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Search indexed NASA NTRS and DOE OSTI research on propulsion, heat transfer, battery materials and energy systems. Follow report and document links to the original sources.

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At least 1,225 records · Page 68
All sourcesNASA NTRSDOE OSTI
DOE OSTI2025

Quantitative Imaging of Cobalt Phthalocyanine Distribution on Carbon Nanotubes: A Deep Learning Approach to Catalyst Characterization

Electrochemical reduction of carbon dioxide (CO 2 ) offers a pathway to valuable products, with catalysts playing a crucial role. This study investigates the distribution of cobalt tetraaminophthalocyanine (CoPc-NH 2 ) immobilized on carbon nanotubes (CNTs), utilizing high-angle annular dark-field scanning transmission electron microscopy (HAADF-STEM) to characterize CoPc-NH 2 distribution. A challenge in the quantitative HAADF-STEM analysis is the introduction of bias from manual Co atom identification. To address this, we developed and trained a convolutional neural network (CNN) using a data set generated from images of CoPc-NH 2 /CNT samples with varying Co loadings. The CNN, implemented in TensorFlow and Keras, facilitated Co atom detections. Analysis of the CNN-generated data confirmed a correlation between Co loading and surface density, consistent with findings from UV–vis spectroscopy. Furthermore, the application of Ripley’s L(d) function highlighted the presence of slight Co atom clustering. Furthermore, this work demonstrates the utility of the combined HAADF-STEM and CNN approach for providing spatially resolved information about catalyst distribution on nonplanar supports, revealing structural details that are typically lost through other characterization methods.

HAADF-STEM↗
DOE OSTI2026

High Pressure X-ray Diffraction and Equation of State of Hydrazine

Synchrotron X-ray diffraction has been used to investigate the structure and equation of state (EOS) of hydrazine (N 2 H 4 ) up to 54.3 GPa at 298 K. The diffraction patterns could be fit to a monoclinic unit-cell structure and put strong constraints on previously reported phase transitions documented by vibrational spectroscopy over this pressure range. Pressure–volume ( P–V ) data were fit using a Vinet EOS, yielding parameters: V 0 = 45.2 Å 3 /molecule (fixed), K 0 = 11.8(7) GPa, and K 0 ′ = 6.5(2). Previously measured high-pressure vibrational frequency shifts were used to estimate the vibrational free energy and model P–V–T isotherms from 0 to 1200 K. The results of the P–V–T isotherms are compared to existing shock Hugoniot data on hydrazine and 298 K isotherms for assemblages of possible decomposition products. This comparison suggests dissociation at high density under shock loading. Good correspondence was found between the static lattice EOS as calculated by the model and the previously reported EOS as calculated by density functional theory. Finally, these results resolve existing uncertainties about the EOS and crystal symmetry of hydrazine at high pressure and provide valuable baseline information on this important energetic material.

diffraction↗
DOE OSTI2022

A Data-Driven Democratized Control Architecture for Regional Transmission Operators

As probably the most complicated and critical infrastructure system, U.S. power grids become increasingly vulnerable to extreme events such as cyber-attacks and severe weather, as well as higher DER penetrations and growing information mismatch among system operators, utilities (transmission or generation owners), and end-users. This paper proposes a data-driven democratized control architecture considering two democratization pathways to assist transmission system operators, with a targeted use case of developing online proactive islanding strategies. Detailed discussions on load capability profiling at transmission buses and disaggregation of DER generations are provided and illustrated with real-world utility data. By Combining network and operational constraints, transmission system operators can be equipped with new tools built on top of this architecture, to derive accurate, proactive, and strategic islanding decisions to incorporate the wide range of dynamic portfolios and needs when facing extreme events or unseen grid contingencies.

Power System Reliability, Islanding, Democratized ↗
DOE OSTI2021

Crack Stability in Breached Fuel

This report describes the fracture mechanics formalism to evaluate the stability of cracks in a fuel cladding. Recognized consensus-body linear elastic fracture mechanics (LEFM) was applied to identify the crack instability length, or the length at which unstable mechanical crack extension would occur, as a function of pellet swelling loading (radial strain and fraction conversion from UO 2 to U 3 O 8 ) at the local cracked cladding region for two postulated fracture toughness (K IC ) values of the cladding. The crack opening displacement (COD) and the crack opening area (COA) were also identified. This analysis informs evaluations for crack extension and the potential for pellet debris loss from the fuel rod for cases of pellet oxidation in dry storage canisters where inadvertent residual water may undergo radiolysis causing oxidizing conditions to pellets exposed to the canister environment through breached cladding.

