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At least 127 records · Page 7
All sourcesNASA NTRSDOE OSTI
DOE OSTI2025

Fractionation of Filamentous Algae from Mixed Biofilms

Filamentous algae, which grow in long, hair-like filaments within biofilms, play a crucial role in wastewater treatment due to their ability to produce significant biomass and their resistance to predation compared to traditional microalgal treatments. These algae can effectively uptake and utilize pollutants, particularly excessive nitrogen (ammonia, nitrate, nitrite) and phosphorus (phosphate), making filamentous algae valuable for wastewater treatment, as well as bioethanol and biodiesel production due to high lipid productions. However, each algal species possesses different capacities, necessitating a thorough genetic identification and understanding of each community. A major challenge in accurately assessing these communities is the lack of coverage in large sequencing databases which can lead to misrepresentation of the true composition and abundance of organisms and overall sequencing bias. To address this, I evaluated chemical and physical techniques for separating filamentous algae from mixed biofilms to achieve clean genetic sequencing results. I employed pH washing (0.001M HCl, 0.001M HCl, DiH2O, 0.0001M HCl, 0.001M HCl) for chemical treatment, followed by physical separation through centrifugation (5000rpm, 6500rpm) or filtration (2mm, 250um, 75um). The most successful method was deionized water washing, which yielded clear differences across stacked filters; the 2mm filtrate showed high levels of filamentous algae, with microalgae eluting in the 75um filtrate or remaining within agglutinations of algae larger filters. Base washing eluted the highest concentrations of microalgae, with larger filter sizes retaining more filamentous algae, indicating the breakdown of extracellular polymeric substances (EPS). Our downstream plans include sending the high-throughput next-generation sequencing to confirm the purity and ratios of filamentous and non-filamentous algae, as well as bacteria present, thereby validating the success of our treatments. Potential applications include creating community-based fractions for analysis, refining current sequencing data with clearer isolations, and generating designer biofilms to enhance our understanding of community interactions.

59 BASIC BIOLOGICAL SCIENCES↗
DOE OSTI2017

Embedded Filaments in IRAS 05463+2652: Early Stage of Fragmentation and Star Formation Activities

We present a multiwavelength data analysis of IRAS 05463+2652 (hereafter I05463+2652) to study star formation mechanisms. A shell-like structure around I05463+2652 is evident in the Herschel column density map, which is not associated with any ionized emission. Based on the Herschel submillimeter images, several parsec-scale filaments (including two elongated filaments, “s-fl” and “nw-fl” having lengths of ∼6.4 and ∼8.8 pc, respectively) are investigated in the I05463+2652 site. The Herschel temperature map depicts all these features in a temperature range of ∼11–13 K. 39 clumps are identified and have masses between ∼70--945 M{sub ⊙}. The majority of clumps (having M{sub clump}≳300 M{sub ⊙}) are distributed toward the shell-like structure. 175 young stellar objects (YSOs) are selected using the photometric 1–5 μm data and a majority of these YSOs are distributed toward the four areas of high column density (≳5×10{sup 21} cm{sup −2}; A {sub V} ∼ 5.3 mag) in the shell-like structure, where massive clumps and a spatial association with filament(s) are also observed. The knowledge of observed masses per unit length of elongated filaments and critical mass length reveals that they are supercritical. The filament “nw-fl” is fragmented into five clumps (having M{sub clump}∼100--545 M{sub ⊙}) and contains noticeable YSOs, while the other filament “s-fl” is fragmented into two clumps (having M{sub clump}∼170--215 M{sub ⊙}) without YSOs. Together, these observational results favor the role of filaments in the star formation process in I05480+2545. This study also reveals the filament “s-fl,” containing two starless clumps, at an early stage of fragmentation.

