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All sourcesNASA NTRSDOE OSTI
DOE OSTI2021

X-ray diffraction and in situ pressurization of dentine apatite reveals nanocrystal modulus stiffening upon carbonate removal

Bone-like materials comprise carbonated-hydroxyapatite nanocrystals (c-Ap) embedding a fibrillar collagen matrix. The mineral particles stiffen the nanocomposite by tight attachment to the protein fibrils creating a high strength and toughness material. The nanometer dimensions of c-Ap crystals make it very challenging to measure their mechanical properties. Mineral in bony tissues such as dentine contains 2~6 wt.% carbonate with possibly different elastic properties as compared with crystalline hydroxyapatite. Here we determine strain in biogenic apatite nanocrystals by directly measuring atomic deformation in pig dentine before and after removing carbonate. Transmission electron microscopy revealed the platy 3D morphology while atom probe tomography revealed carbon inside the calcium rich domains. High-energy X-ray diffraction in combination with in situ hydrostatic pressurization quantified reversible c-Ap deformations. Additionally, crystal strains differed between annealed and ashed (decarbonated) samples, following 1 or 10 h heating at 250 °C or 550 °C respectively. Measured bulk moduli (K) and a-/c-lattice deformation ratios (η) were used to generate synthetic K syn and ηsyn identifying the most likely elastic constants C 33 and C 13 for c-Ap. These were then used to calculate the nanoparticle elastic moduli. For ashed samples, we find an average E 11 =107 GPa and E 33 =128 GPa corresponding to ~5% and ~17% stiffening of the a-/c-axes of the nanocrystals as compared with the biogenic nanocrystals in annealed samples. Ashed samples exhibit ~10% lower Poisson's ratios as compared with the 0.25~0.36 range of carbonated apatite. Carbonate in c-Ap may therefore serve for tuning local deformability within bony tissues.

36 MATERIALS SCIENCE↗
DOE OSTI2014

Genome packaging in EL and Lin68, two giant phiKZ-like bacteriophages of P. aeruginosa

A unique feature of the Pseudomonas aeruginosa giant phage phiKZ is its way of genome packaging onto a spool-like protein structure, the inner body. Until recently, no similar structures have been detected in other phages. We have studied DNA packaging in P. aeruginosa phages EL and Lin68 using cryo-electron microscopy and revealed the presence of inner bodies. The shape and positioning of the inner body and the density of the DNA packaging in EL are different from those found in phiKZ and Lin68. This internal organization explains how the shorter EL genome is packed into a large EL capsid, which has the same external dimensions as the capsids of phiKZ and Lin68. The similarity in the structural organization in EL and other phiKZ-like phages indicates that EL is phylogenetically related to other phiKZ-like phages, and, despite the lack of detectable DNA homology, EL, phiKZ, and Lin68 descend from a common ancestor. - Highlights: • We performed a comparative structural study of giant P. aeruginosa phages: EL, Lin68 and phiKZ. • We revealed that the inner body is a common feature in giant phages. • The phage genome size correlates with the overall dimensions of the inner body.

60 APPLIED LIFE SCIENCES↗
DOE OSTI2014

Analysis of stimulated Raman backscatter and stimulated Brillouin backscatter in experiments performed on SG-III prototype facility with a spectral analysis code

Experiments about the observations of stimulated Raman backscatter (SRS) and stimulated Brillouin backscatter (SBS) in Hohlraum were performed on Shenguang-III (SG-III) prototype facility for the first time in 2011. In this paper, relevant experimental results are analyzed for the first time with a one-dimension spectral analysis code, which is developed to study the coexistent process of SRS and SBS in Hohlraum plasma condition. Spectral features of the backscattered light are discussed with different plasma parameters. In the case of empty Hohlraum experiments, simulation results indicate that SBS, which grows fast at the energy deposition region near the Hohlraum wall, is the dominant instability process. The time resolved spectra of SRS and SBS are numerically obtained, which agree with the experimental observations. For the gas-filled Hohlraum experiments, simulation results show that SBS grows fastest in Au plasma and amplifies convectively in C{sub 5}H{sub 12} gas, whereas SRS mainly grows in the high density region of the C{sub 5}H{sub 12} gas. Gain spectra and the spectra of backscattered light are simulated along the ray path, which clearly show the location where the intensity of scattered light with a certain wavelength increases. This work is helpful to comprehend the observed spectral features of SRS and SBS. The experiments and relevant analysis provide references for the ignition target design in future.

