Engineering Papers⌕ Search

SEARCH · Engineering Papers

Results for “sample thickness”

Search indexed NASA NTRS and DOE OSTI research on propulsion, heat transfer, battery materials and energy systems. Follow report and document links to the original sources.

Quote a phrase for an exact phrase match. Source license links do not imply unrestricted reuse.

At least 1,189 records · Page 66

A test of the applicability of independent scattering to high albedo planetary regoliths

We show that 'independent scattering' is a useful approximation for high albedo particles whose size and packing density are similar to typical particles in the lunar regolith. Laboratory measurements of the intensity and linear polarization of light scattered from a laboratory sample of glass spheres of know size and composition are compared to radiative transfer calculations of the same observable quantities. Mie scattering is integrated over the size distribution of the particles to determine the mean phase and polarization functions, or phase matrix, of the particle. Assuming that the particles scatter independently, the 'doubling method' is used to rigorously calculate multiple scattering in an optically thick layer of these anisotropically scattering particles. All of the major features 'predicted' in the calculated intensity (double peaks at small phase angles) and polarization (negative branch at small phase angles, large positive peak near 20 degrees phase, and small polarization elsewhere) are observed in the laboratory measurements, with good quantitative agreement indicated at phase angles less than 90 degrees. Even though the particles are supported by physical contact with each other in the sample, as are the particles in planetary regoliths, the independent scattering calculation yields a good approximation to both the intensity and polarization. The physical parameters input to the calculation are only the size distribution of the particles and their complex index of refraction (composition). Significant advantages of this approach are that the phase matrix is calculated from basic physical principles and both the intensity and polarization are determined simultaneously. This model may have broad applications to the interpretation of photometry, spectroscopy, and polarimetry of the icy regoliths of high albedo satellites. The intent of this effort is to perform a controlled experiment that tests the utility of the independent scattering assumption

Goguen, J. D.↗

Porosity, swelling, and composition evolution in high-burnup monolithic U-Mo fuel

The microstructural progression of very high-burnup (>8 × 10 21 fissions/cm 3 ) monolithic uranium-molybdenum (U-10wt.%Mo) was analyzed, providing crucial insights into the behavior of post-recrystallized nuclear fuel, where scant data exists. Three focused ion beam cuboids sourced from a fuel plate with varying local burnups of 8.86 × 10 21 , 9.05 × 10 21 , and 9.36 × 10 21 fissions/cm 3 were characterized. The porosity and composition of the samples were evaluated to characterize the evolution of the microstructure as a function of fission density and different locations on the fuel plate, while simultaneously isolating plate-specific parameters such as Zr diffusion barrier thickness, hot-isostatic-pressing conditions, enrichment, and reactor conditions. The porosity was segmented, and the three-dimensional distribution of the porosity was extrapolated from the two-dimensional segmentation. The composition was assessed and quantified using energy-dispersive X-ray spectroscopy areal mapping. The porosity fraction increased as a function of the burnup from 27.77±0.51, 35.12±1.54, and 37.71±0.44 % for 8.86 × 10 21 , 9.05 × 10 21 , and 9.36 × 10 21 fissions/cm 3 , respectively. When compared to literature, the porosity volume fraction plateaus at burnups greater than 6 × 10 21 fissions/cm 3 , while the pore size grows linearly as a function of fission density. The number of large pores increased in number density as a function of burnup, while the smallest pores (<0.3 µm) increased up to 9.05 × 10 21 fissions/cm 3 , followed by a decrease at 9.36 × 10 21 fissions/cm 3 . The delamination and cracking in the fuel plate propagated through an interconnected porosity sublayer identified ∼5 µm from the diffusion barrier. The local swelling of the specimens was within or near the prediction bounds of the Robinson-Williams model for local swelling. The fission products, strontium, barium, cerium, and cesium, precipitated into the pores, while neodymium accumulated adjacent to the pores. Furthermore, these findings have direct implications for the development of fuel performance codes and the accurate documentation of the microstructure evolution in high burnup U-Mo, thus enhancing the safety and efficiency of nuclear fuel usage.

