Resistance Welding Simulation of a Thermoplastic Composite Lap Shear Coupon
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Crystallization kinetics↗
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Mineralogy, Petrology and Oxygen Fugacity of the LaPaz Icefield Lunar Basaltic Meteorites and the Origin of Evolved Lunar Basalts
LAP 02205 is a 1.2 kg lunar mare basalt meteorite found in the Lap Paz ice field of Antarctica in 2002 [1]. Four similar meteorites were also found within the same region [1] and all five have a combined mass of 1.9 kg (LAP 02224, LAP 02226, LAP 02436 and LAP 03632, hereafter called the LAP meteorites). The LAP meteorites all contain a similar texture, mineral assemblage, and composition. A lunar origin for these samples comes from O isotopic data for LAP 02205 [1], Fe/Mn ratios of pyroxenes [1-5], and the presence of distinct lunar mineralogy such as Fe metal and baddeleyite. The LAP meteorites may represent an area of the Moon, which has never been sampled by Apollo missions, or by other lunar meteorites. The data from this study will be used to compare the LAP meteorites to Apollo mare basalts and lunar basaltic meteorites, and will ultimately help to constrain their origin.
Collins, S. J.↗
Advances in the analysis and design of adhesive-bonded joints in composite aerospace structures
Several aspects of adhesive-bonded joint analysis and design are presented from the reference of size of structure or load intensity. This integrates the individual characterizations of double-lap, single-lap, stepped-lap, tapered-lap and scarf joints. The paper includes an overview of bonded joint selection from the standpoints of design, fabrication, and processing, each bearing in mind the influence of such considerations on the strength of the joint. A case study is presented of the optimization of a specific relatively thick titanium-to-graphite epoxy stepped-lap joint, using the digital computer analysis program A4EG. The factors accounted for are adhesive plasticity, adherend stiffness imbalance, adherend thermal mismatch, and change of material properties within the range of temperature environment and with load direction. The strength increases obtainable by refining the initial design are demonstrated.
Hart-Smith, L. J.↗
Design, fabrication and test of graphite/polyimide composite joints and attachments for advanced aerospace vehicles
Results of an experimental program to develop several types of graphite/polyimide (GR/PI) bonded and bolted joints for lightly loaded flight components for advanced space transportation systems and high speed aircraft are presented. Tasks accomplished include: a literature survey; design of static discriminator specimens; design allowables testing; fabrication of test panels and specimens; small specimen testing; and standard joint testing. Detail designs of static discriminator specimens for each of the four major attachment types are presented. Test results are given for the following: (1) transverse tension of Celion 3000/PMR-15 laminate; (2) net tension of a laminate for both a loaded and unloaded bolt hole; (3) comparative testing of bonded and co-cured doublers along with pull-off tests of single and double bonded angles; (4) single lap shear tests, transverse tension and coefficient of thermal expansion tests of A7F (LARC-13 amide-imide modified) adhesive; and (5) tension tests of standard single lap, double lap, and symmetric step lap bonded joints. Also, included are results of a finite element analysis of a single lap bonded composite joint.
Barclay, D. L.↗
Flexibilized copolyimide adhesives
Two copolyimides, LARC-STPI and STPI-LARC-2, with flexible backbones were processed and characterized as adhesives. The processability and adhesive properties were compared to those of a commercially available form of LARC-TPI. Lap shear specimens were fabricated using adhesive tape prepared from each of the three polymers. Lap shear tests were performed at room temperature, 177 C, and 204 C before and after exposure to water-boil and to thermal aging at 204 C for up to 1000 hours. The three adhesive systems possess exceptional lap shear strengths at room temperature and elevated temperatures both before and after thermal exposure. LARC-STPI, because of its high glass transition temperature provided high lap shear strengths up to 260 C. After water-boil, LARC-TPI exhibited the highest lap shear strengths at room temperature and 177 C, whereas the LARC-STPI retained a higher percentage of its original strength when tested at 204 C. These flexible thermoplastic copolyimides show considerable potential as adhesives based on this study and because of the ease of preparation with low cost, commercially available materials.
