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NASA NTRS2008

Superconducting Detector Arrays for Astrophysics

The next generation of astrophysics instruments will feature an order of magnitude more photon sensors or sensors that have an order of magnitude greater sensitivity. Since detector noise scales with temperature, a number of candidate technologies have been developed that use the intrinsic advantages of detector systems that operate below 1 Kelvin. Many of these systems employ of the superconducting phenomena that occur in metals at these temperatures to build ultrasensitive detectors and low-noise, low-power readout architectures. I will present one such system in use today to meet the needs of the astrophysics community at millimeter and x-ray wavelengths. Our group at NASA in collaboration with Princeton, NIST, Boulder and a number of other groups is building large format arrays of superconducting transition edge sensors (TES) read out with multiplexed superconducting quantum interference devices (SQUID). I will present the high sensitivity we have achieved in multiplexed x-ray sensors with the TES technology and describe the construction of a 1000-sensor TES/SQUID array for microwave measurements. With our collaboration's deployment of a kilopixel TES array for 2 mm radiation at the Atacarna Cosmology Telescope in November 2007, we have first images of the lensed Cosmic Microwave Background at fine angular scales.

Chervenak, James↗

NASA NTRS2000

The Fast Alternative Cryogenic Experiment Testbed

One of the challenges in the area of cryogenics for space exploration in the next millennium is providing the capability for inexpensive, frequent, access to space. Faced with this challenge during the International Space Station (ISS) build era, when other Space Shuttle manifesting opportunities are unavailable, a "proof of concept" cryostat has been developed to demonstrate the ability to accommodate low temperature science investigations within the constraints of the Hitchhiker siderail carrier. The Hitchhiker siderail carrier is available on a "mass available" basis during the ISS build era. In fact, several hitchhiker payloads flew with the deployment of the Unity module. Hitchhiker siderail carrier payloads have historically flown an average of about four times a year. A hybrid Solid Neon - Superfluid Helium cryostat has been developed with Janis Research Company to accommodate instruments of 16.5 cm diameter and 30 cm. length. This hybrid approach was taken in part to provide adequate on-orbit lifetime for instruments with high (conducted) heat loads from the instrumentation wiring. Mass, volume, lifetime and the launch hold scenario were all design drivers. In addition, with Ball Aerospace and Technologies Corporation, a multichannel VME architecture Germanium Resistance Thermometer (GRT) readout and heater control servo system has been developed. In a flight system, the cryostat and electronics payloads would be umbilically attached in a paired Hitchhiker siderail mount, and permit on-orbit command and telemetry capability. The results of performance tests of both the cryostat, and a helium sample instrument will be presented. The instrument features a self contained, miniaturized, nano-Kelvin resolution High Resolution Thermometer (HRT). This high level of thermal resolution is achieved through the utilization of a dc Superconducting Quantum Interference Device (SQUID). Although developed for the Low Temperature Microgravity Fundamental Physics investigator community, many design features are applicable in fields such as infrared and x-ray astronomy.