22 GENERAL STUDIES OF NUCLEAR REACTORS↗
DOE OSTI2021

Crack Stability in Breached Fuel

This report describes the fracture mechanics formalism to evaluate the stability of cracks in a fuel cladding. Recognized consensus-body linear elastic fracture mechanics (LEFM) was applied to identify the crack instability length, or the length at which unstable mechanical crack extension would occur, as a function of pellet swelling loading (radial strain and fraction conversion from UO 2 to U 3 O 8 ) at the local cracked cladding region for two postulated fracture toughness (K IC ) values of the cladding. The crack opening displacement (COD) and the crack opening area (COA) were also identified. This analysis informs evaluations for crack extension and the potential for pellet debris loss from the fuel rod for cases of pellet oxidation in dry storage canisters where inadvertent residual water may undergo radiolysis causing oxidizing conditions to pellets exposed to the canister environment through breached cladding.

11 NUCLEAR FUEL CYCLE AND FUEL MATERIALS↗
NASA NTRS1973

Skylab Rescue Space Vehicle OAT No. 1 Plugs in Test

A test is described which demonstrates the compatibility of the Skylab Rescue Space Vehicle systems, the ground support equipment, and off-site support facilities by proceeding through a simulated launch countdown, liftoff, and flight. The functions of propellant loading, umbilical ejection, holddown arm release, service arm retraction, liftoff, and inflight separation are simulated. An external power source supplies transfer power to internal, and instrument unit commands are simulated by the digital command system. The test outline is presented along with a list of references, intercommunications information, radio frequency matrix, and interface control chart.

Jevitt, S. J.↗
NASA NTRS1974

Skylab study of water quality

The author has identified the following significant results. Analysis of S-190A imagery from 1 EREP pass over 3 reservoirs in Kansas establishes a strong linear correlation between the red/green radiance ratio and suspended solids. This result compares quite favorably to ERTS MSS CCT results. The linear fits RMS for Skylab is 6 ppm as compared to 12 ppm for ERTS. All of the ERTS satellite passes yielded fairly linear results with typical RMS values of 12 ppm. However, a few of the individual passes did yield RMS values of 5 or 6 ppm which is comparable to the one Skylab pass analyzed. In view of the cloudy conditions in the Skylab photos, yet good results, the indications are that S-190A may do somewhat better than the ERTS MSS in determining suspended load. More S-190A data is needed to confirm this. As was the case with the ERTS MSS, the Skylab S-190A showed no strong correlation with other water quality parameters. S-190B photos because of their high resolution can provide much first look information regarding relative degrees of turbidity within various parts of large lakes and among smaller bodies of water.

Yarger, H. L.↗
NASA NTRS1985

Loads and Aeroelasticity Division research and technology accomplishments for FY 1984 and plans for FY 1985

The loads and aeroelasticity divisions research accomplishments are presented. The work under each branch or technical area, described in terms of highlights of accomplishments during the past year and highlights of plans for the current year as they relate to 5 year plans for each technical area. This information will be useful in program coordination with other government organizations and industry in areas of mutual interest.

Gardner, J. E.↗
NASA NTRS1993

AGENDA: A task organizer and scheduler

AGENDA will be the main tool used in running the SPOT 4 Earth Observation Satellite's Operational Control Center. It will reduce the operator's work load and make the task easier. AGENDA sets up the work plan for a day of operations, automatically puts the day's tasks into sequence and monitors their progress in real time. Monitoring is centralized, and the tasks are run on different computers in the Center. Once informed of any problems, the operator can intervene at any time while an activity is taking place. To carry out the various functions, the operator has an advanced, efficient, ergonomic graphic interface based on X11 and OSF/MOTIF. Since AGENDA is the heart of the Center, it has to satisfy several constraints that have been taken into account during the various development phases. AGENDA is currently in its final development stages.

Fratter, Isabelle↗
NASA NTRS1994

Fuzzy logic application for modeling man-in-the-loop space shuttle proximity operations

A software pilot model for Space Shuttle proximity operations is developed, utilizing fuzzy logic. The model is designed to emulate a human pilot during the terminal phase of a Space Shuttle approach to the Space Station. The model uses the same sensory information available to a human pilot and is based upon existing piloting rules and techniques determined from analysis of human pilot performance. Such a model is needed to generate numerous rendezvous simulations to various Space Station assembly stages for analysis of current NASA procedures and plume impingement loads on the Space Station. The advantages of a fuzzy logic pilot model are demonstrated by comparing its performance with NASA's man-in-the-loop simulations and with a similar model based upon traditional Boolean logic. The fuzzy model is shown to respond well from a number of initial conditions, with results typical of an average human. In addition, the ability to model different individual piloting techniques and new piloting rules is demonstrated.

