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Search indexed NASA NTRS and DOE OSTI research on propulsion, heat transfer, battery materials and energy systems. Follow report and document links to the original sources.

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At least 127 records · Page 7
All sourcesNASA NTRSDOE OSTI
DOE OSTI2026

High-resolution bandpass x-ray imaging with crystal reflectors: Overcoming geometric aberrations

The imaging problem of a specular reflector is revisited. Retaining terms through the second order in the reflector surface expansion, we derive the form of the aberration-limiting aperture for arbitrary magnification, assuming no bandwidth limitations. A permissible relative aperture size of the reflector is limited by a set relative aberration tolerance and scales with the tangent of the central glancing angle of incidence. These limiting aberrations become practically insignificant near backscattering. The results extend to x-ray diffracting crystals in symmetric Bragg geometry shaped as an ellipsoid of revolution. This geometry permits polychromatic imaging for hard x-rays over a bandwidth defined by the accepted range of Bragg angles, thereby suppressing aberrations of higher orders. We assess ellipsoidal crystal imagers using ray tracing simulations for two high-magnification designs with Bragg angles far from and close to backscattering. Finally, in both cases, the ellipsoidal crystals produce images of higher quality compared to those formed by equivalent toroidal crystal imagers.

Bragg reflection↗
DOE OSTI2020

Two-dimensional image edge enhancement using two orders of Bragg diffraction

The process of two-dimensional image edge enhancement with an acousto-optical spatial filter using two orders of light diffraction is studied. It is theoretically shown that the diffraction that occurs in a paratellurite crystal on a ‘slow’ acoustic wave propagating orthogonally to the optical axis of the crystal allows enhancing a two-dimensional edge of an image, transferred by optical radiation with a wavelength of 0.63 μm in a wide band of acoustic frequencies 25 – 50 MHz. Enhancement of a two-dimensional image edge at an acoustic frequency of 29 MHz is experimentally demonstrated. (paper)

71 CLASSICAL AND QUANTUM MECHANICS, GENERAL PHYSIC↗
DOE OSTI2020

Experimental studies of 1.5 – 1.6 μm high-power single-frequency semiconductor lasers

High-power semiconductor laser systems based on 1.5 – 1.6 μm single-frequency distributed feedback (DFB) lasers with a sidewall Bragg diffraction grating are developed and their current – voltage, light – current, and spectral characteristics are experimentally studied. The characteristics of conventional lasers with a Fabry – Perot cavity and DFB lasers fabricated from one and the same heterostructure are compared. At a pump current not exceeding 700 mA, a conventional laser with a cavity length of 1.6 mm and a mesa-stripe width of 3 μm emits a power no lower than 200 mW versus 150 mW of the DFB laser; both lasers are mounted in a housing 11 mm in diameter. The DFB laser mounted in a butterfly housing emits a power no lower than 100 mW at the exit of the single-mode cable at a pump current not exceeding 500 mA, which, at a 60 % coupling efficiency, corresponds to a power no lower than 165 mW; the side-mode suppression ratio in this case is no lower than 53 dB. It is shown that the wavelength deviation with changing pump current and temperature is almost an order of magnitude lower for the DFB laser than for the conventional laser. (paper)

36 MATERIALS SCIENCE↗
DOE OSTI2026

Structural origin of resonant diffraction in RuO2

We report Ru L3-edge resonant X-ray diffraction studies on single crystal and (001) oriented epitaxial films of RuO2. We investigate the distinct Q = (100) and (001) Bragg-forbidden reflections as a function of incident energy, azimuthal angle, and temperature. The results show that the observed resonant diffraction in RuO2 is fully consistent with a resonant charge anisotropy signal of structural origin permitted by the parent (non-magnetic) rutile P42/mnm space group. These results significantly constrain the magnetic contribution to the resonant diffraction signal and indicate the unlikely existence of k = 0 antiferromagnetic order in RuO2.