Nash, Alfred↗

NASA NTRS2011

Network-Capable Application Process and Wireless Intelligent Sensors for ISHM

Intelligent sensor technology and systems are increasingly becoming attractive means to serve as frameworks for intelligent rocket test facilities with embedded intelligent sensor elements, distributed data acquisition elements, and onboard data acquisition elements. Networked intelligent processors enable users and systems integrators to automatically configure their measurement automation systems for analog sensors. NASA and leading sensor vendors are working together to apply the IEEE 1451 standard for adding plug-and-play capabilities for wireless analog transducers through the use of a Transducer Electronic Data Sheet (TEDS) in order to simplify sensor setup, use, and maintenance, to automatically obtain calibration data, and to eliminate manual data entry and error. A TEDS contains the critical information needed by an instrument or measurement system to identify, characterize, interface, and properly use the signal from an analog sensor. A TEDS is deployed for a sensor in one of two ways. First, the TEDS can reside in embedded, nonvolatile memory (typically flash memory) within the intelligent processor. Second, a virtual TEDS can exist as a separate file, downloadable from the Internet. This concept of virtual TEDS extends the benefits of the standardized TEDS to legacy sensors and applications where the embedded memory is not available. An HTML-based user interface provides a visual tool to interface with those distributed sensors that a TEDS is associated with, to automate the sensor management process. Implementing and deploying the IEEE 1451.1-based Network-Capable Application Process (NCAP) can achieve support for intelligent process in Integrated Systems Health Management (ISHM) for the purpose of monitoring, detection of anomalies, diagnosis of causes of anomalies, prediction of future anomalies, mitigation to maintain operability, and integrated awareness of system health by the operator. It can also support local data collection and storage. This invention enables wide-area sensing and employs numerous globally distributed sensing devices that observe the physical world through the existing sensor network. This innovation enables distributed storage, distributed processing, distributed intelligence, and the availability of DiaK (Data, Information, and Knowledge) to any element as needed. It also enables the simultaneous execution of multiple processes, and represents models that contribute to the determination of the condition and health of each element in the system. The NCAP (intelligent process) can configure data-collection and filtering processes in reaction to sensed data, allowing it to decide when and how to adapt collection and processing with regard to sophisticated analysis of data derived from multiple sensors. The user will be able to view the sensing device network as a single unit that supports a high-level query language. Each query would be able to operate over data collected from across the global sensor network just as a search query encompasses millions of Web pages. The sensor web can preserve ubiquitous information access between the querier and the queried data. Pervasive monitoring of the physical world raises significant data and privacy concerns. This innovation enables different authorities to control portions of the sensing infrastructure, and sensor service authors may wish to compose services across authority boundaries.

Figueroa, Fernando↗

NASA NTRS2010

Summary of 2006 to 2010 FPMU Measurements of International Space Station Frame Potential Variations

Electric potential variations on the International Space Station (ISS) structure in low Earth orbit are dominated by contributions from interactions of the United States (US) 160 volt solar arrays with the relatively high density, low temperature plasma environment and inductive potentials generated by motion of the large vehicle across the Earth?s magnetic field. The Floating Potential Measurement Unit (FPMU) instrument suite comprising two Langmuir probes, a plasma impedance probe, and a floating potential probe was deployed in August 2006 for use in characterizing variations in ISS potential, the state of the ionosphere along the ISS orbit and its effect on ISS charging, evaluating effects of payloads and visiting vehicles, and for supporting ISS plasma hazard assessments. This presentation summarizes observations of ISS frame potential variations obtained from the FPMU from deployment in 2006 through the current time. We first describe ISS potential variations due to current collection by solar arrays in the day time sector of the orbit including eclipse exit and entry charging events, potential variations due to plasma environment variations in the equatorial anomaly, and visiting vehicles docked to the ISS structure. Next, we discuss potential variations due to inductive electric fields generated by motion of the vehicle across the geomagnetic field and the effects of external electric fields in the ionosphere. Examples of night time potential variations at high latitudes and their possible relationship to auroral charging are described and, finally, we demonstrate effects on the ISS potential due to European Space Agency and US plasma contactor devices.

Minow, Joseph I.↗

NASA NTRS2008

Wireless Sensor Network Handles Image Data

To relay data from remote locations for NASA s Earth sciences research, Goddard Space Flight Center contributed to the development of "microservers" (wireless sensor network nodes), which are now used commercially as a quick and affordable means to capture and distribute geographical information, including rich sets of aerial and street-level imagery. NASA began this work out of a necessity for real-time recovery of remote sensor data. These microservers work much like a wireless office network, relaying information between devices. The key difference, however, is that instead of linking workstations within one office, the interconnected microservers operate miles away from one another. This attribute traces back to the technology s original use: The microservers were originally designed for seismology on remote glaciers and ice streams in Alaska, Greenland, and Antarctica-acquiring, storing, and relaying data wirelessly between ground sensors. The microservers boast three key attributes. First, a researcher in the field can establish a "managed network" of microservers and rapidly see the data streams (recovered wirelessly) on a field computer. This rapid feedback permits the researcher to reconfigure the network for different purposes over the course of a field campaign. Second, through careful power management, the microservers can dwell unsupervised in the field for up to 2 years, collecting tremendous amounts of data at a research location. The third attribute is the exciting potential to deploy a microserver network that works in synchrony with robotic explorers (e.g., providing ground truth validation for satellites, supporting rovers as they traverse the local environment). Managed networks of remote microservers that relay data unsupervised for up to 2 years can drastically reduce the costs of field instrumentation and data rec

