at large numbers and in new forms for the Internet of Things and wearable and implantable technologies, we also explore a broader material set. Semiconductor nanoparticles and biomolecules are prized for their size-, shape-, and composition-dependent properties and for their solution-based assembly and integration into devices that are enabling unconventional manufacturing and new device functions.

36 MATERIALS SCIENCE↗

DOE OSTI2022

Material aspects of giga-Hertz ZnO TFTs for wireless systems

Abstract Having enabled high-value application capabilities through mass production of flat-panel displays, X-ray imagers, and solar panels, Large-Area Electronics (LAE) holds potential to open new frontiers in wireless applications for the Internet of Things and 5G/6G, by enabling unprecedented spatial control and power efficiency through large size and flexible form factor of radiative apertures. However, this requires boosting operation frequencies from the traditional limits in the range of 10–100’s of mega-Hertz to multi giga-Hertz. In this paper, we discuss critical device metrics, to characterize zinc-oxide (ZnO) thin-film transistor (TFT) operation frequency for both active (for signal amplification) and passive components in LAE-based circuits and systems. We then describe the key structural and material approaches towards recently demonstrated LAE-based giga-Hertz wireless systems employing ZnO TFTs. Bringing LAE to the giga-Hertz regime provides a path towards flexible and meter-scale monolithic integrated wireless systems. Graphical abstract

Ma, Yue (ORCID:0000000186724090)↗

DOE OSTI2024

Reinforcement Learning as a Parsimonious Alternative to Prediction Cascades: A Case Study on Image Segmentation

Deep learning architectures have achieved state-of-the-art (SOTA) performance on computer vision tasks such as object detection and image segmentation. This may be attributed to the use of over-parameterized, monolithic deep learning architectures executed on large datasets. Although such large architectures lead to increased accuracy, this is usually accompanied by a larger increase in computation and memory requirements during inference. While this is a non-issue in traditional machine learning (ML) pipelines, the recent confluence of machine learning and fields like the Internet of Things (IoT) has rendered such large architectures infeasible for execution in low-resource settings. For some datasets, large monolithic pipelines may be overkill for simpler inputs. To address this problem, previous efforts have proposed decision cascades where inputs are passed through models of increasing complexity until the desired performance is achieved. However, we argue that cascaded prediction leads to sub-optimal throughput and increased computational cost due to wasteful intermediate computations. To address this, we propose PaSeR (Parsimonious Segmentation with Reinforcement Learning) a non-cascading, cost-aware learning pipeline as an efficient alternative to cascaded decision architectures. Through experimental evaluation on both real-world and standard datasets, we demonstrate that PaSeR achieves better accuracy while minimizing computational cost relative to cascaded models. Further, we introduce a new metric IoU/GigaFlop to evaluate the balance between cost and performance. On the real-world task of battery material phase segmentation, PaSeR yields 179% improvement over SOTA MatPhase model and a 196% improvement over IDK Cascades under the IoU/GigaFlop metric. We also demonstrate PaSeR’s adaptability to complementary models trained on a noisy MNIST dataset, where it outperforms all baselines on IoU/GigaFlop by an average of 44%.

Srikshan, Bharat↗

DOE OSTI2022

Cloud-Control of Legacy Building Automation System: A case study

As Internet of Things devices and cloud-based platforms become more mature, Energy Management and Information Systems (EMIS) are increasingly gaining momentum in the building industry. In large commercial buildings, Fault-Detection and Diagnostic (FDD) and energy information systems (EIS) are now established technologies with tens of providers and thousands of deployment sites across North America. The new frontier for the EMIS technology is now represented by control systems that use advanced system optimization (ASO) methods to improve the operations of the HVAC system. Given the complexity of the integration of such systems with the existing building automation systems (BAS) and the higher risk involved with direct control of the HVAC, these systems are still emerging in the market. This paper presents the results of a project in which a start-up company partnered with a research institution to develop a cloud-based software EMIS solution and deployed it in a university campus in California. The software system included advanced sensing, data acquisition, storage and advanced control and analytics applications developed on top of the native BAS. The new platform controls ten buildings on the campus and the FDD and the ASO applications deployed on this platform were able to generate energy savings of up to 35% and 25% in certain buildings for each functionality respectively. Where the platform did not save energy, it improved building service (air quality). Lessons learned include the importance of collaborating with and training the building operators and evaluating whether the legacy system can work reliably with the new technology.