Brown, Robert B.↗
NASA NTRS2007

Strain Measurement Using FBG on COPV in Stress Rupture Test

White Sands Test Facility (WSTF) was requested to perform ambient temperature hydrostatic pressurization testing of a Space Transportation System (STS) 40-in. Kevlar Composite Overwrapped Pressure Vessel (COPV). The 40-in. vessel was of the same design and approximate age as the STS Main Propulsion System (MPS) and Orbiter Maneuvering System (OMS) vessels. The NASA Engineering Safety Center (NESC) assembled a team of experts and conducted an assessment that involved a review of national Kevlar COPY data. During the review, the STS COPVs were found to be beyond their original certification of ten years. The team observed that the likelihood of STS COPV Stress rupture, a catastrophic burst before leak failure mode, was greater than previously believed. Consequently, a detailed assessment of remaining stress rupture life became necessary. Prior to STS-114, a certification deviation was written for two flights of OV-103 (Discovery) and OV-104 (Atlantis) per rationale that was based on an extensive review of the Lawrence Livermore National Laboratories, COPV data, and revisions to the STS COPV stress levels. In order to obtain flight rationale to extend the certification deviation through the end of the Program, the Orbiter Project Office has directed an interagency COPV team to conduct further testing and analysis to investigate conservatism in the stress rupture model and evaluate material age degradation. Additional analysis of stress rupture life requires understanding the fiber stresses including stress that occurs due to thru-wall composite compression in COPV components. Data must be obtained at both zero gauge pressure (pre-stress) and at the component operating pressure so that this phenomenon can be properly evaluated. The zero gauge pressure stresses are predominantly a result of the autofrettage process used during vessel manufacture. Determining these pre-stresses and the constitutive behavior of the overwrap at pressure will provide necessary information to better predict the remaining life of the STS COPVs. The primary test objective is obtaining data to verify the hypothesis of a radially oriented thru-thickness stress-riser in the COPV composite whose magnitude is a function of the applied pressure and the load history. The anticipated load dependent response follows from the constitutive behavior of the composite overwrap so data to quantify its nonlinear and time dependent response will be sought. The objective of the Fiber Braggs Gratings (FBGs) were to advance the state-of-the-art by developing techniques using FBG sensors that are capable of assessing stress-rupture degradation in Kevlar COPVs in a health monitoring mode (1). Moreover, they sought to answer questions of how embedded sensors affect overall integrity of the structure. And lastly, they sought to provide an important link in the overall stress rupture study that will help close the loop on the COPV fabrication process. NDE inspection methods will be used from start to finish and FBG will be an integral link within the overall chain.

Banks, Curtis↗
NASA NTRS2009

Design and Calibration of a Flowfield Survey Rake for Inlet Flight Research

The Propulsion Flight Test Fixture at the NASA Dryden Flight Research Center is a unique test platform available for use on NASA's F-15B aircraft, tail number 836, as a modular host for a variety of aerodynamics and propulsion research. For future flight data from this platform to be valid, more information must be gathered concerning the quality of the airflow underneath the body of the F-15B at various flight conditions, especially supersonic conditions. The flow angularity and Mach number must be known at multiple locations on any test article interface plane for measurement data at these locations to be valid. To determine this prerequisite information, flight data will be gathered in the Rake Airflow Gauge Experiment using a custom-designed flowfield rake to probe the airflow underneath the F-15B at the desired flight conditions. This paper addresses the design considerations of the rake and probe assembly, including the loads and stress analysis using analytical methods, computational fluid dynamics, and finite element analysis. It also details the flow calibration procedure, including the completed wind-tunnel test and posttest data reduction, calibration verification, and preparation for flight-testing.