70 PLASMA PHYSICS AND FUSION TECHNOLOGY↗
DOE OSTI2014

Quasi-classical description of molecular dynamics based on Egorov's theorem

Egorov's theorem on the classical propagation of quantum observables is related to prominent quasi-classical descriptions of quantum molecular dynamics as the linearized semiclassical initial value representation, the Wigner phase space method, or the statistical quasiclassical method. The error estimates show that different accuracies are achievable for the computation of expectation values and position densities. Numerical experiments for a Morse model of diatomic iodine and confined Henon–Heiles systems in various dimensions illustrate the theoretical results.

37 INORGANIC, ORGANIC, PHYSICAL, AND ANALYTICAL CH↗
DOE OSTI2015

Probing environment fluctuations by two-dimensional electronic spectroscopy of molecular systems at temperatures below 5 K

Two-dimensional (2D) electronic spectroscopy at cryogenic and room temperatures reveals excitation energy relaxation and transport, as well as vibrational dynamics, in molecular systems. These phenomena are related to the spectral densities of nuclear degrees of freedom, which are directly accessible by means of hole burning and fluorescence line narrowing approaches at low temperatures (few K). The 2D spectroscopy, in principle, should reveal more details about the fluctuating environment than the 1D approaches due to peak extension into extra dimension. By studying the spectral line shapes of a dimeric aggregate at low temperature, we demonstrate that 2D spectra have the potential to reveal the fluctuation spectral densities for different electronic states, the interstate correlation of static disorder and, finally, the time scales of spectral diffusion with high resolution.

37 INORGANIC, ORGANIC, PHYSICAL, AND ANALYTICAL CH↗
DOE OSTI2014

Effective field theory of dark energy: a dynamical analysis

The effective field theory (EFT) of dark energy relies on three functions of time to describe the dynamics of background cosmology. The viability of these functions is investigated here by means of a thorough dynamical analysis. While the system is underdetermined, and one can always find a set of functions reproducing any expansion history, we are able to determine general compatibility conditions for these functions by requiring a viable background cosmology. In particular, we identify a set of variables that allows us to transform the non-autonomous system of equations into an infinite-dimensional one characterized by a significant recursive structure. We then analyze several autonomous sub-systems, obtained truncating the original one at increasingly higher dimension, that correspond to increasingly general models of dark energy and modified gravity. Furthermore, we exploit the recursive nature of the system to draw some general conclusions on the different cosmologies that can be recovered within the EFT formalism and the corresponding compatibility requirements for the EFT functions. The machinery that we set up serves different purposes. It offers a general scheme for performing dynamical analysis of dark energy and modified gravity models within the model independent framework of EFT; the general results, obtained with this technique, can be projected into specific models, as we show in one example. It also can be used to determine appropriate ansätze for the three EFT background functions when studying the dynamics of cosmological perturbations in the context of large scale structure tests of gravity.

79 ASTRONOMY AND ASTROPHYSICS↗
DOE OSTI2017

Neutron stars structure in the context of massive gravity

Motivated by the recent interests in spin−2 massive gravitons, we study the structure of neutron star in the context of massive gravity. The modifications of TOV equation in the presence of massive gravity are explored in 4 and higher dimensions. Next, by considering the modern equation of state for the neutron star matter (which is extracted by the lowest order constrained variational (LOCV) method with the AV18 potential), different physical properties of the neutron star (such as Le Chatelier's principle, stability and energy conditions) are investigated. It is shown that consideration of the massive gravity has specific contributions into the structure of neutron star and introduces new prescriptions for the massive astrophysical objects. The mass-radius relation is examined and the effects of massive gravity on the Schwarzschild radius, average density, compactness, gravitational redshift and dynamical stability are studied. Finally, a relation between mass and radius of neutron star versus the Planck mass is extracted.

79 ASTRONOMY AND ASTROPHYSICS↗
DOE OSTI2014

Sampling strategies for subsampled segmented EPI PRF thermometry in MR guided high intensity focused ultrasound

