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At least 1,207 records · Page 67

A Comparison of Fabrication Techniques for Hollow Retroreflectors

Despite the wide usage of hollow retroreflectors, there is limited literature involving their fabrication techniques and only two documented construction methods could be found. One consists of an adjustable fixture that allows for the independent alignment of each mirror, while the other consists of a modified solid retroreflector that is used as a mandrel. Although both methods were shown to produce hollow retroreflectors with arcsecond dihedral angle errors, a comparison and analysis of each method could not be found which makes it difficult to ascertain which method would be better suited to use for precision-aligned retroreflectors. Although epoxy bonding is generally the preferred method to adhere the three mirrors, a relatively new method known as hydroxide-catalysis bonding (HCB) presents several potential advantages over epoxy bonding. HCB has been used to bond several optical components for space-based missions, but has never been applied for construction of hollow retroreflectors. In this paper we examine the benefits and limitations of each bonding fixture as well as present results and analysis of hollow retroreflectors made using both epoxy and HCB techniques.

optics↗

The Influence of Dihedral Angle Error Stability on Beam Deviation for Hollow Retro-Reflectors

Retro-reflectors consist of three reflective optical surfaces, which are oriented to reflect the input beam by 180 ◦. For retro-reflector components, it is common to specify an angular beam deviation tolerance, or rather the deviation from the exact 180 def return direction. Precision-aligned retro-reflectors provide 180 deg beam deviation with tolerances on the order of an arcsecond. It is well known that the performance of the retro-reflector depends on the ability to precisely orient the reflective surfaces at mutually perpendicular angles. Precision assembly is therefore critical to ensure highly accurate beam deviation. The dihedral angle errors, and hence the reflected beam deviation, can be measured for the retro-reflector after fabrication, typically by using interferometric techniques. Yet, what is not commonly reported for a fabricated retro-reflector is the stability of the angular beam deviation. For instance, thermo-mechanical effects of the components will contribute to variations in the return beam direction. While the actual stability is design-specific one can develop a mathematical representation for the expected change in the reflected beam direction as a function of the variation in the dihedral angle errors. Presented here is a mathematical formulation for a hollow retro-reflector's beam deviation as a function of the dihedral angle error stability.

Swank, Aaron J.↗

High Accuracy Coronagraph Flight Model For WFIRST–CGI Raw Contrast Sensitivity Analysis

A high-accuracy high-fidelity flight wavefront control (WFC) model is developed for detailed raw contrast sensitivity analysis of WFIRST-CGI. Built upon features of recently testbed validated model, it is further refined to combine a full Fresnel propagation diffraction model for high accuracy contrast truth evaluation, and an economical compact model for WFC purposes. Extensive individual raw contrast error sensitivities are evaluated systematically, both as known imperfections and as unknown calibration errors, for both spectroscopy mode and wide field-of-view mode with shaped pupil coronagraph. More than 90 distinct error items were identified, including system aberrations, optical misalignment, component manufacturing error, telescope interface related errors, etc. The result forms the basis for raw contrast error budget flow down to a sub-system level, where detailed specifications needed to aid in component design and manufacturing, mechanical alignment and instrument integration, and verification and validation operations. Evaluations are mostly automated, making it relatively easy for repeat runs of revised design or at new desired error quantity. Top error sensitivities and contrast floor contributors are discussed and several observations are noted.

Poberezhskiy, Ilya↗

Dual-pace transient heat conduction in vertically aligned carbon nanotube arrays induced by structure separation

Vertically aligned arrays of carbon nanotubes (CNTs) are attractive for a wide range of macroscopic applications which can exploit the remarkable properties of individual nanotubes. In this work, an abnormal behavior of CNT bundles in heat conduction is discovered under the transient electro-thermal characterization. The measured voltage change over the sample shows a dual-pace thermal response (DTR), which could not be fitted using a single thermal diffusivity heat transfer model. Instead, two thermal diffusivities are determined from the DTR phenomenon. Three rounds of cryogenic experiments are conducted to investigate the physics behind DTR phenomenon. It starts to emerge when the temperature is reduced to a certain level. After two rounds of cryogenic experiments, the DTR phenomenon becomes permanent from 295 K to 10 K. The nano-scale structure separation induced by the increased thermal strain leads to macroscale structure separation, which results in two parallel heat conduction paths responsible for the DTR phenomenon. By building a new parallel heat transfer model taking both the transient and steady-state electrical and thermal response into consideration, the area ratio of separated CNTs is determined. Furthermore, this result uncovers the existence of coiled morphology and nano-structure evolution of CNTs under cryogenic state and its effect on thermal and electrical transport, especially on their transient behaviors. Knowledge of the thermal transport in these CNTs arrays is important considering the fact that transient thermal response strongly affects their mechanical, optical, and electrical behaviors.

