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NASA NTRS2016

Propulsion Technology Assessment: Science and Enabling Technologies to Explore the Interstellar Medium

Led by the Keck Institute for Space Studies at the California Institute of Technology, the Advanced Concepts Office at NASA's George C. Marshall Space Flight Center conducted a study to assess what low-thrust advanced propulsion system candidates, existing and near term, could deliver a small, Voyager-like satellite to our solar system's heliopause, approximately 100 AU from the center of the sun, within 10 years and within a 2025-2035 launch window. The advanced propulsion system trade study consisted of three candidates, including a Magnetically Shielded Miniature (MaSMi) Hall thruster, a solar sail and an electric sail. Two aerial densities, and thus characteristic accelerations, 0.426 mm/sq s and 0.664 mm/sq s were analyzed for the solar sail option in order understand the impact of near and long term development of this technology. Similarly, two characteristic accelerations, 1 mm/s2 and 2 mm/sq s, were also analyzed for the electric sail option in addition to tether quantities of 10 and 20, respectively, and individual tether length of 20 km. A second analysis was conducted to determine what existing solid rocket motor kick stage(s) would be required to provide additional thrust at various points in the trajectory, assuming an earth departure characteristic energy capability provided by a Space Launch System (SLS) Block 1B vehicle architecture carrying an 8.4 meter payload fairing. Two trajectory profiles were considered, including an escape trajectory using a Jupiter gravity assist (E-Ju), and an escape trajectory first performing a Jupiter gravity assist followed by an Oberth maneuver around the sun and an optional Saturn gravity assist (E-Ju-Su-Sa). The Oberth maneuver would need to be performed very close to the sun, wherein this study assumed a perihelion distance of approximately 11 solar radii, or 0.05 AU, away from the surface. The heat shield technology required to perform this type of ambitious maneuver was assumed to be similar to that of NASA's Solar Probe Plus mission, which is slated to launch in July 2018. With respect to a SLS Block 1B earth departure characteristic energy capability of 100 km2/sq s for the E-Ju trajectory option, results indicated that compared to having no advanced propulsion system onboard, both the MaSMi Hall thruster and solar sail options subtract approximately 8 to 10 years from the total trip time while the electric sail outperforms all options by subtracting up to 20 years. With respect to an average kick stage velocity capability of 2.5 to 3.5 km/s at perihelion, the most sensitive segment of the E-Ju-Su-Sa trajectory option, results indicated that both the MaSMi Hall thrust and solar sail options only subtract 1 to 3 years from the total trip time whereas the electric sail again outperforms all other options by subtracting up to 5 years. In other words, if the Technology Readiness Level of an electric sail could be increased in time, this propulsion technology could not only enable a satellite to reach 100 AU in 10 years but it could potentially do so even faster. Completing such an ambitious mission in that short of a timespan would be very attractive to many as it would be well within the average career span of any of those involved.

Hopkins, Randall C.↗
NASA NTRS2013

Low Noise Amplifiers for 140 Ghz Wide-Band Cryogenic Receivers

We report S-parameter and noise measurements for three different Indium Phosphide 35-nanometer-gate-length High Electron Mobility Transistor (HEMT) Low Noise Amplifier (LNA) designs operating in the frequency range centered on 140 gigahertz. When packaged in a Waveguide Rectangular-6.1 waveguide housing, the LNAs have an average measured noise figure of 3.0 decibels - 3.6 decibels over the 122-170 gigahertz band. One LNA was cooled to 20 degrees Kelvin and a record low noise temperature of 46 Kelvin, or 0.64 decibels noise figure, was measured at 152 gigahertz. These amplifiers can be used to develop receivers for instruments that operate in the 130-170 gigahertz atmospheric window, which is an important frequency band for ground-based astronomy and millimeter-wave imaging applications.

High Electron Mobility Transistors (HEMTs)↗
NASA NTRS1972

Theory of two coupled lasers.

A transmitting window is used to weakly couple two resonant optical cavities. When active medium is placed in one cavity, the system describes a laser coupled to a resonant cavity, while active medium in both cavities describes two coupled lasers. Equations of motion for the fields in the two cavities are found. These equations are solved in the steady state when the cavities are sufficiently closely tuned that the lasers in the two cavities oscillate with the same frequency. In the locked situation, the second cavity tends to stabilize the frequency of operation against changes in length of the first cavity. When there is no active medium in the second cavity, and that cavity becomes very long, the laser acts as if it were looking into free space.