11 - NUCLEAR FUEL CYCLE AND FUEL MATERIALS↗

Optical properties of differing nanolayered structures of divalent europium doped barium fluoride thin films synthesized by pulsed laser deposition

Optically-active thin films are employed in a variety of applications, such as LEDs and photovoltaics, due to their ability to act as up- or down-photon energy converters. Their performance depends critically on their composition and structure; thus, the use of novel synthesis techniques that allow for their control at the nanoscale level can result in improved efficiency and practicality. Here, layered thin films consisting of Eu 2+ - doped BaF 2 nanocrystalline layers separated by amorphous Al 2 O 3 were synthesized via sequential pulsed laser deposition using three separate targets for the different components; this synthesis technique provides precise control of layer thickness at the nanoscale along with dopant distribution within the film. Cross-sectional transmission electron microscopy analysis verified the desired nano-layering. Post-deposition heat treatments in a nitrogen atmosphere resulted in samples exhibiting steady emission with a broad peak ranging from 400 to 600 nm and a shoulder at 410 nm. The CIE 1931 chromaticity coordinates are x = 0.26-0.29 and y = 0.32-0.35 and vary as a function of the sample configuration. Because the chromaticity coordinates are close to those of a pure white light (x = 0.33, y = 0.33), these films demonstrate advantageous properties for applications with UV-pumped white light LEDs.

36 MATERIALS SCIENCE↗

BERT Non-Destructively Probes the Microstructure of Dissimilar Welds [Poster]

Energy-resolved neutron imaging (ERNI) utilizes contrast provided by diffraction. Microstructure with >100µm grains as in cast, annealed or welded materials is difficult to characterize by X-ray or electron-based methods $\Rightarrow$ Well-suited for neutron Bragg-edge radiography. BERT was applied to dissimilar welds of Inconel on steel produced by additive manufacturing. Viewing the sample at time-of-flight/energy/wavelength where a single grain orientation dominates the attenuation allows to map grain orientations. Similarly to electron-backscatter diffraction (EBSD) but on cm length scales and through-thickness. Combined with texture measurements on the HIPPO instrument, identifying major grain orientations, 2D and 3D grain orientation maps are feasible. Results can guide development of thermo-mechanical treatment avoiding or introducing such microstructures, characterize dissimilar welds, interpretation of acoustic signals for quality control, guide destructive examination with X-rays/electrons, or provide data for codes predicting such microstructures.

36 MATERIALS SCIENCE↗

Preliminary comparison of material charging properties using single-energy and multienergy electron beams

Results of tests designed to compare the charging properties of spacecraft material under a monoenergetic beam and under a continuously distributed beam are summarized. In the test setup the electron source was mounted in the top of a cylindrical vacuum chamber. A sheet of 5-mil-thick Kapton was placed on an insulated metal substrate at the bottom of the vacuum chamber. The dc current arriving on the substrate was measured and a field meter measured the potential of the test sample. A retarding potential analyzer measured the energy spectrum of the incident electron beam. With the monoenergetic beam, the sample charged to 12 kV and electrical discharges occurred. With the multi-energy spectra the samples charged to only 6 kV and 4 kV, and no discharger were observed. In these experiments, no effort was made to duplicate the spectra occurring in space. The tests were intended to simply to compare spacecraft material charging properties using monoenergetic and continuous multi-energy beams.

Adamo, R. C.↗

Human exposure in low Earth orbit

Human exposure to trapped electrons and protons in low Earth orbit (LEO) is evaluated on a basis of a simple approximation of the human geometry for spherical shell shields of varying thickness. A data base is presented that may be used to make preliminary assessment of the impact of radiation exposure constraints on human performance. Detailed shielding studies should be performed before final design considerations. A sample impact assessment is discussed on the basis of presently accepted allowable exposure limits. A brief discussion is given on the anticipated impact of an ongoing reassessment of allowable exposure limits.