Progar, Donald J.↗
Latent transforming growth factor beta1 activation in situ: quantitative and functional evidence after low-dose gamma-irradiation
The biological activity of transforming growth factor beta1 (TGF-beta) is controlled by its secretion as a latent complex in which it is noncovalently associated with latency-associated peptide (LAP). Activation is the extracellular process in which TGF-beta is released from LAP, and is considered to be a primary regulatory control. We recently reported rapid and persistent changes in TGF-beta immunoreactivity in conjunction with extracellular matrix remodeling in gamma-irradiated mouse mammary gland. Our hypothesis is that these specific changes in immunoreactivity are indicative of latent TGF-beta activation. In the present study, we determined the radiation dose response and tested whether a functional relationship exists between radiation-induced TGF-beta and collagen type III remodeling. After radiation exposures as low as 0.1 Gy, we detected increased TGF-beta immunoreactivity in the mammary epithelium concomitant with decreased LAP immunostaining, which are events consistent with activation. Quantitative image analysis demonstrated a significant (P=0.0005) response at 0.1 Gy without an apparent threshold and a linear dose response to 5 Gy. However, in the adipose stroma, loss of LAP demonstrated a qualitative threshold at 0.5 Gy. Loss of LAP paralleled induction of collagen III immunoreactivity in this tissue compartment. We tested whether TGF-beta mediates collagen III expression by treating animals with TGF-beta panspecific monoclonal antibody, 1D11.16, administered i.p. shortly before irradiation. Radiation-induced collagen III staining in the adipose stroma was blocked in an antibody dose-dependent manner, which persisted through 7 days postirradiation. RNase protection assay revealed that radiation-induced elevation of total gland collagen III mRNA was also blocked by neutralizing antibody treatment. These data provide functional confirmation of the hypothesis that radiation exposure leads to latent TGF-beta activation, support our interpretation of the reciprocal shift in immunoreactivity as evidence of activation, and implicate TGF-beta as a mediator of tissue response to ionizing radiation. The sensitivity of activation to low radiation doses points to a potential role for TGF-beta in orchestrating tissue response to oxidative stress. As such, radiation may be useful as a probe to delineate the consequences of latent TGF-beta activation in situ.
NASA Discipline Radiation Health↗
A Rb-Sr and Sm-Nd Isotope Geochronology and Trace Element Study of Lunar Meteorite LaPaz Icefield 02205
Rubidium-strontium and samarium-neodymium isotopes of lunar meteorite LaPaz Icefield (LAP) 02205 are consistent with derivation of the parent magma from a source region similar to that which produced the Apollo 12 low-Ti olivine basalts followed by mixing of the magma with small amounts (1 to 2 wt%) of trace element-enriched material similar to lunar KREEP-rich sample SaU 169. The crystallization age of LAP 02205 is most precisely dated by an internal Rb-Sr isochron of 2991+/-14 Ma, with an initial Sr-87/Sr-88 at the time of crystallization of 0.699836+/-0.000010. Leachable REE-rich phosphate phases of LAP 02205 do not plot on a Sm-Nd mineral isochron, indicating contamination or open system behavior of the phosphates. Excluding anomalous phases from the calculation of a Sm-Nd isochron yields a crystallization age of 2992+/-85 (initial Epsilon Nd-143 = +2.9+/-0.8) that is within error of the Rb-Sr age, and in agreement with other independent age determinations for LAP 02205 from Ar-Ar and U-Pb methods. The calculated Sm-147/Nd-144 source ratios for LAP 02205, various Apollo 12 and 15 basalts, and samples with strong affinities to KREEP (SaU 169, NWA 773, 15386) are uncorrelated with their crystallization ages. This finding does not support the involvement of a common KREEP component as a heat source for lunar melting events that occurred after crystallization of the lunar magma ocean.