79 ASTRONOMY AND ASTROPHYSICS↗
DOE OSTI2019

Alignment between Filaments and Galaxy Spins from the MaNGA Integral-field Survey

Halos and galaxies acquire their angular momentum during the collapse of the surrounding large-scale structure. This process imprints alignments between galaxy spins and nearby filaments and sheets. Low-mass halos grow by accretion onto filaments, aligning their spins with the filaments, whereas high-mass halos grow by mergers along filaments, generating spins perpendicular to the filament. Here, we search for this alignment signal using filaments identified with the "Cosmic Web Reconstruction" algorithm applied to the Sloan Digital Sky Survey Main Galaxy Sample and galaxy spins from the Mapping Nearby Galaxies at Apache Point Observatory (MaNGA) integral-field unit survey. MaNGA produces a map of the galaxy's rotational velocity, allowing direct measurement of the galaxy's spin direction, or unit angular momentum vector projected onto the sky. We find no evidence for alignment between galaxy spins and filament directions. We do find hints of a mass-dependent alignment signal, which is in 2σ–3σ tension with the mass-dependent alignment signal in the MassiveBlack-II and Illustris hydrodynamical simulations. However, the tension vanishes when galaxy spin is measured using the Hα emission line velocity rather than stellar velocity. Lastly, in simulations we find that the mass-dependent transition from aligned to anti-aligned dark matter halo spins is not necessarily present in stellar spins: we find a stellar spin transition in Illustris but not in MassiveBlack-II, highlighting the sensitivity of spin-filament alignments to feedback prescriptions and subgrid physics.

79 ASTRONOMY AND ASTROPHYSICS↗
DOE OSTI2026

Weak-lensing Detection of Intercluster Filaments in Three Nearby Cluster Systems

Abstract Direct detection of intercluster filaments is challenging due to their low surface density, resulting in a weak deflection field. We present weak-lensing detections of intercluster filaments using wide-field Dark Energy Camera observations from the Local Volume Complete Cluster Survey. A matched-filter method was applied to identify filamentary structures in three nearby ( z < 0.1) systems centered on A401, A2029, and A3558. We discover two filaments (>3 σ ) in each system, with the strongest detections (5.2 σ –5.8 σ ) around A401 and A2029. In particular, we report the first robust weak-lensing detections (≳5 σ ) of the intercluster bridges connecting the cluster pairs A401/399, A2029/2033, A2029/SIG, and A3558/3556. Adopting a filament convergence model motivated by numerical simulations, we infer the maximum convergence ( κ 0 ) and characteristic width ( h c ) for all six filaments, yielding κ 0 ∼ 0.016–0.040 and h c ∼ 0.23–0.43 Mpc. The performance of the matched-filter technique is validated using mock shear catalogs and further tested on a null field around A2351. We explore the potential of using the B-mode lensing signal of filaments to suppress cluster-induced shear contamination. We also quantify the biasing effect of closely separated terminal clusters to the filament signal. These results demonstrate the feasibility of directly mapping dark matter filaments with current and future wide-field weak-lensing datasets.

Shinde, Rahul [Brown University] (ORCID:0000000273↗
NASA NTRS1981

The field and plasma configuration of a filament overlying a solar bipolar magnetic region

This paper presents an analytic model for a finite-size straight filament suspended horizontally in a steady state over a bipolar magnetic region. The equations of magnetostatic equilibrium are integrated exactly. The solution obtained illustrates the roles played by the electric current, magnetic field, pressure, and plasma weight in the balance of force everywhere in space. A specific example of a filament of diameter 50,000 km, with a density two orders of magnitude over the corona and supported by a magnetic field of about 4 gauss is included. The filament temperature can take values ranging from a small fraction to a few times the coronal temperature, depending on the internal electric current of the filament. To produce a cool filament, such as the quiescent prominence, the solution is required to have an internal field with a strong component along the filament, giving rise to helical structures. A hot filament such as the X-ray coronal loop can be produced as a twisted magnetic flux tube embedded in a strong background field aligned parallel to the filament and having lower density and temperature. The basic steps of construction can be used to develop models more realistic than the ones presented for their analytic simplicity.

