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At least 1,243 records · Page 69
All sourcesNASA NTRSDOE OSTI
DOE OSTI2015

Analysis of stress corrosion cracking in alloy 718 following commercial reactor exposure

Alloy 718 is generally considered a highly corrosion-resistant material but can still be susceptible to stress corrosion cracking (SCC). The combination of factors leading to SCC susceptibility in the alloy is not always clear enough. In this paper, alloy 718 leaf spring (LS) materials that suffered stress corrosion damage during two 24-month cycles in pressurized water reactor service, operated to >45 MWd/mtU burn-up, was investigated. Compared to archival samples fabricated through the same processing conditions, little microstructural and property changes occurred in the material with in-service irradiation, contrary to high dose rate laboratory-based experiments reported in literature. Though the lack of delta phase formation along grain boundaries would suggest a more SCC resistant microstructure, grain boundary cracking in the material was extensive. Crack propagation routes were explored through focused ion beam milling of specimens near the crack tip for transmission electron microscopy as well as in polished plan view and cross-sectional samples for electron backscatter diffraction analysis. It has been shown in this study that cracks propagated mainly along random high-angle grain boundaries, with the material around cracks displaying a high local density of dislocations. The slip lines were produced through the local deformation of the leaf spring material above their yield strength. Also, the cause for local SCC appears to be related to oxidation of both slip lines and grain boundaries, which under the high in-service stresses resulted in crack development in the material.

22 GENERAL STUDIES OF NUCLEAR REACTORS↗
DOE OSTI2024

Temperature-Dependent Mechanical Anisotropy in Textured Zircaloy Cladding

This work evaluates deformation activity in textured zircaloy-4 cladding with the aim of elucidating the mechanisms that govern mechanical behavior across a temperature range anticipated in reactor service. In particular, the dependence of mechanical anisotropy on temperature and stress state (ratio of applied stresses) is examined via uniaxial and biaxial tensile experiments at room temperature and 400 °C. The mechanical behavior was interpreted based on micro-texture and dominant slip system activity. Thermal activation of basal systems is found as a key mechanism affecting mechanical behavior across the temperature range. The biaxial stress states produce resolved shear stresses contrasting to uniaxial stress states. As a result, mechanical testing and implications for reactor pellet-cladding mechanical interaction stress conditions are discussed.

11 NUCLEAR FUEL CYCLE AND FUEL MATERIALS↗
DOE OSTI2016

Three-dimensional lattice Boltzmann simulations of microdroplets including contact angle hysteresis on topologically structured surfaces

In this study, the dynamical behavior of a droplet on topologically structured surface is investigated by using a three-dimensional color-gradient lattice Boltzmann model. A wetting boundary condition is proposed to model fluid-surface interactions, which is advantageous to improve the accuracy of the simulation and suppress spurious velocities at the contact line. The model is validated by the droplet partial wetting test and reproduction of the Cassie and Wenzel states. A series of simulations are conducted to investigate the behavior of a droplet when subjected to a shear flow. It is found that in Cassie state, the droplet undergoes a transition from stationary, to slipping and finally to detachment states as the capillary number increases, while in Wenzel state, the last state changes to the breakup state. The critical capillary number, above which the droplet slipping occurs, is small for the Cassie droplet, but is significantly enhanced for the Wenzel droplet due to the increased contact angle hysteresis. In Cassie state, the receding contact angle nearly equals the prediction by the Cassie relation, and the advancing contact angle is close to 180°, leading to a small contact angle hysteresis. In Wenzel state, however, the contact angle hysteresis is extremely large (around 100°). Finally, high droplet mobility can be easily achieved for Cassie droplets, whereas in Wenzel state, extremely low droplet mobility is identified.

97 MATHEMATICS AND COMPUTING↗
DOE OSTI2017

25 April 2015 Gorkha Earthquake in Nepal Himalaya (Part 2)

The response from the geosciences community working on Himalaya in general, and the 2015 Nepal earthquakes in specific, was overwhelming, and after a rigorous review process, thirteen papers were selected and published in Part-1. We are still left with a few good papers which are being brought out as Part–2 of the special issue. Here, we describe how in the opening article Jean-Louis Mugnier and colleagues attempt to provide a structural geological perspective of the 25 April 2015 Gorkha earthquake and highlight the role of segmentation in generating the Himalayan mega-thrusts. They could infer segmentation by stable barriers in the HT that define barrier-type earthquake families. In yet another interesting piece of work, Pandey and colleagues map the crustal structure across the earthquake volume using Receiver function approach and infer a 5-km thick low velocity layer that connects to the MHT ramp. They are also able to correlate the rupture termination with the highest point of coseismic uplift. The last paper by Shen et al. highlights the usefulness of INSAR technique in mapping the coseismic slip distribution applied to the 25 April 2015 Gorkha earthquake. Finally, they infer low stress drop and corner frequency which coupled with hybrid modeling explain the low level of slip heterogeneity and frequency of ground motion.

