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At least 127 records · Page 7

FMR thermomagnetic studies up to 900 C of lunar soils and potential magnetic analogues

Using a recently developed furnace, ferromagnetic resonance (FMR) thermomagnetic studies up to 900 C were employed to measure the Curie points of the superparamagnetic (SP) and single domain (SD) particles in lunar soils and potential magnetic analogue materials. Based on measured Curie points of 775 C, the SP and SD particles in lunar soils 10084-853, 12070-29, 14161-46, and 67010-4 are essentially pure metallic Fe. Synthetic and terrestrial samples containing magnetite, titanomaghemites, and magnetite-like particles have measured Curie points below 600 C are thus not magnetic analogues of lunar soils.

Morris, R. V.↗

Comparative studies of grain size separates of 60009

Five samples from 60009, the lower half of a double drive tube, were analyzed via grain-size methods, with particle types classified and counted in the coarser grain sizes. Studies were undertaken of particle types and distributions by petrographic methods, of magnetic fractions, of the size splits and magnetic splits as analyzed by ferromagnetic resonance (FMR) techniques, of maturity (based on agglutinate content, FMR index Is/FeO, mean size of sub-cm material, magnetic fraction), of possible reworking or mixing in situ, and of depositional history. Maturity indices are in substantial agreement for all of the five samples. Strong positive correlation of percent agglutinates and percent bedrock-derived lithic fragments, combined with negative correlation of those components with percent single crystal plagioclase, argue against in situ reworking of the same soil.

Mckay, D. S.↗

Lunar sample analysis

Flameless atomic abosrption, X-ray photoemission spectroscopy, ferromagnetic resonance, scanning electron microscopy, and Moessbauer spectroscopy were used to investigate the evolution of the lunar regolith, the transport of volatile trace metals, and the surface composition of lunar samples. The development of a model for lunar volcanic eruptions is also discussed.

Housley, R. M.↗

Depositional history of the Apollo 16 deep drill core

Ferromagnetic resonance and magnetic hysteresis loop measurements were performed on 212 samples from the Apollo 16 deep drill core. The total iron content is generally uniform with a mean value of 5.7 plus or minus 0.9 wt%. The soils range in maturity from immature to mature. Two major contacts were observed. The contact at 13 cm depth represents a fossil surface whereas the contact at 190 cm depth has no time-stratigraphic significance. The data suggest that the core section below 13 cm depth was deposited in a single impact event and subjected to meteoritic gardening for about 450 m.y. However, our data do not preclude deposition by a series of closely spaced events. About 50 m.y. ago, the top 13 cm were added. Comparison with the Apollo 16 double drive tube 60009/60010 does not yield any evidence for a stratigraphic correlation with the deep drill core.

Gose, W. A.↗

Grain size, petrographic, and FMR studies of the double core 60009/10 - A study of soil evolution

Six samples from the upper core 60010 of the double drive core 60009/60010 were analyzed for grain size distribution, petrographic particle types and abundances, magnetic fraction, and ferromagnetic resonance. It was found that the magnetic fraction of these soils is not equivalent to the agglutinate fraction, and magnetic separation partitions high-FeO agglutinate from low-FeO agglutinates. Various maturity indices are in essential agreement. The deposition of most or all of the core could have occurred in a single event. If that is the case, the core units have no time-stratigraphic significance and do not reflect individual cratering events.

Mckay, D. S.↗

Remanent magnetization stratigraphy of lunar cores

Depth dependent fluctuations have been observed in the natural remanent magnetizations (NRM) of drive cores and drill strings from Apollo 16 and 17 missions. Partial demagnetization of unstable secondary magnetizations and identification of characteristic error signals from a core which is known to have been recently disturbed allow us to identify and isolate the stable NRM stratigraphy in double drive core 60010/60009 and drill strings 60002-60004. The observed magnetization fluctuations persist after normalization to take into account depth dependent variations in the carriers of stable NRM. We tentatively ascribe the stable NRM stratigraphy to instantaneous records of past magnetic fields at the lunar surface and suggest that the stable NRM stratigraphy technique could develop as a new relative time-stratigraphic tool, to be used with other physical measurements such as relative intensity of ferromagnetic resonance and charged particle track density to study the evolution of the lunar regolith.

