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At least 1,189 records · Page 66

Thermal-vacuum testing and in-situ optical alignment measurements of the HALOE telescope/sun sensor assembly

Design features, test data and projected performance levels of the telescope/sun sensor assembly for the Halogen Occultation Experiment (HALOE) on board the Upper Atmosphere Research Satellite are described. HALOE will gather data on stratospheric chemical species with an IR telescope pointed through the atmosphere at the sun during occultation periods. The pointing accuracy will need to be 1 arcmin elevation and 1.6 arcmin azimuthal. Adjustments of the gimbaled instrument are guided by a sun sensor and its associated electronics. The components were subjected to thermal-vacuum, optical boresight stability tests and the data generated were compared with a finite element model of the telescope and sun sensor. The tests consisted of exposure to various thermal gradients while the telescope and sun sensor alignments were tracked by optical deflectometry. The thermal behavior was compared with predictions made with a finite difference model. Alignments were within tolerable ranges and the thermal behavior model was concluded valid for predicting the thermal behavior of orbiting instruments.

Foss, R. A.↗

Structural, Thermal, and Optical Performance (STOP) Modeling and Results for the James Webb Space Telescope Integrated Science Instrument Module

The James Webb Space Telescope includes the Integrated Science Instrument Module (ISIM) element that contains four science instruments (SI) including a Guider. We performed extensive structural, thermal, and optical performance(STOP) modeling in support of all phases of ISIM development. In this paper, we focus on modeling and results associated with test and verification. ISIMs test program is bound by ground environments, mostly notably the 1g and test chamber thermal environments. This paper describes STOP modeling used to predict ISIM system performance in 0g and at various on-orbit temperature environments. The predictions are used to project results obtained during testing to on-orbit performance.

structural↗

Measured dynamic aperture and detuning of nonlinear integrable optics

One of the most promising advantages of nonlinear integrable optics is strong amplitude dependent tune shift without degrading the dynamic aperture. The integrable optics test accelerator (IOTA) at Fermilab is constructed around nonlinear lattice elements of the elliptical type as described by Danilov and Nagaitsev. Detuning and dynamic aperture scans in IOTA were performed using a fast dipole kicker and a low emittance electron beam. The evolution of the dynamic aperture and detuning for different configurations of the integrable optics lattice are presented.

43 PARTICLE ACCELERATORS↗

Measured Dynamic Aperture and Detuning of Nonlinear Integrable Optics

One of the most promising advantages of nonlinear integrable optics is strong amplitude dependent tune shift without degrading the dynamic aperture. The integrable optics test accelerator (IOTA) at Fermilab is constructed around nonlinear lattice elements of the elliptical type as described by Danilov and Nagaitsev. Detuning and dynamic aperture scans in IOTA were performed using a fast dipole kicker and a low emittance electron beam. The evolution of the dynamic aperture and detuning for different configurations of the integrable optics lattice are presented.

43 PARTICLE ACCELERATORS↗

Experimental investigation of a simulated LOX injector flow field and other nonintrusive measurement efforts

Efforts to improve the characteristics of fuel-oxidizer mixing in liquid rocket combustors have lead to a swirl element design for a liquid oxygen injector which is being considered for use on the STME. For the design which is the subject of this investigation, the oxygen enters the injector element perpendicular to the injector axis and nearly tangent to the circular injector wall. This swirl element is at one end of a tube and the injector exit is at the other. This geometric configuration creates a plume in the shape of a conical sheet. This sheet is either primarily contiguous liquid or droplets depending on the pressure drop in the injector and the distance from the injector exit. Probe-based devices such as two-dimensional grid patternators have been used to investigate simulated LOX injector flow fields (Hulka). The primary work described herein is an effort to use optical techniques to investigate the plume of a swirl injector element. For this investigation, a high pressure (500 psig) cold flow test facility was constructed. Water was used as the LOX simulate and air pressure was used to drive the injector flow field. Laser-induced fluorescence (LIF) from dye seeded into the water was used to obtain quantitative measurements of the time-averaged water concentration distribution in the plume. Scattered laser light and LIF were used for time averaged plume visualization and scattered light from a strobe with a 1 microsecond pulse was used for time-resolved plume visualization. During the Summer Faculty Fellowship for which this report was developed, an additional effort, unrelated to the swirl injector investigation, was made to resolve fluctuations in the combustion product composition in the exhaust of a hybrid rocket motor. A brief description of this effort is included herein.