Prakash, Anand Krishnan↗

DOE OSTI2020

5G Enabled Energy Innovation: Advanced Wireless Networks for Science (Workshop Report)

Rapidly expanding, new telecommunications infrastructure based on 5G technologies will disrupt and transform how we design, build, operate, and optimize scientific infrastructure and the experiments and services enabled by that infrastructure, from continental-scale sensor networks to centralized scientific user facilities, from intelligent Internet of Things devices to supercomputers. Concurrently, 5G will introduce, or exacerbate, challenges related to protecting infrastructure and associated scientific data as well as to fully leveraging opportunities related to expanded infrastructure scale and complexity. The U.S. Department of Energy (DOE) Office of Science operates scientific infrastructure, supporting some of the nation’s most advanced intellectual discoveries, spanning the country and including 30 world-class user facilities from supercomputers to accelerators. Along with field experiments and remote observatories, every aspect of DOE’s scientific enterprise will be affected by 5G, which amounts to a complete renovation of the underpinnings of the nation’s information infrastructure. In this report we explore the scientific opportunities and new research challenges associated with 5G, ranging from scalability to heterogeneity to cybersecurity. The rapid commercial deployment of 5G opens the opportunity to rethink and reinvent DOE’s scientific infrastructure and experimentation, from intelligent sensor networks at unprecedented scales to a digital continuum of cyberinfrastructure spanning low-power sensors, high-performance computing embedded within and at the edge of the network, and DOE’s large-scale user instrument and computing facilities. New programming paradigms, workflow and data frameworks, and AI-based system design, operation, and autonomous adaptation and optimization will be necessary in order to exploit these new opportunities. Field deployments and centralized scientific instruments can also be revolutionized, moving (without traditional performance penalties) from wired to wireless connectivity for data and control systems, improving flexibility, and opening new sensing modalities, including the use of the 5G electromagnetic spectrum itself as an environmental probe. For DOE science, in contrast to commercial 5G applications and settings, devices will be deployed in extreme environments such as cryogenically cooled instrument control systems and in remote settings with harsh conditions, requiring the design of new materials for RF communication and edge processing to operate in these regimes. Concurrently, 5G infrastructure comprises both hardware and sophisticated software systems - currently closed and proprietary. The cybersecurity challenges to 5G-empowered reinvention mirror the complexity and variety of new 5G features, from virtualization to private network slices to ubiquitous access. Research is also needed in order to accelerate the development of secure and open 5G software infrastructure, reducing reliance on hardware and software produced outside the United States and providing the transparency and rigorous evaluation and testing afforded through open software. Twelve broad research thrusts are laid out in four chapters, with a companion fifth chapter (and three additional research thrusts) underscoring the needs and opportunities for an aggressive testbed program co-designed by networking experts and scientists involved in the 15 research thrusts. The urgency of undertaking this research is fueled by a global, accelerating deployment of new telecommunications infrastructure that is designed for entertainment and commercial applications - barely scratching the surface of what 5G can do to extend U.S. leadership in scientific discovery.

42 ENGINEERING↗

DOE OSTI2020

5G Enabled Energy Innovation: Advanced Wireless Networks for Science

Digital wireless communication has become a foundational technology for the nation. The U.S. Department of Energy’s Office of Science (DOE-SC) is the Nation’s largest supporter of basic research in the physical sciences discovering new materials, designing advanced microelectronics, and understanding the physics of radio frequency signaling. The expanding national rollout of a new fifth-generation (5G) mobile network, coupled with the torrent of scientific data generated by next-generation devices such as battery-powered Internet of Things (IoT) sensors, has created an urgent need to enhance cutting-edge wireless technology. Breakthroughs in the deployment, integration, security, and operational range of wireless networking can provide new scientific capabilities for the next decade - from autonomous mobile instruments for scientific user facilities to intelligent sensors networks distributed over thousands of kilometers to study environmental processes. To realize this promise, however, we must continue to drive innovations in computing, artificial intelligence (AI), advanced materials, high-speed networking, and microelectronics. In March 2020, the DOE-SC convened a workshop to identify the potential opportunities and explore the scientific challenges of advanced wireless technologies.

