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DOE OSTI2018

Characterization of a large-area iQID imager for safeguards applications

Environmental sampling and sample analyses by the International Atomic Energy Agency is a key method for verifying declarations in international safeguards agreements. Quantitative Digital Autoradiography for Environmental Samples is a system developed by Pacific Northwest National Laboratory to examine environmental swipe samples (ESS) prior to subsequent, destructive analysis. This approach is passive and noninvasive for imaging beta and gamma emissions, which transmit through the plastic bags containing the ESS. Alpha particle imaging is also possible with different ESS containers. This technology is based on a portable, real-time, event-counting, high spatial resolution system called iQID (ionizing-radiation Quantum Imaging Detector), which is made from commercial, off-the-shelf components. This includes a scintillator in direct contact with a micro-channel plate image intensifier and a lens for imaging the intensified scintillation events onto a CCD/CMOS camera. The QDARES large-area iQID includes a fiber-optic taper coupled to the image intensifier which increases the imaging area to a ~100 cm square with a 105 mm x 105 mm taper. In this study, we describe new characterization results, including spatial resolution, energy response, minimum detectable activity for several isotopes, detector uniformity, and count-rate capability.

98 NUCLEAR DISARMAMENT, SAFEGUARDS, AND PHYSICAL P↗

DOE OSTI2023

Full Spectrum, 350 - 2500 nm, Leaf and Canopy Spectral Reflectance, Seward Peninsula, Alaska, 2017

Full-range (350 - 2500 nm) leaf and canopy reflectance spectra of various Arctic tundra ecosystem endmembers, including species-level leaf reflectance, canopy-scale species endmember spectra, plot-scale spectra, and transect spectra as well as non-vegetated surface (NVS) spectra. The datasets were collected at the three core NGEE-Arctic watersheds, Kougarok, Teller, and Council within the larger Seward Peninsula, Alaska region. The data were collected in the months of July and August of 2017 using a full-range Spectra Vista Corporation (SVC) HR-1024i spectroradiometer. Leaf-level spectra were collected with the original SVC leaf clip/plant probe connected to the spectrometer through a 1.15 meter long fiber optic cable, while canopy-scale reflectance was collected with an 8-degree field-of-view (FOV) foreoptic lens. All spectral measurements were collected as calibrated surface radiance and converted to surface reflectance using a 99.99% reflective Spectralon white reference standard. For those canopy spectra collected with associated functional trait data, the FOV of the instrument was positioned to include the same leaves harvested for functional trait measurements, including leaf mass per area (LMA) and foliar carbon and nitrogen content (see associated dataset). This data package includes 26 files in a variety of formats including processed canopy and leaf spectra (*.csv), processed dGPS locations (*.csv and *.kmz), digital photographs of spectral targets (*.jpg) and raw data from spectroradiometer and dGPS instruments (compressed as tar.gz). Metadata files include data descriptions (_dd.csv) for tabular data and a key to species symbols used in data files. All included files are listed and described in NGA110_flmd.csv.The Next-Generation Ecosystem Experiments: Arctic (NGEE Arctic), was a research effort to reduce uncertainty in Earth System Models by developing a predictive understanding of carbon-rich Arctic ecosystems and feedbacks to climate. NGEE Arctic was supported by the Department of Energy's Office of Biological and Environmental Research.The NGEE Arctic project had two field research sites: 1) located within the Arctic polygonal tundra coastal region on the Barrow Environmental Observatory (BEO) and the North Slope near Utqiagvik (Barrow), Alaska and 2) multiple areas on the discontinuous permafrost region of the Seward Peninsula north of Nome, Alaska.Through observations, experiments, and synthesis with existing datasets, NGEE Arctic provided an enhanced knowledge base for multi-scale modeling and contributed to improved process representation at global pan-Arctic scales within the Department of Energy's Earth system Model (the Energy Exascale Earth System Model, or E3SM), and specifically within the E3SM Land Model component (ELM).