Low, B. C.↗
NASA NTRS1995

KAO and AAT observations of the Galactic Center filaments

We have used the Kuiper Airborne Observatory (KAO) and the Anglo-Australian Telescope (AAT) to investigate the nature of the filamentary radio emission from the Galactic center region. KAO observations of the FIR line and continuum emission from the radio peak G0.095+0.012 and the E2 thermal radio filament northeast of the Galactic center can be produced by numerous nearby stars with T(sub eff) approx. 35,000 K; these can account for both the FIR luminosity and the excitation of the gas. Much of the FIR continuum and most of the strong (Si II) (34.8 micron) line emission are probably produced in the ionized gas of the filament. The FIR (O III) 52 and 88 micron lines imply an electron density of a few hundred; when compared with the radio emission measure, this implies the filament is roughly tubular or somewhat flattened in the plane of the sky. The (O III) and (S III) lines show higher excitation associated with the filament, and suggest that exciting stars may be located within the filaments and/or southeast of the E2 filament. AAT observations in the near infrared (NIR) in fact reveal a nearby cluster of hot stars southeast of the E2 filament. Additional hot stars, not identifiable from their NIR spectra, are likely to be present. These stars and those in the cluster can plausibly produce the observed radio and FIR emission in the region. The morphology of the filament is not explained by existing information however.

Erickson, Edwin F.↗
NASA NTRS1995

Single crystal silicon filaments fabricated in SOI: A potential IR source for a microfabricated photometric CO2 sensor

The objective of this project was to design, fabricate, and test single crystal silicon filaments as potential black body IR sources for a spectrophotometric CO2 sensing microsystem. The design and fabrication of the silicon-on-insulator (SOI) filaments are summarized and figures showing the composite layout of the filament die (which contains four filaments of different lengths -- 500 microns, 1 mm, 1.5 mm and 2 mm -- and equal widths of 15 microns) are presented. The composite includes four mask layers: (1) silicon - defines the filament dimensions and contact pads; (2) release pit - defines the oxide removed from under the filament and hence, the length of the released filament; (3) Pyrex pit - defines the pit etched in the Pyrex cap (not used); and (4) metal - defines a metal pattern on the contact pads or used as a contact hole etch. I/V characteristics testing of the fabricated SOI filaments is described along with the nitride-coating procedures carried out to prevent oxidation and resistance instability.

Tu, Juliana↗
NASA NTRS2001

Stabilization of posture by precision touch of the index finger with rigid and flexible filaments

Light touch of the index finger with a stationary surface at non-mechanically supportive force levels (<100 g) greatly attenuates the body sway of standing subjects. In three experiments, we evaluated the properties of finger contact and of the contacted object necessary to produce postural stabilization in subjects standing heel-to-toe with eyes closed, as well as how accurately hand position can be controlled. Experiment 1 involved finger contact with flexible filaments of different bending strengths, a flat surface, and an imagined spatial position. Contact with the flat surface was most effective in attenuating sway; the flexible filaments were much less effective but still significantly better than imagined contact. Experiment 2 compared the effectiveness of finger contact with a flexible filament, a rigid filament of the same diameter, a flat surface, and an imagined spatial position. The rigid filament and flat surface conditions were equally effective in attenuating body sway and were greatly superior to contact with the flexible filament, which was superior to imagined contact. Experiment 3 included five conditions: arms by sides; finger "contact" with an imagined spatial position; finger contact with a flat surface; finger contact with a flexible filament attempting to maintain it bent; and contact with the flexible filament attempting not to bend it. The arms by sides and finger "contact" with an imagined position conditions did not differ significantly; all three conditions involving actual finger contact showed significantly less center of pressure and hand sway, but contact with the flat surface was most effective in attenuating both postural and hand displacement. In all three experiments, the level of force applied in fingertip contact conditions was far below that necessary to provide mechanical stabilization. Our findings indicate that: (1) stimulation of a small number of receptors in the fingertip is adequate to allow stabilization of sway, (2) fingertip force levels as low as 5-10 g provide some stabilization, (3) contact with a stationary spatial referent is most effective, and (4) independent control of arm and torso occurs when finger contact is allowed.