Flynn, Darin C.↗
NASA NTRSDate not supplied

Auroral ovals versus flare ribbons: Optical footprints of explosive magnetic field reconfiguration in Earth’s magnetosphere and the Sun’s corona

Despite drastically different plasma conditions in the two systems, eruptive energy release events in solar active regions and in Earth’s magnetosphere have a lot in common. Both solar active region eruptions and the substorm activity in the nightside magnetosphere are known to be associated with an abrupt large-scale reorganization of the supporting magnetic systems enabling the conversion and dissipation of the stored free magnetic energy. The rate of energy accumulation in either system tends to be by orders of magnitude slower than the energy release rate, leading to the formation of an impulsive loading-unloading cycle involving a relatively long pre-reconnection phase (substorm growth phase, pre-flare stressing of an active region magnetic field), a short and explosive reconnection phase (substorm breakup and expansion, eruptive flares and CMEs), and a prolonged post-reconnection phase (substorm recovery phase and the post-flare active region reconfiguration). In Earth’s magnetosphere, this loading-unloading cycle is diagnosed by monitoring characteristic changes in the particle precipitation pattern in the northern and southern auroral ovals marking the boundary between the open and close magnetic flux. The position, shape, structure, and dynamics of the auroral borealis were shown to communicate critically important information about an upcoming substorm, the location and timing of the initial reconnection onset, and the subsequent return of the magnetosphere to a lower-energy state. On the Sun, a similar role is played by the chromospheric flare ribbons which enable a detailed diagnostics of the overlying reconnecting magnetic field. In this talk, we’ll discuss similarities and differences in using auroral and flare ribbon observations for monitoring eruptive energy release in respectively Earth’s magnetosphere and solar corona. Special emphasis will be placed on the quantitative interpretation of the two types of optical signatures for empirical diagnostics of the underlying reconnection activity and for constraining its theoretical models. We’ll also compare forecasting capabilities of the two types of optical signatures in the context of space weather prediction objectives.

V. M. Uritskiy↗
NASA NTRS1990

Dynamic load-sharing using predicted process resource requirements

Heuristics which use predicted process resource requirements to make scheduling decisions are proposed. Four heuristics are presented. The first two, MINQ and SMPL, employ centralized scheduling and the remaining two, DMINQ and FDMINQ, use distributed scheduling. These heuristics are first compared against random scheduling and then against two conventional heuristics, CENTEX and DISTED, which schedule processes solely based on system state information. Results based on trace-driven simulations show that the proposed centralized heuristics offer significantly improved mean response time and they require fewer status update messages. In experiments using the same status update rates, SMPL response times were, on the average, 22 percent lower than those for CENTEX; MINQ response times were, on the average, 18 percent lower. The simulations also showed that MINQ and SMPL can perform as well as, or better than, CENTEX while using up to 70 percent fewer status update messages. The use of fewer status update messages imposes less overhead on the system. The use of prediction for distributed scheduling produced similar results. When prediction was used to filter small processes and execute them locally a 50 percent improvement in response times was obtained.

Goswami, Kumar K.↗
DOE OSTI2020

Investigating Core Gaps and the Development of Subcomponent Validation Methods for Wind Turbine Blades: Preprint

Core gaps are a common manufacturing defect observed in wind blade composite sandwich constructions, which occur when sheets of core material are not properly butted up against each other in the mold. The aim of this study was to characterize core gaps in composite sandwich constructions at the coupon scale. This was to gain an initial understanding of the defect before developing appropriate methodologies for more complex subcomponents as part of a much broader wind blade structural validation and damage tolerance program. Long beam flexure in 4-point-bending was chosen as the most appropriate loading scenario. Beam specimens were characterized with and without 10 mm core gaps in fiberglass/balsa sandwich beams. The core gaps were characterized with two separate resin systems; a Hexion epoxy and Arkema's Elium resins system (a novel, infusible thermoplastic). Results showed that the Elium beams without the core gaps were had a 15% lower static strength than their epoxy counterparts. The introduction of the core gap to the epoxy beams reduced their static strength by 35%. The Elium beams, however, exhibited negligible strength reductions with the inclusion of the core gap. Overall, this characterization study provided pertinent information with regards to core gaps as a manufacturing defect to allow for continued development of damage tolerance and subcomponent validation methodologies with the inclusion of manufacturing defects.