Wilson, J. W.↗

Space-exposure effects on optical-baffle coatings at far-infrared wavelengths

Reflectance of six optical-black coatings was remeasured over the near-infrared to the far-infrared region after nearly six years in space aboard the Long Duration Exposure Facility satellite. Measurements were made at room temperature and at cryogenic temperatures. The most notable effect was a general decrease in reflectance for typical samples at all wavelengths. Analysis indicates that this decrease is caused by an increase in absorption resulting from an increase in the imaginary part of the index of refraction, and not by a change in thickness, or increased surface roughness giving rise to increased scattering. These results suggest that such optical-baffle materials will provide enhanced performance as a result of aging in the space environment.

Blue, M. D.↗

Grazing incidence X-ray reflectivity - Studies for the AXAF observatory

The energy bandwidth and total throughput of a grazing incidence optics system is a strong function of the X-ray reflectivity of the surface coating. In support of the Advanced X-ray Astrophysics Facility (AXAF), studies are underway to evaluate and characterize the reflectivity of potential AXAF coatings. Here we report on results obtained for Au, Ir, and Ni coatings produced by electron-beam evaporation, evaporation with ion-assist, and sputtering. Effects of coating thickness and deposition angle have been evaluated at 6.4 and 8.1 keV; the highest reflectivities are those of the thinner, about 200 A vs about 700 A, coatings. While considerable variations exist, the best Ir samples have higher reflectivity than any of the Au coatings. Data results have been compared with models for theoretical reflectivity, particularly with regard to the effective density of the coatings. Independent measurements of the coating densities have been carried out for comparison with the reflectivity results.

Slane, P.↗

Ultrasonic Resonance Spectroscopy of Composite Rims for Flywheel Rotors

Flywheel energy storage devices comprising multilayered composite rotor systems are being studied extensively for utilization in the International Space Station. These composite material systems were investigated with a recently developed ultrasonic resonance spectroscopy technique. The ultrasonic system employs a continuous swept-sine waveform and performs a fast Fourier transform (FFT) on the frequency response spectrum. In addition, the system is capable of equalizing the amount of energy at each frequency. Equalization of the frequency spectrum, along with interpretation of the second FFT, aids in the evaluation of the fundamental frequency. The frequency responses from multilayered material samples, with and without known defects, were analyzed to assess the capabilities and limitations of this nondestructive evaluation technique for material characterization and defect detection. Amplitude and frequency changes were studied from ultrasonic responses of thick composite rings and a multiring composite rim. A composite ring varying in thickness was evaluated to investigate the full thickness resonance. The frequency response characteristics from naturally occurring voids in a composite ring were investigated. Ultrasonic responses were compared from regions with and without machined voids in a composite ring and a multiring composite rim. Finally, ultrasonic responses from the multiring composite rim were compared before and after proof spin testing to 63,000 rpm.

Harmon, Laura M.↗

On the Cloud Observations in JAXA's Next Coming Satellite Missions

The use of JAXA's next generation satellites, the EarthCARE and the GCOM-C, for observing overall cloud systems on the Earth is discussed. The satellites will be launched in the middle of 2010-era and contribute for observing aerosols and clouds in terms of climate change, environment, weather forecasting, and cloud revolution process study. This paper describes the role of such satellites and how to use the observing data showing concepts and some sample viewgraphs. Synergistic use of sensors is a key of the study. Visible to infrared bands are used for cloudy and clear discriminating from passively obtained satellite images. Cloud properties such as the cloud optical thickness, the effective particle radii, and the cloud top temperature will be retrieved from visible to infrared wavelengths of imagers. Additionally, we are going to combine cloud properties obtained from passive imagers and radar reflectivities obtained from an active radar in order to improve our understanding of cloud evolution process. This is one of the new techniques of satellite data analysis in terms of cloud sciences in the next decade. Since the climate change and cloud process study have mutual beneficial relationship, a multispectral wide-swath imagers like the GCOM-C SGLI and a comprehensive observation package of cloud and aerosol like the EarthCARE are both necessary.