Spencer, M. B.↗
NASA NTRS2016

Propulsion Technology Assessment: Science and Enabling Technologies to Explore the Interstellar Medium

As part of a larger effort led by the Keck Institute for Space Studies at the California Institute of Technology, the Advanced Concepts Office at NASA’s George C. Marshall Space Flight Center conducted a study to assess what low-thrust advanced propulsion system candidates, existing and near term, could deliver a small, Voyager-like satellite to our solar system’s heliopause, approximately 100 AU from the center of the sun, within 10 years and within a 2025 to 2035 launch window. The advanced propulsion system trade study consisted of three candidates, including a Magnetically Shielded Miniature (MaSMi) Hall thruster, a solar sail and an electric sail. Two aerial densities, and thus characteristic accelerations, 0.426 mm/s(exp 2) and 0.664 mm/s(exp 2), were analyzed for the solar sail option in order understand the impact of near and long term development of this technology. Similarly, two characteristic accelerations, 1 mm/s(exp 2) and 2 mm/s(exp 2), were also analyzed for the electric sail option in addition to tether quantities of 10 and 20, respectively, and individual tether length of 20 km. A second analysis was conducted to determine what existing solid rocket motor kick stage(s) would be required to provide additional thrust at various points in the trajectory, assuming an earth departure characteristic energy capability provided by a Space Launch System (SLS) Block 1B vehicle architecture carrying an 8.4 meter payload fairing. Two trajectory profiles were considered, including an escape trajectory using a Jupiter gravity assist (E-Ju), and an escape trajectory first performing a Jupiter gravity assist followed by an Oberth maneuver around the sun and an optional Saturn gravity assist (E-Ju-Su-Sa). The Oberth maneuver would need to be performed very close to the sun, wherein this study assumed a perihelion distance of approximately 11 solar radii, or 0.05 AU, away from the surface. The heat shield technology required to perform this type of ambitious maneuver was assumed to be similar to that of NASA’s Solar Probe Plus mission, which is slated to launch in July 2018. With respect to a SLS Block 1B earth departure characteristic energy capability of 100 km(exp 2)/s(exp 2) for the E-Ju trajectory option, results indicated that compared to having no advanced propulsion system onboard, both the MaSMi Hall thruster and solar sail options subtract approximately 8 to 10 years from the total trip time while the electric sail outperforms all options by subtracting up to 20 years. With respect to an average kick stage velocity capability of 2.5 to 3.5 km/s at perihelion, the most sensitive segment of the E-Ju-Su-Sa trajectory option, results indicated that both the MaSMi Hall thrust and solar sail options only subtract 1 to 3 years from the total trip time whereas the electric sail again outperforms all other options by subtracting up to 5 years. In other words, if the Technology Readiness Level of an electric sail could be increased in time, this propulsion technology could not only enable a satellite to reach 100 AU in 10 years but it could potentially do so even faster. Completing such an ambitious mission in that short of a timespan would be very attractive to many as it would be well within the average career span of any of those involved.

Hopkins, Randall C.↗
NASA NTRS2004

Forecasting Coronal Mass Ejections from Magnetograms

We report further results from our ongoing assessment of magnetogram-based measures of active-region nonpotentiality (magnetic shear and twist) and size as predictors of coronal mass ejections (CMEs). From a set of 36 vector magnetograms of bipolar active regions (Falconer, Moore, & Gary 2004, ApJ, submitted), we have found that (1) each of our 5 measures of active-region nonpotentiality has a 75-80% success rate in predicting whether an active region will produce a CME within 2 days after the magnetogram, (2) the correlation of each of these measures with CME production in this window is statistically significant (confidence level greater than 95%), (3) our measure of active-region size has a 65% success rate in predicting CMEs in this window, but (4) the correlation between active-region size and CME productivity is not statistically significant (confidence level approximately 80%). As part of the work under our pending 2003 LWS TR&T proposal, we will double our sample to approximately 70 active regions in order to demonstrate a statistically significant correlation between active-region size and CME productivity, and to determine whether this correlation is a byproduct of any Sun-produced correlation between magnetic twist and size of active regions. Since the 2002 LWS Science Workshop, we have found a measure of active-region nonpotentiality (the length of strong-gradient neutral line) that can be measured from a line-of-sight magnetogram, and we have generalized this measure and the corresponding measure from a vector magnetogram (the length of strong-shear neutral line) so that they can be applied to multiple-bipole complex active regions as well as to bipolar active regions. Preliminary results will be presented from application of these two generalized measures to our sample of bipolar active regions and to a new sample of multiple-bipole active regions.