Hartfield, Roy J., Jr.↗

MHz free electron laser x-ray diffraction and modeling of pulsed laser heated diamond anvil cell

A new diamond anvil cell experimental approach has been implemented at the European x-ray Free Electron Laser, combining pulsed laser heating with MHz x-ray diffraction. In this report we use this setup to determine liquidus temperatures under extreme conditions, based on the determination of time-resolved crystallization. The focus is on a Fe-Si-O ternary system, relevant for planetary cores. This time-resolved diagnostic is complemented by a finite-element model, reproducing temporal temperature profiles measured experimentally using streaked optical pyrometry. This model calculates the temperature and strain fields by including (i) pressure and temperature dependencies of material properties, and (ii) the heat-induced thermal stress, including feedback effect on material parameter variations. Making our model more realistic, these improvements are critical as they give 7000 K temperature differences compared to previous models. Laser intensities are determined by seeking minimal deviation between measured and modeled temperatures. Combining models and streak optical pyrometry data extends temperature determination below detection limit. The presented approach can be used to infer the liquidus temperature by the appearance of SiO 2 diffraction spots. In addition, temperatures obtained by the model agree with crystallization temperatures reported for Fe–Si alloys. Our model reproduces the planetary relevant experimental conditions, providing temperature, pressure, and volume conditions. Those predictions are then used to determine liquidus temperatures at experimental timescales where chemical migration is limited. This synergy of novel time-resolved experiments and finite-element modeling pushes further the interpretation capabilities in diamond anvil cell experiments.

36 MATERIALS SCIENCE↗

Structural considerations for fabrication and mounting of the AXAF HRMA optics

A methodology is described which minimizes optics distortion in the fabrication, metrology, and launch configuration phases. The significance of finite element modeling and breadboard testing is described with respect to performance analyses of support structures and material effects in NASA's AXAF X-ray optics. The paper outlines the requirements for AXAF performance, optical fabrication, metrology, and glass support fixtures, as well as the specifications for mirror sensitivity and the high-resolution mirror assembly. Analytical modeling of the tools is shown to coincide with grinding and polishing experiments, and is useful for designing large-area polishing and grinding tools. Metrological subcomponents that have undergone initial testing show evidence of meeting force requirements.

Cohen, Lester M.↗

Optical-Input, Optical-Output Morphological Processor

Some advantages of optical and electronic processing combined. Proposed optical-input/optical-output morphological processor is optoelectronic assembly performing some binary operations on picture elements of binary input image, yielding processed binary output image. Number of such processors cascaded to form more complicated image-processing system. Use of optics as connection medium makes rate of processing faster than in all-electronic system designed to perform same overall processing functions. At the same time, use of electronics as processing medium provides flexibility of reconfiguration not available in all-optical system.