satellite remote sensing↗

Novel Applications of Focused Ion Beam Technique for Planetary Sample Analyses

We are using innovative FIB techniques to prepare samples of planetary materials for different types of coordinated analyses using ion microprobes, synchrotron beamlines, and specialized transmission electron microscopy (TEM) techniques. In these cases, the FIB sample preparation is the critical step in enabling these specialized analyses. We discuss several examples below utilizing the FEI Quanta3D instrument at the NASA Johnson Space Center. Trace element analyses utilizing synchrotron x-ray fluorescence. The trace element content of mineral grains in comet dust provides important clues on their formation and processing in the early solar system. We preformed coordinated analyses of a comet dust particle that had been prepared using ultramicrotomy for TEM analysis. Following the TEM analyses, we extracted a 70 nm thick section from a region of the carbon (C) film of the TEM grid, for additional analyses. A carbon ring ~2-3 μm thick was deposited on top of the C film using the FIB. The C film on the outer rim of the ring was milled away using various patterns to uniformly release the stresses on the film, preventing rupture and collapse, and was attached to the micromanipulator needle. We then isolated the ring completely and transferred the section to a silicon sample holder for analysis using the HXN (hard X-ray nanoprobe) beamline at NSLSII at Brookhaven National Lab. Coordinated Analyses of Presolar Grains. Rare sub-m presolar grains that originate in evolved stars and supernovae, occur in primitive astromaterials and are identified by their exotic isotopic compositions. Coordinated analyses of these grains using NanoSIMS, TEM, and other techniques on the same grain is enabled by innovative FIB sample preparation. In order to obtain subsequent isotopic analyses of Mg and Fe, contributions from surrounding grains were minimized. We precisely deposited a protective cap of Pt on top of the grain to preserve the grain of interest and then milled away about 5 μm diameter of the surrounding material. Following the isotopic analyses, the spindle was extracted and thinned to electron transparency for TEM microstructural analyses. In situ heating TEM experiments on lunar samples. We extracted a FIB thin section from Apollo 17 lunar rock 76015. To avoid ion-beam damage, e-beam deposition was used to deposit the first 500 nm of the C strap, followed by ion beam-assisted deposition of ~3 μm carbon. We performed an ex situ lift-out of the section and placed the section on one of the elements of a microelectromechanical systems (MEMS) - specialized heating substrate and attached the section to the substrate by depositing small C straps with the FIB. The heating chips utilize silicon nitride windows to support the samples and provide uniform heating while enabling TEM imaging. The heating chip was loaded into a Hitachi “Blaze” heating holder and analyzed using a Hitachi HF5000 at the University of Arizona.