Banerjee, S. K.↗

Particle track densities in double drive tube 60009/10

Measurements are reported of particle track densities in grains from a suite of eleven samples from the Apollo 16 double drive tube 60009/10. All of the samples studied in 60009 show a clearly bimodal distribution of track densities in plagioclase. This bimodal distribution is interpreted to indicate a mixing of a relatively immature soil with a relatively mature soil. This mixing was not followed by any appreciable reworking which would have altered the distribution. The three lower samples in 60010 also show a bimodal distribution. However, the three uppermost samples show a unimodal distribution. The percentage of high track density plagioclase grains shows a good correlation with the other maturity indices of agglutinate content and the ferromagnetic resonance intensity.

Blanford, G. E.↗

Depositional history of core section 74001 - Depth profiles of maturity, FeO, and metal

Samples from every 0.5-cm interval of soil in core section 74001 have been studied by ferromagnetic resonance (FMR) and magnetic techniques. The values of the FMR maturity index show that the 74001 samples are very immature (the index ranges from 0.14 to 0.29 units) and have not seen appreciable, if any, surface exposure since their deposition. In fact, the small amount of fine-grained metal in the 74001 samples is probably not acquired as a result of their exposure to the micrometeoroid flux at the lunar surface. Thus, the black-glass soil of 74001 was deposited very rapidly, probably in a single episode or several closely spaced episodes of lunar fire fountaining. The average concentration of FeO and its standard deviation for all the 74001 samples are 22.5 + or - 0.3 wt.%. Since the FeO concentration is so uniform, no large variations in the major-element chemistry of 74001 are expected, with the possible exception of the volatile elements. The concentration of coarse-grained metal, which is measured magnetically, and its standard deviation are 0.15 + or - 0.01 wt.%. The coarse-grained metal probably precipitated contemporaneously with the silicate and oxide phases in the black-glass droplets.

Morris, R. V.↗

Characterization of lunar ferromagnetic phases by the effective linewidth method

The effective line-width technique, first developed to study the physics of microwave relaxation in ferrites, has been successfully applied to lunar matter. Effective line-width measurements have been made on two selected samples containing disperse spherical metallic iron particles below 40 microns in diam. The data were obtained for fields from 7 to 12 kOe and a temperature range 125 - 300 K. The effective line width was field-independent and temperature-independent at 650 - 750 Oe. The high-field tails of the ferromagnetic resonance absorption were highly Lorentzian. From the relatively large and temperature-independent high-field effective line widths, it appears that (1) the metallic iron phases in lunar soil are rather impure; (2) the impurities are passive, in that there is no evidence for a temperature peak process; and (3) these samples contain no appreciable magnetite.

Patton, C. E.↗

FMR and magnetic studies of Luna 24 soils and greater than 1 mm soil particles

Six Luna 24 soils (24077, 24109, 24149, 24174, 24182, 24210), their grain-size separates, and twenty-five greater than 1 mm soil particles were analyzed by ferromagnetic resonance (FMR) and static magnetic techniques. The values of the FMR maturity index for the soils ranged from 19.0 to 39.0 units; soils 24077 and 24109 are submature and soils 24149, 24174, 24182, and 24210 are immature. The metallic iron contents of the soils ranged from 0.30 to 0.51 wt % and are commensurate with their maturities. The 'best estimate' value for the concentration of metallic iron of Luna 24 mare basalts is 0.038 wt %.

Morris, R. V.↗

Particle track densities in the Luna 24 core

We report track density measurements in soil grains at six locations in the Luna 24 core. Irradiation levels are generally high precluding information on the depositional history, but indicating that the soils were exposed at the lunar surface at sometime in the past. Maturity levels determined from track density parameters disagree with those determined from ferromagnetic resonance and agglutinate contents. This discrepancy is not understood, but it could possibly indicate an ancient epoch of increased solar-flare activity.

Blanford, G. E.↗

Primordial Pb, radiogenic Pb and lunar soil maturation

Pb-204 is directly correlated with the reduced Fe measured by ferromagnetic resonance. A similar correlation has been noted for hydrolyzable carbon (Pillinger et al., 1974). An enrichment of these elements appears to have occurred during soil maturation. In contrast to Pb-204, radiogenic Pb is reported to be lost during soil maturation (Church et al., 1976). Radiogenic Pb is present in mineral grains and may be lost by solar wind sputtering (or volatilization) and not resupplied. Pb-204 coating grain surfaces acts as a reservoir to provide the Pb-204 being extracted in the reduced Fe formation process. Venting or some other volatile release mechanism may replenish the surface-related Pb-204.