Purpose: To investigate k-space subsampling strategies to achieve fast, large field-of-view (FOV) temperature monitoring using segmented echo planar imaging (EPI) proton resonance frequency shift thermometry for MR guided high intensity focused ultrasound (MRgHIFU) applications. Methods: Five different k-space sampling approaches were investigated, varying sample spacing (equally vs nonequally spaced within the echo train), sampling density (variable sampling density in zero, one, and two dimensions), and utilizing sequential or centric sampling. Three of the schemes utilized sequential sampling with the sampling density varied in zero, one, and two dimensions, to investigate sampling the k-space center more frequently. Two of the schemes utilized centric sampling to acquire the k-space center with a longer echo time for improved phase measurements, and vary the sampling density in zero and two dimensions, respectively. Phantom experiments and a theoretical point spread function analysis were performed to investigate their performance. Variable density sampling in zero and two dimensions was also implemented in a non-EPI GRE pulse sequence for comparison. All subsampled data were reconstructed with a previously described temporally constrained reconstruction (TCR) algorithm. Results: The accuracy of each sampling strategy in measuring the temperature rise in the HIFU focal spot was measured in terms of the root-mean-square-error (RMSE) compared to fully sampled “truth.” For the schemes utilizing sequential sampling, the accuracy was found to improve with the dimensionality of the variable density sampling, giving values of 0.65 °C, 0.49 °C, and 0.35 °C for density variation in zero, one, and two dimensions, respectively. The schemes utilizing centric sampling were found to underestimate the temperature rise, with RMSE values of 1.05 °C and 1.31 °C, for variable density sampling in zero and two dimensions, respectively. Similar subsampling schemes with variable density sampling implemented in zero and two dimensions in a non-EPI GRE pulse sequence both resulted in accurate temperature measurements (RMSE of 0.70 °C and 0.63 °C, respectively). With sequential sampling in the described EPI implementation, temperature monitoring over a 192 × 144 × 135 mm{sup 3} FOV with a temporal resolution of 3.6 s was achieved, while keeping the RMSE compared to fully sampled “truth” below 0.35 °C. Conclusions: When segmented EPI readouts are used in conjunction with k-space subsampling for MR thermometry applications, sampling schemes with sequential sampling, with or without variable density sampling, obtain accurate phase and temperature measurements when using a TCR reconstruction algorithm. Improved temperature measurement accuracy can be achieved with variable density sampling. Centric sampling leads to phase bias, resulting in temperature underestimations.

42 ENGINEERING↗
DOE OSTI2019

Well Casing Baseline Analysis for the Bayou Choctaw Strategic Petroleum Reserve Site

This report analyzes data from multi-arm caliper (MAC) surveys taken at the Bayou Choctaw Strategic Petroleum Reserve site to determine baseline statistics for the original innermost cemented casing or the subsequent installed liner. Along with analyzing the internal diameters from the MAC surveys, this analysis looks to approximate casing weight, an important metric for determining the strength of well sections. Casing weight is calculated for each section, survey, and well. Results from the analysis show most wells reflect the dimensions in the original as-built drawings. There are, however, several exceptions. Some well sections have calculated wall thicknesses outside API tolerance. In addition, some well section depths differ from the as-built drawings. All results are discussed on a well-by-well basis. Where applicable, information from this report should be used to update as-built drawings and aid in creating more accurate well models for future studies.

02 PETROLEUM↗
NASA NTRS1973

Unsteady turbulent boundary layer analysis

The governing equations for an unsteady turbulent boundary layer on a swept infinite cylinder, composed of a continuity equation, a pair of momentum equations and a pair of turbulent energy equations which include upstream history efforts, are solved numerically. An explicit finite difference analog to the partial differential equations is formulated and developed into a computer program. Calculations were made for a variety of unsteady flows in both two and three dimensions but primarily for two dimensional flow fields in order to first understand some of the fundamental physical aspects of unsteady turbulent boundary layers. Oscillating free stream flows without pressure gradient, oscillating retarded free stream flows and monotonically time-varying flows have all been studied for a wide frequency range. It was found that to the lowest frequency considered, the lower frequency bound being determined by economic considerations (machine time), there were significant unsteady effects on the turbulent boundary layer.

Singleton, R. E.↗
NASA NTRS1981

Highly separated transonic flows

Attention is given to the wind tunnel, to photographic visualization of the flow, and to measurements by pressure probes, hot wire anemometry and laser anemometry. The simultaneous use of different means of measurement provided a good description of the phenomenon, and indicated the existence of shocks and their stability, as well as the existence of the bubble, its dimensions, and in particular, the reattachment of its front. The results show that the bursting (or transition) of the bubble front is produced at an unstable position and creates a point of turbulent intensity which diffuses over the entire height of the flow.