42 ENGINEERING↗

DOE OSTI2020

Unattended Dual Current Monitor (UDCM)

Researchers at Los Alamos National Laboratory have developed the Unattended Dual Current Monitor (UDCM). The UDCM is an ideal solution for current measurement needs such as ion chamber gamma measurements. This data acquisition system simplifies hardware requirements for current applications, and provides added reliability, flexibility, and compatibility as compared with the legacy Miniature Gamma Ray and Neutron Detector (MiniGRAND) technology. It is lightweight, can be portable or mounted, is manufactured using COTS parts, and features a modern Internet-of-Things (IoT) enabled design.

46 INSTRUMENTATION RELATED TO NUCLEAR SCIENCE AND ↗

DOE OSTI2020

Facility Cybersecurity Framework Best Practices

Federal facilities are increasingly adopting automation and connecting to the Internet creating an energy-internet-of-things environment that converges operational technology (OT) and information technology (IT). Today's buildings increasingly weave together networked sensors and cyber and physical systems that enable data to be collected, aggregated, exchanged, stored and monetized in new ways. Building technological advances have created new energy technology, services, markets and value creation opportunities (e.g. transactive energy, two-way grid communications, machine learning, and increased use of renewable and distributed energy resources). But as larger data sets are being exchanged at faster speeds between an increasing number of OT systems, it becomes more difficult to protect the security of the data lifecycle and the physical equipment it interacts with. These challenges are especially difficult to overcome because the economic and environmental gain (interoperability, big data, social networks and ubiquitous information sharing) are driving these prominent trends in the digital age. Often cybersecurity is an afterthought. The U.S. Department of Energy’s (DOE) Federal Energy Management Program (FEMP) funded the Pacific Northwest National Laboratory (PNNL) to develop various cybersecurity tools, trainings, and reports to aid federal facility managers – and other building owners and operators – in better applying frameworks and lessons learned from the National Institute of Standards and Technology (NIST) Cybersecurity Framework (CSF), risk management framework (RMF), DOE’s cybersecurity capability maturity model (C2M2), and a wide variety of industry best practices and guidance documents (i.e., NIST 800 series, Department of Defense United Facilities Criteria). This set of tools, collectively known as the FEMP Facility-Related Control System Cyber Toolkit (FRCS Cyber Toolkit)2, is focused on cybersecurity concerns from facility-related control systems and other operational technology (OT), such as industrial control systems (ICS). The FRCS Cyber Toolkit can be applied across six of the sixteen critical infrastructure sectors designated by the Department of Homeland Security, including government facilities, healthcare and public health, commercial facilities (e.g., public assembly, offices, lodging), financial services (e.g., banking and insurance), emergency services (e.g., fire and police stations), and information technology. With increasingly converged IT and OT systems, it is crucial to address OT cybersecurity considerations and assess how the seam of these two systems could impact the overall cybersecurity posture of a facility. The objective of this report is to provide an overview of the best possible method to use FRCS Cyber Toolkit (section 2.0) and distilled cybersecurity best practices for the federal facilities to address growing non-linear cyber threats (section 3.0). Recommendations in this document are aggregated from several NIST and other documents (see Appendix A for additional details).

97 MATHEMATICS AND COMPUTING↗

DOE OSTI2020

Cyber Secure Sensor Network for Fossil Fuel Power Generation Assets Monitoring

The energy sector is undergoing digital transformation which is to say more and more power generation assets have become automated and connected to the internet. The connected sensors can tap into plants to monitor the health of assets and manage fleets remotely. These are just some of the benefits digitalization is bringing to the power industry. Within a power plant, control systems are no longer concerned with one system or one piece of equipment, but rather whole fleet of assets inter-connected with smart sensors which have the function of continuously monitoring and transmitting real-time operational data to operators. These connected systems will form a part of the industrial internet of things (IIoT). The big data scenarios provide benefits of performing system prognostics and optimization which is a key selling point of power plant digitalization.