Rahman, Z.↗

40 Years of Processing Pieces of Space

This year marks the 40th year anniversary for the Antarctic Search for Meteorite (ANSMET) program. In 1976, the ANSMET program led the first expedition to Antarctica. The ANSMET program is a US-led field-based science project that recovers meteorite samples from Antarctica. Once a year from late November to late January, a field team consisting of 8 to 12 people, spends 6-8 weeks camping on the ice and collecting meteorites. Since 1976, more than 22,000 meteorite samples have been recovered. These meteorites come from asteroids, planets and other bodies of the solar system. Once collected, the Antarctic meteorites are shipped to NASA/Johnson Space Center (JSC) Houston, TX. in a refrigerated truck and are kept frozen to minimize oxidation until they are ready for initial processing. In Antarctica each meteorite is given a field tag which consists of numbers, once in the lab, this is replaced by an official tag, consisting of the Antarctic field location and year collected. The types and numbers of meteorites that have been classified include 849 carbonaceous chondrites, 135 enstatites, 512 achondrites, 64 stony, 115 irons, 48 others (27 R chondrites, 7 ungrouped), 6,161 H chondrites, 7,668 L chondrites, and 4,589 LL chondrites. Although 80-85 percent of the collected meteorites fall in the ordinary chondrite group, the other approximately 15 percent represent rare types of achondrites and carbonaceous chondrites. These rare meteorites include 25 lunar meteorites, 15 Martian meteorites, scores of various types of carbonaceous chondrites, and unique achondrites. The Antarctic meteorites that have been collected are processed in the Meteorite Processing Lab at JSC in Houston, TX. Initial processing of the meteorites begins with thawing/drying the meteorites in a nitrogen glove box for 24 to 48 hours. The meteorites are then photographed, measured, weighed and a description of the interior and exterior of each meteorite is written. The meteorite is broken and a representative sample, either a 1-3 gram chip or thin section is sent to the Smithsonian Institution for classification. After Antarctic meteorites have been classified and approved by the Nomenclature Committee of the Meteoritical Society, they are announced in the Antarctic Meteorite Newsletter, which is published twice per year (fall and spring) so that scientists may review which meteorites are available to study. Requests for Antarctic Meteorite samples are welcomed from research scientists, regardless of their current state of funding for meteorite studies. Since its inception over 3,300 requests have been made for pieces of these meteorites and over 400 investigators worldwide are active in the study of meteorites.. Research on these samples has been published in more than1500 peer reviewed articles; a listing of papers for any meteorite sample can be generated by accessing http://curator.jsc.nasa.gov/antmet/referencesearch.cfm. Antarctic meteorite samples requested by scientists are prepared several different ways. Most samples are prepared as chips, either using a rock splitter or using a chisel and chipping bowl. In special situations, a researcher may request a meteorite slab in which case the samples are cut using a diamond-bladed bandsaw inside of a dry nitrogen glove box. The meteorites are always cut in a 100 percent liquid-free environment. Additionally, thin/thick sections of Antarctic meteorites are also prepared at JSC. The meteorite thin section lab at JSC can prepare standard 30-micron thin sections, thick sections of variable thickness (100 to 200 microns), or demountable sections using superglue, all section are prepared without using water. Although many of the techniques used back in the '70's are still used today, advances in computers, software, databases, available tools and instrumentation have helped to streamline and shorten the duration of the classification process. In conjunction with present day missions to asteroids and other planets, meteorite studies have not only led to a better understanding of the complex histories of these bodies but have also tied certain meteorite groups to particular asteroid bodies. New meteorite discoveries by the ANSMET program provide a cost effective method for obtaining samples of previously unsampled bodies, allowing scientists to learn more about the origin, composition, and evolution of the solar system. Preservation in our cleanrooms at NASA allows material to be archived for future generations and advances in instrumentation and analysis.

Satterwhite, C. E.↗

First Results From Nb3Sn Coatings of 2.6 GHz Nb SRF Cavities Using DC Cylindrical Magnetron Sputtering System

A DC cylindrical magnetron sputtering system has been commissioned and operated to deposit Nb3Sn onto 2.6 GHz Nb SRF cavities. After optimizing the deposition conditions in a mock-up cavity, Nb-Sn films are deposited first on flat samples by multilayer sequential sputtering of Nb and Sn, and later annealed at 950 °C for 3 hours. X-ray diffraction of the films showed multiple peaks for the Nb3Sn phase and Nb (substrate). No peaks from any Nb- Sn compound other than Nb3Sn were detected. Later three 2.6 GHz Nb SRF cavities are coated with ~1 μm thick Nb3Sn. The first Nb3Sn coated cavity reached close to Eacc = 8 MV/m, demonstrating a quality factor Q0 of 3.2 × 108 at Tbath = 4.4 K and Eacc = 5 MV/m, about a factor of three higher than that of Nb at this temperature. Q0 was close to 1.1 × 109, dominated by the residual resistance, at 2 K and Eacc = 5 MV/m. The Nb3Sn coated cavities demonstrated Tc in the range of 17.9 – 18 K. Here we present the commissioning experience, s ystem optimization, and the first results from the Nb3Sn fabrication on flat samples and SRF cavities.

72 PHYSICS OF ELEMENTARY PARTICLES AND FIELDS↗

Strip-based Scintillation Detector for Dual-readout High-granularity Calorimetry

New calorimeter technology is being developed for future collider experiments. We are developing a calorimeter that integrates two technologies, a high-granularity calorimeter and a dual-readout calorimeter, and has high time resolution at a picosecond level. The proposed calorimeter is a sampling calorimeter based on scintillation and Cherenkov detectors with high-granularity readout. The Cherenkov detector has a picosecond level time resolution. For the high-granularity scintillation detector, scintillator strips of 300mm × 30mm ×3mm-thick are aligned horizontally and vertically to realize an effective 30mm-square-cell segmentation. Prototype strips with different designs and scintillator materials were tested to compare the performance.