54 ENVIRONMENTAL SCIENCES↗

DOE OSTI2023

Full spectrum (350-2500 nm) leaf and canopy spectral reflectance, Seward Peninsula, Alaska, 2019

Full-range (350 - 2500 nm) leaf and canopy reflectance spectra of various Arctic tundra ecosystem endmembers, including species-level leaf reflectance, canopy-scale species endmember spectra, plot-scale spectra, and transect spectra. These data were collected in support of ongoing NASA ABoVE AVIRIS data synthesis work. The datasets were collected at the NGEE-Arctic watershed sites, Kougarok MM64 and MM80, and Teller MM27 on the Seward Peninsula, Alaska. The data were collected in July 2019 using a full-range Spectra Vista Corporation (SVC) HR-1024i spectroradiometer. Leaf-level spectra were collected with the original SVC leaf clip/plant probe connected to the spectrometer through a 1.15 meter long fiber optic cable, while canopy-scale reflectance was collected with an 8-degree field-of-view (FOV) foreoptic lens. All spectral measurements were collected as calibrated surface radiance and converted to surface reflectance using a 99.99% reflective Spectralon white reference standard. For those canopy spectra collected with associated functional trait data, the FOV of the instrument was positioned to include the same leaves harvested for functional trait measurements, including leaf mass per area (LMA) and foliar carbon and nitrogen content (see leaf trait data package for these data). Canopy spectra were obtained for 23 different species, and leaf spectra for 8 species. This data package includes processed canopy and leaf spectra (*.csv), processed dGPS locations (*.csv and *.kmz), digital photographs of spectral targets (*.jpg) and raw data from spectroradiometer and dGPS instruments (compressed as tar.gz). Metadata files include data descriptions (_dd.csv) for tabular data and a key to species symbols used in data files. All included files are listed and described in NGA212_flmd.csv.The Next-Generation Ecosystem Experiments: Arctic (NGEE Arctic), was a 15-year research effort (2012-2027) to reduce uncertainty in Earth System Models by developing a predictive understanding of carbon-rich Arctic ecosystems and feedbacks to climate. NGEE Arctic was supported by the Department of Energy's Office of Biological and Environmental Research. The NGEE Arctic project had two field research sites: 1) located within the Arctic polygonal tundra coastal region on the Barrow Environmental Observatory (BEO) and the North Slope near Utqiagvik (Barrow), Alaska and 2) multiple areas on the discontinuous permafrost region of the Seward Peninsula north of Nome, Alaska. Through observations, experiments, and synthesis with existing datasets, NGEE Arctic provided an enhanced knowledge base for multi-scale modeling and contributed to improved process representation at global pan-Arctic scales within the Department of Energy's Earth system Model (the Energy Exascale Earth System Model, or E3SM), and specifically within the E3SM Land Model component (ELM).

54 ENVIRONMENTAL SCIENCES↗

NASA NTRS2004

Hand-Held Color Meters Based on Interference Filters

Small, inexpensive, hand-held optoelectronic color-measuring devices based on metal-film/dielectric-film interference filters are undergoing development. These color meters could be suitable for use in a variety of applications in which there are requirements to quantify or match colors for aesthetic purposes but there is no need for the high spectral resolution of scientific-grade spectrometers. Such applications typically occur in the paint, printing, and cosmetic industries, for example. The figure schematically depicts a color meter of this type being used to measure the color of a sample in terms of the spectrum of light reflected from the sample. Light from a white source (for example, a white light-emitting diode) passes through a collimating lens to the sample. Another lens collects some of the light reflected from the sample and focuses the light onto the input end of optical fiber. Light emerging from the output end of the optical fiber illuminates an array of photodetectors covered with metal/dielectric-film interference filters like those described in Metal/Dielectric-film Interference Color Filters (NPO-20217), NASA Tech Briefs, Vol. 23, No. 2 (February 1999), page 70. Typically, these are wide-band-pass filters, as shown at the bottom of the figure. The photodetector array need not be of any particular design: it could be something as simple as an assembly containing several photodiodes or something as elaborate as an active-pixel sensor or other imaging device. What is essential is that each of the photodetectors or each of several groups of photodetectors is covered with a metal/dielectric-film filter of a different color. In most applications, it would be desirable to have at least three different filters, each for a spectral band that contains one of the three primary additive red, green, and blue colors. In some applications, it may be necessary to have more than three different color filters in order to characterize subtle differences in color (or in the sensation of color) that cannot be characterized with sufficient precision by use of the primary colors alone.