20 FOSSIL-FUELED POWER PLANTS↗

DOE OSTI2021

Review of Intrusion Detection Methods and Tools for Distributed Energy Resources

Recent trends in the growth of distributed energy resources (DER) in the electric grid and newfound malware frameworks that target internet of things (IoT) devices is driving an urgent need for more reliable and effective methods for intrusion detection and prevention. Cybersecurity intrusion detection systems (IDSs) are responsible for detecting threats by monitoring and analyzing network data, which can originate either from networking equipment or end-devices. Creating intrusion detection systems for PV/DER networks is a challenging undertaking because of the diversity of the attack types and intermittency and variability in the data. Distinguishing malicious events from other sources of anomalies or system faults is particularly difficult. New approaches are needed that not only sense anomalies in the power system but also determine causational factors for the detected events. In this report, a range of IDS approaches were summarized along with their pros and cons. Using the review of IDS approaches and subsequent gap analysis for application to DER systems, a preliminary hybrid IDS approach to protect PV/DER communications is formed in the conclusion of this report to inform ongoing and future research regarding the cybersecurity and resilience enhancement of DER systems.

45 MILITARY TECHNOLOGY, WEAPONRY, AND NATIONAL DEF↗

DOE OSTI2021

An Observational Understanding of Connected Lighting Systems

As part of the Internet of Things (IoT), connected lighting systems provide additional control capabilities and nonlighting-related services (such as communications and data infrastructure) to reduce energy use while increasing both application efficiency and system value. But the positive or negative energy impact of implementing these systems is still largely unknown due to the variety of human factors associated with installation, maintenance, and use. These complications interfere with adoption and acceptance rates of products that will play a significant role in achieving energy savings long-term. Next Generation Lighting Systems, or NGLS, developed and implemented an observational research methodology for connected lighting systems. The methodology was implemented at an indoor (classroom/office) Living Lab at Parsons School of Design in New York City, and an outdoor (parking lot) Living Lab at Virginia Tech Transportation Institute in Blacksburg, Virginia. Although this report focuses on the approach to indoor installations, observational research in both settings provides insight to the type, scale, and frequency of issues across available products as experienced by installing contractors, end users, and other stakeholders.

32 ENERGY CONSERVATION, CONSUMPTION, AND UTILIZATI↗

DOE OSTI2021

Impact of Connected Communities

Buildings account for 35% of CO 2 emissions and almost 40% of the United States’ energy use. High-performance homes and neighborhoods play an important role in supporting efforts to decarbonize the US power system by 2035. Significant reductions in CO 2 emissions within the residential sector can be realized through electrification of loads paired with the flexibility created by leveraging smart Internet of Things (IoT) capabilities to shift energy use based on grid signals, thus improving generation/distribution efficiency and maximizing the use of renewable generation capacity. All of this can be achieved while allowing smart home appliances and equipment to meet homeowner needs – including reducing power bills - while optimizing operation in conjunction with the grid using novel control techniques. The Grid-Interactive Efficient Buildings Roadmap by the US Department of Energy’s (DOE’s) Building Technologies Office (BTO) notes that implementing grid-interactive efficient building (GEB) technology has the potential to reduce CO 2 emissions by 80 million tons/year—roughly equivalent to 17 million cars. To achieve this vision, the US Department of Energy’s Oak Ridge National Laboratory (ORNL)—in collaboration with Southern Company Research & Development, Alabama Power, Georgia Power, BTO and the US DOE’s Office of Electricity (OE) —is developing and demonstrating novel connected communities at two locations. Southern Company in turn engaged with industry partners, including design firms, residential developers, and residential HVAC and appliance manufacturers because their participation would be critical to the success of the initial research project, as well as the future scaling to the Southern Company service territory and beyond. Impacts of the Connected Communities projects in Alabama and Georgia are outlined including: energy, grid services and data management learnings; homeowner feedback; vendor engagement; adoption by utilities; technical, policy and business model challenges.