Rankenburg, K.↗
Computer-Controlled Cylindrical Polishing Process for Development of Grazing Incidence Optics for Hard X-Ray Region
The presentation includes grazing incidence X-ray optics, motivation and challenges, mid spatial frequency generation in cylindrical polishing, design considerations for polishing lap, simulation studies and experimental results, future scope, and summary. Topics include current status of replication optics technology, cylindrical polishing process using large size polishing lap, non-conformance of polishin lap to the optics, development of software and polishing machine, deterministic prediction of polishing, polishing experiment under optimum conditions, and polishing experiment based on known error profile. Future plans include determination of non-uniformity in the polishing lap compliance, development of a polishing sequence based on a known error profile of the specimen, software for generating a mandrel polishing sequence, design an development of a flexible polishing lap, and computer controlled localized polishing process.
Khan, Gufran Sayeed↗
Scheduling Position, Navigation and Time Service Requests from Non-dedicated Lunar Constellations
This paper presents a centralized scheduler that satisfies user requests for Position, Navigation, and Time (PNT) services from an ad-hoc, non-dedicated orbital constellation around the Moon. Traditional, dedicated GNSS networks provide service 24/7, which allows users to acquire localization services at-will. For ad-hoc networks, a coordinated schedule is needed to ensure Quality of Service (QoS) guarantees for user localization, while satisfying non-dedicated assets’ usage constraints. This scheduler bridges this coordination gap by leveraging Mixed Integer-Linear Programming (MILP) to schedule this “as-needed” localization service while respecting the constraints on each asset. In upcoming decades there is expected to be a substantial increase in Lunar missions. Many of these missions will feature low-cost surface assets near the moon’s polar regions and small-sat science missions in orbit. Most missions need PNT capabilities to ensure safe operations and meet their science objectives, but low-cost missions may not be able to support the large power, mass, and weight that a weak GNSS or DSN based navigation solution would entail. Asset localization has been demonstrated using a decentralized extended Kalman Filter (DEKF) in the previously presented Lunar Autonomous PNT System (LAPS). Within the LAPS simulation environment, a module has been developed to generate the coordinated user-asset schedules described above; this Service Scheduler Module (SSM) allows for complete end-to-end testing of the entire system. Within SSM, a user service request consists of a location on the Lunar surface, a cumulative service duration, and a window in which service must occur. SSM takes as input these requests and the LAPS-predicted positional degree of precision as the QoS for each available set of orbital assets. A simple, baseline MILP model is formulated to provide the highest-precision service balanced across all requests. To reflect the non-dedicated nature of the constellation, this baseline model is augmented with additional asset-specific load capacity constraints or availability constraints. The load capacity constraints limit total time spent providing service, and the availability constraints reflect blockout times or availability windows when the assets are not otherwise occupied. SSM outputs two schedules: the user schedule to indicate their service times and expected QoS, and a satellite schedule to be transmitted to the orbiting constellation, describing when each non-dedicated asset provides PNT service. SSM is predominantly implemented in MATLAB and allows the use of any MILP solver to generate the resulting schedules. This paper describes the SSM - LAPS interface, how the output of LAPS is used to construct the MILP, and how SSM provides user localization service while satisfying constraints. It will also demonstrate the tool’s flexibility for formulating schedules for the end user and the constellation, focusing on scenarios that match real-world proposed missions. It will detail how SSM can be used to compare the addition of load capacity constraints, satellite availability constraints, and QoS guarantees for the users. Finally, we describe how SSM can be used to support the design of the ad-hoc constellation itself. The resulting integrated capability will support the design of future ad-hoc Lunar PNT networks, enabling high-quality, low-cost Lunar exploration
Swarm↗
Ultrasonic Evaluation of Thermal Degradation in Adhesive Bonds
The critical role played by adhesive bonds in lap joints is well known. A good knowledge of the mechanical properties of adhesive bonds in lap joints is a prerequisite to the design and reliable prediction of the performance of these bonded structures. Furthermore, the lap joint may be subject to high-temperature environments in service. Early detection of the degree of thermal degradation in adhesive bonds is required under these circumstances. A variety of ultrasonic nondestructive evaluation (NDE) techniques can be used to determine the thickness and the elastic moduli of adhesively bonded joints. In this paper we apply a previously developed technique based on the leaky Lamb wave (LLW) experiment to investigate the possibility of characterizing the thermal degradation of adhesive bonds in lap joints. The degradation of the adhesive bonds is determined through comparison between experimental data and theoretical calculations.
