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At least 1,207 records · Page 67

Stability of human sera collected for clinical chemistry determinations

Problems in collecting and shipping human sera for clinical chemical analyses affect their stability and require proper preservation methods. It is shown that glutamic pyruvate transaminase is very unstable and serum cannot be shipped unless the shipping time is carefully controlled and is less than two days under refrigeration. A limit of four days handling time and avoidance of light exposure are required in bilirubin testing of specimens. Addition of 11 mg of a 10 to 1 mixture of finely powdered sodium fluoride and thymol per ml of blood to preserve specimen stability en route to a central laboratory prevents glycolysis. A citrate buffer at pH 6.2 in serum to be tested for alkaline phosphatase lessens decline at room temperature.

Townsend, F. M.↗

The development of an inert simulant for HNS/teflon explosive

The report describes the development and evaluation of an inert simulant for the thermally stable, heat-resistant plastic-bonded explosive HNS/Teflon. The simulant is made by dry blending vinylidene fluoride, melamine and Teflon which when compared has a pressed density and thermal properties corresponding closely to the explosive. In addition, the machinability and handling characteristics of the simulant are similar to the explosive.

Elban, W. L.↗

Thermoluminescent dosimetry for the Apollo 16 microbial response to space environment experiment (M191)

Lithium fluoride thermoluminescent chips were used to provide an integrated dose from the broad spectrum of ionizing radiation to the Microbial Response to Space Environment Experiment (M191). The chips were positioned in the flight hardware to provide data on ionizing radiation within specific volume segments. A uniform radiation dose of 4.8 x 0.001 plus or minus 2 x 0.0001 joule/kg resulted.

Brown, R. D.↗

Performance characteristics of proximity focused ultraviolet image converters

Performance characteristics of Bendix type BX 8025-4522 proximity focused image tubes for ultraviolet to visible light conversion are presented. Quantum efficiency, resolution, background, geometric distortion, and environmental test results are discussed. The converters use magnesium fluoride input windows with Cs - Te photocathodes, and P-11 phosphors on fiber optic output windows.

Williams, J. T.↗

Irradiation test of tungsten clad uranium carbide-zirconium carbide ((U,Zr)C) specimens for thermionic reactor application at conditions conductive to long-term performance

Uranium carbide fueled, thermionic emitter configurations were encapsulated and irradiated. One capsule contained a specimen clad with fluoride derived chemically vapor deposited (CVD) tungsten. The other capsule used a duplex clad specimen consisting of chloride derived on floride derived CVD tungsten. Both fuel pins were 16 millimeters in diameter and contained a 45.7-millimeter length of fuel.

Creagh, J. W. R.↗

Movable-molybdenum-reflector reactivity experiments for control studies of compact space power reactor concepts

An experimental reflector reactivity study was made with a compact cylindrical reactor using a uranyl fluoride - water fuel solution. The reactor was axially unreflected and radially reflected with segments of molybdenum. The reflector segments were displaced incrementally in both the axial and radial dimensions, and the shutdown of each configuration was measured by using the pulsed-neutron source technique. The reactivity effects for axial and radial displacement of reflector segments are tabulated separately and compared. The experiments provide data for control-system studies of compact-space-power-reactor concepts.

Fox, T. A.↗

Study of carbon compounds in Apollo 12 and 14 lunar samples.

The results of gas-chromatography and high-resolution mass spectroscopy studies of gases released on deuterium fluoride dissolution of Apollo 12 and 14 lunar samples are reported. The results confirm previous observations that CH4 and C2H6 are released as well as CD4, C2D4, C2D6, and higher deuterated hydrocarbons. The yields correlate with the total carbon content of the samples, and the CH4 and C2H6 released may be regarded as indigenous, while the deuterated products result from hydrolysis of carbide material. The results provide the first experimental confirmation of the hypothesis that the CH4 derives from solar wind interactions.

Holland, P. T.↗

Solubilities of noble gases in magnetite - Implications for planetary gases in meteorites.

Solubilities of noble gases in magnetite were determined by growing magnetite in a noble-gas atmosphere between 450 and 700 K. Henry's law is obeyed at pressures up to .01 atm for He, Ne, Ar and up to .00001 atm for Kr, Xe, with the following distribution coefficients at 500 K: He 0.042, Ne 0.016, Ar 3.6, Kr 1.3, Xe 0.88, some 100 to 100,000 times higher than previous determinations on silicate and fluoride melts. Apparent heats of solution are in sharp contrast with earlier determinations on melts which were small and positive, but are comparable to the values for clathrates. Presumably the gases are held in anion vacancies.

Lancet, M. S.↗

Ultraviolet proximity focussed converters for use in a satellite SEC-TV system.

Performance characteristics of Bendix type BX08025-4522 proximity-focussed vacuum-ultraviolet to visible-light image converters are presented. The converters are to be used with SEC vidicons as detectors for an echelle spectrograph on the International Ultraviolet Explorer astronomical satellite. Magnesium fluoride input windows with Cs-Te photocathodes are used in the converters, with P-11 phosphors on the fiber optic output windows. Quantum efficiencies, modulation transfer function, background, geometric distortion, and environmental test results are presented for the wavelength region from 1150 to 3500 A.-

Feibelman, W. A.↗

Flame resistant elastic elastomeric fiber

Compositions exhibit elastomeric properties and possess various degrees of flame resistance. First material polyurethane, incorporates halogen containing polyol and is flame resistant in air; second contains spandex elastomer with flame retardant additives; and third material is prepared from fluorelastomer composition of copolymer of vinylidene fluoride and hexafluoropropylene.