36 MATERIALS SCIENCE↗
DOE OSTI2024

Bragg Spot Finder (BSF): a new machine-learning-aided approach to deal with spot finding for rapidly filtering diffraction pattern images

Macromolecular crystallography contributes significantly to understanding diseases and, more importantly, how to treat them by providing atomic resolution 3D structures of proteins. This is achieved by collecting X-ray diffraction images of protein crystals from important biological pathways. Spotfinders are used to detect the presence of crystals with usable data, and the spots from such crystals are the primary data used to solve the relevant structures. Having fast and accurate spot finding is essential, but recent advances in synchrotron beamlines used to generate X-ray diffraction images have brought us to the limits of what the best existing spotfinders can do. This bottleneck must be removed so spotfinder software can keep pace with the X-ray beamline hardware improvements and be able to see the weak or diffuse spots required to solve the most challenging problems encountered when working with diffraction images. In this paper, we first present Bragg Spot Detection (BSD), a large benchmark Bragg spot image dataset that contains 304 images with more than 66 000 spots. We then discuss the open source extensible U-Net-based spotfinder Bragg Spot Finder (BSF), with image pre-processing, a U-Net segmentation backbone, and post-processing that includes artifact removal and watershed segmentation. Finally, we perform experiments on the BSD benchmark and obtain results that are (in terms of accuracy) comparable to or better than those obtained with two popular spotfinder software packages ( Dozor and DIALS ), demonstrating that this is an appropriate framework to support future extensions and improvements.

36 MATERIALS SCIENCE↗
DOE OSTI2025

DXRD : a user-friendly suite of two- and multiple-beam dynamical X-ray diffraction programs

The DXRD program suite consisting of a series of dynamical theory programs is introduced for computing dynamical X-ray diffraction from single crystals. Its interactive graphical user interfaces (GUIs) allow general users to make complicated calculations with minimal effort. It can calculate plane-wave Darwin curves of single crystals (or multiple crystals) for both the Bragg and Laue cases, including grazing-incidence diffraction and backward diffraction (with Bragg angles approaching 90°). It is also capable of simulating rocking curves for divergent incident X-ray beams with finite bandwidths. A unique feature of DXRD is that it provides a convenient GUI-based multiple-beam diffraction program that can accurately compute arbitrary N-beam diffraction of any geometry using a universal 4N × 4N matrix method. DXRD also provides a mapping program for plotting all the multiple-beam diffraction lines (monochromator glitches) in the azimuth–energy coordinate system. All these functions make DXRD a convenient and powerful software tool for designing crystal-based synchrotron/X-ray optics (monochromators, analyzers, polarizers, phase plates etc.) and for crystal characterization, X-ray spectroscopy and X-ray diffraction teaching.

Bragg reflection↗
DOE OSTI2021

High-power narrow spectrum GaSb-based DBR lasers emitting near 2.1 µm

Stable high-power narrow-linewidth operation of the 2.05–2.1 µm GaSb-based diode lasers was achieved by utilizing the sixth-order surface-etched distributed Bragg reflector (DBR) mirrors. The DBR multimode devices with 100 µm wide ridge waveguides generated ~850 mW in the continuous wave (CW) regime at 20°C. The device CW output power was limited by thermal rollover. The laser emission spectrum was defined by Bragg reflector reflectivity at all operating currents in a wide temperature range. Finally, the devices operated at DBR line with detuning from gain peak exceeding 10 meV.

77 NANOSCIENCE AND NANOTECHNOLOGY↗
NASA NTRS1969

Polarimeter for celestial X rays.

Polarimeter using 45 degree Bragg angle reflection applied to rocket payload design for determining polarization of celestial sources X rays

Kalata, K.↗
NASA NTRS1974

Stellar and solar X-ray polarimetry

Astronomical stellar and solar studies involving X-ray polarimetry are discussed along with the statistical limitations inherent in polarimeter measurements and the design principles of a number of polarimeter types. Attention is given to photoelectric polarimeters, secondary fluorescence X-ray polarimeters, Borrmann-effect polarimeters, circular polarization analyzers, gamma-ray polarimeters, and multilayer reflection polarimeters. Bragg crystal polarimeters are considered, taking into account the theory of the polarimeter operation, aspects of instrument design, and the occurrence of systematic errors. The design and the performance of a rocket and a satellite Thomson-scattering polarimeter are also examined.

Novick, R.↗
NASA NTRS1975

A large-area lithium-fluoride Bragg spectrometer for stellar X-ray astronomy

A large-area Bragg spectrometer used to search for the Fe XXV X-ray emission lines of Sco X-1 is described. The device has 3400 sq cm of LiF on nine crystal panels aligned perpendicular to the longitudinal axis of the rocket. X rays satisfying the Bragg condition reflect into an array of nine companion proportional counters. A pointing system incorporating a free gyroscope with 2 degrees of freedom assures that target X rays are reflected at the required angle and produces repeated spectral scans of the X-ray continuum, which are later superimposed to correct temporal effects. The instrument is capable of detecting a narrow line flux from Sco X-1 of about .01 photons/sq cm/sec.