42 ENGINEERING↗

Multispectral and thermal surface imagery and surface elevation mosaics - Pendleton Feb 2023

This data set contains high-resolution image products (orthomosaics) acquired from midsized uncrewed aerial systems that have been processed for value-added quality. The instrument Altum multispectral imager by Micasense, captures in six bands (blue - 475nm, green - 560nm, red - 668nm, red edge - 717nm, near-infrared - 840 and LWIR/thermal - 11000nm. The optical bands are converted to reflectance via custom code using the instantaneous band horizontal irradiance ratio to the radiance of the pixel. The code used to develop these images first uses tools from the Micasense Python library to apply dark level corrections, row gradient corrections, and radiometric corrections. Next, it uses the processing API from Agisoft Metashape software to align and mosaic the processed imagery, following the processes developed by the USGS' structure from motion workflow documentation. Captures from different altitudes are used to produce an orthomosaic at each height. A tif image containing information related to the six spectral bands, and a digital elevation model (DEM), a tif image containing information related to the elevation of the surveyed terrain. 1 https://www.arm.gov/publications/tech_reports/handbooks/doe-sc-arm-tr-281.pdf 2 https://micasense.github.io/imageprocessing/MicaSense%20Image%20Processing%20Setup.html 3 https://pubs.usgs.gov/of/2021/1039/ofr20211039.pdf

54 ENVIRONMENTAL SCIENCES↗

Solvent-Dependent Dynamics of Cellulose Nanocrystals in Process-Relevant Flow Fields

Flow-assisted alignment of anisotropic nanoparticles is a promising route for the bottom-up assembly of advanced materials with tunable properties. While aligning processes could be optimized by controlling factors such as solvent viscosity, flow deformation, and the structure of the particles themselves, it is necessary to understand the relationship between these factors and their effect on the final orientation. In this study, we investigated the flow of surface-charged cellulose nanocrystals (CNCs) with the shape of a rigid rod dispersed in water and propylene glycol (PG) in an isotropic tactoid state. In situ scanning small-angle X-ray scattering (SAXS) and rheo-optical flow-stop experiments were used to quantify the dynamics, orientation, and structure of the assigned system at the nanometer scale. The effects of both shear and extensional flow fields were revealed in a single experiment by using a flow-focusing channel geometry, which was used as a model flow for nanomaterial assembly. Due to the higher solvent viscosity, CNCs in PG showed much slower Brownian dynamics than CNCs in water and thus could be aligned at lower deformation rates. Moreover, CNCs in PG also formed a characteristic tactoid structure but with less ordering than CNCs in water owing to weaker electrostatic interactions. The results indicate that CNCs in water stay assembled in the mesoscale structure at moderate deformation rates but are broken up at higher flow rates, enhancing rotary diffusion and leading to lower overall alignment. Albeit being a study of cellulose nanoparticles, the fundamental interplay between imposed flow fields, Brownian motion, and electrostatic interactions likely apply to many other anisotropic colloidal systems.

36 MATERIALS SCIENCE↗

An Educational Program on Concentrated Solar Power and Heliostats for Power Generation and Industrial Processes