NASA Discipline Neuroscience↗
NASA NTRS2005

Flare Emission Onset in the Slow-Rise and Fast-Rise Phases of an Erupting Solar Filament Observed with TRACE

We observe the eruption of an active-region solar filament of 1998 July 11 using high time cadence and high spatial resolution EUV observations from the TRACE sareiii'ce, along with soft X-ray images from the soft X-ray telescope (SXT) on the Yohkoh satellite, hard X-ray fluxes from the BATSE instrument on the (CGRO) satellite and from the hard X-ray telescope (HXT) on Yohkoh, and ground-based magnetograms. We concentrate on the initiation of the eruption in an effort to understand the eruption mechanism. First the filament undergoes slow upward movement in a "slow rise" phase with an approximately constant velocity of approximately 15 km/s that lasts about 10-min, and then it erupts in a "fast-rise" phase, reaching a velocity of about 200 km/s in about 5-min, followed by a period of deceleration. EUV brightenings begin just before the start of the filament's slow rise, and remain immediately beneath the rising filament during the slow rise; initial soft X-ray brightenings occur at about the same time and location. Strong hard X-ray emission begins after the onset of the fast rise, and does not peak until the filament has traveled a substantial altitude (to a height about equal to the initial length of the erupting filament) beyond its initial location. Our observations are consistent with the slow-rise phase of the eruption resulting from the onset of "tether cutting" reconnection between magnetic fields beneath the filament, and the fast rise resulting from an explosive increase in the reconnection rate or by catastrophic destabilization of the overlying filament-carrying fields. About two days prior to the event new flux emerged near the location of the initial brightenings, and this recently- emerged flux could have been a catalyst for initiating the tether-cutting reconnection. With the exception of the initial slow rise, our findings qualitatively agree with the prediction for erupting-flux-rope height as a function of time in a model discussed by Chen & Shibata (2000) based on reconnection between emerging flux and a flux rope.

Sterling, A. C.↗
NASA NTRS2005

Mineralized Remains of Morphotypes of Filamentous Cyanobacteria in Carbonaceous Meteorites

The quest for conclusive evidence of microfossils in meteorites has been elusive. One difficulty arises from the fact than many abiotic or inorganic microstructures, mineral grains, and coating artifacts can mimic the smaller representatives of the microbial world that possess very simple morphologies (unicellular cocci or bacilli). However, there exist a wide variety of large, filamentous trichomic prokaryotic microorganisms (cyanobacteria and sulfur bacteria) with sufficiently well known and complex morphologies that they can be recognized and are known to be of unquestionable biogenic origin. The taphonomic modes of fossilization and their of their life habits and processes frequently result in distinctive chemical biosignatures associated with carbonization, silicification, calcification, phosphatization and metal-binding properties of their cell-walls, trichomes, sheaths and extracellular polymeric substances (EPS). Strong differences of mineral concentrations in closely associated and visibly differentiated cellular microstructures provide strong evidence of biogenicity. This evidence is further enhanced by the detection of recognizable and distinct microstructures (e.g., uniseriate or multiseriate filaments, trichomes, sheaths, cells of proper sizes and size distributions) and growth characteristics (e.g., basal or apical cells, true or false branching of trichomes, tapered or uniform filaments, robust or thin sheaths) and reproductive and nitrogen fixation habits (e.g., baeocytes, hormogonia, akinetes and heterocysts), Microfossils of cyanobacteria and cyanobacterial mats and stromatolites have been recognized a described from many of the most ancient rocks on Earth. The crucial problem lies in developing valid protocols and methodologies for establishing that the putative microfossils are truly indigenous and not merely recent microbial contaminants. During the past several years, we have conducted Field Emission Scanning Electron Microscopy (FESEM) investigations of freshly fractured interior surfaces of carbonaceous meteorites, terrestrial rocks, and recent microbial extremophiles and filamentous cyanobacteria. These studies have resulted in the detection in a several carbonaceous meteorites of the mineralized remains of a wide variety of complex filamentous trichomic microorganisms. These embedded forms are consistent in size and microstructure with well-preserved morphotypes of mat- forming filamentous trichomic cyanobacteria and the degraded remains of microfibrils of cyanobacterial sheaths. We present the results of comparative imaging studies and EDAX elemental analyses of recent cyanobacteria (e.g. Calothrix, Oscillatoria, and Lyngbya) that are similar in size, morphology and microstructure to morphotypes found embedded in meteorites. EDAX elemental studies reveal that forms found in carbonaceous meteorites often have highly carbonized sheaths in close association with permineralized filaments, trichomes and microbial cells. Ratios of critical bioelements (C:O, C:N, C:P, and C:S) reveal dramatic differences between microfossils in Earth rocks and meteorites and in filaments, trichomes, hormogonia, and cells of recent cyanobacteria.