Falconer, D. A.↗
NASA NTRS2009

A Method for Determining the Nominal Occular Hazard Zone for Gaussian Beam Laser Rangers with a Firmware Controlled Variable Focal Length

LIDAR systems that maintain a constant beam spot size on a retroreflector in order to increase the accuracy of bearing and ranging data must use a software controlled variable position lens. These systems periodically update the estimated range and set the position of the focusing lens accordingly. In order to precisely calculate the r NOHD for such a system, the software method for setting the variable position lens and gaussian laser propagation can be used to calculate the irradiance at any point given the range estimation. NASA s Space Shuttle LIDAR, called the Trajectory Control Sensor (TCS), uses this configuration. Analytical tools were developed using Excel and VBA to determine the radiant energy to the International Space Station (ISS) crewmembers eyes while viewing the shuttle on approach and departure. Various viewing scenarios are considered including the use of through-the-lens imaging optics and the window transmissivity at the TCS wavelength. The methodology incorporates the TCS system control logic, gaussian laser propagation, potential failure mode end states, and guidance from American National Standard for the Safe Use of Lasers (ANSI Z136.1-2007). This approach can be adapted for laser safety analyses of similar LIDAR systems.

Picco, C. E.↗
NASA NTRS2003

Control of the Laser Interferometer Space Antenna

The detection of gravity waves will open a new window of observation on the universe. Unlike typical observatories, which detect electromagnetic waves traveling through space-time, the Laser Interferometer Space Antenna (LISA) will detect ripples in space-time itself. Science targets include galactic binaries, merging supermassive black holes, intermediate-mass/seed black holes, and cosmological backgrounds. Gravity waves are detected by measuring the strain in space, i.e. the change in distance between a set of masses (test masses or proof masses) separated by a great distance. Ground based detection of gravity waves by Laser Interferometer Gravitational Wave Observatory (LIGO) and other observatories are possible with laser interferometry; hut the relatively short arm length (4 km) and seismic noise limit the measurement band to above 10 Hz on Earth. LISA also uses laser interferometric measurement of the change in distance between test masses, but does it in space. Each LISA spacecraft embodies two test masses. Space allows very long arm lengths (5 million km for LISA) and a very quiet acceleration environment (3.5x10(exp -15) meters per second squared/Hertz (sup 0.5) for LISA), which allows for the detection of gravity wave strains to a best sensitivity of 3x10(exp -24) strain/Hertz (sup 0.5) over the measurement band of 10(exp -4) to 10(exp -1) Hertz for a one-year observation. The LISA mission consists of three spacecraft in heliocentric orbit. The orbits are chosen so that the three spacecraft form a roughly equilateral triangle with its center located at a radius of 1 AU and 20 degrees behind the Earth, as shown. Requirements are placed on the rotational and translational dynamics of each spacecraft to ensure that the proper sensitivity for science measurements can be achieved.

Maghami, Peiman↗
NASA NTRS1998

Line Intensity and Position Measurements and Derived Band Parameters of the 31103-00001 C-12 O-16(2) Band and its Two Nearby Hot Bands

A set of CO2 spectra from 4500 to 4780/cm has been obtained an Ames with 1500 m path length using a Bomem DA8 FTS. This spectral region contains a number of weak bands and minor isotopic bands that have been studied at high resolution in the reflection spectrum of Venus by Mandin. Improved laboratory intensity and position measurements should assist modeling the Venus reflection spectra and improve understanding of Venus' upper atmosphere. Also, the laboratory measurements will assist DND intensity computations of weaker bands that cannot be measured, but which are nevertheless significant absorbers in Venus' hot, deep CO2, atmosphere. For example, some of the weaker bands that are members of the same polyads as the bands in this presentation lie in the nearby 2.3 microns emission window in Venus' night-side spectrum.