The objective of this project was to design and implement a comprehensive educational and applied research program in Concentrated Solar Thermal Power (CSTP) and heliostat technologies at Northeastern University. In alignment with the U.S. Department of Energy's Heliostat Consortium (HelioCon) goals, the project aimed to expand student and public understanding of CSTP systems while simultaneously contributing to workforce development and the broader decarbonization strategy. A particular emphasis was placed on integrating hands-on student design projects and publicly disseminating educational content relevant to CSTP systems. The project addressed a critical gap in renewable energy education: CSTP and heliostats, despite their importance in utility-scale solar energy, are rarely included in standard mechanical engineering programs. This project established new pathways for students to engage with the topic through the creation of a 4-credit graduate/senior elective course, development of five industry-facing short courses, and the inclusion of CSTP-based capstone design projects. Over two academic years, 36 students across six senior design teams developed and tested technologies such as deformable heliostats, beacon-based tracking systems, and solar-powered pyrolizers for biomass-to-biochar conversion. Concurrently, 30 undergraduate and graduate students were enrolled in the new academic course centered around CSTP principles. To ensure the relevance and accessibility of the short course content, the project team engaged with industry professionals, technical policy stakeholders, and potential course participants through structured surveys and informal consultations. Feedback from 28 respondents guided the structure, length, and delivery format of the courses - resulting in a modular design broken into five workshops. The feedback emphasized the need for flexible, asynchronous delivery and practical case studies, particularly in areas such as heliostat control, thermal storage, and solar fuel production. This engagement helped align the courses with the evolving knowledge demands of the renewable energy workforce and ensured that participants from both technical and policy backgrounds could meaningfully benefit from the material. The research and educational activities advanced the understanding of heliostat control systems, optical performance under misalignment, and thermal system integration in solar-driven pyrolysis applications. Methods and designs explored in this project proved to be both technically effective and economically feasible at the lab scale. Prototypes were constructed using commercially available components and custom-fabricated elements, demonstrating that meaningful performance improvements can be achieved with modest material and fabrication costs, supporting the feasibility of student-led research in this field. The public benefit of this project is twofold. First, it cultivates a pipeline of engineers trained to be familiar with CSTP principles, an essential workforce need identified by the Department of Energy for achieving its 2030 cost and deployment targets. Second, it contributes openly accessible educational materials, course content, and experimental frameworks to the broader community, enabling other institutions to adopt or adapt similar programming. Through outreach activities, curriculum integration, and technical exposure, this project contributes to a more informed and capable renewable energy workforce while supporting innovation in heliostat and CSTP system design. A new technical report is being prepared to document the development of the course and its outcomes, with plans to publish it in the ASME Open Access Journal of Engineering to ensure global accessibility, free of cost.

14 SOLAR ENERGY↗

The Magsat three axis arc second precision attitude transfer system

The Magsat Attitude Transfer System (ATS), which provides attitude alteration in pitch, yaw, and roll is described. A remote vector magnetometer extends from Magsat on a 20 ft boom, requiring vector orientation by reference to coordinate axes determined by a set of star mapping cameras. The ATS was designed to perform in a solar illuminated environment by using an optically narrow bandwidth with synchronous demodulation at 9300 A. The pitch/yaw optical design, the electrooptics, and signal and switching diagrams are provided. Simple mirrors with no moving parts are placed on the magnetometer to reflect a collimated beam from the ATS for attitude indication, which is accurate to one part in 96. Alignment was completed within 24 hr after launch.

Schenkel, F. W.↗

Dynamics of the Uranian Rings

Some of the problems of the shepherding satellite model of Goldreich ant tremaine are discussed. The following topics are studied: (1) optical depths of the all the observed narrow rings; (2) satellite and ring separation timescales; (3) ring edge sharpness; (4) shock formation in narrow rings; (5) the existence of small satellites near the Uranian rings; and (6) the apse and node alignments of the eccentric and inclined rings.

Dermott, S. F.↗

Moisture effects and control for the UVCS composite structure

The Ultraviolet Coronagraph Spectrograph (UVCS) is an optical instrument to be flown on the European spacecraft Solar Heliospheric Observatory (SOHO) to the sun-earth L1 point. The stability requirements of the instrument require the moisture content of the pseudoisotropic composite material not to exceed 0.06 percent during alignment and calibration. This paper describes the steps necessary to meet this requirement. These steps include a dynamic moisture content analysis, selection of bake out conditions and moisture controls, verification sampling, and use of witness specimens to monitor the moisture content during the prelaunch life of the structure.