Rao, N. Purnachandra↗
DOE OSTI2017

Geodetic imaging of thermal deformation in geothermal reservoirs - production, depletion and fault reactivation

Here, we investigate thermally induced surface deformation in geothermal systems. To define source mechanisms at depth, we assess the mechanical process of subsurface deformation by assuming a spherically cooled fractured reservoir in an infinite medium and derive relations that define magnitudes of thermal contraction, stress change and permeability evolution. The magnitude of thermal deformation in typical geothermal system is larger than anticipated and suggests two different modalities of surface subsidence – thermal contraction and fault reactivation. Here, surface deformation (vertical displacement, surface tilt and horizontal strain) induced by the two different modalities are assessed with Mogi (contraction) and Okada (slip) models and compared with instrumental sensitivity of high precision surface geodetic tools. Here, we show that 1 year of geothermal operation at 10 MW with a power plant conversion efficiency of 12% can yield ~ 3.0 × 10 4 m 3 of subsurface volume change. For a reservoir at 2000 m depth, this induces ~ 1.7 mm of vertical surface displacement, ~ 800 nano-radians of surface tilt and ~ 900 nano-strains of surface strain. This result implies that typically observed magnitudes of surface subsidence (order of cm/year) are naturally expected in massive (100 MW scale) geothermal operations and observed surface subsidence may largely be the result of thermal contraction. Conversely, thermal unloading can trigger fault reactivation. Analysis with an Okada slip model shows these shear offsets on pre-existing faults can also result in surface deformations of considerable magnitude. Our analysis of field operational data from various geothermal projects suggests that both thermal contraction and slow fault reactivation may contribute to the observed large surface deformation. Comparison of predicted deformation with instrumental sensitivity of high precision surface tools confirms that geodetic signals, especially tilt and strain, are indeed sufficiently large to describe reservoir evolution and to potentially deconvolve reservoir parameters of interest, such as permeability.

15 GEOTHERMAL ENERGY↗
DOE OSTI2015

Tensile and compressive creep behavior of extruded Mg–10Gd–3Y–0.5Zr (wt.%) alloy

The tensile and compressive creep behavior of an extruded Mg–10Gd–3Y–0.5Zr (wt.%) alloy was investigated at temperatures ranging from 200 °C to 300 °C and under stresses ranging from 30 MPa to 120 MPa. There existed an asymmetry in the tensile and compressive creep properties. The minimum creep rate of the alloy was slightly greater in tension than in compression. The measured values of the transient strain and initial creep rate in compression were greater than those in tension. The creep stress exponent was approximately 2.5 at low temperatures (T < 250 °C) and 3.4 at higher temperatures both in tension and in compression. The compression creep activation energy at low temperatures and high temperatures was 83.4 and 184.3 kJ/mol respectively, while one activation energy (184 kJ/mol) represented the tensile–creep behavior over the temperature range examined. Dislocation creep was suggested to be the main mechanism in tensile creep and in the high-temperature regime in compressive creep, while grain boundary sliding was suggested to dominate in the low-temperature regime in compressive creep. Precipitate free zones were observed near grain boundaries perpendicular to the loading direction in tension and parallel to the loading direction in compression. Electron backscattered diffraction analysis revealed that the texture changed slightly during creep. Non-basal slip was suggested to contribute to the deformation after basal slip was introduced. In the tensile–creep ruptured specimens, intergranular cracks were mainly observed at general high-angle boundaries. - Highlights: • Creep behavior of an extruded Mg–RE alloy was characterized by EBSD. • T5 aging treatment enhanced the tension–compression creep asymmetry. • The grains grew slightly during tensile creep, but not for compressive creep. • Precipitate free zones (PFZs) were observed at specific grain boundaries. • Intergranular fracture was dominant and cracks mainly originated at GHABs.