degradation lap joints mechanical properties bonde↗
Analysis and design of advanced composite bounded joints
Advances in the analysis of adhesive-bonded joints are presented with particular emphasis on advanced composite structures. The joints analyzed are of double-lap, single-lap, scarf, stepped-lap and tapered-lap configurations. Tensile, compressive, and in-plane shear loads are covered. In addition to the usual geometric variables, the theory accounts for the strength increases attributable to adhesive plasticity (in terms of the elastic-plastic adhesive model) and the joint strength reductions imposed by imbalances between the adherends. The solutions are largely closed-form analytical results, employing iterative solutions on a digital computer for the more complicated joint configurations. In assessing the joint efficiency, three potential failure modes are considered. These are adherend failure outside the joint, adhesive failure in shear, and adherend interlaminar tension failure (or adhesive failure in peel). Each mode is governed by a distinct mathematical analysis and each prevails throughout different ranges of geometric sizes and proportions.
Hart-Smith, L. J.↗
Test and analysis of Celion 3000/PMR-15, graphite/polyimide bonded composite joints: Data report
Standard single lap, double lap and symmetric step lap bonded joints of Celion 3000/PMR-15 graphite/polyimide composite were evaluated. Composite to composite and composite to titanium joints were tested at 116 K (-250 F), 294 K (70 F) and 561 K (550 F). Joint parameters evaluated are lap length, adherend thickness, adherend axial stiffness, lamina stacking sequence and adherend tapering. Advanced joint concepts were examined to establish the change in performance of preformed adherends, scalloped adherends and hybrid systems. The material properties of the high temperature adhesive, designated A7F, used for bonding were established. The bonded joint tests resulted in interlaminar shear or peel failures of the composite and there were very few adhesive failures. Average test results agree with expected performance trends for the various test parameters. Results of finite element analyses and of test/analysis correlations are also presented.
Cushman, J. B.↗
Test and analysis of Celion 3000/PMR-15, graphite/polyimide bonded composite joints: Summary
Standard single lap, double lap and symmetric step lap bonded joints of Celion 3000/PMR-15 graphite/polyimide composite were evaluated. Composite to composite and composite to titanium joints were tested at 116K (-250 F), 294K (70 F) and 561K (550 F). Joint parameters evaluated were lap length, adherend thickness, adherend axial stiffness, lamina stacking sequence and adherend tapering. Tests of advanced joint concepts were also conducted to establish the change in performance of preformed adherends, scalloped adherends and hybrid systems. Special tests were conducted to establish material properties of the high temperature adhesive, designated A7F, used for bonding. Most of the bonded joint tests resulted in interlaminar shear or peel failures of the composite. There were very few adhesive failures. Average test results agree with expected performance trends for the various test parameters. Results of finite element analyses and of test/analysis correlations are also presented.
Cushman, J. B.↗
Evaluation of a high temperature adhesive for fabricating graphite/PMR-15 polyimide structures
Tests are conducted to measure shear strength, shear modulus and flatwise tensile strength of the A7F (amide-imide modified LARC-13) adhesive system. An investigation is also conducted to determine the effect of geometric material parameters, and elevated temperature on the static strength of standard joints. Single-lap and double-lap composite joints, and single, double and step lap composite to metal joints are characterized. A series of advanced joints consisting of preformed adherends, adherends with scalloped edges and joints with hybrid interface plies are tested and compared to baseline single and double-lap designs.