17 WIND ENERGY↗
DOE OSTI2022

Effects of oxygen on the adsorption/oxidation of aqueous Sb(III) by Fe-loaded biochar: An X-ray absorption spectroscopy study

Fe-loaded biochar (FeBC) has been considered for Sb(III) adsorption, but the effects of oxygen (O 2 ) on the adsorption need further investigation. Liquid-/solid-phase analyses were conducted to investigate the role of O 2 in the Sb(III) adsorption by FeBC. The adsorption was best described by the pseudo-second-order (PSO) model for kinetic results and by the Langmuir model for thermodynamic results. More than 96.8 % of Sb(III) was adsorbed by FeBC, and available O 2 increased the liquid-phase Sb(III) oxidation efficiency by 2.1–7.5 times. The peak changes at ~1640 and 3450 cm -1 in FTIR spectra indicated the occurrence of inner-sphere complexation between Sb(III)/Sb(V) and hydroxyl (–OH)/carboxyl (–COOH) groups in FeBC under aerobic and anaerobic conditions. Fe/Sb X-ray absorption spectroscopy (XAS) analysis results showed aqueous Sb(III) complexed to the edge-sharing Fe(III)-O-Fe(III) in FeBC. Regardless of whether O 2 was available or not, solid-phase edge-sharing Fe(III)-O-Sb(V) complexes (~3.05 Å), which had lower toxicity and migration ability than aqueous Sb(III), formed through a ligand-to-metal charge-transfer (LMCT) process. More than 91 % of adsorbed Sb(III) was oxidized to edge-sharing Fe(III)-O-Sb(V) complexes in 3 h. Additionally, the Sb(V) from liquid-phase oxidation could also directly complex to the Fe(III)-O-Fe(III) and form edge-sharing Fe(III)-O-Sb(V) complexes. Here these results provide evidence to inform further FeBC application for the Sb-contaminated water treatment.

54 ENVIRONMENTAL SCIENCES↗
DOE OSTI2022

An Engineered Multifunctional Composite for Passive Sensing, Power Harvesting, and In Situ Damage Identification with Enhanced Mechanical Performance

A multifunctional fiber-reinforced composite with passive self-sensing, energy-harvesting, and damage detection capabilities is presented. In this work, barium titanate piezoelectric microparticles are deposited on basalt fibers by a scalable, low-cost, environmentally friendly continuous feed-through process. The resulting composite derives a superior interlaminar shear strength from the microparticle-modified fiber–matrix interfaces. The composite also demonstrates passive self-sensing capabilities that produce electrical signals proportional to various dynamic loading events. Vibration and strain-controlled experiments are performed on composite beams to quantify the sensitivity and power output as a function of input acceleration and strain. Furthermore, these composite-generated electrical signals are used to identify in situ damage initiation for structural health monitoring to inform composite damage prior to structural failure. In brief, this truly multifunctional composite simultaneously displays a sensitivity of 0.5–2.6 mV g -1 at a resolution of 0.045–0.20g (g = gravitational acceleration), energy harvesting in the range of nW cc -1 , and prediction of early damage by exhibiting 0.017–1.17 mV peaks in voltage–time history profiles while assuring ≈20% improved interlaminar shear strength.

37 INORGANIC, ORGANIC, PHYSICAL, AND ANALYTICAL CH↗
DOE OSTI2024

Extended-MHD simulations of disruption mitigation via massive gas injection in SPARC

Recent developments to the M3D-C1 code enable higher fidelity modeling of disruptions, and can be applied in the design verification of reactor-scale tokamaks. Among these new capabilities is a method to mesh conducting vessel structures such as coils and passive plates, packing of the toroidal mesh around gas injectors, as well as anisotropic resistivity inside the vessel structures. We present extended-magnetohydrodynamic (MHD) simulations of disruption mitigation via massive gas injection (MGI) in SPARC. The goal of this study is to inform the disruption mitigation layout of SPARC and aid in the design of an effective gas injector configuration. Fully three-dimensional simulations with M3D-C1 are carried out for various injector configurations with the primary goal of determining the effect of different MGI parameters on heat loads and vessel forces. The simulations include a model for impurity ionization, recombination, advection and radiation, as well as spatially resolved conducting structures around the plasma. A localized mixture of deuterium and neon with a small toroidal and poloidal width is injected in up to six locations. We demonstrate that M3D-C1 can model a rapid shutdown via MGI using narrow and more realistic gas plumes than in previous simulations. As a result of the q = 1 surface in the SPARC baseline case a sawtooth is observed early in the simulations. Despite the sawtooth and the onset of edge MHD instabilities, the impurity distribution remains localized around the injector locations, but enables a radiative shutdown of the plasma. We find that using the maximum of six gas injectors results in a lower peaking factor and leads to a more even distribution of radiation toroidally than using two injectors.

70 PLASMA PHYSICS AND FUSION TECHNOLOGY↗