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At least 1,189 records · Page 66

Linear and nonlinear viscoelasticity of concentrated thermoresponsive microgel suspensions

We present an integrated experimental and theoretical study of the dynamics and rheology of self-crosslinked, slightly charged, temperature responsive soft poly(N-isopropylacrylamide) (pNIPAM) microgels over a wide range of concentration and temperature spanning the sharp change in particle size and intermolecular interactions across the lower critical solution temperature (LCST). Dramatic, non-monotonic changes in viscoelasticity are observed as a function of temperature, with distinct concentration dependence in the dense fluid, glassy, and soft-jammed regimes. Motivated by our experimental observations, we formulate a minimalistic model for the size dependence of a single microgel particle and the change of the interparticle interaction from purely repulsive to attractive upon heating. Using microscopic equilibrium and time-dependent statistical mechanical theories, theoretical predictions are quantitatively compared with experimental measurements of the shear modulus. Good agreement is found for the nonmonotonic temperature behavior that originates as a consequence of the competition between reduced microgel packing fraction and increasing interparticle attractions. Furthermore, testable predictions are made for nonlinear rheological properties such as the yield stress and strain. To our knowledge, this is the first attempt to quantitatively understand in a unified manner the viscoelasticity of dense, temperature-responsive microgel suspensions spanning a wide range of temperatures and concentrations.

42 ENGINEERING↗

Machine learning with knowledge constraints for process optimization of open-air perovskite solar cell manufacturing

Perovskite photovoltaics (PV) have achieved rapid development in the past decade in terms of power conversion efficiency of small-area lab-scale devices; however, successful commercialization still requires further development of low-cost, scalable, and high-throughput manufacturing techniques. One of the critical challenges of developing a new fabrication technique is the high-dimensional parameter space for optimization, but machine learning (ML) can readily be used to accelerate perovskite PV scaling. Herein, we present an ML-guided framework of sequential learning for manufacturing process optimization. We apply our methodology to the Rapid Spray Plasma Processing (RSPP) technique for perovskite thin films in ambient conditions. With a limited experimental budget of screening 100 process conditions, we demonstrated an efficiency improvement to 18.5% as the best-in-our-lab device fabricated by RSPP, and we also experimentally found 10 unique process conditions to produce the top-performing devices of more than 17% efficiency, which is 5 times higher rate of success than the control experiments with pseudo-random Latin hypercube sampling. Our model is enabled by three innovations: (a) flexible knowledge transfer between experimental processes by incorporating data from prior experimental data as a probabilistic constraint; (b) incorporation of both subjective human observations and ML insights when selecting next experiments; (c) adaptive strategy of locating the region of interest using Bayesian optimization first, and then conducting local exploration for high-efficiency devices. Furthermore, in virtual benchmarking, our framework achieves faster improvements with limited experimental budgets than traditional design-of-experiments methods (e.g., one-variable-at-a-time sampling). This framework shows the capability of incorporating researchers’ domain knowledge into the ML-guided optimization loop; therefore, it has the potential to facilitate the wider adoption of ML in scaling to perovskite PV manufacturing.

14 SOLAR ENERGY↗

National Security Research Center

Born out of a need to make LANL Weapons Program archival material available to scientists and engineers. Material is the result of decades of consolidation of mini-libraries and mini archives at LANL. Latest consolidation brought together LANL’s digital archives and physical archives. Houses 75+ years of nuclear weapons research, designs, procedures, videos, photos, and other reports.