Snyder, G. Jeffrey↗

DOE OSTI2018

Lens design challenges for scintillator-based neutron imaging

Neutron imaging is an important diagnostic to study inertial confinement fusion (ICF) implosions at the National Ignition Facility (NIF) using neutrons emitted in the fusion reactions. Analysis of time-gated images of the primary fusion (14.1 MeV) and down-scattered (6-12 MeV) neutrons based on their time-of-flight allows for the reconstruction of the burning hot spot undergoing fusion and the surrounding cold fuel. The Los Alamos National Laboratory (LANL) Advanced Imaging team has been providing these images since 2011. Currently, two additional lines of sight are being designed and built for NIF to allow three-dimensional reconstructions. Neutron imaging relies on the conversion of neutrons into light to be captured by an imaging system through the use of a scintillator. Although the current neutron imaging system utilizes a fiber scintillator array, a newly designed imaging system will consist of a thick monolithic scintillator and custom-designed lenses to collect the light. The custom lens has to resolve an image produced in the thick volume of the scintillator and therefore needs a large depth of field.

42 ENGINEERING↗

NASA NTRS1988

Real-Time Keratometer

Optical/electronic keratometer system produces contour map of corneal surface illuminated by infrared light pulses. Prevents operator error and eliminates need to apply fluorescent liquids to cornea. Keratometer provides both video display and numerical recording for corneal-transplant and radial-keratotomy surgery and for contact-lens fitting. Optical system of keratometer, circular grating pattern transmitted to corneal surface reflected onto identical circular grating on surface of fiber plate, producing Moire pattern. Data-analysis-and-display mode, laser light pulsed, and Moire pattern converted to digital information in frame grabber. Digital picture information sent to computer for processing and display.

Frazer, Robert E.↗

DOE OSTI2014

TH-C-17A-12: Integrated CBCT and Optical Tomography System On-Board a Small Animal Radiation Research Platform (SARRP)

Purpose: We present a newly developed on-board optical tomography system for SARRP. Innovative features include the compact design and fast acquisition optical method to perform 3D soft tissue radiation guidance. Because of the on-board feature and the combination of the CBCT, diffusive optical tomography (DOT), bioluminescence and fluorescence tomography (BLT and FT), this integrated system is expected to provide more accurate soft tissue guidance than an off-line system as well as highly sensitive functional imaging in preclinical research. Methods: Images are acquired in the order of CBCT, DOT and then BLT/FT, where the SARRP CBCT and DOT are used to provide the anatomical and optical properties information to enhance the subsequent BLT/FT optical reconstruction. The SARRP stage is redesigned to include 9 imbedded optical fibers in contact with the animal's skin. These fibers, connected to a white light lamp or laser, serve as the light sources for the DOT or FT, respectively. A CCD camera with f/1.4 lens and multi-spectral filter set is used as the optical detector and is mounted on a portable cart ready to dock into the SARRP. No radiation is delivered during optical image acquisition. A 3-way mirror system capable of 180 degree rotation around the animal reflects the optical signal to the camera at multiple projection angles. A special black-painted dome covers the stage and provides the light shielding. Results: Spontaneous metastatic bioluminescent liver and lung tumor models will be used to validate the 3D BLT reconstruction. To demonstrate the capability of our FT system, GastroSense750 fluorescence agent will be used to imaging the mouse stomach and intestinal region in 3D. Conclusion: We expect that this integrated CBCT and optical tomography on-board a SARRP will present new research opportunities for pre-clinical radiation research. Supported by NCI RO1-CA 158100.