Source record↗

NASA NTRSDate not supplied

The Gandalf Staff: A Mobile Tool for Lunar Exploration (2nd year of development)

The Gandalf Staff is a mobile tool designed to be a flexible device supporting crewed and uncrewed operations on the lunar surface. The core of the device is a 24v battery with communications and data storage systems. Initial optional components supporting crewed Extra-Vehicular Activity (EVA) include a LiDAR and 360˚ camera. These provide 3D mapping of the traverse for documentation, and to aid future planning. The mapping also creates outreach opportunities for the public to “stand beside” the astronaut in Virtual Reality (VR). The staff provides external lighting for field site illumination in the south polar region low sun angle environment. Navigation instruments for crew position determination with Lunar Search and Rescue (LunaSAR) are also included. The staff itself can be used as a walking aid or as a splint for Incapacitated Crew Rescue (ICR). As a stand-alone device, the staff operates as a long duration untended science platform collecting environmental data and sending it to a lunar base station. The stand-alone mode requires connection to an auxiliary power source (e.g. solar array) and energy storage system (e.g. battery), so it could become an electrical recharging station. To make rapid progress in the 1st year, and also to demonstrate innovative project management techniques, NASA guided a private industry partner, T STAR, in leading Capstone Engineering student teams at Texas A&M University (TAMU) for proof-of-concept development and testing. These teams developed the power system and demonstrated successful integration of LiDAR, WiFi communications, and external lighting subsystems. Another industry team at Jacobs Technology prototyped a tripod to hold the staff upright. For the 2nd year (FY’22), NASA will again collaborate with partners to prototype enhanced power and lighting concepts. Year 2 will also add new capability for LunaSAR and geophysical science instrumentation using a heat probe. The heat probe is based upon Apollo heritage but modified to measure subsurface volatile ice regimes at the Artemis landing site. Components of the Gandalf Staff can be developed, tested, and deployed independently, or on the integrated staff, rovers, or utility trailers. The project supports crew safety, lunar sample curation, mission science, and public outreach goals of NASA. PLAIN TEST SUMMARY: Gandalf Staff is a 24v battery powered mobile tool for the lunar surface supporting crewed geologic field site exploration, or as a stand-alone science platform. As a tool assisting astronauts conducting field geology, the Gandalf Staff provides external lighting to illuminate shadowed regions on the surface. It also documents the process of collecting rocks and dust samples using a LiDAR (laser range instrument) and cameras. The staff provides a beacon for emergency location of astronauts and augments communications when the astronauts are blocked by large boulders. As a standalone science platform, the Gandalf Staff provides a power system for instruments and sensors to measure the lunar environment over long periods of time. The staff gathers data and sends the results to a lunar base station for analysis.

External Lighting↗

NASA NTRSDate not supplied

Preliminary Assessment of the Impact on the V-Band Oxygen Channels From Satellite Communication Uplinks