Austin, James D.↗

Diffusivity Measured as a Function of Concentration

Optical diagnostic techniques have become an integral part of many measurements in industrial and research laboratories. Many types of interferometers and their phase-shifted versions have been used to measure optical wave fronts for lens testing and combustion and fluid flow diagnostics. One such instrument is the point diffraction interferometer (PDI), which is considered to be robust because it has a common-path design. However, the PDI is difficult to align and has limited measurement range for liquid phase applications. Interferometry and schlieren techniques have been widely used for many years for gas flow visualization.

Rashidnia, Nasser↗

NIRCam: The JWST Near-IR Camera and Slitless Spectrograph

NIRCam is the primary near-infrared camera for JWST. It is well-suited for a wide variety of star formation and other scientific studies and will also be used for aligning the JWST primary mirror segments and telescope. NIRCam will provide high sensitivity, high spatial resolution images in a variety of filters over the 0.6 - 5 μm wavelength region including coronagraphic modes and slitless spectroscopic capabilities. NIRCam consists of two identical optical modules that have adjacent 2.2' x 2.2' fields of view on the sky. Each module is composed of two channels that observe the same field at short (< 2.4 μm) or long (> 2.4 μm) wavelengths simultaneously, with optimized spatial sampling in each channel. NIRCam optical elements include narrow (R = 100), medium (R = 10), and wide (R <= 4) filters, coronagraphic imaging spot and bar masks, and grisms that provide wide-field or time-series slitless spectroscopy. These major NIRCam features will be introduced, and some applications to galactic star formation will be briefly presented.

Greene, Thomas↗

Metabolic Vessel for Impedance Spectroscopy and Electrochemistry (MVISE): The Ground Mapping Unit for the Lunar Explorer Instrument for Space Biology Applications (LEIA)​

The BioSensor payload on the upcoming LEIA platform aboard a CLPS lander will carry yeast to the moon to study response to radiation and lunar gravity. The LEIA BioSensor is designed to monitor metabolic activity using absorbance in conjunction with alamarBlue for measuring colorimetric changes as proxy measurement for redox potential. The science data returned from small spacecraft mission modules like LEIA is limited as it relies solely on optical measurements, necessitating a corresponding ground mapping unit that is equipped with multiple electrochemical sensors for accurate mapping of the optical data and operates fully automatically. This technology development work discusses the extensive design and optimization efforts put into the ground mapping unit, MVISE. MVISE is a custom designed, 3D-printed vessel with an agitation system, with six different electrochemical sensor probes, and ports for sample collection and a pressure release valve. The sensors provide real-time data, with dry absorbance measurements aligning with LEIA flight hardware and wet measurements demonstrating invasive sensor design enabling a comparison between the two setups. The 3D printer resin was tested for mechanical robustness, biocompatibility, and resistance to autoclave sterilization. The inner walls were coated with food-grade epoxy, ensuring a smooth finish to prevent microbial lodging and dye staining. The MVISE has successfully passed a week-long leak test and is now undergoing active biology tests. The MVISE prototype will be prepared for radiation tests, with three identical units being tested for varying radiation levels and culture compositions at the NASA Space Radiation Laboratory in November 2024. The integrated sensor approach proposed in this work will enable the accurate mapping of the BioSentinel/LEIA optical flight data to six sensor parameters on the ground unit for better science data return and will enable the first effort to evaluate classical biochemical sensor measurements by comparing and contrasting their responses.

Chinmayee Govinda Raj↗

Binary pseudo-random array standard for extreme ultraviolet lithography tool characterization

Extreme ultraviolet (EUV) imaging tools play a crucial role in EUV lithography. Achieving high accuracy in EUV metrology is essential for advanced semiconductor manufacturing. A thorough characterization of the instrumentation in use is required. Binary pseudo-random arrays (BPRAs) are an established standard for calibrating and characterizing optical instruments in the frequency domain. Here, we expand the BPRA standard to applications in EUV imaging. To extend the technology to the EUV spectral range, a high-resolution BPRA target with the smallest feature size of 40 nm is developed. The EUV BPRA target establishes an in situ and portable calibration and alignment standard for EUV imaging. The target is patterned by means of electron-beam lithography, using a nickel absorber with a thickness of 39 nm. The substrate is a 4″ silicon wafer with a molybdenum/silicon multilayer coating. To demonstrate the efficacy of the target and develop the instrument calibration protocol, the target is imaged on the Sharp Hyper-NA Actinic Reticle Review Project EUV mask microscope. Power spectral density (PSD) data are presented. The characteristics of the imaging system are imprinted on the PSD. The modulation transfer function is extracted from the PSD data. A partially coherent imaging model is used as a reference to the experimental results.