96 KNOWLEDGE MANAGEMENT AND PRESERVATION↗

The Mars Hopper: Development, Simulation and Experimental Validation of a Radioisotope Exploration Probe for the Martian Surface

An advanced exploration probe has been proposed by the Center for Space Nuclear Research (CSNR) to acquire detailed data from the Martian surface and subsurface, ‘hop’ large distances to multiple sites in short periods of time and perform this task repeatedly. Although several similar flying vehicles have been proposed utilizing various power sources and complex designs, e.g. solar-electric and chemical-based, the CSNR’s Mars Hopper is based on a radioisotope thermal rocket (RTR) concept. The Mars Hopper’s design relies on the high specific energies [J/kg] of radioisotopes and enhances their low specific power [W/kg] through the use of a thermal capacitance material to store thermal energy over time. During operation, the RTR transfers the stored thermal energy to a flowing gas, which is then expanded through a converging-diverging nozzle, producing thrust. Between flights, the platform will have ample time to perform in-depth science at each location while the propellant tanks and thermal capacitor recharge. Recharging the propellant tanks is accomplished by sublimation freezing of the ambient CO2 atmosphere with a cryocooler, followed by heating and pressurization to yield a liquid storage state. The proposed Mars Hopper will undergo a ballistic flight, consuming the propellant in both ascent and descent, and by using multiple hopper platforms, information can be gathered on a global scale, enabling better resource resolution and providing valuable information for a possible Mars sample-return mission. The CSNR, collaborating with the Idaho National Laboratory (INL) and three universities (University of Idaho, Utah State University and Oregon State University), has identified key components and sub-systems necessary for the proposed hopper. Current project activities include the development of a lab-scale prototypic Mars Hopper and test facility, along with computational fluid dynamics (CFD)/thermal-hydraulic models to yield a better understanding of the heat transfer process and complex nature of turbulent CO2 flow. Laboratory experimentation will aid design iterations and the development of both tethered and free-flying terrestrial hoppers that utilize an electrically heated core. The knowledge base acquired from these activities will refine the Mars Hopper’s future performance and optimize the RTR core components prior to constructing the final design.

33 ADVANCED PROPULSION SYSTEMS↗

Canada's Underground Research Laboratory (1980-2014) - 16274

In 1980, Canada initiated a long-term, comprehensive research and development program of geologic characterization and large-scale in situ geotechnical experiments in a subsurface facility, the Underground Research Laboratory (URL). The URL was excavated specifically to evaluate the concept of permanent disposal of used CANDU{sup R} nuclear reactor fuel in a deep geological repository (DGR) constructed in Canadian Shield granite. Key phases of the URL included siting, detailed site characterization and monitoring, construction, operation, decommissioning, and closure. Much collaborative research with international organizations was undertaken at the URL and continues, even after the closure of the facility, through the ongoing Enhanced Sealing Project (ESP). The ESP monitors the engineered performance of a full-scale composite shaft seal that was emplaced during URL closure to permanently seal the main URL access shaft across a sub-horizontal hydraulically active fracture zone. Currently the ESP is jointly funded by Canadian Nuclear Laboratories (CNL) (Canada), Posiva (Finland), and Andra (France), and monitoring is planned to continue until the end of 2016. Decades of programmatic experience at the URL have shown that knowledge continuity is integral to supporting the development of a safe geological disposal facility for high level nuclear waste. This paper outlines the history of the URL and describes some technical lessons learned from its 30-plus years of construction, operation, and closure activities. (authors)