Giver, Lawrence P.↗
NASA NTRS1984

Dust streaks on Mars: Colors and photometry

Photometric studies of crater related bright and dark streaks have strongly supported the hypothesis that the bright streaks are excess dust deposits and dark streaks are erosional windows in a partial dust cover. Red-blue (and red-violet) plots show that bright streaks are consistent with mosaics of bright red dust and background material. Here the plains are also consistent with a partial dust cover; the dark streak is the least covered area. Bright and dark streaks both reverse contrast relative to surrounding plains at phase angles over 100 deg in violet filter images. The similar phase behavior of both bright and dark streaks supports the idea that they are both changes in the amount of dust cover. Red-violet plots of bright streaks are most easily explained by mosaics of optically thick dust and plains material. Lengths of bright streaks are independent of their contrasts. This suggests the streak deposition, if in the mosaic patterns indicated above, is a function of available sites of deposition, rather than atmospheric dust loading. Contrasts of dark streaks with plains indicate the plains have fractional dust covers nealy as great as the maximum additional cover in bright streaks. The bright streaks thus store little of the global supply of dust.

Thomas, P.↗
NASA NTRS1995

NASA Tech Briefs, November 1995

The contents include: 1) Mission Accomplished; 2) Resource Report: Marshall Space Flight Center; 3) NASA 1995 Software of the Year Award; 4) Microbolometers Based on Epitaxial YBa2Cu3O(sub 7-x) Thin Films; 5) Garnet Random-Access Memory; 6) Fabrication of SNS Weak Links on SOS Substrates; 7) High-Voltage MOSFET Switching Circuit; 8) Asymmetric Switching for a PWM H-Bridge Power Circuit; 9) Better Ohmic Contacts for InP Semiconductor Devices; 10) Low-Bandgap Thermovoltaic Materials and Devices; 11) Digital Frequency-Differencing Circuit; 12) Imaging Magnetometer; 13) Computer-Assisted Monitoring of a Complex System; 14) Buffered Telemetry Demodulator; 15) Compact Multifunction Inspection Head; 16) Optical Detection of Fractures in Ceramic Diaphragms; 17) Eddy-Current Detection of Cracks in Reinforced Carbon/Carbon; 18) Apparent Thermal Conductivity of Multilayer Insulation; 19) Optimizing Misch-Metal Compositions in Metal Hydride Anodes; 20) Device for Sampling Surface Contamination; 21) Probabilistic Failure Assessment for Fatigue; 22) Probabilistic Fatigue and Flaw-Propagation Analysis; 23) Windows Program for Driving the TDU-850 Printer; 24) Subband/Transform MATLAB Functions for Processing Images; 25) Computing Equilibrium Chemical Compositions; 26) Program Processes Thermocouple Readings; 27) ICAN-Second-Generation Integrated Composite Analyzer; 28) Integrated Composite Analyzer with Damping Capabilities; 29) Computing Efficiency of Transfer of Microwave Power; 30) Program Calculates Power Demands of Electronic Designs; 31) Cost-Estimation Program; 32) Program Estimates Areas Required by Electronic Designs; 33) Program to Balance Mapped Turbopump Assemblies; 34) BiblioTech; 35) Controlling Mirror Tilt With a Bimorph Actuator; 36) Burst-Disk Device Simulates Effect of Pyrotechnic Device; 37) Bearing-Mounting Concept Accommodates Thermal Expansion; 38) Parallel-Plate Acoustic Absorbers for Hot Environments; 39) Adjustable-Length Strut Withstands Large Cyclic Loads; 40) Tool Indicates Contact Angles in Bearing Raceways; 41) Gravity Slides With Magnetic Braking; 42) High-Torque, Lightweight, Pneumatically Driven Wrench for Small Spaces; 43) Device for Testing Compatibility of an O-Ring; 44) Magnetic Heat Pump Containing Flow Diverters; 45) Variable-Tilt Helicopter Rotor Mast; 46) "Beach-Ball" Robotic Rovers; 47) Apparatus Would Measure Temperatures of Ball Bearings; 48) Flexible Borescope for Inspecting Ducts; 49) Texturing Copper To Reduce Secondary Emission of Electrons; 50) Automated Laser Cutting in Three Dimensions; 51) Algorithm Helps Monitor Engine Operation; 52) Flexible Revision of Data-Processing Communications; 53) Software for Managing the Use of Land; 54) Thermal Strap Increases Cryocooling Efficiency; 55) Reversible Nut With Engagement Indication; 56) Control Algorithms for Kinematically Redundant Manipulators; 57) Computed Hydrogen-Flow Splits in a Rocket Engine; 58) Pressure and Thermal Modeling of Rocket Launches; 59) Field of View of a Spacecraft Antenna: Analysis and Software; 60) Digital Controller for Laser-Beam-Steering Subsystem; 61) More About Beam-Steering Subsystem for Laser Communication; 62) Digital Controller for Laser-Beam-Steering Subsystem: Part 2; 63) Interface Circuit Board for Space-Shuttle Communications; 64) Automated Planning of Spacecraft Telecommunications; 65) Artifacts of Spectral Analysis of Instrument Readings; 66) Neural-Network Controller for Vibration Suppression; 67) Adaptive Finite-Element Computation in Fracture Mechanics; 68) Attitude Control for the Cassini Spacecraft; 69) Analytical Model for Fluid Dynamics in a Microgravity Environment; 70) Study of Rocket-Engine Joints Bonded by NVCU/NARloy-Z; 71) Improved Silicon Nitride for Advanced Heat Engines; 72) Parameters for Welding Aluminum/Lithium Alloys; 73) Lightweight Composite Intertank Structure; 74) Foil Patches Seal Small Vacuum Leaks; 75) Data Base on Cables and Connectors; 76) Effect of Clock Mode on Radiation Hardnessf an ADC; and 77) Fault-Tolerant Control for a Robotic Inspection System.