60 APPLIED LIFE SCIENCES↗

DOE OSTI2015

Discovery of two gravitationally lensed quasars in the Dark Energy Survey

In this study, we present spectroscopic confirmation of two new lensed quasars via data obtained at the 6.5m Magellan/Baade Telescope. The lens candidates have been selected from the Dark Energy Survey (DES) and WISE based on their multi-band photometry and extended morphology in DES images. Images of DES J0115-5244 show two blue point sources at either side of a red galaxy. Our long-slit data confirm that both point sources are images of the same quasar at z s = 1.64. The Einstein Radius estimated from the DES images is 0.51''. DES J2146-0047 is in the area of overlap between DES and the Sloan Digital Sky Survey (SDSS). Two blue components are visible in the DES and SDSS images. The SDSS fiber spectrum shows a quasar component at z s = 2.38 and absorption compatible with Mg II and Fe II at z l = 0.799, which we tentatively associate with the foreground lens galaxy. The long-slit Magellan spectra show that the blue components are resolved images of the same quasar. Furthermore, the Einstein Radius is 0.68'' corresponding to an enclosed mass of 1.6 × 10 11 M ⊙ . Three other candidates were observed and rejected, two being low-redshift pairs of starburst galaxies, and one being a quasar behind a blue star. These first confirmation results provide an important empirical validation of the data-mining and model-based selection that is being applied to the entire DES dataset.

74 ATOMIC AND MOLECULAR PHYSICS↗

NASA NTRS1994

Improved Composite Fabrication Process Minimizes Damage To Fibers

Document describes improved process for making fiber/matrix composite materials, especially SiC-fiber/metal-matrix materials that fail gradually when overstressed. Gradual-failure characteristic imparted by coating fibers with relatively soft material that yields in compliance with deformations of matrix.

Petrasek, Don↗

NASA NTRS1992

Laser velocimeter for near-surface measurements

The present invention relates to a laser Doppler velocimeter for near-wall measurements which includes at least one beam-turning device. The beam-turning device receives laser light, reflects and redirects the light at various angles in order to obtain measurements for all three velocity components at grazing incident angles. The beam-turning device includes a mirror or prism at one end which reflects the received light in a particular direction. A collector lens receives the particle scattered light from which the relevant velocity components are determined. The beam-turning device can also be a miniature fiber optic head which outputs laser light and can be turned in any direction.

Johnson, Dennis A.↗

DOE OSTI2018

Fabrication of the DESI corrector lenses

The Dark Energy Spectroscopic Instrument (DESI) is under construction to measure the expansion history of the Universe using the Baryon Acoustic Oscillation technique. The spectra of 35 million galaxies and quasars over 14000 square degrees will be measured during the life of the experiment. A new prime focus corrector for the KPNO Mayall telescope will deliver light to 5000 fiber optic positioners. The fibers in turn feed ten broad-band spectrographs. We describe the DESI corrector optics, a series of six fused silica and borosilicate lenses. The lens diameters range from 0.8 to 1.1 meters, and their weights 84 to 237 kg. Most lens surfaces are spherical, and two are challenging 10 th -order polynomial aspheres. The lenses have been successfully polished and treated with an antireflection coating at multiple subcontractors, and are now being integrated into the DESI corrector barrel assembly at University College London. We describe the final performance of the lenses in terms of their various parameters, including surface figure, homogeneity, and others, and compare their final performance against the demanding DESI corrector requirements. Also we describe the reoptimization of the lens spacing in their corrector barrel after their final measurements are known. Finally we assess the performance of the corrector as a whole, compared to early budgeted estimates.

46 INSTRUMENTATION RELATED TO NUCLEAR SCIENCE AND ↗

DOE OSTI2021

Kerr-lens mode-locked Cr:ZnS oscillator reaches the spectral span of an optical octave

We report, to the best of our knowledge, the first super-octave femtosecond polycrystalline Cr:ZnS laser at the central wavelength 2.4 µm. The laser is based on a non-polarizing astigmatic X-folded resonator with normal incidence mounting of the gain element. The chromatic dispersion of the resonator is controlled with a set of dispersive mirrors within one third of an optical octave over 2.05–2.6 µm range. The resonator’s optics is highly reflective in the range 1.8–2.9 µm. The components of the oscillator’s output spectrum at the wavelengths 1.6 µm and 3.2 µm are detected at –60 dB with respect to the main peak. Average power of few-cycle Kerr-lens mode-locked laser is 1.4 W at the pulse repetition frequency 79 MHz. That corresponds to 22% conversion of cw radiation of Er-doped fiber laser, which we used for optical pumping of the Cr:ZnS oscillator.