24 POWER TRANSMISSION AND DISTRIBUTION↗

DOE OSTI2020

Specifying Calibration of Environmental Sensors

The emergence of the Internet of Things is resulting in an increased ability of devices and systems to share data and is generating increasing interest in integrating sensors into a variety of devices deployed in the built environment. The value of such data is a function of how the data can be used. Data-producing devices and systems that enable valuable use-cases in turn can be seen as more valuable. Lighting systems are particularly interesting platforms for integrated sensors. Both indoor and outdoor lighting devices are becoming more connected, and their location is often ideally suited for hosting environmental sensors that can characterize the properties of indoor or outdoor spaces in ways that support a wide variety of use cases, from improving air quality to supporting fault diagnostics and prediction. The value of environmental-sensor-driven use-cases and the lighting systems that house them is dependent to some degree on sensor accuracy. Environmental sensors utilize a wide variety of sensing techniques or technologies and have varying accuracy. More-accurate, laboratory-grade products or reference standards are often used to characterize, refine, calibrate, adjust, and monitor devices that are deployed, or are intended to be deployed, in physical spaces of interest. Sensors or reference standards need to be calibrated periodically to ensure that their use yields accurate measurements. Calibration needs, however, vary in sophistication, based on user and use-case requirements. This paper provides guidance for evaluating the performance of environmental sensors so as to ensure that they meet user or use-case needs. It describes best practices that have been developed for a) calibrating sensors to ensure some known level of accuracy, and b) determining whether calibration-laboratory accreditation meets user or use-case needs. Excerpts from laboratory scopes of accreditation are shared to reveal the diversity of terminology and format among them. In an effort to aid those who currently have sensors calibrated or who have new or changing needs for sensor calibration, rationale is provided for why a specification might be used to request calibration services that meet specific needs. Commercially available calibration-service providers that are accredited for environmental-sensor calibration are compared and contrasted, and a specification template that might be used for requesting this calibration is presented. The specification template should be tailored to meet each user’s needs. To illustrate, an example set of environmental-sensor test conditions (reflecting the planned usage of the device to be calibrated) is used to develop a customized calibration specification, and commercially available service providers are assessed in terms of their qualifications for calibration to that particular implementation of the specification template.

42 ENGINEERING↗

DOE OSTI2021

Facility Cybersecurity Framework Best Practices Version 2.0

32 ENERGY CONSERVATION, CONSUMPTION, AND UTILIZATI↗

DOE OSTI2021

Facility Cybersecurity Framework Best Practices Version 2.0

32 ENERGY CONSERVATION, CONSUMPTION, AND UTILIZATI↗

DOE OSTI2020

Roundtable Report: Terahertz and 6G Wireless Communications in Science and Extreme Environments

The main objective of the roundtable is to bring together computer scientists and wireless communications experts from industry, academia, and government to explore the electromagnetic spectrum in the Terahertz (THz) bands for ultra-high-speed short-distance wireless communications in extreme environments. This new generation of THz wireless communications is the key to future machine-to-machine communications critical for the mass deployment of an intelligent Internet of Things (IoT). The roundtable discussion explores THz and 6G wireless technologies along with Visible Light Communications (VLC), intelligent reflection surfaces, free-space quantum and optical communications, and nano communications. The roundtable considers the suitability of these technologies for extreme environments from the nanoscale to the mesoscale for the following: scientific facilities and associated instruments, as well as industry, and manufacturing. Such use cases are not traditionally the primary customer of commercial wireless networks which are focused on personal broadband voice and data communications. Finally, the discussion identifies high-level opportunities and challenges for leveraging THz and 6G wireless communications and related Artificial Intelligence (AI) that can catalyze the advancement of the development of hyperconnected smart scientific instruments and facilities.

97 MATHEMATICS AND COMPUTING↗