Source record↗
NASA NTRS1990

Wide-bandgap epitaxial heterojunction windows for silicon solar cells

It is shown that the efficiency of a solar cell can be improved if minority carriers are confined by use of a wide-bandgap heterojunction window. For silicon (lattice constant a = 5.43 A), nearly lattice-matched wide-bandgap materials are ZnS (a = 5.41 A) and GaP (a = 5.45 A). Isotype n-n heterojuntions of both ZnS/Si and GaP/Si were grown on silicon n-p homojunction solar cells. Successful deposition processes used were metalorganic chemical vapor deposition (MO-CVD) for GaP and ZnS, and vacuum evaporation of ZnS. Planar (100) and (111) and texture-etched - (111)-faceted - surfaces were used. A decrease in minority-carrier surface recombination compared to a bare surface was seen from increased short-wavelength spectral response, increased open-circuit voltage, and reduced dark saturation current, with no degradation of the minority carrier diffusion length.

Landis, Geoffrey A.↗
NASA NTRS1983

The NH3 spectrum in Saturn's 5 micron window

Spectra of Saturn's 5-micron window were obtained at the Infrared Telescope Facility on Mauna Kea, Hawaii. The spectra have a resolution of 1.2/cm, and some exhibit extremely low amounts of approximately 300-micron ppt telluric H2O. The Saturn spectra show absorptions by the 2nu2 band of NH3. Long-path laboratory comparison spectra of NH3 were acquired and show considerable deviations in intensity from theoretical predictions. The calibration of Saturn's observed NH3 features with the laboratory data gives 2.0 + or - 0.5 m-amagat of NH3 using the 2nu2 Q-branch at 5.32 microns. The R(1) and R(2) lines yield an abundance about 3 times greater. Absorptions outside the range of the Q-branch can be accounted for by solid NH3 of 10-20 microns equivalent path length. The origin of Saturn's 5-micron flux is mostly thermal with some admixture of solar reflected radiation. A depletion of Saturn's NH3 abundance below the solar value is indicated, but confirmation of this conclusion will require a better understanding of the atmospheric penetration depth at 5 microns and more rigorous modeling of the spectral line formation.

Bjoraker, G. L.↗
NASA NTRSDate not supplied

Passive Dust Mitigation Technologies Being Developed for Demonstration Under Patch Plate Materials Compatibility Analysis Task