46 INSTRUMENTATION RELATED TO NUCLEAR SCIENCE AND ↗

Editors’ Choice—Natural Convection Boundary Layer Thickness at Elevated Chloride Concentrations and Temperatures and the Effects on a Galvanic Couple

The natural convection boundary layer ( δ n c ) and its influence on cathodic current in a galvanic couple under varying electrolytes as a function of concentration (1 − 5.3 M NaCl) and temperature (25 °C−45 °C) were understood. Polarization scans were obtained under quiescent conditions and at defined boundary layer thicknesses using a rotating disk electrode on platinum and stainless steel 304L (SS304L); these were combined to determine δ n c . With increasing chloride concentration and temperature, δ n c decreased. Increased mass transport (Sherwood number) results in a decrease in δ n c , providing a means to predict this important boundary. Using Finite Element Modeling, the cathodic current was calculated for an aluminum alloy/SS304L galvanic couple as a function of water layer ( WL ) thickness and cathode length. Electrolyte domains were delineated, describing (i) dominance of ohmic resistance over mass transport under thin WL , (ii) the transition from thin film to bulk conditions at δ n c , and (iii) dominance of mass transport under thick WL . With increasing chloride concentration, cathodic current decreased due to decreases in mass transport. With increasing temperature, increased cathodic current was related to increases in mass transport and solution conductivity. This study has implications for sample sizing and corrosion prediction under changing environments.

25 ENERGY STORAGE↗

Low surface pressure models for Titan's atmosphere

The inversion model for the atmosphere of Titan is reviewed. The basic features of the model are: a cold surface (80 K), a warm stratosphere (160 K) and a low surface pressure (20 mbar). The model is consistent with all existing thermal infrared spectrophotometry, but it cannot preclude the existence of an opaque, cloud, thick atmosphere. The model excludes other gases than methane as bulk constituents. Radio wavelengths observations, including recent data from the very large array, are discussed. These long wavelength observations may be the only direct means of sampling the surface environment before an entry probe or flyby.

Caldwell, J.↗

Spatial conductivity measurements on high T(sub c) superconducting films

High T(sub c) superconducting thin and thick films have potential applications in future NASA flight projects. In anticipation of film use, the Materials Branch is developing a nondestructive, non-contact method of measuring the spatial variation of conductivity across a film sample. This method uses a computer-controlled, X-Y positioning table to scan a conventional eddy current probe across the surface of a film. The induced changes in impedance caused by variations in film conductivity are recorded during the scanning process. Ultimately the two-dimensional data set is displayed using imaging equipment on a personal computer.

Vansant, J. Timothy↗

Study of dust in the vicinity of Dione using the Voyager 1 plasma wave instrument

The flyby of Voyager 1 at Saturn yielded the detection of a large variety of plasma waves, for example, chorus, hiss, and electron cyclotron harmonics. Just before the outbound equator crossing, the Voyager 1 plasma wave instrument detected a strong, well-defined low-frequency enhancement in signal levels. Initially, it was thought that this enhancement was due to plasma waves, but more recently it was suggested that dust impacts might be at least partial contributors. In this report we present evidence that dust impacts are partly responsible for the low-frequency enhancement. A new method of analysis which relies mainly on the 16-channel spectrum analyzer has been used to derive the dust impact rate. The available wideband waveform observations (which have been used previously to study dust impacts) were useful for calibrating the impact rate from the spectrum analyzer data. The mass and hence size of the dust particles were also obtained by analyzing the response of the plasma wave spectrum and analyzer. The results show that the region sampled by Voyager 1 is populated by dust particles that have rms masses of up to a few times 10(exp -11) g and sizes of up to a few microns. The dust particle number density is of the order of 10(exp -3)/cu m. The optical depth of the region sampled by the spacecraft is approximately 10(exp -6). The particle population is centered at 2470 (+/- 150) km south of the equatorial plane and has a north-south FWHM (full-width, half-maximum) thickness of 4130 (+/- 450) km. The dust may be part of the E ring or a localized ringlet assoicated with Dione.

Tsintikidis, D.↗