We calculate the percentage of time that an ATMS-like instrument [1] will be illuminated by the uplink beam of one of the proposed V-band communication system and estimate the damage resulting from such exposure. Using a combination of openly available information and educated guesses about the location and characteristics of the up/down link terminals, we constructed the ground segment of a hypothetical high-speed communication network. The space segment of the network was constructed from the orbital data of the existing Starlink constellation [2] of 6223 communication satellites (comsats) which is used as strawman to represent any other possible constellation of communication satellites. It is shown that without a very delicate balance of frequency allocations (science vs telecommunications), coupled with extremely steep and deep bandpass-defining filters, and strict adherence to the agreed limits (i.e. no out-of-band transmissions) the deployment of the telecommunication network leads to almost-complete loss of some important geophysical data. For the analysis we use the spectral characteristics of the ATMS instrument with the ephemeris for the NOAA-21 satellite [3]. The analysis is conducted for the USA and the simulation covers 8 consecutive days in July 2024. Effective and accurate microwave remote sensing of the atmosphere depends on the availability of interference-free spectrum windows at frequencies which are prescribed by physical processes [e.g. 4]. The family of resonant lines of the oxygen molecule near 60 GHz provides a unique opportunity to sample the vertical distribution of temperature and density from space, and it has been exploited for weather and climate studies from polar-orbiting satellites since 1978 (MSU on TIROS-N [5]). It remains a staple in the payloads operated by Russia, China, USA, Japan, France, India, UK, Ukraine [6] which are built around a common blueprint: a few wide-band (hundreds of MHz) channels around 50 GHz to sample the atmosphere and the surface while several more channels with high spectral resolution (few MHz) sample the individual resonant lines. Accurate retrieval of the environmental parameters depends upon the data provided by both sets of channels, and the their location in frequency space is not arbitrary and cannot be altered at will [7, 8]. The introduction of 5G technology in 2019 has driven telecommunication companies to request more bandwidth to be dedicated to their devices. This additional bandwidth is only available in spectral regions traditionally reserved for environmental and astrophysical research, such as the V-band between 50 and 60 GHz for up/downlink between satellites in low-earth orbits and terminals connected to fiberoptics network for distribution to high-speed local internet services. The power broadcast by the uplink communication leg is many orders of magnitude greater than the natural thermal signal emitted from the Earth scene. If the ground antenna were to perfectly align with the passive instrument’s antenna, the spaceborne receiver would suffer permanent, irreparable damage. While a direct boresight-to-boresight conjunction is extremely unlikely (even with a large constellation of satellites the fraction of the celestial sphere occupied by the satellites remains minuscule) the finite size of the ground station’s antenna beam in the sky suggests that the ATMS will be in the near background (as seen from the ground station) of one of the communication satellites and will be illuminated by either the main lobe or the near sidelobes of the uplink antenna more often than it is desirable. For our analysis we first calculate the position of the ATMS with respect to each of the ground stations at a resolution of 0.2 sec, then calculate the position of each of the comsats which are at least 25 deg above the station’s local horizon; finally we calculate the angle between the line-of-sight of the ATMS and the line-of-sight of the comsat. We assume that the gain pattern of the ground station is circularly symmetric; the angle-off-station-boresight then provides an attenuation of the uplink power which we use to assess the likely effect upon the passive instrument’s operations. We assume that each ground station can communicate with all the comsats in its field of view; this implies that, on average, a ground station can engage with 46 comsats simultaneously. The analysis is repeated for the case when the uplink broadcast within the ATMS passive channels (in-band scenario) and for the case when the uplink is limited to frequencies adjacent to the ATMS channels (out-of-band scenario). The antenna of the ground station is modelled as having a HPBW (Half-Power Beam Width) of 0.16 deg and EIRP (Equivalent Isotropic Radiated Power) of 70 dBW. We account for the geometric dissipation of the signal caused by the satellite orbital altitude, the attenuation induced by atmospheric gasses at 51 GHz and the mismatch between the circular polarization of the ground-based transmitting antenna and the linear polarization of the satellite-borne receiving antenna. The damages on ATMS are estimated from bench-level measurement conducted at the ATMS’ manufacturer facilities [unpublished].

passive microwave↗

NASA NTRS1998

MEMS Applications in Aerodynamic Measurement Technology

Microelectromechanical systems (MEMS) embodies the integration of sensors, actuators, and electronics on a single substrate using integrated circuit fabrication techniques and compatible bulk and surface micromachining processes. Silicon and its derivatives form the material base for the MEMS technology. MEMS devices, including microsensors and microactuators, are attractive because they can be made small (characteristic dimension about 100 microns), be produced in large numbers with uniform performance, include electronics for high performance and sophisticated functionality, and be inexpensive. For aerodynamic measurements, it is preferred that sensors be small so as to approximate measurement at a point, and in fact, MEMS pressure sensors, wall shear-stress sensors, heat flux sensors and micromachined hot wires are nearing application. For the envisioned application to wind tunnel models, MEMS sensors can be placed on the surface or in very shallow grooves. MEMS devices have often been fabricated on stiff, flat silicon substrates, about 0.5 mm thick, and therefore were not easily mounted on curved surfaces. However, flexible substrates are now available and heat-flux sensor arrays have been wrapped around a curved turbine blade. Electrical leads can also be built into the flexible substrate. Thus MEMS instrumented wind tunnel models do not require deep spanwise grooves for tubes and leads that compromise the strength of conventionally instrumented models. With MEMS, even the electrical leads can potentially be eliminated if telemetry of the signals to an appropriate receiver can be implemented. While semiconductor silicon is well known for its electronic properties, it is also an excellent mechanical material for MEMS applications. However, silicon electronics are limited to operations below about 200 C, and silicon's mechanical properties start to diminish above 400 C. In recent years, silicon carbide (SiC) has emerged as the leading material candidate for applications in high temperature environments and can be used for high-temperature MEMS applications. With SiC, diodes and more complex electronics have been shown to operate to about 600 C, while the mechanical properties of SiC are maintained to much higher temperatures. Even when MEMS devices show benefits in the laboratory, there are many packaging challenges for any aeronautics application. Incorporating MEMS into these applications requires new approaches to packaging that goes beyond traditional integrated circuit (IC) packaging technologies. MEMS must interact mechanically, as well as electrically with their environment, making most traditional chip packaging and mounting techniques inadequate. Wind tunnels operate over wide temperature ranges in an environment that is far from being a 'clean-room.' In flight, aircraft are exposed to natural elements (e.g. rain, sun, ice, insects and dirt) and operational interferences(e.g. cleaning and deicing fluids, and maintenance crews). In propulsion systems applications, MEMS devices will have to operate in environments containing gases with very high temperatures, abrasive particles and combustion products. Hence deployment and packaging that maintains the integrity of the MEMS system is crucial. This paper presents an overview of MEMS fabrication and materials, descriptions of available sensors with more details on those being developed in our laboratories, and a discussion of sensor deployment options for wind tunnel and flight applications.