Yu, Jeffrey W.↗

Intercontinental Bistatic Radar Test Observation of Asteroid 1998 WT24

We describe the first intercontinental planetary radar test performed in Italy observing the near Earth asteroid (NEA) 33342 (1998 WT24) in December 2001 by means of the bistatic configurations Goldstone (California, USA)-Medicina (Italy) and Evpatoria (Ukraine)-Medicina. The experiment goal was to characterize the system for realtime radar follow-up observations of NEAs and artificial orbiting debris, in the framework of a feasibility study which aims at using the Sardinia Radio Telescope, at present under construction, also as a planetary radar facility. We report the preliminary results of the radar observations carried out by the IRA-CNR (Instituto di Radioastronomia - Consiglio Nazionale delle Ricerche) and the OATo (Osservatorio Astronomico di Torino) groups, aimed at exploring the scientific potentials of a new space radar program, using the existing facilities in Italy. The planetary radar technique is uniquely capable of investigating geometry and surface properties of various solar system objects, demonstrating advantages over the optical methods in its high spatial resolution and ability to obtain three-dimensional images. A single radar detection allows to obtain extremely accurate orbital elements, improving the instantaneous positional uncertainties by orders of magnitude with respect to an optically determined orbit. Radar is a powerful means to spatially resolve NEAs by measuring the distribution of the echo power in time delay (range) and Doppler frequency (line-of-sight velocity) with extreme precision in each coordinate, as it provides detailed information about the target physical properties like size, shape, rotation, near-surface bulk density and roughness and internal density distribution. The Medicina 32m antenna had been successfully used for the first time as the receiving part of a bistatic configuration during a test experiment (September 2001) held to check the capabilities of the entire data acquisition system. This test was possible thanks to the collaboration undertaken with the Evpatoria radar station, and consisted in the observation of the ETALON-1 low orbit satellite

Righini, S.↗

The composite classification problem in optical information processing

Optical pattern recognition allows objects to be recognized from their images and permits their positional parameters to be estimated accurately in real time. The guiding principle behind optical pattern recognition is that a lens focusing a beam of coherent light modulated with an image produces the two-dimensinal Fourier transform of that image. When the resulting output is further transformed by the matched filter corresponding to the original image, one obtains the autocorrelation function of the original image, which has a peak at the origin. Such a device is called an optical correlator and may be used to recognize the locate the image for which it is designed. (From a practical perspective, an approximation to the matched filter must be used since the spatial light modulator (SLM) on which the filter is implemented usually does not allow one to independently control both the magnitude and phase of the filter.) Generally, one is not just concerned with recognizing a single image but is interested in recognizing a variety of rotated and scaled views of a particular image. In order to recognize these different views using an optical correlator, one may select a subset of these views (whose elements are called training images) and then use a composite filter that is designed to produce a correlation peak for each training image. Presumably, these peaks should be sharp and easily distinguishable from the surrounding correlation plane values. In this report we consider two areas of research regarding composite optical correlators. First, we consider the question of how best to choose the training images that are used to design the composite filter. With regard to quantity, the number of training images should be large enough to adequately represent all possible views of the targeted object yet small enough to ensure that the resolution of the filter is not exhausted. As for the images themselves, they should be distinct enough to avoid numerical difficulties yet similar enough to avoid gaps in which certain views of the target will be unrecognized. One method that we introduce to study this problem is called probing and involves the creation of the artificial imagery. The second problem we consider involves the clasification of the composite filter's correlation plane data. In particular, we would like to determine not only whether or not we are viewing a training image, but, in the former case, we would like to determine which training image is being viewed. This second problem is investigated using traditional M-ary hypothesis testing techniques.

Hall, Eric B.↗

Innovative recycling of high purity silver from silicon solar cells by acid leaching and ultrasonication