36 MATERIALS SCIENCE↗
DOE OSTI2016

Microstructure characterization of LAE442 magnesium alloy processed by extrusion and ECAP

The magnesium alloy LAE442 was processed by extrusion and equal channel angular pressing (ECAP) to achieve ultrafine grained microstructure. Detailed characterization of the microstructure was performed by scanning electron microscope, electron back scattered diffraction (EBSD) and transmission electron microscope. The initial, as-cast, microstructure consisted of large grains of ~ 1 mm. The grain refinement due to the processing by severe plastic deformation led to a decrease of the average grain size to ~ 1.7 μm after the final step of ECAP. A detailed characterization of secondary phases showed the precipitation of Al{sub 11}RE{sub 3}, Al{sub 2}Ca and Al{sub 10}RE{sub 2}Mn{sub 7} intermetallic phases. X-ray diffraction measurements proved that Li is dissolved within the magnesium matrix in the as-cast condition. Newly formed Al{sub 3}Li phase was observed after ECAP. The texture formation due to the extrusion and ECAP was different from that in the other magnesium alloys due to the activation of non-basal slip systems as a result of the decrease of the c/a ratio. - Highlights: • Combined extrusion and equal channel angular pressing results in significant grain refinement by factor 1000 approximately. • Al{sub 11}RE{sub 3}, Al{sub 2}Ca and Al{sub 10}RE{sub 2}Mn{sub 7} secondary phases are present in the as-cast material while Li was dissolved in the Mg matrix. • Extrusion and ECAP have no effect on the composition of the secondary phases but they influence strongly their distribution. • Texture evolution is affected by decrease of c/a ratio due to the presence of Li and resulting activation of non-basal slip.

36 MATERIALS SCIENCE↗
DOE OSTI2016

In-situ EBSD study of deformation behavior of retained austenite in a low-carbon quenching and partitioning steel via uniaxial tensile tests

Through using in-situ electron back-scattered diffraction and uniaxial tensile tests, this work mainly focuses on the deformation behavior of retained austenite (RA) in a low-carbon quenching and partitioning (Q&P) steel. In this paper, three different types of RA can be distinguished from different locations, respectively, RA grains at the triple edges, twinned austenite and RA grains positioned between martensite. The results have shown that grains at the triple edges and twinned austenite could transform easily with increasing strain, i.e. are less stable when compared with RA grains distributed between martensite that could resist a larger plastic deformation. Meanwhile, the strain leads to rotations of RA grains distributed at the triple edges and between martensite. Moreover, RA grains with a similar orientation undergone similar rotations with the same true strain. These RA grains rotated along a specific slip plane and slip direction and the grain rotation is taken as a significant factor to improve the ductility of steel. In addition, grain sizes of RA decreased gradually with an increase of true strain and smaller (0–0.2 μm) grains were more capable of resisting the deformation. According to kernel average misorientation (KAM) analysis, it can be found that strain distribution is preferentially localized near martensite–austenite phase boundaries and in the interior of martensite. The average KAM values increased continuously with increasing true strain. - Highlights: •The in-situ and ex-situ tensile specimens differ to some extent in mechanical properties. •Retained austenite grains at the triple edges and twinned austenite transformed easily at the early stage of true strain. •Film-like retained austenite grains only rotated prior to the transformation during straining. •Retained austenite grains having with a similar orientation experienced similar rotations during the same true strain.

36 MATERIALS SCIENCE↗
DOE OSTI2016

Microstructure characterization of 316L deformed at high strain rates using EBSD

Specimens from split Hopkinson pressure bar experiments, at strain rates between ~ 1000–9000 s{sup −1} at room temperature and 500 °C, have been studied using electron backscatter diffraction. No significant differences in the microstructures were observed at different strain rates, but were observed for different strains and temperatures. Size distribution for subgrains with boundary misorientations > 2° can be described as a bimodal lognormal area distribution. The distributions were found to change due to deformation. Part of the distribution describing the large subgrains decreased while the distribution for the small subgrains increased. This is in accordance with deformation being heterogeneous and successively spreading into the undeformed part of individual grains. The variation of the average size for the small subgrain distribution varies with strain but not with strain rate in the tested interval. The mean free distance for dislocation slip, interpreted here as the average size of the distribution of small subgrains, displays a variation with plastic strain which is in accordance with the different stages in the stress-strain curves. The rate of deformation hardening in the linear hardening range is accurately calculated using the variation of the small subgrain size with strain. - Highlights: •Only changes in strain, not strain rate, gave differences in the microstructure. •A bimodal lognormal size distribution was found to describe the size distribution. •Variation of the subgrain fraction sizes agrees with models for heterogeneous slip. •Variation of subgrain size with strain describes part of the stress strain curve.