Hoover, Richard B.↗
NASA NTRS2006

Using SOHO to Understand CME-Producing Quiet-Region Filament Eruptions

In recent years we have been studying solar eruptions in an attempt to determine their primary initiation mechanism. We have focused on events involving filaments, because motions of the filaments just prior to their violent eruption are indicative of changes in the entire magnetic field system involved in the eruption. When the pre-eruption filament resides in a quiet region, the motions leading up to eruption are slower than in similar eruptions in active regions due to the weaker magnetic field strength and correspondingly lower Alfven velocities. These early motions manifest themselves in a slow rise (a few km/s) of the filament, in some cases lasting several hours. After this the filament and associated magnetic structures erupt rapidly, accelerating to speeds of a few 10 kmh over a few minutes. Because of their slow evolution, quiet-region eruptions such as these can be effectively studied in EUV with SOHO/EIT, with its regular cadence of about 12 min. For several cases we have combined EIT images with SOHO/MDI magnetograms and data from other other instruments, and compared our observations with predictions from various eruption scenarios, in particular the "breakout" (Antiochos 1998), "tether cutting" (e.g., Moore et al. 2001), and MHD instability mechanisms. Here we present a representative example of a quiet-region eruption involving a filament ejection, that occurred on 2001 February 28 in a magnetically quadrupolar region and produced a halo CME in SOHO/LASCO images. In addition to EIT and MDI, we analyzed spectral data from SOHO/CDS and soft X-ray (SXR) images from Yohkoh/SXT. We found that flux emergence occurred near one end of the filament, and that both this emergence and resulting microflaring in SXRs and EUV were temporally and spatially closely related to the start of the filament's slow rise. Intensity changes (dimmings and brightenings) in the EIT and SXT images indicate that fields far removed from the erupting core were involved in the eruption, and that breakout-type reconnection did occur. Our observations allow us to investigate whether breakout was the trigger of the eruption, or merely a consequence of a more fundamental eruption process such as tether cutting or MHD instability occurring in a complex magnetic environment.

Sterling, A. C.↗
NASA NTRS2013

An SDO/AIA-Observed Filament Eruption Triggered by a Lid-Removal Onset Mechanism

An eruption of a solar filament often presages the onset of a more general solar eruption, often leading to a solar flare and coronal mass ejection (CME). Among the mechanisms suggested for triggering eruptions are flux cancellation, flux emergence, tether‐cutting reconnection, and breakout reconnection. Here we present an example of a filament eruption due to a different trigger mechanism, which we call ``lid removal,'' whereby a magnetic structure overlying the filament is removed by a preceding adjacent eruption, rendering MHD unstable the magnetic system containing the filament and resulting in the subsequent eruption of the filament. This filament eruption occurred on 23 Jan 2013, and was well‐seen in SDO/AIA 193 Ang images. Prior to its eruption the filament was at an approximately constant height above the solar surface for approx. 4 hours, before smoothly lifting off. Evidence for the overlying "lid'' field was difficult to discern in 193 Ang images, but was apparent in hotter coronal images, such as SDO/AIA 335. Removal of the lid field was due to an eruption of that field visible in the hotter‐corona images. In this way, the lid‐removal filament‐eruption mechanism is similar to recent observations of connected or cascading eruptions originating from magnetically‐linked locations.