Hill, S. G.↗
Thermal QNDE detection of airframe disbonds
Thermographic characterization of aircraft bonded lap joints offers a quick noncontacting technique to acquire information for structural integrity assessment. This paper discusses recent research to optimize the technique and determine the limits of its applicability. The temperature of the outer surface of the lap joint is increased by the application of heat flux from either flash or quartz lamp heaters. The time dependence of the surface temperature of the lap joint is imaged radiometrically. Measurements are presented for a range of specimens, ranging from samples fabricated with well characterized disbonds to actual aircraft. A technique for processing these images to enhance the contrast between bonded and disbonded regions of the lap joint is presented. Numerical models of the technique simulate the procedure. These simulations provide a cost efficient method for optimizing the technique by varying parameters such as the time for application of heat. These simulations facilitate the definition of parameters difficult to determine experimentally, such as the minimum air gap required for a disbond to be detected. Good agreement between measurements and these simulations is found.
Aging Aircraft↗
Joint Strength Optimization and Damping Assessment of NiTi-Polymer Matrix Hybrid Composites
Approaches to optimize the adhesive joint strength between shape memory alloy ribbons and carbon fiber-reinforced epoxy composites were investigated for potential use as either an actuating structure or a dampening composite for structural applications. The interfacial bond strength between nickel-titanium (NiTi) and a polymer matrix composite (PMC) was measured by double lap shear testing as a function of NiTi surface treatment and adhesive material. The effect of NiTi surface treatment on damping was investigated using dynamic mechanical analysis. Lap shear data show that treating the surfaces of NiTi ribbons by light sandblasting and primer application increased the interfacial bond strength by 20 percent over the baseline composite structure. Lap shear data also reveal that out of three different film adhesives investigated, samples bonded with AF 191U and Hysol® 9696U display the highest adhesive joint strengths. Optical microscopy reveals that most samples failed by either cohesive failure within the adhesive or by adhesive failure at either the adhesive/PMC or NiTi/adhesive interface. Adhering NiTi to the PMC did not appear to negatively impact damping performance; however, a more thorough examination into NiTi's role on vibration damping should be investigated.
lap shear↗
Improvement of adhesive-bonded structural joints
Investigation is described of methods for obtaining uniform shear stress distribution in adhesives used in double-lap bonded joints. Design rules for reducing adhesive peak shear stresses are listed. Test results of an analysis of straight-lap joint design and stepped-lap joint design are given.
Evensen, H. A.↗
Analysis of bonded joints
A refined elastic analysis of bonded joints which accounts for transverse shear deformation and transverse normal stress was developed to obtain the stresses and displacements in the adherends and in the bond. The displacements were expanded in terms of polynomials in the thicknesswise coordinate; the coefficients of these polynomials were functions of the axial coordinate. The stress distribution was obtained in terms of these coefficients by using strain-displacement and stress-strain relations. The governing differential equations were obtained by integrating the equations of equilibrium, and were solved. The boundary conditions (interface or support) were satisfied to complete the analysis. Single-lap, flush, and double-lap joints were analyzed, along with the effects of adhesive properties, plate thicknesses, material properties, and plate taper on maximum peel and shear stresses in the bond. The results obtained by using the thin-beam analysis available in the literature were compared with the results obtained by using the refined analysis. In general, thin-beam analysis yielded reasonably accurate results, but in certain cases the errors were high. Numerical investigations showed that the maximum peel and shear stresses in the bond can be reduced by (1) using a combination of flexible and stiff bonds, (2) using stiffer lap plates, and (3) tapering the plates.
Srinivas, S.↗