36 MATERIALS SCIENCE↗
DOE OSTI2018

Microstructure development in a high-nickel austenitic stainless steel using EBSD during in situ tensile deformation

Highlights: • The number of low angle boundaries increases significantly at strains ≥ 9.5%. • Grain rotation was observed to lead to grain subdivision and even fragmentation. • Annealing twins deform due to accumulation of dislocations near their boundaries. • No deformation twins were observed and deformation took place by dislocation slip. - Abstract: Plastic deformation of surface grains has been observed by electron backscatter diffraction technique during in situ tensile testing of a high-nickel austenitic stainless steel. The evolution of low- and high-angle boundaries as well as the orientation changes within individual grains has been studied. The number of low-angle boundaries and their respective misorientation increases with increasing strain and some of them also evolve into high-angle boundaries leading to grain fragmentation. The annealing twin boundaries successively lose their integrity with increasing strain. The changes in individual grains are characterized by an increasing spread of orientations and by grains moving towards more stable orientations with <111> or <001> parallel to the tensile direction. No deformation twins were observed and deformation was assumed to be caused by dislocation slip only.

36 MATERIALS SCIENCE↗
DOE OSTI2018

Enabling high resolution strain mapping in zirconium alloys

Highlights: • Optimisation of speckle patterns suitable for high resolution digital image correlation in a zirconium alloy • Evidence of distinct strain patterning at the macro and micro scale • Analysis of strain heterogeneity in a neighbouring low and high strain band • Paved the way for future studies on strain localization in zirconium alloys subjected to hydriding and irradiation damage - Abstract: High Resolution Digital Image Correlation (HRDIC) has been established recently as a novel displacement mapping technique during mechanical loading experiments to quantify strain localisation down to the level of individual slip traces. This is achieved by the creation of a nano-scale gold pattern naturally formed during remodelling of a thin gold layer that was sputtered onto the region of interest. To date, the gold remodelling is carried out in a water vapourisation environment, which excludes the technique to be applied to materials that readily form noticeable oxide layers in such environments. The current paper describes a recently developed gold remodelling technique using a styrene-argon environment at substantially lower temperatures than the water-vapour based technique. The material used in the present work is a zirconium alloy where we first demonstrate the problem of oxide formation during remodelling in water vapour and the benefit of the modified remodelling procedure. The error associated with the spatial drift was assessed for different interrogation window sizes followed by detailed analysis of the subsequent strain maps produced using the styrene remodelled patterns after tensile deformation to nominal applied strains of ~3.5% and ~7.0%. The level of detail captured demonstrate the suitability of styrene-argon-based remodelling for materials like Zr alloys with the strain maps showing clear strain patterning on both a transgranular and single grain scale with the possibility of quantifying strain across a single slip trace.

36 MATERIALS SCIENCE↗
DOE OSTI2018

Cyclic plastic deformation behaviour of a directionally solidified nickel base superalloy at 850 °C: Damage micromechanisms

Highlights: • Isothermal LCF life of CM 247 DS is reduced using R = 0 instead of R = −1. • Reduction in LCF life is significant at lower values of Δε/2. • Reduction in fatigue life is attributed to the development of sustained mean stress. • Sustained mean stress prevents the slip transfer from γ-channels to γ′-precipitates. • Sustained mean stress promotes dislocation network formation and looping. - Abstract: Dislocation based deformation micromechanisms during low cycle fatigue deformation of nickel base superalloy CM 247 DS LC at 850 °C was investigated by conducting fatigue tests employing constant strain amplitudes for strain ratio (R) values of 0, −1 and carrying out extensive SEM and TEM examinations. Cyclic life of the alloy reduces for all fatigue tests conducted employing R = 0 in comparison with R = −1 owing to sustained mean stress developed during fatigue at R = 0. TEM examinations confirmed that sustained mean stress developed during low strain amplitude fatigue test (Δε/2 = 0.5%) using R = 0 condition prevented slip transfer from γ-channels to γ′-precipitates and resulted in the formation of dislocation substructures such as networks, nodes etc. and also promoted dislocation looping around γ′-precipitates. Lower fatigue life at R = 0 is mainly attributed to the development of these types of substructures, which promotes strain localization in both intra as well intergranular regions. Whereas, in specimen fatigue tested (Δε/2 = 0.5%) using R = −1 condition, shearing of γ′-precipitates by APB coupled dislocation and formation of stacking faults were observed. The formation and nature of stacking faults were analysed using weak beam imaging technique. Stacking fault formed during fatigue tests using R = −1 condition matured to micro-twins when Δε/2 value was increased to 0.8%. The mechanism of formation of these microtwins is discussed in detail. SEM based microstructural and fractographic examinations revealed that mean stress induced creep effect resulted in intergranular crack initiation and grain boundary cavitation during fatigue tests under R = 0 condition and therefore verified the facts revealed in TEM studies.