71 CLASSICAL AND QUANTUM MECHANICS, GENERAL PHYSIC↗

NASA NTRS2005

Method and apparatus for a multibeam beacon laser assembly for optical communications

An optical beacon is comprised of a telescope having a primary focal plane or Coud? focal plane, a plurality of fiber coupled laser sources for generating a plurality of beams, a collimator for collimating the plurality of beams, and optics for combining and focusing the plurality of collimated beams onto the primary or Coud? focal plane of the telescope. The telescope propagates the optical beacon, which is arranged into a ring of incoherent plurality of collimated beams. The apparatus further comprises fiber splitters coupled to each laser source to provide at least eight beams from at least four laser sources. The optics comprises a prism assembly, a combiner lens, a focusing lens and a field lens for focusing the plurality of collimated beams onto the primary focal plane or Coud? focal plane of the telescope.

Biswas, Abhijit↗

DOE OSTI2024

Visible to near-infrared spectral reflectance along the NGEE-Arctic tram transect, Utqiagvik (Barrow), Alaska, 2015-2018

Canopy spectral reflectance collected measured in 2015-2018 along the NGEE-Arctic tram located on the Barrow Environmental Observatory (BEO), Barrow, Alaska. Measurements were made using a PP-Systems UniSpec-DC spectrometer mounted on an automatically operated instrument cart. Spectra were collected at 137 stop points at 0.5 m intervals along the tram transect. Transect runs were collected daily, or multiple times per day, from April or May through to August or September each year. Downwelling radiance was measured using a 2 meter fiber optic cable connected to a cosine diffuser. Upwelling (i.e. reflected) radiance was measured using a 2 meter cable connected to a 12 degree field-of-view (FOV) lens. Canopy reflectance was calculated using the ratio of upwelling to downwelling radiance measured over a 99.99% reflectance Spectralon standard measured at the start of each measurement set. Unprocessed spectral data are presented in .spu files. Metadata are provided in csv files, and the instrument manual (pdf). The Next-Generation Ecosystem Experiments: Arctic (NGEE Arctic), was a 15-year research effort (2012-2027) to reduce uncertainty in Earth System Models by developing a predictive understanding of carbon-rich Arctic ecosystems and feedbacks to climate. NGEE Arctic was supported by the Department of Energy's Office of Biological and Environmental Research. The NGEE Arctic project had two field research sites: 1) located within the Arctic polygonal tundra coastal region on the Barrow Environmental Observatory (BEO) and the North Slope near Utqiagvik (Barrow), Alaska and 2) multiple areas on the discontinuous permafrost region of the Seward Peninsula north of Nome, Alaska. Through observations, experiments, and synthesis with existing datasets, NGEE Arctic provided an enhanced knowledge base for multi-scale modeling and contributed to improved process representation at global pan-Arctic scales within the Department of Energy's Earth system Model (the Energy Exascale Earth System Model, or E3SM), and specifically within the E3SM Land Model component (ELM).

54 ENVIRONMENTAL SCIENCES↗

DOE OSTI2018

Inhomogeneity of Cellulose Microfibril Assembly in Plant Cell Walls Revealed with Sum Frequency Generation Microscopy

Sum frequency generation (SFG) vibrational spectroscopy can selectively detect and analyze noncentrosymmetric components interspersed in amorphous matrices; this principle has been used for studies of nanoscale structure and mesoscale assembly of cellulose in plant cell walls. However, the spectral information averaged over a large area or volume cannot provide regiospecific or tissue-specific information of different cells in plants. Here, we demonstrate spatially resolved SFG analysis and imaging by combining a broad-band SFG spectroscopy system with an optical microscope. The system was designed to irradiate both narrow-band 800 nm and broad-band tunable IR beams through a single reflective objective lens, but from opposite sides of the surface normal direction of the sample. The developed technique was used to reveal inhomogeneous distributions of cellulose microfibrils within single cell walls, such as cotton fibers and onion epidermis as well as among different tissues in Arabidopsis inflorescence stems and bamboo culms. SFG microscopy can be used for vibrational spectroscopic imaging of other biological systems in complement to conventional Fourier transform infrared spectroscopy and confocal Raman microscopy.