Precious and scarce silver (Ag) is used as a front electrical contact in silicon solar panels. With massive amounts of solar panel waste coming to end-of-life, it is imperative to recover all the Ag from these modules. In this paper, we propose a novel method to easily reclaim Ag from end-of-life silicon solar cells using low concentration sulfuric acid (H 2 SO 4 ) leaching followed by ultrasonication. Our process simplifies the Ag recycling procedure by directly recovering the Ag contacts from solar cells, eliminating the need for secondary precipitation/electrodeposition. First, scanning electron microscopy (SEM) with energy dispersive X-ray spectroscopy (EDX) and X-ray photoelectron spectroscopy (XPS) was used to study the leaching and ultrasonication process on rejected solar wafers. Next, a solar panel from landfill was heated in a furnace to burn off the polymer encapsulant. The silicon wafers were then collected from the burning process and leached in 2 M H 2 SO 4 at two different shaking speeds for 48 hours at room temperature. Finally, the end-of-life silicon wafer pieces were collected, sonicated in water, and then the sonication water was centrifuged to show a proof-of-concept to recover the Ag contacts. Inductively coupled plasma optical emission spectroscopy (ICPOES) is used to monitor dissolved elements in the leachate as a function of time and shaking speed. XPS is used to evaluate the composition of the silicon cell wafer surface before and after H 2 SO 4 leaching. SEM is used to image the recovered Ag contacts morphology and EDX confirms the recovered particles contain high amounts of Ag. Furthermore, a proposed schematic illustrates the authors’ hypothesis for the peeling mechanism.

14 SOLAR ENERGY↗

Laser glazing of cold sprayed coatings for the mitigation of stress corrosion cracking in light water reactor (LWR) applications

The effect of laser power, traverse speed, and cold spray coating thickness were examined with the goal of mitigating and repairing stress corrosion cracking (SCC) in light water reactor (LWR) environment. For this purpose, SCC-susceptible Alloy 600 substrate material was coated with SCC-resistant Alloy 690 via the cold spray technique. The cold spray coated substrate was then laser-glazed using various laser parameters. Single pass and multiple pass laser glazed regions were created to determine the effects. For this purpose, the area of the fusion zone, depth of the fusion zone, and elemental composition of the cross section were examined by optical microscopy, scanning electron microscopy, and energy dispersive spectroscopy. Additionally, it was shown that chromium dilution from the laser glazed region into the substrate is not a significant factor in laser glazed cold spray coated samples. Separate laser glazed samples were subjected to ASTM 633C to determine coating adhesion. Finally, by using interrupted SCC crack growth rate tests, it was shown that low traverse speeds and high laser powers produce deep fusion zones within the cold sprayed coating and substrate that can be used to seal pre-existing cracks, thus stopping SCC growth.

36 MATERIALS SCIENCE↗

Heat affected zone liquation cracking evaluation on FeMnAl alloys

FeMnAl steels are currently generating a lot of interest with potential applications for structural parts in armored vehicles due to their lower density and outstanding mechanical properties. Despite the extensive mechanical performance and heat treatment exploration of this alloy class, further weldability investigation is required for future large-scale deployment. In the present study, the liquation cracking of four heats of cast FeMnAl alloys was investigated by the spot-Varestraint technique. The study focuses primarily on the effect of the major elements of the FeMnAl system: C, Mn and Al. Optical and electron microscopy were employed to investigate the microstructural features, and CALPHAD was employed to aid the discussion regarding the alloy’s composition differences and their effect on the liquation cracking susceptibility. The study was able to identify that compositions with the higher Mn, C, and lower Al presented the highest liquation cracking susceptibility. Conversely, composition presenting lower Mn, C, and Al showed the most resistant behavior. Furthermore, lower Al content promoted a fully-γ microstructure at low temperatures, which encouraged the appearance of longer cracks as a γ-matrix is more susceptible to HAZ cracking than a fully ferritic (α) or duplex (α + γ) microstructure.