Reshotko, E.↗

NASA NTRS2006

Ice-Borehole Probe

An instrumentation system has been developed for studying interactions between a glacier or ice sheet and the underlying rock and/or soil. Prior borehole imaging systems have been used in well-drilling and mineral-exploration applications and for studying relatively thin valley glaciers, but have not been used for studying thick ice sheets like those of Antarctica. The system includes a cylindrical imaging probe that is lowered into a hole that has been bored through the ice to the ice/bedrock interface by use of an established hot-water-jet technique. The images acquired by the cameras yield information on the movement of the ice relative to the bedrock and on visible features of the lower structure of the ice sheet, including ice layers formed at different times, bubbles, and mineralogical inclusions. At the time of reporting the information for this article, the system was just deployed in two boreholes on the Amery ice shelf in East Antarctica and after successful 2000 2001 deployments in 4 boreholes at Ice Stream C, West Antarctica, and in 2002 at Black Rapids Glacier, Alaska. The probe is designed to operate at temperatures from 40 to +40 C and to withstand the cold, wet, high-pressure [130-atm (13.20-MPa)] environment at the bottom of a water-filled borehole in ice as deep as 1.6 km. A current version is being outfitted to service 2.4-km-deep boreholes at the Rutford Ice Stream in West Antarctica. The probe (see figure) contains a sidelooking charge-coupled-device (CCD) camera that generates both a real-time analog video signal and a sequence of still-image data, and contains a digital videotape recorder. The probe also contains a downward-looking CCD analog video camera, plus halogen lamps to illuminate the fields of view of both cameras. The analog video outputs of the cameras are converted to optical signals that are transmitted to a surface station via optical fibers in a cable. Electric power is supplied to the probe through wires in the cable at a potential of 170 VDC. A DC-to-DC converter steps the supply down to 12 VDC for the lights, cameras, and image-data-transmission circuitry. Heat generated by dissipation of electric power in the probe is removed simply by conduction through the probe housing to the visible features of the lower structure of the ice sheet, including ice layers formed at different times, bubbles, and mineralogical inclusions. At the time of reporting the information for this article, the system was just deployed in two boreholes on the Amery ice shelf in East Antarctica and after successful 2000 2001 deployments in 4 boreholes at Ice Stream C, West Antarctica, and in 2002 at Black Rapids Glacier, Alaska. The probe is designed to operate at temperatures from 40 to +40 C and to withstand the cold, wet, high-pressure [130-atm (13.20-MPa)] environment at the bottom of a water-filled borehole in ice as deep as 1.6 km. A current version is being outfitted to service 2.4-km-deep boreholes at the Rutford Ice Stream in West Antarctica. The probe (see figure) contains a sidelooking charge-coupled-device (CCD) camera that generates both a real-time analog video signal and a sequence of still-image data, and contains a digital videotape recorder. The probe also contains a downward-looking CCD analog video camera, plus halogen lamps to illuminate the fields of view of both cameras. The analog video outputs of the cameras are converted to optical signals that are transmitted to a surface station via optical fibers in a cable. Electric power is supplied to the probe through wires in the cable at a potential of 170 VDC. A DC-to-DC converter steps the supply down to 12 VDC for the lights, cameras, and image-datatransmission circuitry. Heat generated by dissipation of electric power in the probe is removed simply by conduction through the probe housing to the visible features of the lower structure of the ice sheet, including ice layers formed at different times, bubbles, and mineralogical inclusions. At thime of reporting the information for this article, the system was just deployed in two boreholes on the Amery ice shelf in East Antarctica and after successful 2000 2001 deployments in 4 boreholes at Ice Stream C, West Antarctica, and in 2002 at Black Rapids Glacier, Alaska. The probe is designed to operate at temperatures from 40 to +40 C and to withstand the cold, wet, high-pressure [130-atm (13.20-MPa)] environment at the bottom of a water-filled borehole in ice as deep as 1.6 km. A current version is being outfitted to service 2.4-km-deep boreholes at the Rutford Ice Stream in West Antarctica. The probe (see figure) contains a sidelooking charge-coupled-device (CCD) camera that generates both a real-time analog video signal and a sequence of still-image data, and contains a digital videotape recorder. The probe also contains a downward-looking CCD analog video camera, plus halogen lamps to illuminate the fields of view of both cameras. The analog video outputs of the cameras are converted to optical signals that are transmitted to a surface station via optical fibers in a cable. Electric power is supplied to the probe through wires in the cable at a potential of 170 VDC. A DC-to-DC converter steps the supply down to 12 VDC for the lights, cameras, and image-datatransmission circuitry. Heat generated by dissipation of electric power in the probe is removed simply by conduction through the probe housing to the adjacent water and ice.