36 MATERIALS SCIENCE↗
DOE OSTI2018

Effects of initial microstructures on serrated flow features and fracture mechanisms of a nickel-based superalloy

Highlights: • Uniaxial tensile tests are performed on a nickel-based superalloy at 473 K–973 K and low strain rates. • Effects of initial microstructures on serrated flow features, and fracture characteristics are analyzed. • The dislocation across slip in the matrix is responsible for the serrated flow. • Nucleation and growth of micro-voids is the main fracture mechanism of ST and HS superalloys. • The better tensile ductility is obtained with raising the deformation temperatures for the SAT superalloy. - Abstract: The uniaxial tensile experiments are performed on a nickel-based superalloy with different initial microstructures at intermediate temperatures (473–973) K and low strain rates (0.0001–0.001) s{sup −1}. Effects of initial microstructures on plastic deformation mechanisms, serrated flow features, and fracture characteristics are analyzed. It is clearly demonstrated that the plastic deformation mechanism of serrated flow is irrelevant to the initial microstructures, and the dislocation across slip in the matrix is responsible for the serrated flow. However, the effects of initial microstructures on fracture mechanisms are obvious, i.e., the main fracture mechanism of the ST (solution treated) and HS (solution plus γ′/γ″ phases aging precipitation) superalloys are the nucleation and growth of micro-voids, which accelerates the break of carbides and interfacial failure of carbides/matrix. While for the SAT (solution plus δ phases aging precipitation) superalloy, δ phases and carbides play a significant role in the nucleation of micro-voids. Furthermore, the increase of the deformation temperature reduces the elongation to fracture of the ST and HS superalloys. However, the better tensile ductility is obtained with raising the deformation temperatures for the SAT superalloy.

36 MATERIALS SCIENCE↗
DOE OSTI2018

Work hardening behavior and tensile properties of a high-Mn damping steel at elevated temperatures

Highlights: • Stability of austenite and ε-martensite was varied by changing the temperature of deformation. • Work hardening behavior was affected by the effects of TRIP, TWIP, DSA and dislocation slip. • Ultimate elongation was significantly decreased when ε → α′ transformation was too hard to occur. - Abstract: An austenite/ε-martensite dual-phase high-Mn damping steel was tensile deformed at elevated temperatures to conduct a comprehensive study about the effects of transformation-induced plasticity (TRIP), twinning-induced plasticity (TWIP), dynamic strain aging (DSA) and dislocation slip (DS) on its work hardening behavior and tensile properties. The results showed that the work hardening behavior of high-Mn damping steel can be divided into two stages. In stage-I, the main factor influencing the work hardening changed from γ → ε transformation to DS as the deformation temperature was increased. In the second stage, the work hardening exponent and ultimate tensile strength were large when intense DSA occurred at 80 °C and 120 °C, although ε → α′ transformation became more difficult at elevated temperatures. Tensile deformation at 200 °C promoted ε → γ transformation, such that the work hardening exponent and ultimate elongation were significantly decreased. In the later stage of deformation at 260 °C, TWIP effect effectively enhanced the work hardening as deformation-induced ε → α′ transformation occurred at low deformation temperatures.

36 MATERIALS SCIENCE↗
DOE OSTI2018

Deformation behavior of HCP titanium alloy: Experiment and Crystal plasticity modeling

The deformation behavior of commercially pure titanium is studied using experiments and a crystal plasticity model. Compression tests along the rolling, transverse, and normal-directions, and tensile tests along the rolling and transverse directions are performed at room temperature to study the activation of slip and twinning in the hexagonal closed packed titanium. A detailed EBSD based statistical analysis of the microstructure is performed to develop statistics of both {10-12} tensile and {11-22} compression twins. A simple Monte Carlo (MC) twin variant selection criterion is proposed within the framework of the visco-plastic self-consistent (VPSC) model with a dislocation density (DD) based law used to describe dislocation hardening. In the model, plasticity is accommodated by prismatic, basal and pyramidal slip modes, and {10-12} tensile and {11-22} compression twinning modes. Thus, the VPSC-MC model successfully captures the experimentally observed activation of low Schmid factor twin variants for both tensile and compression twins modes. The model also predicts macroscopic stress-strain response, texture evolution and twin volume fraction that are in agreement with experimental observations.