12 MANAGEMENT OF RADIOACTIVE AND NON-RADIOACTIVE W↗

The role of peer review and science for advancing public understanding

We live in a time of rapid change. The Covid-19 pandemic has united the world to understand and develop solutions to protect the health and wellbeing of society. At the same time, access to information on the internet and social media has exploded. People are exposed to information with many claims. Some of the information is relevant and accurate. A significant fraction may be inaccurate, biased, and potentially dangerous. With Covid-19, the information might point to cures that are toxic or risks that are not relevant. The scientific community has developed a process to develop and convey knowledge. The validation of results and their interpretation is critical to advancing knowledge. The core of the scientific process is based on developing a hypothesis-driven concept, designing and executing an experimental approach to prove or disprove the hypothesis, conducting a statistical analysis of the results to confirm their validity, and interpreting their meaning and impact. When their work is completed the scientist prepares to publish the work. Publication requires peer review. Hypotheses, experimental approaches, results, and interpretation of results are independently and anonymously reviewed by a scientific peer. The reviewers are selected based on their expertise in the field. The peer review process is essential for the integrity of the scientific process. Without a robust scientific process, society cannot discriminate between validated results and interpretations and biased, inaccurate, and potentially dangerous conjecture. With inaccurate science society and policy makers may make poor decisions that could hurt people and the world around them. While scientists should not censor information available to the public, scientists have a responsibility to inform the public. We must articulate what the scientific process is and why it is essential when considering the validity of information. Scientist are responsible for pointing out when public information has not been vetted through a scientific process and therefore cannot be considered conclusive. Scientists are responsible for highlighting information that has been generated and vetted with the scientific process. Over time, our goal is for the public to value the scientific process based on peer review. The public could become enlightened to the necessity for peer review to support decisions and action. Scientists need to contribute to advancing public knowledge. When invited to serve as a peer reviewer, scientists have a responsibility to contribute to the process. We all are extremely busy making peer review a distraction. While peer review does not directly benefit our own work and career, it benefits our chosen field of science. This is very important for the research area that our journal, Water-Energy Nexus, is focusing on. We cover the convergence of science and technology integrating across large spatial ranges (micro to global) in environmental pollution and the balance of remediation issues with energy use. Water-Energy Nexus wants to provide scientists with a platform for scientific debate and discussion on this rich and complicated topic. With the manuscripts submitted to WEN cover integrated research topics across a broad range of subjects from environment sciences through energy engineering, the role of peer review is essential. Peer review on a new submission to WEN should not be biased towards a specific science field. It should be done considering the complex nature of issues in the water-energy nexus. Scientists need to contribute to the public dialog. To accomplish these goals, we need to be honest, accurate, articulate, and use understandable language. The impact of WEN is very diverse affecting society in many ways. The scientific audience for WEN is diverse and readers may not fully understand the content of the papers outside their research expertise. Therefore, scientists, especially those who want to contribute to WEN, should work with communications specialists to convey message to benefit society. The audience includes the general public and researchers outside the author’s core specialty. While the peer-reviewed journal article is the cornerstone of our careers and critical for advancing scientific knowledge, a general interest story could benefit society even more. The author cannot lose sight that our work has two audiences, the science community, and more importantly, our family, friends, neighbors, and policy makers.

54 ENVIRONMENTAL SCIENCES↗

High pressure shock tube ignition delay time measurements during oxy-methane combustion with high levels of CO 2 dilution

For this study, ignition delay times and methane species time-histories were measured for methane/O 2 mixtures in a high CO 2 diluted environment using shock tube and laser absorption spectroscopy. The experiments were performed between 1300 K and 2000 K at pressures between 6 and 31 atm. The test mixtures were at an equivalence ratio of 1 with CH 4 mole fractions ranging from 3.5% -5% and up to 85% CO 2 with a bath of argon gas as necessary. The ignition delay times and methane time histories were measured using pressure, emission, and laser diagnostics. Predictive ability of two literature kinetic mechanisms (GRI 3.0 and ARAMCO Mech 1.3) was tested against current data. In general, both mechanisms performed reasonably well against measured ignition delay time data. The methane time-histories showed good agreement with the mechanisms for most of the conditions measured. A correlation for ignition delay time was created taking into the different parameters showing that the ignition activation energy for the fuel to be 49.64 kcal/mol. Through a sensitivity analysis, CO 2 is shown to slow the overall reaction rate and increase the ignition delay time. To the best of our knowledge, we present the first shock tube data during ignition of methane/CO 2 /O 2 under these conditions. In conclusion, current data provides crucial validation data needed for development of future kinetic mechanisms.