Stockman, H. S., Jr.↗
NASA NTRS1977

Distributed feedback acoustic surface wave oscillator

An acoustic surface wave oscillator is constructed from a semiconductor piezoelectric acoustic surface wave amplifier by providing appropriate perturbations at the piezoelectric boundary. The perturbations cause Bragg order reflections that maintain acoustic wave oscillation under certain conditions of gain and feedback.

Elachi, C.↗
NASA NTRS1982

Intercomparison of wind speeds inferred by the SASS, altimeter, and SMMR

The operational theory, control algorithms, and comparisons with surface-determined wind speeds for the scatterometer (SASS), altimeter (ALT), and passive microwave radiometer (SMMR) on board the Seasat satellite are presented. Radiative scattering combining specular reflections and Bragg resonance scattering are noted to occur at tilting waves and sea foam, two conditions highly correlated with wind speed. SASS scans swaths of 70, 200, and 700 km from nadir, the SMMR covers a 150 km strip. Normalized radar sections are derived from the SASS and ALT telemetry, and brightness temperature from the SMMR. ALT winds were found to be biased about 3 m/sec low, while intercomparison between the SMMR and SASS data showed a mean difference of 0.3 m/sec with a standard deviation from measured winds of 1.7 m/sec or less. The effects of land thermal emissions, rain, and sun glint are discussed, and good viewing conditions are concluded to result in 2 m/sec accuracy.

Wentz, F. J.↗
DOE OSTI2023

Two-beam Bragg diffraction, filtering, and delays

We summarize transmission and reflection amplitudes of Bragg-crystals based on two-beam Bragg diffraction theory. Then, we consider a specific case of infinitely thick and symmetrical Bragg-crystal and its reflective properties in spectral and angular domain. We obtain analytical expressions for filtering width and respective delay amplitudes, temporal delay from spectral phase shift and spatial displacement from angular phase shift.

43 PARTICLE ACCELERATORS↗
DOE OSTI2020

Hard x-ray standing-wave photoemission study of the interfaces in a BiFeO$_3$/La$_{0.7}$Sr$_{0.3}$MnO$_3$ superlattice

Hybrid multiferroics such as BiFeO$_3$ (BFO) and La$_{0.7}$Sr$_{0.3}$MnO$_3$ (LSMO) heterostructures are highly interesting functional systems due to their complex electronic and magnetic properties. One of the key parameters influencing the emergent properties is the quality of interfaces, where varying interdiffusion lengths can give rise to different chemistry and distinctive electronic states. Here we report high-resolution depth resolved chemical and electronic investigation of BFO/LSMO superlattice using standing-wave hard X-ray photoemission spectroscopy in the first-order Bragg as well as near-total-reflection geometry. Our results show that the interfaces of BFO on top of LSMO are atomically abrupt, while the LSMO on top of BFO interfaces show an interdiffusion length of around 1.2 unit cells. The two interfaces also exhibit different chemical gradients, with the BFO/LSMO interface being Sr-terminated by a spectroscopically distinctive high binding energy component in Sr 2p core-level spectra, which is spatially contained within 1 unit cell from the interface. From the electronic point of view, unique valence band features were observed for bulk-BFO, bulk-LSMO and their interfaces. Our X-ray optical analysis revealed a unique electronic signature at the BFO/LSMO interface, which we attribute to the coupling between those respective layers. Valence band decomposition based on the Bragg-reflection standing-wave measurement also revealed the band alignment between BFO and LSMO layers. Our work demonstrates that standing-wave hard x-ray photoemission is a reliable non-destructive technique for probing depth-resolved electronic structure of buried layers and interfaces with sub-unit-cell resolution. Equivalent investigations can be successfully applied to a broad class of material such as perovskite complex oxides with emergent interfacial phenomena.