With the Artemis program, we are planning longer stays on the surface, with more activities that have the potential to put the astronauts and equipment in contact with greater quantities of lunar dust. The success of these missions will depend on our understanding of material interactions with lunar dust and the development of ways to mitigate dust effects in cases where exposure to dust will lead to failure of components, unacceptable loss of power or thermal control, unacceptable loss of visibility, or health issues. Passive dust mitigation by coating or surface alteration is one method that is being developed and demonstrated under the Space Technology Mission Directorate’s Game Changing Technology, Dust Mitigation Program as part of the Patch Plate Materials Compatibility Assessment Task. The goal of the task is to alter the surfaces of materials in order to passively reduce the adhesion of dust, demonstrate their performance in relevant ground-based tests using lunar simulants, and prepare them for demonstration through experiment on the lunar surface. Optically transparent, sputter deposited, work function matching coatings are being developed to reduce adhesion of dust to windows, lenses and display panels by matching the minimum energy to remove an electron from the surface to that of lunar dust in order to reduce adhesion due to charge transfer. Low surface energy coatings and surfaces for thermal control are also being developed to reduce the bonding of dust with the surface enabling it to be removed more easily. Conductive coatings with the ability to shed dust more easily are being developed for use with the active Electrodynamic Dust Shield technology to help reduce the power needed to remove dust from the surface. Passive dust mitigation surfaces for metals such as aluminum, stainless steel, and titanium are being developed that reduce the area of dust contact with the surfaces through topographical modification using laser ablation patterning to impart hierarchical topographies with nanometer to micrometer length scales in a single step. Topographically modified polymeric materials, both those with extensive space heritage and those with lower technology readiness levels, are also being evaluated. Space suit fabric surfaces that can reduce dust penetration into and through the fabric are also being investigated as well as pristine and topographically modified ceramic materials that exhibit high wear resilience. An overview of the passive dust mitigation surfaces and coatings being developed under this task, ground testing being conducted using lunar simulants, characterization techniques, and materials preparation for flight sample delivery for integration into the Alpha Space Regolith Adherence Characterization experiment going to the lunar surface on a Commercial Lunar Payload Services (CLPS) lander in 2023 will be discussed.

Lunar dust, passive mitigation, lunar simulant, co↗
NASA NTRS1994

Optical Analysis of an Ultra-High resolution Two-Mirror Soft X-Ray Microscope

This work has summarized for a Schwarzschild microscope some relationships between numerical aperture (NA), magnification, diameter of the primary mirror, radius of curvature of the secondary mirror, and the total length of the microscope. To achieve resolutions better than a spherical Schwarzschild microscope of 3.3 Lambda for a perfectly aligned and fabricated system. it is necessary to use aspherical surfaces to control higher-order aberrations. For an NA of 0.35, the aspherical Head microscope provides diffraction limited resolution of 1.4 Lambda where the aspherical surfaces differ from the best fit spherical surface by approximately 1 micrometer. However, the angle of incidence varies significantly over the primary and the secondary mirrors, which will require graded multilayer coatings to operate near peak reflectivities. For higher numerical apertures, the variation of the angle of incidence over the secondary mirror surface becomes a serious problem which must be solved before multilayer coatings can be used for this application. Tolerance analysis of the spherical Schwarzschild microscope has shown that water window operations will require 2-3 times tighter tolerances to achieve a similar performance for operations with 130 A radiation. Surface contour errors have been shown to have a significant impact on the MTF and must be controlled to a peak-to-valley variation of 50-100 A and a frequency of 8 periods over the surface of a mirror.

Shealy, David L.↗
NASA NTRSDate not supplied

GC/MS Method Development for Separating Lunar Volatile Ice Simulant Headspace Gases