42 ENGINEERING↗

Integrated dispersion compensated mode-locked quantum dot laser

Quantum dot lasers are excellent on-chip light sources, offering high defect tolerance, low threshold, low temperature variation, and high feedback insensitivity. Yet a monolithic integration technique combining epitaxial quantum dot lasers with passive waveguides has not been demonstrated and is needed for complex photonic integrated circuits. We present here, for the first time to our knowledge, a monolithc offset quantum dot integration platform that permits formation of a laser cavity utilizing both the robust quantum dot active region and the versatility of passive GaAs waveguide structures. This platform is substrate agnostic and therefore compatible with the quantum dot lasers directly grown on Si. As an illustration of the potential of this platform, we designed and fabricated a 20 GHz mode-locked laser with a dispersion-engineered on-chip waveguide mirror. Due to the dispersion compensation effect of the waveguide mirror, the pulse width of the mode-locked laser is reduced by a factor of 2.8.

Zhang, Zeyu (ORCID:0000000271576272)↗

Autonomous Radiation Cartographer (ARC) System Training Manual

This training manual is designed to provide end users with a comprehensive knowledge base for the safe and effective use of the Autonomous Radiation Cartographer (ARC) System. The ARC is a fully autonomous radiation detection robot based on the Spot Robot platform manufactured by Boston Dynamics.

42 ENGINEERING↗

Enterprise: Exploration of Concepts, Perspectives and Implications for Systems Engineering

The purpose of this paper is to explore the concept of ‘enterprise’ in the context of Systems Engineering (SE). The term ‘enterprise’ has been used extensively to generally describe large complex entities that have an extensive scope of operations. However, a deeper examination of ‘enterprise’ significance for SE can provide insights as our challenges continue with increasingly complex, uncertain, ambiguous, and integrated entities struggling to thrive in the future. The paper explores three central topics. First, the concept of enterprise is introduced as a central aspect of the future focus for SE, as recognized in the INCOSE SE Vision 2035. Second, a more detailed examination of the enterprise concept is developed in relationship to SE. The thrust of this examination is to understand the nature and role of ‘enterprise’ across a broad spectrum of literature and knowledge, ultimately providing a more informed perspective of enterprise for SE. As part of this exploration, a bibliometric analysis of the term ‘enterprise’ is performed. This exploration extracts key themes (clusters) in the ‘enterprise’ literature. Third, challenges for further development and inculcation of ‘enterprise’ within the SE discipline and support for realization of the SE 2035 Vision are suggested. These challenges point out the need to ‘think differently’ about ‘enterprise’ within the SE context. ‘Enterprise’ is proposed as a central, albeit different, perspective for the SE discipline. Finally, the paper closes with a first–generation perspective for ‘enterprise’ in pursuit of the SE Vision 2035.

42 ENGINEERING↗

An Educational Program on Concentrated Solar Power and Heliostats for Power Generation and Industrial Processes