Behar, Alberto↗

NASA NTRS2005

A High-power Electric Propulsion Test Platform in Space

This paper will describe the results of the preliminary phase of a NASA design study for a facility to test high-power electric propulsion systems in space. The results of this design study are intended to provide a firm foundation for subsequent detailed design and development activities leading to the deployment of a valuable space facility. The NASA Exploration Systems Mission Directorate is sponsoring this design project. A team from the NASA Johnson Space Center, Glenn Research Center, the Marshall Space Flight Center and the International Space Station Program Office is conducting the project. The test facility is intended for a broad range of users including government, industry and universities. International participation is encouraged. The objectives for human and robotic exploration of space can be accomplished affordably, safely and effectively with high-power electric propulsion systems. But, as thruster power levels rise to the hundreds of kilowatts and up to megawatts, their testing will pose stringent and expensive demands on existing Earth-based vacuum facilities. These considerations and the human access to near-Earth space provided by the International Space Station (ISS) have led to a renewed interest in space testing. The ISS could provide an excellent platform for a space-based test facility with the continuous vacuum conditions of the natural space environment and no chamber walls to modify the open boundary conditions of the propulsion system exhaust. The test platform could take advantage of the continuous vacuum conditions of the natural space environment. Space testing would provide open boundary conditions without walls, micro-gravity and a realistic thermal environment. Testing on the ISS would allow for direct observation of the test unit, exhaust plume and space-plasma interactions. When necessary, intervention by on-board personnel and post-test inspection would be possible. The ISS can provide electrical power, a location for diagnostic instruments, data handling and thermal control. The platform will be designed to accommodate the side-by-side testing of multiple types of electric thrusters. It is intended to be a permanent facility in which different thrusters can be tested over time. ISS crews can provide maintenance for the platform and change out thruster test units as needed. The primary objective of this platform is to provide a test facility for electric propulsion devices of interest for future exploration missions. These thrusters are expected to operate in the range of hundreds of kilowatts and above. However, a platform with this capability could also accommodate testing of thrusters that require much lower power levels. Testing at the higher power levels would be accomplished by using power fiom storage devices on the platform, which would be gradually recharged by the ISS power generation system. This paper will summarize the results of the preliminary phase of the study with an explanation of the user requirements and the initial conceptual design. The concept for test operations will also be described. The NASA project team is defining the requirements but they will also reflect the inputs of the broader electric propulsion community including those at universities, commercial enterprises and other government laboratories. As a facility on the International Space Station, the design requirements are also intended to encompass the needs of international users. Testing of electric propulsion systems on the space station will help advance the development of systems needed for exploration and could also serve the needs of other customers. Propulsion systems being developed for commercial and military applications could be tested and certification testing of mature thrusters could be accomplished in the space environment.