Howarth, J. T.↗

Self-lubricating plasma-sprayed composites for sliding contact bearings to 900 C

Plasma-sprayed composites which have good oxidation-resistance and self-lubricating characteristics to 900 C were developed. The composites are a Nichrome matrix containing dispersed glass for oxidation protection and calcium fluoride for lubrication. They are applied to bearing surfaces in layers about 0.050 cm thick by plasma-spraying; the layers are then machined to a thickness of 0.025 cm. Oscillating bearing tests were performed in air to 900 C at unit radial loads up to 3.5 times 10 to the 7th power Newtons per square meter (5000 psi) and a thrust load of 1960 Newtons (440 lb). Bearings with a composite liner in the bore were in good condition after over 50,000 oscillating cycles accumulated during repeated bearing temperature cycles between 25 and 900 C.

Sliney, H. E.↗

Testing and evaluation of solid lubricants for gas bearings

The testing and results of testing solid film lubricants for gas lubricated bearing applications are reported. The tests simulated operational hazards of tilting pad gas bearings. The presence of a low coefficient of friction and the endurance of the solid film lubricant were the criteria for judging superior performance. All solid lubricants tested were applied to a plasma sprayed chrome oxide surface. Molybdenum disulfide and graphite fluoride were the solid lubricants tested; other test parameters included the method of application of the solid lubricant and the surface finish of the plasma sprayed coating. In general, the application of a solid film lubricant was found to significantly improve the coefficient of friction of the rubbing surfaces.

Albrecht, P. R.↗

Improved thermoelectrically cooled quartz crystal microbalance

Design changes in the thermoelectrically-cooled quartz microbalance, which is used to monitor surface contamination in space simulation chambers, is described in terms of its extended temperature range, increased temperature control, mass sensitivity, and cooling power. The mass sensor uses 20 MHz quartz crystals having a sensitivity of 8.8 x 10 to the minus tenth power g/sq cm - Hz. The crystals are optically polished, metal plated, and overplated with magnesium fluoride to simulate an optical surface. The microbalance temperature circuitry is designed to readout and control surface temperature between 100 C and minus 59 C to plus or minus 0.5 C, and readout only temperature between minus 60 C and minus 199 C using auxiliary liquid nitrogen cooling. Data is included on the measurement of oil contamination of surfaces as a function of temperature in space simulation chambers.

D. McKeown↗

Development of fine diameter mullite fiber

Results are presented of a program to develop and evaluate mullite fiber with a mean diameter under two microns. The two micron fiber is produced by a blowing process at room temperature from a low viscosity (10-25 poise) solution. The blown fiber was evaluated for dimensional stability in thermal cycling to 1371 C, and was equivalent to the 5 micron spun B and W mullite fiber. An additive study was conducted to evaluate substitutes for the boron. Three levels of chromium, lithium fluoride, and magnesium were added to the standard composition in place of boron and the fiber produced was evaluated for chemical and dimensional stability in thermal cycling to 1371 C. The magnesium was the most chemically stable, but the chrome additive imparted the best dimensional stability.

Long, W. G.↗

An ellipsometer with variable angle of incidence for studies in ultrahigh vacuum

The windows for the vacuum chamber are incorporated into the optical bench system by means of flexible bellows which allow measurements to be made over a large range of angle of incidence, one of which is chosen so that maximum sensitivity is obtained. The principal angle of incidence was determined, and straightforward corrections for strain birefringence of vacuum chamber windows were made. Atomically clean surfaces of sodium chloride and lithium fluoride were investigated to verify the performance of the system. Submonolayer and monolayer coverage of water on these surfaces could be detected. On cleavage planes of NaCl, a first monolayer of adsorbed water is complete at about one torr only.

Walter, H. U.↗

Techniques for the analysis of gases sequentially released from lunar samples

Description of two methods for the analysis of light gases that are sequentially evolved from 2 to 10 mg of lunar sample. A hydrofluoric acid hydrolysis of lunar material is achieved by repeated exposure of the sample to hydrogen fluoride. In the second technique, gases are evolved from lunar samples by the stepwise heating of these samples to 1400 C. The gases evolved by either hydrolysis or pyrolysis are analyzed in a gas chromatographic system using a helium ionization detector. The sensitivities of this detector for the gases, as analyzed, range from 20 picograms/sec for hydrogen to 0.2 picogram/sec for carbon dioxide.

Desmarais, D. J.↗

Performance characteristics of proximity focused ultraviolet image converters

Performance characteristics of Bendix type BX 8025-4522 proximity focused image tubes for UV to visible light conversion are presented. Quantum efficiency, resolution, background, geometric distortion, and environmental test results are discussed. The converters use magnesium fluoride input windows with Cs-Te photocathodes and P-11 phosphors on fiber optic output windows.

Williams, J. T.↗

Dynamic load capacities of graphite fiber: Polyimide composites in oscillating plain bearings to 340 C (650 F)

Load capacities were determined for plain spherical bearings with self-lubricating spherical elements of graphite-fiber-reinforced-polyimide, and for plain cylindrical bearings with thin-wall liners of the composite in the bearing bores. Composites consisted of a 1-to-1 weight ratio of graphite fibers and polyimide. Oscillation was at an amplitude of + or - 15 deg at a frequency of 1 hertz. Bearings with composite ball material had a load capacity of approximately 69 MN/sq m (10 000 psi) at room temperature 25 MN/sq m (3600 psi) at 340 C (650 F). Bearings with thin-wall composite liners had much higher load capacities of 280 MN/sq m (40 000 psi) at room temperature amd 240 MN/sq m (35 000 psi) at 320 C (600 F). Friction coefficients were in the range of 0.12 to 0.19. The addition of 10 wt.% graphite fluoride solid lubricant to the composition of the thin-wall liners reduced friction coefficients into the range of 0.10 to 0.12.

Sliney, H. E.↗