The objective of this project was to design and implement a comprehensive educational and applied research program in Concentrated Solar Thermal Power (CSTP) and heliostat technologies at Northeastern University. In alignment with the U.S. Department of Energy's Heliostat Consortium (HelioCon) goals, the project aimed to expand student and public understanding of CSTP systems while simultaneously contributing to workforce development and the broader decarbonization strategy. A particular emphasis was placed on integrating hands-on student design projects and publicly disseminating educational content relevant to CSTP systems. The project addressed a critical gap in renewable energy education: CSTP and heliostats, despite their importance in utility-scale solar energy, are rarely included in standard mechanical engineering programs. This project established new pathways for students to engage with the topic through the creation of a 4-credit graduate/senior elective course, development of five industry-facing short courses, and the inclusion of CSTP-based capstone design projects. Over two academic years, 36 students across six senior design teams developed and tested technologies such as deformable heliostats, beacon-based tracking systems, and solar-powered pyrolizers for biomass-to-biochar conversion. Concurrently, 30 undergraduate and graduate students were enrolled in the new academic course centered around CSTP principles. To ensure the relevance and accessibility of the short course content, the project team engaged with industry professionals, technical policy stakeholders, and potential course participants through structured surveys and informal consultations. Feedback from 28 respondents guided the structure, length, and delivery format of the courses - resulting in a modular design broken into five workshops. The feedback emphasized the need for flexible, asynchronous delivery and practical case studies, particularly in areas such as heliostat control, thermal storage, and solar fuel production. This engagement helped align the courses with the evolving knowledge demands of the renewable energy workforce and ensured that participants from both technical and policy backgrounds could meaningfully benefit from the material. The research and educational activities advanced the understanding of heliostat control systems, optical performance under misalignment, and thermal system integration in solar-driven pyrolysis applications. Methods and designs explored in this project proved to be both technically effective and economically feasible at the lab scale. Prototypes were constructed using commercially available components and custom-fabricated elements, demonstrating that meaningful performance improvements can be achieved with modest material and fabrication costs, supporting the feasibility of student-led research in this field. The public benefit of this project is twofold. First, it cultivates a pipeline of engineers trained to be familiar with CSTP principles, an essential workforce need identified by the Department of Energy for achieving its 2030 cost and deployment targets. Second, it contributes openly accessible educational materials, course content, and experimental frameworks to the broader community, enabling other institutions to adopt or adapt similar programming. Through outreach activities, curriculum integration, and technical exposure, this project contributes to a more informed and capable renewable energy workforce while supporting innovation in heliostat and CSTP system design. A new technical report is being prepared to document the development of the course and its outcomes, with plans to publish it in the ASME Open Access Journal of Engineering to ensure global accessibility, free of cost.

14 SOLAR ENERGY↗

A Hybrid Biological-Organic Photochemical Half-Cell for Generating Dihydrogen

In this final report we describe our work on the fabrication of a hybrid biological/organic photochemical half-cell that couples Photosystem I, which produces electrons at a highly reducing redox potential, with a hydrogenase enzyme, which catalyzes H 2 evolution at high rates when provided with a source of electrons. We considered it far too ambitious at the present stage of knowledge to attempt to design a system that carries out the reaction 2H 2 O + 8hv → 2H 2 + O 2 in a single photochemical step, hence, we focused our work on optimizing the half-cell reaction 2H + + 2e - + 2hv → H 2 . The challenge has been to deliver low-potential electrons from PS I to H 2 ase rapidly, at high quantum yield, and with high thermodynamic efficiency. To accomplish this, we engineered a molecular wire that connects the [4Fe-4S] clusters of PS I with those of the hydrogenase enzyme. In doing so, the highly reducing electrons generated by PS I are transferred by quantum mechanical tunneling to the enzyme. The core idea was to connect the terminal Fe/S cluster of Photosystem I to the distal Fe/S cluster of H 2 ase through a covalently bonded “molecular wire” consisting of an 8-carbon hydrocarbon wire terminated on both ends with a sulfhydryl group. By providing a direct electron transfer pathway through signa bonds, diffusion chemistry is avoided, and, because the tether length and redox potentials were properly chosen, a rate of electron transfer between the two enzymes was achieved that twice exceeded the rate of electron transfer in natural photosynthesis. We also devised a way to utilize the FA and FB clusters of Photosystem I to serve as a reservoir so that electrons could be extracted from the quinone binding sites and passed through a similar molecular wire to the bound hydrogenase. The additional induction of the IsiA antenna pigments by iron starvation led to an optical cross section twice that of the naturally-occurring Photosystem I, thus further raising the rates of electron transfer to the enzyme. We were likewise able to re-engineer a naturally-occurring dicluster ferredoxin to replace the hydrocarbon molecular wire as the tether between Photosystem I and the hydrogenase enzyme. Finally, we developed techniques to place Photosystem I on electrodes and in block copolymer interfaces and we were able to measure photocurrents approaching 35.0 ± 3.5 mA cm -2 upon illumination of these assembled devices, which are among the highest reported so far for such systems on a per protein basis.