36 MATERIALS SCIENCE↗

Effects of head modeling errors on the spatial frequency representation of MEG

Abstract Objectives. We aim to investigate the effects of head model inaccuracies on signal and source reconstruction accuracies for various sensor array distances to the head. This allows for the assessment of the importance of head modeling for next-generation magnetoencephalography (MEG) sensors, optically-pumped magnetometers (OPM). Approach. A 1-shell boundary element method (BEM) spherical head model with 642 vertices of radius 9 cm and conductivity of 0.33 S m −1 was defined. The vertices were then randomly perturbed radially up to 2%, 4%, 6%, 8% and 10% of the radius. For each head perturbation case, the forward signal was calculated for dipolar sources located at 2 cm, 4 cm, 6 cm and 8 cm from the origin (center of the sphere), and for a 324 sensor array located at 10 cm to 15 cm from the origin. Equivalent current dipole (ECD) source localization was performed for each of these forward signals. The signal for each perturbed spherical head case was then analyzed in the spatial frequency domain, and the signal and ECD errors were quantified relative to the unperturbed case. Main results. In the noiseless and high signal-to-noise ratio (SNR) case of approximately ≥6 dB, inaccuracies in our spherical BEM head conductor models lead to increased signal and ECD inaccuracies when sensor arrays are placed closer to the head. This is true especially in the case of deep and superficial sources. In the noisy case however, the higher SNR for closer sensor arrays allows for an improved ECD fit and outweighs the effects of head geometry inaccuracies. Significance. OPMs may be placed directly on the head, as opposed to the more commonly used superconducting quantum interference device sensors which must be placed a few centimeters away from the head. OPMs thus allow for signals of higher spatial resolution to be captured, resulting in potentially more accurate source localizations. Our results suggest that an increased emphasis on accurate head modeling for OPMs may be necessary to fully realize its improved source localization potential.

Yeo, Wan-Jin (ORCID:0000000241417123)↗

Parallel Broadband Femtosecond Reflection Spectroscopy at a Soft X-Ray Free-Electron Laser

X-ray absorption spectroscopy (XAS) and the directly linked X-ray reflectivity near absorption edges yield a wealth of specific information on the electronic structure around the resonantly addressed element. Observing the dynamic response of complex materials to optical excitations in pump–probe experiments requires high sensitivity to small changes in the spectra which in turn necessitates the brilliance of free electron laser (FEL) pulses. However, due to the fluctuating spectral content of pulses generated by self-amplified spontaneous emission (SASE), FEL experiments often struggle to reach the full sensitivity and time-resolution that FELs can in principle enable. Here, we implement a setup which solves two common challenges in this type of spectroscopy using FELs: First, we achieve a high spectral resolution by using a spectrometer downstream of the sample instead of a monochromator upstream of the sample. Thus, the full FEL bandwidth contributes to the measurement at the same time, and the FEL pulse duration is not elongated by a monochromator. Second, the FEL beam is divided into identical copies by a transmission grating beam splitter so that two spectra from separate spots on the sample (or from the sample and known reference) can be recorded in-parallel with the same spectrometer, enabling a spectrally resolved intensity normalization of pulse fluctuations in pump–probe scenarios. We analyze the capabilities of this setup around the oxygen K- and nickel L-edges recorded with third harmonic radiation of the free electron laser in Hamburg (FLASH), demonstrating the capability for pump–probe measurements with sensitivity to reflectivity changes on the per mill level.

36 MATERIALS SCIENCE↗

Selected Area Deposition of High Purity Gold for Functional 3D Architectures

Selected area deposition of high purity gold films onto nanoscale 3D architectures is highly desirable as gold is conductive, inert, plasmonically active, and can be functionalized with thiol chemistries, which are useful in many biological applications. Here, we show that high-purity gold coatings can be selectively grown with the Me 2 Au (acac) precursor onto nanoscale 3D architectures via a pulsed laser pyrolytic chemical vapor deposition process. The selected area of deposition is achieved due to the high thermal resistance of the nanoscale geometries. Focused electron beam induced deposits (FEBID) and carbon nanofibers are functionalized with gold coatings, and we demonstrate the effects that laser irradiance, pulse width, and precursor pressure have on the growth rate. Furthermore, we demonstrate selected area deposition with a feature-targeting resolutions of ~100 and 5 µm, using diode lasers coupled to a multimode (915 nm) and single mode (785 nm) fiber optic, respectively. The experimental results are rationalized via finite element thermal modeling.

3-dimensional nanostructures↗