36 MATERIALS SCIENCE↗
DOE OSTI2018

A study on tensile properties of Alloy 709 at various temperatures

In recent years, there have been several advancements in energy production from both fossil fuels and the alternate “clean” sources such as nuclear fission. These advancements are fueled by the need for more efficient systems that will optimize the use of the depleting fossil fuel reserves and shift the focus to cleaner sources of energy. The efficiency of any power generation cycle is dependent on the ability of the structural material to withstand increased peak operating temperatures. Advanced austenitic stainless steels have been in the focus as structural material for the next generation nuclear power plants, due to their strength, corrosion resistance, weldability and the wide range of temperatures at which the austenite phase is stable. Alloy 709, a recently developed advanced austenitic stainless steel, is being investigated in this paper. Here in this study, tensile tests were conducted on dog-bone samples of Alloy 709 in an in-situ scanning electron microscope (SEM) loading and heating stage, equipped with electron backscatter diffraction (EBSD), at various temperatures. The in-situ experiments indicated that the material primarily accommodated deformation by slip at lower temperatures. Void formation and coalescence at grain boundaries preceded slip at higher temperatures. Although crack initiation at all elevated temperatures was intergranular, the crack propagation through the material and the final fracture was transgranular ductile. Additionally, tensile tests were conducted on larger cylindrical samples at 550, 650 and 750 °C in air. The results of tests conducted in air and in-situ were found to be in agreement, at these temperatures.

36 MATERIALS SCIENCE↗
DOE OSTI2023

Analysis of orientation-dependent deformation mechanisms in additively manufactured Zr using in-situ micromechanical testing: Twinning and orientation gradient

Here, orientation-dependent plasticity in zirconium (Zr)-alloy, which is produced through ultrasonic additive manufacturing (UAM) with subsequent hot-isostatic pressing (HIP), was analyzed by recording electron backscattered diffraction (EBSD) data during in-situ micromechanical testing. Three (0001) plane orientations of a hexagonal close-packed (HCP) structure were analyzed parallel to (1) the rolling direction [X||tensile direction (TD)], (2) the build direction [Z], and (3) the transverse direction [Y]. The analysis revealed that the grains with ~<0001>||TD show twin-dominant plasticity with three variants from {10 $\overline{1}$ 2}<$\overline{1}$ 011>; minor slipping with ($10\overline{1}$ 1)[$\overline{2}$ 113], and ($11\overline{2}$ 2)[$\overline{1} \overline{1}$ 23] pyramidal slip has also been observed. However, grains with orientation ~<0001>⊥TD are mainly sensitive to dislocations assisted plasticity-leading to orientation gradients formation. Furthermore, the neck formation was identified as originating from higher populated micro-crack locations and their association with localized plasticity at defect points in the UAM material. These results demonstrate that minimization of impurities to enable grain growth across prior foil interfaces makes HIP an effective methodology for producing Zr plate, with deformation characteristics expected for conventionally manufactured Zr.

36 MATERIALS SCIENCE↗
DOE OSTI2024

Crystal plasticity modeling and analysis for the transition from intergranular to transgranular failure in nickel-based alloy Inconel 740H at elevated temperature

The precipitation-strengthened Nickel alloy Inconel® 740H® (IN740H) exhibits increased ductility at higher applied strain rates during quasi-static tensile tests at an elevated temperature of 760°C. The examination of fracture surfaces in this context reveals a noteworthy transition of underlying fracture mechanisms from transgranular to intergranular fracture as the applied strain rate decreases from 1×10 -3 / s to 0.83×10 -4 / s . To thoroughly understand the mechanical response of IN740H under these conditions, this study develops a crystal plasticity finite element (CPFE) model. Further, this model incorporates various deformation mechanisms including dislocation slips, climb, and grain boundary sliding, which are relevant to the test conditions. The model is calibrated using data from both tensile tests at different strain rates and creep tests across a broad stress range at 760°C, enabling the accurate determination of model parameters for each mechanism. Simulation results well captured the experimental observations of different failure modes. At higher strain rates, the model shows a dominance of dislocation slip leading to heterogeneous plastic deformation and formation of transgranular shear bands causing the failure, while at lower strain rates, an increased activity of grain boundary sliding causes grain boundaries crack leading to intergranular failure.

37 INORGANIC, ORGANIC, PHYSICAL, AND ANALYTICAL CH↗