14 SOLAR ENERGY↗

Development of a Kalman filter estimator for simulation and control of particulate matter distribution of a diesel catalyzed particulate filter

The knowledge of the temperature and particulate matter mass distribution is essential for monitoring the performance and durability of a catalyzed particulate filter. A catalyzed particulate filter model was developed, and it showed capability to accurately predict temperature and particulate matter mass distribution and pressure drop across the catalyzed particulate filter. However, the high-fidelity model is computationally demanding. Therefore, a reduced order multi-zone particulate filter model was developed to reduce computational complexity with an acceptable level of accuracy. In order to develop a reduced order model, a parametric study was carried out to determine the number of zones necessary for aftertreatment control applications. The catalyzed particulate filter model was further reduced by carrying out a sensitivity study of the selected model assumptions. The reduced order multi-zone particulate filter model with 5 × 5 zones was selected to develop a catalyzed particulate filter state estimator considering its computational time and accuracy. Next, a Kalman filter–based catalyzed particulate filter estimator was developed to estimate unknown states of the catalyzed particulate filter such as temperature and particulate matter mass distribution and pressure drop (Δ P) using the sensor inputs to the engine electronic control unit and the reduced order multi-zone particulate filter model. A diesel oxidation catalyst estimator was also integrated with the catalyzed particulate filter estimator in order to provide estimates of diesel oxidation catalyst outlet concentrations of NO 2 and hydrocarbons and inlet temperature for the catalyzed particulate filter estimator. The combined diesel oxidation catalyst–catalyzed particulate filter estimator was validated for an active regeneration experiment. The validation results for catalyzed particulate filter temperature distribution showed that the root mean square temperature error by using the diesel oxidation catalyst–catalyzed particulate filter estimator is within 3.2 °C compared to the experimental data. Similarly, the Δ P estimator closely simulated the measured total Δ P and the estimated cake pressure drop error is within 0.2 kPa compared to the high-fidelity catalyzed particulate filter model.

Engineering↗

Inter-well connectivity detection in CO 2 WAG projects using statistical recurrent unit models

Routine well-wise injection and production measurements contain significant information on subsurface structure and properties. Data-driven technology that interprets surface data into subsurface structure or properties can assist operators in making informed decisions by providing a better understanding of field assets. Our machine-learning framework is built on the statistical recurrent unit (SRU) model and interprets well-based injection/production data into inter-well connectivity without relying on a geologic model. We test it on synthetic and field-scale CO 2 EOR projects utilizing the water-alternating-gas (WAG) process. SRU is a special type of recurrent neural network (RNN) that allows for better characterization of temporal trends, by learning various statistics of the input at different time scales. In our application, the complete states (injection rate, pressure and cumulative injection) at injectors and pressure states at producers are fed to SRU as the input and the phase rates at producers are treated as the output. Once the SRU is trained and validated, it is then used to assess the connectivity of each injector to any producer using permutation variable importance method, wherein inputs corresponding to an injector are shuffled and the increase in prediction error at a given producer is recorded as the importance (connectivity metric) of the injector to the producer. This method is tested in both synthetic and field-scale cases. The validation of the proposed data-driven inter-well connectivity assessment is performed using synthetic data from simulation models where inter-well connectivity can be easily measured using the streamline-based flux allocation. The SRU model is shown to offer excellent prediction performance on the synthetic case. Despite significant measurement noise and frequent well shut-ins imposed in the field-scale case, the SRU model offers good prediction accuracy, the overall relative error of the phase production rates at most producers ranges from 10% to 30%. It is shown that the dominant connections identified by the data-driven method and streamline method are in close agreement. This significantly improves confidence in our data-driven procedure. The novelty of this work is that it is purely data-driven method and can directly interpret routine surface measurements to intuitive subsurface knowledge. Furthermore, the streamline-based validation procedure provides physics-based backing to the results obtained from data analytics. This study results in a reliable and efficient data analytics framework that is well-suited for large field applications.