Reed, G. W., Jr.↗

The surface exposure /maturity/ of lunar soils - Some concepts and I sub s/FeO compilation

Surface exposure (or, equivalently, maturity) indices of lunar soils are a measure of residence time of soil in the upper one millimeter of the regolith. Several concepts concerning the use of and terminology associated with maturity indices are discussed. For reasons which include its generally-applicable nature and large data base, the ferromagnetic resonance (FMR) surface exposure (maturity) index I sub s/FeO (the ratio of the value of the intensity in arbitrary units of the FMR resonance at g equal to about 2.1 to the FeO concentration) is particularly suitable and useful. A compilation of values of I sub s/FeO for 164 Apollo surface and trench soils and six Luna 24 core soils is given.

Morris, R. V.↗

Eddy current probe response to open and closed surface flaws

A general analysis of eddy current response to certain types of open and closed surface flaws is presented for both standard low-frequency and ferromagnetic-resonance (FMR) probes. It is shown analytically that for two-dimensional and three-dimensional surface flaws interrogated by a uniform probe field, the crack opening sensitivity increases with the operating frequency of the probe, this behavior being due to the Faraday induction effect. Experiments with low-frequency probes operating at or below 1 MHz and with the FMR probe operating at approximately 1000 MHz confirm this increase of the crack mouth opening displacement for practical situations where the probe field is not uniform in the vicinity of the flaw.

Auld, B. A.↗

Cosmic ray production curves below reworking zones

A method is presented for calculating cosmic ray production profiles below reworking zones. The method uses an input reworking depth determined from data such as signatures in the depth profile of ferromagnetic resonance intensity and input cosmic ray production profiles for an undisturbed surface. Reworking histories are simulated using Monte Carlo techniques, and depth profiles are used to determine cosmic ray exposure age limits with a specified probability. It is shown that the track density profiles predict cosmic ray exposure ages in lunar cores that are consistent with values determined by other methods. Results applied to neutron fluence and spallation rare gases eliminate the use of reworking depth as an adjustable parameter and give cosmic ray exposure ages that are compatible with each other.

Blanford, G. E.↗

Origins and size distribution of metallic iron particles in the lunar regolith

The metallic iron concentration has been measured in three ranges of metal particle diameters for 79 lunar soils by a combination of static magnetic and ferromagnetic resonance techniques. Based on these measurements, a model has been developed which apportions the total metallic iron content of lunar soils between three components: (1) metallic iron particles produced from the exposure-induced reduction of ferrous iron; they range from 40 to 330 A in diameter and are predominantly associated with agglutinate glass; (2) metallic iron particles derived from the metallic phases of the micrometeorites involved in the formation of agglutinate glass; these particles are mostly greater than 300 A in diameter; and (3) metallic iron particles in the source materials such as bedrock and breccias; these are usually greater than 330 A in diameter. The maximum concentration of metallic iron in lunar regolith is estimated at about 0.7 equiv. wt% in highland regions (approximately 5.0 wt% FeO) and about 1.0 equiv. wt% in mare regions (approximately 15.0 wt% FeO).

Morris, R. V.↗

On the location of acid-hydrolysable carbon in lunar soil fines

Soil fines exposed on the lunar surface accumulate small metallic iron particles and solar wind-derived carbon. In previous work, it has been suggested that an intimate association exists between one particular carbon phase, hydrolysable carbon, and very fine iron droplets, where the carbon is in solid solution in the iron. The earlier hypothesis of a constant carbon in iron concentration across a broad range of droplet sizes is testable by combining hydrolysable carbon determinations with a variety of magnetic measurements sensitive to different droplet diameters. New measurements of ferromagnetic resonance response on density and magnetic separates from size fractions of soil 12023 are interpreted as evidence that hydrolysable carbon is preferentially associated with the larger, magnetically stable single-domain iron particles rather than with the smaller superparamagnetic droplets. For the former, there is a quite uniform ratio of iron to carbon both within a series of separates from a single soil, and among soils of widely varying FeO content.

Fallick, A. E.↗

Stratigraphy and geochemistry of the Stone mountain core (64001/2)

Ferromagnetic resonance and magnetic data measured on both sections of the double drive tube cord 64001/2 collected on Stone mountain, station four, Apollo 16 are reported, along with instrumental neutron activation analysis data measured on the lower section. These data provide insight into the depositional and irradiational history and the geochemical provenances of the core.

Korotev, R. L.↗