Various investigators propose the lunar surface contains widely distributed volatiles, especially water- like species, i.e. OH and H2O. Surface volatiles are theorized to exist as a hydrated regolith layer, concentrated in extremely cold polar permanently shadowed regions (PSR), and/or solar wind implantation reservoirs in lunar glasses. The proposed sources of lunar surface volatiles range from cometary impacts, solar wind, or a supply present during moon formation. Future Artemis missions aim to collect and return the samples containing volatiles collected near lunar polar craters or PSRs. We, as advanced curation scientists, are responsible for developing techniques and methodologies for preserving returned sample integrity as much as possible. Pristine volatile-bearing samples are invaluable to the scientific community seeking to unravel the history of the solar system. Realistically, a sample will experience alteration during collection, transportation back to earth, and storage. The Planetary Exploration and Astromaterials Research Lab (PEARL) seeks to understand temperature and pressure effects on high-fidelity volatile-containing regolith simulants, the foundation for the future of cold curation. This abstract outlines the separation, identification, and quantification of headspace gases over volatile ice feed stock material using gas chromatography/mass spectrometry (GC/MS). Preliminary objectives concentrated on sample handling, reproducibility, and understanding the elution characteristics for each analyte. Initial GC/MS method development experiments utilized diluted static headspace sample preparation. Diluted samples were used because sampling headspace gases directly from a vial containing liquid analyte resulted in overloading of the column and detector. Overloading is evident based on chromatogram peak shapes and instrument contamination, or carry over, between experiments. A mixture of three alcohols were used for a majority of the sample handling and reproducibility studies. Reproducibility was tested via multiple users, calibration curves, and check standards. Stock solutions of condensed lunar volatile analytes included methanol, ammonia in methanol, hydrogen sulfide in water, and an equal volume mixture of methanol, ethanol, and isopropanol. Current samples use room air as the headspace sample matrix, however future experiments will incorporate an inert purge gas, such as argon or nitrogen. Three mL of each analyte solution were capped in separate 20 mL crimp top GC vials. Dilutions were carried out by removing an aliquot of headspace gases with a calibrated 1 mL gastight syringe and immediately transferring to a 20 mL capped crimp top vial. The GC/MS is a Thermo Fisher Trace 1310/ISQ 7000 with a TriPlus RSH autosampler and split/splitless injector module. The experiments outlined in this abstract use the following hardware: a 2.5 mL gastight headspace syringe tool, 1 mm ID x 78.5 mm length ultra-inert straight injection liner, and a TG-BondQ 30 m × 0.32 mm × 10 μm column. Various parameters, such as hardware selection and the temperature, pressure, and split ratio set points, continue to evolve as the overall experiment is refined. Diluted headspace chromatograms were collected for the individual stock solutions. Retention times, peak shapes, and mass spectra were evaluated and added to the data processing method for each molecule of interest. Figure 1 shows the total ion chromatograms for the three major lunar volatile simulant stock solutions: methanol, 7 N ammonia in methanol, and 0.4% hydrogen sulfide in water. Tailing peak shapes for ammonia (2.98 min rt) and water (4.06 min rt) indicate the molecules are not properly eluting from the selected column with the current separation method. Additionally, hydrogen sulfide and ammonia have overlapping peak windows, which could impact quantification. Ongoing experiments aim to address the peak shape and overlapping via the separation method and hardware selection. Sample preparation reproducibility experiments used stock solution containing equal volumes of a non- interactive mixture of methanol, ethanol, and isopropanol. Mass spectrum ion traces were used to identify and quantify all three alcohols. Peaks were automatically detected, identified, and integrated through the mass spectra detection and processing parameters. Calibration response curves and check standards were used to evaluate the validity of the sample preparation procedure. Figure 2 shows the methanol chromatogram peak area versus total headspace dilution volume transferred from the alcohol mixture vial. The calibration response curves and check standards validate sample preparation procedure. Continuing data analysis efforts are working towards correlating the peak area and instrument response factor to the headspace analyte concentration and condensed phase composition. Static headspace gas chromatography theory relies on Dalton’s law, Raoult’s law, Henry’s Law, and the Kolb and Ettre equation to associate peak area to the analyte composition in a non-ideal solution. Equation 1 is a simplified expression derived from the aforementioned theories. Future experiments involve liquid injections of the individual stock solutions, liquid and headspace analysis of various stock solution combinations, and the addition of regolith simulants to the mixtures. Temperature is another variable expected to affect reaction rates and will be explored.

Cecilia L. Amick↗
NASA NTRS2006

Forecasting Coronal Mass Ejections from Line-of-Sight Magnetograms

We show that the length of strong-gradient, strong-field main neutral line, L(sub SGM), which can be measured from line-of-sight magnetograms such as from SOHO/MDI, is both a measure of active-region nonpotentiality and a useful predictor of an active region's future CME productivity. To demonstrate that L(sub SGM) is a nonpotentiality measure, we show that it is strongly correlated with a direct measure of nonpotentiality. For an appropriate choice of a threshold value, an active region s measured LsGM can be used as a predictor of whether the active region will produce a CME within a few days after the magnetogram. For our set of 36 MSFC vector magnetograms of bipolar active regions, L(sub SGM) is found to have a success rate of 80% for prediction of CME productivity in the 0-2 day window. The development of L(sub SGM) as a method of measuring nonpotentiality for forecasting large, fast CMEs from present space based assets is of value to NASA's Space Exploration Initiative (manned missions to the Moon and Mars)