42 ENGINEERING↗

Joint Appointments: General Principles for Joint Appointments between LANL and University Partners

The Joint Appointment Program provides opportunities for LANL and partner universities to recruit, retain, and recognize premier scientists and engineers by offering them the ability to work in both the LANL and university environments. These interactions enhance the ability of both institutions to achieve their respective research and development missions while providing increased academic strength to educational institutions.

96 KNOWLEDGE MANAGEMENT AND PRESERVATION↗

Initiation of Experimental Campaign to Address Knowledge Gaps Related to Simultaneous Thermal and Gamma Radiation Aging of Crosslinked Polyethylene and Ethylene-Propylene Rubber Cable Insulation

Key cable knowledge gaps identified in the Expanded Materials Degradation Assessment (EMDA) volume on Aging of Cables and Cable Systems (Volume 5) specifically relate to the combined effects of thermal and gamma irradiation stresses on cable insulation materials. These include dose rate effects (DRE), inverse temperature effects (ITE), and synergistic effects (S/E). Extent of radiation-induced polymer degradation is proportional to absorbed dose, but DRE describe the phenomenon in which degree of damage is based not only on total dose, but also on the dose rate experienced during dose accumulation. This can be particularly complicated in the presence of thermal stress as a material spends more time at elevated temperature to receive the same total dose at a lower dose rate. Rates of cable polymer degradation generally increases with temperature, but ITE describes the situation in which polymer material damage under irradiation is greater at lower temperatures than at higher temperatures. Finally, S/E describe the concept that the mechanism of polymer material degradation when exposed to thermal aging and radiation aging in succession may be different than when exposed to thermal and radiation aging concurrently. The experimental campaign at the Pacific Northwest National Laboratory (PNNL) described in this report seeks to address these knowledge gaps through investigation of the degradation of relevant cable insulation materials at select conditions using controlled temperatures, dose rates and total doses. Insulation materials considered were chosen to represent those most commonly found in U.S. nuclear power plants in terms of manufacturers and polymer systems. They include products from manufactures including The Rockbestos Company; The Okonite Company; Boston Insulated Wire & Cable Company; Kerite Company; Anaconda Company; Brand Rex, Inc.; and Samuel Moore Company. The products include the most ubiquitous cross-linked polyethylene (XLPE) and ethylene-propylene rubber (EPR) classes of insulation polymer. Circulating air ovens with remote temperature sensing and control are positioned within the gamma irradiation beam to enable controlled temperatures during radiation exposure. Dose rates are controlled through repeatable positioning of specimens at determined distances from the Cobalt-60 gamma source. Total absorbed doses for comparing temperature and dose rate effects are controlled by removing samples from exposure at pre-determined time points. The effects of gamma beam geometry, source decay and attenuation due to samples, ovens and racks are determined and controlled for using local point dosimetry. The temperature, dose and dose rates selected for the experimental campaign described in this report were determined following input from a range of stakeholders and intended to balance the constraints of the experimental capabilities, available material, project timeline and project funding with the value of the effort in narrowing EMDA-identified knowledge gaps. Results from this campaign are anticipated to reduce uncertainty in the understanding of cable material degradation behavior in nuclear power plant environments and thereby support cable aging management in long term operation.

22 GENERAL STUDIES OF NUCLEAR REACTORS↗

High Temperature Component and Data Link Evaluation

Evaluation of high temperature (HT) microcontrollers for Geothermal applications. The goal was to evaluate the limited microcontrollers capable of operating above 200 degrees Celsius. The knowledge obtained from this research has been documented for contributing to future development of high temperature geothermal tools. Along with this research, a HT data link for communications was developed and evaluated, also for HT geothermal tools.

15 GEOTHERMAL ENERGY↗

Machine Tool Metrology in support of carbide insert production

In the context of lab modernization, careful consideration must be given to existing technologies, processes, and knowledge to support the ongoing production, maintenance, and improvement of products for the nuclear enterprise. This consideration often involves analyzing manufacturing processes both to pursue modernization or automation and to ensure the ability to maintain manufacturing capability.

42 ENGINEERING↗