Sterling, Alphonse C.↗
NASA NTRS2013

An SDO/AIA-Observed Filament Eruption Triggered by a Lid-Removal Onset Mechanism

An eruption of a solar filament often presages the onset of a more general solar eruption, often leading to a solar flare and coronal mass ejection (CME). Among the mechanisms suggested for triggering eruptions are flux cancellation, flux emergence, tether-cutting reconnection, and breakout reconnection. Here we present an example of a filament eruption due to a different trigger mechanism, which we call "lid removal,'' whereby a magnetic structure overlying the filament is removed by a preceding adjacent eruption, rendering MHD unstable the magnetic system containing the filament and resulting in the subsequent eruption of the filament. This filament eruption occurred on 23 Jan 2013, and was well-seen in SDO/AIA 193 Ang images. Prior to its eruption the filament was at an approximately constant height above the solar surface for approx 4 hours, before smoothly lifting off. Evidence for the overlying "lid'' field was difficult to discern in 193 Ang images, but was apparent in hotter coronal images, such as SDO/AIA 335. Removal of the lid field was due to an eruption of that field visible in the hotter‐corona images. In this way, the lid‐removal filament‐eruption mechanism is similar to recent observations of connected or cascading eruptions originating from magnetically‐linked locations.

Sterling, Alphonse C.↗
DOE OSTI2022

Formation of Nano- and Micro-Scale Surface Features Induced by Long-Range Femtosecond Filament Laser Ablation

In this work, we study the characteristics of femtosecond-filament-laser–matter interactions and laser-induced periodic surface structures (LIPSS) at a beam-propagation distance up to 55 m. The quantification of the periodicity of filament-induced self-organized surface structures was accomplished by SEM and AFM measurements combined with the use of discrete two-dimensional fast Fourier transform (2D-FFT) analysis, at different filament propagation distances. The results show that the size of the nano-scale surface features increased with ongoing laser filament processing and, further, periodic ripples started to form in the ablation-spot center after irradiation with five spatially overlapping pulses. The effective number of irradiating filament pulses per spot area affected the developing surface texture, with the period of the low spatial frequency LIPSS reducing notably at a high pulse number. The high regularity of the filament-induced ripples was verified by the demonstration of the angle-of-incidence-dependent diffraction of sunlight. This work underlines the potential of long-range femtosecond filamentation for energy delivery at remote distances, with suppressed diffraction and long depth focus, which can be used in biomimetic laser surface engineering and remote-sensing applications.

36 MATERIALS SCIENCE↗
DOE OSTI2015

Deinococcus radiodurans RecA nucleoprotein filaments characterized at the single-molecule level with optical tweezers

Deinococcus radiodurans can survive extreme doses of ionizing radiation due to the very efficient DNA repair mechanisms that are able to cope even with hundreds of double-strand breaks. RecA, the critical protein of homologous recombination in bacteria, is one of the key components of the DNA-repair system. Repair of double-strand breaks requires RecA binding to DNA and assembly of the RecA nucleoprotein helical filaments. The Escherichia coli RecA protein (EcRecA) and its interactions with DNA have been extensively studied using various approaches including single-molecule techniques, while the D. radiodurans RecA (DrRecA) remains much less characterized. However, DrRecA shows some remarkable differences from E. coli homolog. Here we combine microfluidics and single-molecule DNA manipulation with optical tweezers to follow the binding of DrRecA to long double-stranded DNA molecules and probe the mechanical properties of DrRecA nucleoprotein filaments at physiological pH. Our data provide a direct comparison of DrRecA and EcRecA binding to double-stranded DNA under identical conditions. We report a significantly faster filaments assembly as well as lower values of persistence length and contour length for DrRecA nucleoprotein filaments compared to EcRecA. Our results support the existing model of DrRecA forming more frequent and less continuous filaments relative to those of EcRecA. - Highlights: • We investigate Deinococcus radiodurans RecA interactions with long double-stranded DNA at the single-molecule level. • At physiological pH D. radiodurans RecA forms nucleoprotein filaments significantly faster relative to Escherichia coli RecA. • D. radiodurans RecA-dsDNA nucleoprotein filaments are more flexible and slightly shorter compared to those of E. coli RecA.