37 INORGANIC, ORGANIC, PHYSICAL, AND ANALYTICAL CH↗

NASA NTRS1999

NGST/XRCF Design and Build Wavescope System Pallet

Based on the successful Wavescope demonstration at MSFC at the end of March, the decision was made by the optical testing team to purchase an upgraded Wavescope from AOA. The MSFC version would include: a higher resolution camera (1000 x 1000 pixels); a higher density lenslet array (150 x 150); updated software; and longer cables (to accommodate the remote operation of the Wavescope optical head which was resident in the Beam Guide Tube). The AOA proposal for the new instrument was received in mid-April, and delivered to MSFC in mid-July. A considerable amount of effort was expended to provide the infrastructure needed for Wavescope operation, and to incorporate it into the overall test system. This was provided by the Wavescope System Pallet (WSP) built by UAH. The WSP is illustrated. Several instruments are incorporated on this pallet. These include the: Wavescope optical head; a PDI wavefront sensor; a point spread function sensor; a Leica light-based distance measuring sensor. In addition there is a single mode fiber point source (fed from a separate source pallet) which serves both as a reference for the Wavescope and as a source point for the test mirror. There is a dual function lens which both collimates the beam from the test image point, and images the test mirror onto the lenslet array. There is a high quality Collimator which can provide a flat input wavefront directly into the Wavescope. There are also various aids such as an alignment laser, an alignment telescope, alignment sticks and apertures. The WSP was delivered to MSFC on 7/28/99. An picture shows the WSP installed in the Guide Tube at the X-Ray Calibration Facility (XRCF).

Geary, Joe↗

NASA NTRS2015

Understanding Beam Alignment in a Coherent Lidar System

Optical beam alignment in a coherent lidar (or ladar) receiver system plays a critical role in optimizing its performance. Optical alignment in a coherent lidar system dictates the wavefront curvature (phase front) and Poynting vector) matching of the local oscillator beam with the incoming receiver beam on a detector. However, this alignment is often not easy to achieve and is rarely perfect. Furthermore, optical fibers are being increasingly used in coherent lidar system receivers for transporting radiation to achieve architectural elegance. Single mode fibers also require stringent mode matching for efficient light coupling. The detector response characteristics vary with the misalignment of the two pointing vectors. Misalignment can lead to increase in DC current. Also, a lens in front of the detector may exasperate phase front and Poynting vector mismatch. Non-Interaction of Waves, or the NIW property indicates the light beams do not interfere by themselves in the absence of detecting dipoles. In this paper, we will analyze the extent of misalignment on the detector specifications using pointing vectors of mixing beams in light of the NIW property.

Prasad, Narasimha S.↗

DOE OSTI2014

Methods and apparatus for vertical coupling from dielectric waveguides

A frequency-chirped nano-antenna provides efficient sub-wavelength vertical emission from a dielectric waveguide. In one example, this nano-antenna includes a set of plasmonic dipoles on the opposite side of a SiYV.sub.4 waveguide from a ground plane. The resulting structure, which is less than half a wavelength long, emits a broadband beam (e.g., >300 nm) that can be coupled into an optical fiber. In some embodiments, a diffractive optical element with unevenly shaped regions of high- and low-index dielectric material collimates the broadband beam for higher coupling efficiency. In some cases, a negative lens element between the nano-antenna and the diffractive optical element accelerates the emitted beam's divergence (and improves coupling efficiency), allowing for more compact packaging. Like the diffractive optical element, the negative lens element includes unevenly shaped regions of high- and low-index dielectric material that can be designed to compensate for aberrations in the beam emitted by the nano-antenna.

42 ENGINEERING↗