Falconer, D. A.↗
NASA NTRS2016

Performance of NICER Flight X-Ray Concentrator

Neutron star Interior Composition ExploreR (NICER) is a NASA instrument to be onboard International Space Station, which is equipped with 56 pairs of an X-ray concentrator (XRC) and a silicon drift detector for high timing observations. The XRC is based on an epoxy replicated thin aluminum foil X-ray mirror, similar to those of Suzaku and ASTRO-H (Hitomi), but only a single stage parabolic grazing incidence optic. Each has a focal length of 1.085 m and a diameter of 105 mm, with 24 confocally aligned parabolic shells. Grazing incident angles to individual shells range from 0.4 to 1.4 deg. The flight 56 XRCs have been completed and successfully delivered to the payload integration. All the XRC was characterized at the NASA/GSFC 100-m X-ray beamline using 1.5 keV X-rays (some of them are also at 4.5 keV). The XRC performance, effective area and point spread function, was measured by a CCD camera and a proportional counter. The average effective area is about 44 sq cm at 1.5 keV and about 18 sq cm at 4.5 keV, which is consistent with a micro-roughness of 0.5 nm from individual shell reflectivity measurements. The XRC focuses about 91% of X-rays into a 2mm aperture at the focal plane, which is the NICER detector window size. Each XRC weighs only 325 g. These performance met the project requirement. In this paper, we will present summary of the flight XRC performance as well as co-alignment results of the 56 XRCs on the flight payload as it is important to estimate the total effective for astronomical observations.

X-ray concentrator↗
NASA NTRS2000

Laminar Diffusion Flame Studies (Ground- and Space-Based Studies)

Laminar diffusion flames are of interest because they provide model flame systems that are far more tractable for analysis and experiments than more practical turbulent diffusion flames. Certainly, understanding flame processes within laminar diffusion flames must precede understanding these processes in more complex turbulent diffusion flames. In addition, many properties of laminar diffusion flames are directly relevant to turbulent diffusion flames using laminar flamelet concepts. Laminar jet diffusion flame shapes (luminous flame boundaries) have been of particular interest since the classical study of Burke and Schumann because they are a simple nonintrusive measurement that is convenient for evaluating flame structure predictions. Thus, consideration of laminar flame shapes is undertaken in the following, emphasizing conditions where effects of gravity are small, due to the importance of such conditions to practical applications. Another class of interesting properties of laminar diffusion flames are their laminar soot and smoke point properties (i.e., the flame length, fuel flow rate, characteristic residence time, etc., at the onset of soot appearance in the flame (the soot point) and the onset of soot emissions from the flame (the smoke point)). These are useful observable soot properties of nonpremixed flames because they provide a convenient means to rate several aspects of flame sooting properties: the relative propensity of various fuels to produce soot in flames; the relative effects of fuel structure, fuel dilution, flame temperature and ambient pressure on the soot appearance and emission properties of flames; the relative levels of continuum radiation from soot in flames; and effects of the intrusion of gravity (or buoyant motion) on emissions of soot from flames. An important motivation to define conditions for soot emissions is that observations of laminar jet diffusion flames in critical environments, e.g., space shuttle and space station facilities, cannot involve soot emitting flames in order to ensure that test chamber windows used for experimental observations are not blocked by soot deposits, thereby compromising unusually valuable experimental results. Another important motivation to define conditions where soot is present in diffusion flames is that flame chemistry, transport and radiation properties are vastly simplified when soot is absent, making such flames far more tractable for detailed numerical simulations than corresponding soot-containing flames. Motivated by these observations, the objectives of this phase of the investigation were as follows: (1) Observe flame-sheet shapes (the location of the reaction zone near phi=1) of nonluminous (soot free) laminar jet diffusion flames in both still and coflowing air and use these results to develop simplified models of flame-sheet shapes for these conditions; (2) Observe luminous flame boundaries of luminous (soot-containing) laminar jet diffusion flames in both still and coflowing air and use these results to develop simplified models of luminous flame boundaries for these conditions. In order to fix ideas here, maximum luminous flame boundaries at the laminar smoke point conditions were sought, i.e., luminous flame boundaries at the laminar smoke point; (3) Observe effects of coflow on laminar soot- and smoke-point conditions because coflow has been proposed as a means to control soot emissions and minimize the presence of soot in diffusion flames.

Dai, Z.↗