60 APPLIED LIFE SCIENCES↗
DOE OSTI2017

Fast imaging of filaments in the X-point region of Alcator C-Mod

A rich variety of field-aligned fluctuations has been revealed using fast imaging of D α emission from Alcator C-Mod's lower X-point region. Field-aligned filamentary fluctuations are observed along the inner divertor leg, within the Private-Flux-Zone (PFZ), in the Scrape-Off Layer (SOL) outside the outer divertor leg, and, under some conditions, at or above the X-point. The locations and dynamics of the filaments in these regions are strikingly complex in C-Mod. Changes in the filaments’ generation appear to be ordered by plasma density and magnetic configuration. Filaments are not observed for plasmas with n/n Greenwald ≲ 0.12 nor are they observed in Upper Single Null configurations. In a Lower Single Null with 0.12 ≲ n/n Greenwald ≲ 0.45 and Bx∇B directed down, filaments typically move up the inner divertor leg toward the X-point. Reversing the field direction results in the appearance of filaments outside of the outer divertor leg. With the divertor targets “detached”, filaments inside the LCFS are seen. Lastly, these studies were motivated by observations of filaments in the X-point and PFZ regions in MAST, and comparisons with those observations are made.

70 PLASMA PHYSICS AND FUSION TECHNOLOGY↗
DOE OSTI2023

Characterization of 3D printing filaments containing metal additives and their particulate emissions

Polylactic acid (PLA) filaments are widely used in fused filament fabrication (FFF) processes (3D printing). Filament additives such as metallic particles incorporated into PLA to modify functional and aesthetic features of print objects are becoming increasingly popular. However, the identities and concentrations of low percentage and trace metals in these filaments have not been well described in either the literature or product safety information included with the product. Here, we report the structures and concentrations of metals in selected Copperfill, Bronzefill and Steelfill filaments. We also report size-weighted number concentrations and size-weighted mass concentrations of particulate emissions as a function of print temperature for each filament. Particulate emissions were heterogenous in shape and size with airborne particles below 50 nm diameter dominating the size-weighted particle concentrations and larger particles (approximately 300 nm) dominating the mass weighted particle concentration. Results indicate that potential exposure to particles in the nano-size range increase when using print temperatures above 200o C. Because inhalation exposure to nanoparticles has been linked to adverse health outcomes, we suggest that using lower print temperatures for specific metal-fill filaments may reduce their operational hazard.

36 MATERIALS SCIENCE↗
DOE OSTI2025

High-Resolution Full-Field Structural Microscopy of the Voltage-Induced Filament Formation in VO 2 -Based Neuromorphic Devices

In order to make neuromorphic functions in memristive devices more efficient, information about the structural properties of filament formation at the micro- and mesoscopic scales is necessary. Despite extensive research on VO 2 , a key material due to its filament formation, local operando structural measurements remain challenging and often involve destructive specimen preparation and long rastering times, greatly limiting the scope of experimental studies. Utilizing dark-field X-ray microscopy (DFXM), a fullfield imaging modality, structural signatures of the filament formation process operando are revealed in VO 2 devices. DFXM experiments illustrate that rutile filaments contain isolated monoclinic clusters, indicating structural nonuniformity interior to the filament. The formation of the rutile phase beneath device electrodes was shown to precede filament development, followed by the formation of filament paths guided by nucleation sites within the device. Finally, a medium-term (<30 min) memory mechanism is observed in VO 2 , mediated by sites within the device gap that tend to switch at significantly lower voltages after electrical cycling, a tendency that persists through a brief thermal reset. High spatial resolution, large field-of-view, structure selectivity, and fast signal acquisition of DFXM provided insight into structural features of the filamentary channel and surrounding regions during voltage cycling.

75 CONDENSED MATTER PHYSICS, SUPERCONDUCTIVITY AND↗