BPRA↗

Geometrical Frustration and Defect Formation in Growth of Colloidal Nanoparticle Crystals on a Cylinder: Implications for Assembly of Chiral Nanomaterials

Using a combination of experiment and simulation, we study how two-dimensional (2D) crystals of colloidal nanoparticles grow on cylindrical substrates. The cylindrical geometry allows us to examine growth in the absence of Gaussian curvature but in the presence of a closure constraint - the requirement that a crystal loops back onto itself. In some cases, this constraint results in structures that have been observed previously in theory and nonequilibrium packing experiments: chiral crystals and crystals with linear defects known as "line slips". More generally, though, the structures we see differ from those that have been observed: the line slips are kinked and contain partial vacancies. We show that these structures arise because the cylinder changes how the crystal grows. After a crystal wraps around the cylinder and touches itself, it must grow preferentially along the cylinder axis. As a result, crystals with a chiral line slip tend to trap partial vacancies. Indeed, we find that line slips that are less aligned with the cylinder axis incorporate more partial vacancies on average than the ones that are more aligned. Here, these results show that crystal growth on a cylinder is frustrated by the closure requirement, a finding that may shed some light on the assembly of biological nanosystems such as tobacco mosaic virus and might inform ways to fabricate chiral optical nanomaterials.

37 INORGANIC, ORGANIC, PHYSICAL, AND ANALYTICAL CH↗

Direct-write orientation of charge-transfer liquid crystals enables polarization-based coding and encryption

Abstract Optical polarizers encompass a class of anisotropic materials that pass-through discrete orientations of light and are found in wide-ranging technologies, from windows and glasses to cameras, digital displays and photonic devices. The wire-grids, ordered surfaces, and aligned nanomaterials used to make polarized films cannot be easily reconfigured once aligned, limiting their use to stationary cross-polarizers in, for example, liquid crystal displays. Here we describe a supramolecular material set and patterning approach where the polarization angle in stand-alone films can be precisely defined at the single pixel level and reconfigured following initial alignment. This capability enables new routes for non-binary information storage, retrieval, and intrinsic encryption, and it suggests future technologies such as photonic chips that can be reconfigured using non-contact patterning.

37 INORGANIC, ORGANIC, PHYSICAL, AND ANALYTICAL CH↗

Mirror instability and origin of morningside auroral structure

Auroral optical imagery shows marked differences between auroral features of the evening and morning sectors: the separation between diffuse and discrete auroras in the evening sector is not distinct in the morning sector, which is dominated by auroral patches and multiple banded structures aligned along some direction. Plasma distribution function signatures also show marked differences: downward electron beams and inverted-V signatures prefer the evening sector, while the electron spectra on the morning sector are similar to the diffuse aurora. A theory of morningside auroras consistent with these features was constructed. The theory is based on modulation of the growth rates of electron cyclotron waves by the mirror instability, which is in turn driven by inward-convected ions that have become anisotropic. This modulation produces alternating bands of enhanced and reduced electron precipitation which approximate the observed multiple auroral bands and patches of the morning sector.

Chiu, Y. T.↗

Mirror instability and the origin of morningside auroral structure

Auroral optical imagery shows marked differences between auroral features of the evening and morning sectors: The separation between diffuse and discrete auroras in the evening sector is not distinct in the morning sector, which is dominated by auroral patches and multiple banded structures aligned along some direction. Plasma distribution function signatures also show marked differences: downward electron beams and inverted-V signatures prefer the evening sector, while the electron spectra on the morning sector are similar to the diffuse aurora. We have constructed a theory of morningside auroras consistent with these features. The theory is based on modulation of the growth rates of electron cyclotron waves by the mirror instability, which is in turn driven by inward-convected ions that have become anisotropic. This modulation produces alternating bands of enhanced and reduced electron precipitation which approximate the observed multiple auroral bands and patches of the morning sector.

Chiu, Y. T.↗