Petro, Andrew J.↗

NASA NTRS2015

Final Report on the Detection of Green Monopropellants

In 2014, National Aeronautics and Space Administration (NASA) Kennedy Space Center (KSC) funded a project titled "Familiarization and Detection of Green Monopropellants" utilizing Independent Research and Technology Development (IR&TD) and Center Innovation Fund (CIF) funding. The purpose of the project was to evaluate methods of detection for ammonium dinitramide (ADN) and hydroxylammonium nitrate (HAN). An Engineering Services Contract (ESC) task order was created with the scope of evaluation of several methods of detecting ADN- and HAN-based propellants, as well as development of methods for detection. Detection methods include developed methods such as colorimetric indicating absorbent socks, and commercial-off-the- shelf (COTS) units for ammonia detection. An additional goal of the task order was for ESC to become familiar with ADN's and HAN's material properties and material compatibility. Two approaches were initially investigated as possible methods for the detection of HAN (or AFM315E) and ADN (or LMP-103S). These approaches were colorimetric analysis and instrumentation-based COTS vapor sensors utilization. Initial testing showed that the relatively non-existent vapor pressure of the AF-M315E (of which HAN is a major component) propellant would make the use of COTS sensors difficult for real-time area monitoring of HAN; a small response was detected through the use of active COTS sensors, including the RAE Systems MultiRAE Lite and Drager X-act (registered) 5000, but the levels detected were below the threshold limit value for the toxic gas ammonia. Therefore, a detection system ased upon a colorimetric indicator impregnated into an absorbent material was developed. Preliminary analysis (ESC-245-FDG-001) identified a particularly outstanding candidate as a colorimetric indicator for the detection of the presence of AF-M315E in the form of a Methyl Red (Basic) indicator. Materials impregnated with this indicator exhibit significant color change and the materials are not susceptible to interference from exposure to water or carbon dioxide. The completed detection system for HAN/AF-M315E consists of absorbent socks packed with Fisher Universal Spill Absorbent capable of absorbing and containing any propellant spills that they come into contact with along with indicating wipes. The absorbent socks are also chemically treated with a Methyl Red (Basic) indicator solution to provide the end user with a visual indication that a leak has occurred and proper protective precautions must be undertaken. An added benefit of this detection system is that the absorbent socks should neutralize/absorb any commodity that it comes into contact with (until saturation is reached). Additional adsorbent socks can be deployed until a color change is not seen, indicating that the HAN/AF-M315E contamination has been contained. The indicating wipes provide the user the opportunity to wipe surfaces to determine if there is any HAN/AF-M315E or HAN/AFM315E residue present. The wipes should allow the detection of fuel levels that may be too small to detect with the absorbent socks. The development of a detection system for the ADN/LMP-103S focused on the use of various COTS sensors used as real-time area monitoring devices and personal dosimeters. These COTS based sensor systems were of several different types, including both actively pumped and diffusion-based passive systems, as well as a "rope"-type chemical sensing cable. The results highlighted some of the major differences between the two monopropellants undergoing evaluation. Unlike HAN, ADN (which is the major constituent of LMP-103S) exhibits a much more volatile nature in comparison to AF-M315E. In fact, testing showed that a large percentage of the fuel was lost during the sampling measurement (greater than 10 percent by mass); although this testing cannot tell if the volatile component is the ADN itself or another component of the monopropellant solution. Not surprisingly, all four of the procured vapor-based COTS sensors showed positive results when exposed to solutions of the LMP-103S (ESC-245-FDG-002). The completed detection system for ADN/LMP-103S consists of a combination of two of the tested COTS sensor systems, the RAE Systems MultiRAE Lite and the BW Technologies GasAlert Extreme. These systems are meant to be used in conjunction with one another, which allows for the end-user to have both real-time area monitoring (MultiRAE Lite) as well as a personal dosimeter device (GasAlert Extreme) which can be worn as additional personal protective equipment. An stainless steel extension wand was fabricated and included in the detection system for the MultiRAE Lite to allow for more remote sensing, and connects via the active pumping inlet of the sensor. As stated, the final results of this testing resulted in the production of two "kits" which can be used for the detection of HAN/AF-M315E and ADN/LMP-103s (ESC-245-FDG-003).

Detection↗