Martins, HP↗
NASA NTRS2002

Fiber-Optic Pressure Sensor With Dynamic Demodulation Developed

Researchers at the NASA Glenn Research Center developed in-house a method to detect pressure fluctuations using a fiber-optic sensor and dynamic signal processing. This work was in support of the Intelligent Systems Controls and Operations project under NASA's Information Technology Base Research Program. We constructed an optical pressure sensor by attaching a fiber-optic Bragg grating to a flexible membrane and then adhering the membrane to one end of a small cylinder. The other end of the cylinder was left open and exposed to pressure variations from a pulsed air jet. These pressure variations flexed the membrane, inducing a strain in the fiber-optic grating. This strain was read out optically with a dynamic spectrometer to record changes in the wavelength of light reflected from the grating. The dynamic spectrometer was built in-house to detect very small wavelength shifts induced by the pressure fluctuations. The spectrometer is an unbalanced interferometer specifically designed for maximum sensitivity to wavelength shifts. An optimum pathlength difference, which was determined empirically, resulted in a 14-percent sensitivity improvement over theoretically predicted path-length differences. This difference is suspected to be from uncertainty about the spectral power difference of the signal reflected from the Bragg grating. The figure shows the output of the dynamic spectrometer as the sensor was exposed to a nominally 2-kPa peak-to-peak square-wave pressure fluctuation. Good tracking, sensitivity, and signal-to-noise ratios are evident even though the sensor was constructed as a proof-of-concept and was not optimized in any way. Therefore the fiber-optic Bragg grating, which is normally considered a good candidate as a strain or temperature sensor, also has been shown to be a good candidate for a dynamic pressure sensor.

Lekki, John D.↗
NASA NTRS1990

Dispersive spectroscopy on AXAF

The designs of two transmission grating spectrometers and a Bragg crystal spectrometer that are being developed for the Advanced X-ray Astrophysics Facility (AXAF) are described. The gratings, which are composed of arrays of small facets mounted on plates which can be inserted immediately behind the AXAF telescope, divide the AXAF energy band (80 eV-10 keV) into three regions and attain very high resolving powers for point sources. The Bragg Crystal Spectrometer (BCS) is a focal plane instrument, in which X-rays that satisfy the Bragg law are reflected from a curved crystal which refocuses the beam onto an imaging detector. The BCS achieves the highest spectral resolutions of the AXAF spectrometers: for E values between 500 and 1600 eV, the FWHM of a narrow line is less than 1 eV.

Markert, T. H.↗
NASA NTRS2001

Measurement of distributed strain and temperature based on higher order and higher mode Bragg conditions

A Bragg grating sensor for measuring distributed strain and temperature at the same time comprises an optical fiber having a single mode operating wavelength region and below a cutoff wavelength of the fiber having a multimode operating wavelength region. A saturated, higher order Bragg grating having first and second order Bragg conditions is fabricated in the optical fiber. The first order of Bragg resonance wavelength of the Bragg grating is within the single mode operating wavelength region of the optical fiber and the second order of Bragg resonance wavelength is below the cutoff wavelength of the fiber within the multimode operating wavelength region. The reflectivities of the saturated Bragg grating at the first and second order Bragg conditions are less than two orders of magnitude of one another. In use, the first and second order Bragg conditions are simultaneously created in the sensor at the respective wavelengths and a signal from the sensor is demodulated with respect to each of the wavelengths corresponding to the first and second order Bragg conditions. Two Bragg conditions have different responsivities to strain and temperature, thus allowing two equations for axial strain and temperature to be found in terms of the measure shifts in the primary and second order Bragg wavelengths. This system of equations can be solved for strain and temperature.

Sirkis, James S.↗
DOE OSTI2022

Refinements for Bragg coherent X-ray diffraction imaging: electron backscatter diffraction alignment and strain field computation

Bragg coherent X-ray diffraction imaging (BCDI) allows the 3D measurement of lattice strain along the scattering vector for specific microcrystals. If at least three linearly independent reflections are measured, the 3D variation of the full lattice strain tensor within the microcrystal can be recovered. However, this requires knowledge of the crystal orientation, which is typically attained via estimates based on crystal geometry or synchrotron microbeam Laue diffraction measurements. Presented here is an alternative method to determine the crystal orientation for BCDI measurements using electron backscatter diffraction (EBSD) to align Fe–Ni and Co–Fe alloy microcrystals on three different substrates. The orientation matrix is calculated from EBSD Euler angles and compared with the orientation determined using microbeam Laue diffraction. The average angular mismatch between the orientation matrices is less than ∼6°, which is reasonable for the search for Bragg reflections. The use of an orientation matrix derived from EBSD is demonstrated to align and measure five reflections for a single Fe–Ni microcrystal via multi-reflection BCDI. Using this data set, a refined strain field computation based on the gradient of the complex exponential of the phase is developed. This approach is shown to increase accuracy, especially in the presence of dislocations. The results demonstrate the feasibility of using EBSD to pre-align BCDI samples and the application of more efficient approaches to determine the full lattice strain tensor with greater accuracy.

42 ENGINEERING↗