Farcy, A.↗
NASA NTRS1988

Automatic calibration of space based manipulators and mechanisms

Four tasks in manipulator kinematic calibration are summarized. Calibration of a seven degree of freedom manipulator was simulated. A calibration model is presented that can be applied on a closed-loop robot. It is an expansion of open-loop kinematic calibration algorithms subject to constraints. A closed-loop robot with a five-bar linkage transmission was tested. Results show that the algorithm converges within a few iterations. The concept of model differences is formalized. Differences are categorized as structural and numerical, with emphasis on the structural. The work demonstrates that geometric manipulators can be visualized as points in a vector space with the dimension of the space depending solely on the number and type of manipulator joint. Visualizing parameters in a kinematic model as the coordinates locating the manipulator in vector space enables a standard evaluation of the models. Key results include a derivation of the maximum number of parameters necessary for models, a formal discussion on the inclusion of extra parameters, and a method to predetermine a minimum model structure for a kinematic manipulator. A technique is presented that enables single point sensors to gather sufficient information to complete a calibration.

Everett, Louis J.↗
NASA NTRS1951

Torsion and bending of prismatic rods of hollow rectangular section

The torsion and bending of hollow rectangular beams was investigated without the requirement that wall thickness be small compared with the transverse dimensions. The limits of applicability of the usual Bredt formula are indicated for the case of a square hollow tube in torsion. Formulas are given for bending stresses at different parts of the cross section of a hollow rectangular beam.

BOXES, STRUCTURAL↗
NASA NTRS1993

Thermoelastic response of metal matrix composites with large-diameter fibers subjected to thermal gradients

A new micromechanical theory is presented for the response of heterogeneous metal matrix composites subjected to thermal gradients. In contrast to existing micromechanical theories that utilize classical homogenization schemes in the course of calculating microscopic and macroscopic field quantities, in the present approach the actual microstructural details are explicitly coupled with the macrostructure of the composite. Examples are offered that illustrate limitations of the classical homogenization approach in predicting the response of thin-walled metal matrix composites with large-diameter fibers when subjected to thermal gradients. These examples include composites with a finite number of fibers in the thickness direction that may be uniformly or nonuniformly spaced, thus admitting so-called functionally gradient composites. The results illustrate that the classical approach of decoupling micromechanical and macromechanical analyses in the presence of a finite number of large-diameter fibers, finite dimensions of the composite, and temperature gradient may produce excessively conservative estimates for macroscopic field quantities, while both underestimating and overestimating the local fluctuations of the microscopic quantities in different regions of the composite. Also demonstrated is the usefulness of the present approach in generating favorable stress distributions in the presence of thermal gradients by appropriately tailoring the internal microstructure details of the composite.

Aboudi, Jacob↗
NASA NTRS2000

A Study of the Constrained Vapor Bubble Thermosyphon

The objective of this effort is to better understand the physics of evaporation, condensation, and fluid flow as they affect the heat transfer processes in a constrained vapor bubble heat exchanger (CVBHX). This CVBHX consists of a small enclosed container with a square cross section (inside dimensions. 3 x 3 x 40 mm) partially filled with a liquid. The major portion of the liquid is in the corners, which act as arteries. When a temperature difference is applied to the ends of the CVBHX, evaporation occurs at the hot end and condensation at the cold end resulting in a very effective heat transfer device with great potential in space applications. Liquid is returned by capillary flow in the corners. A complete description of the system and the results obtained to date are given in the papers listed.

Wayner, Peter C., Jr.↗
NASA NTRS2010

Using Whispering-Gallery-Mode Resonators for Refractometry

A method of determining the refractive and absorptive properties of optically transparent materials involves a combination of theoretical and experimental analysis of electromagnetic responses of whispering-gallery-mode (WGM) resonator disks made of those materials. The method was conceived especially for use in studying transparent photorefractive materials, for which purpose this method affords unprecedented levels of sensitivity and accuracy. The method is expected to be particularly useful for measuring temporally varying refractive and absorptive properties of photorefractive materials at infrared wavelengths. Still more particularly, the method is expected to be useful for measuring drifts in these properties that are so slow that, heretofore, the properties were assumed to be constant. The basic idea of the method is to attempt to infer values of the photorefractive properties of a material by seeking to match (1) theoretical predictions of the spectral responses (or selected features thereof) of a WGM of known dimensions made of the material with (2) the actual spectral responses (or selected features thereof). Spectral features that are useful for this purpose include resonance frequencies, free spectral ranges (differences between resonance frequencies of adjacently numbered modes), and resonance quality factors (Q values). The method has been demonstrated in several experiments, one of which was performed on a WGM resonator made from a disk of LiNbO3 doped with 5 percent of MgO. The free spectral range of the resonator was approximately equal to 3.42 GHz at wavelengths in the vicinity of 780 nm, the smallest full width at half maximum of a mode was approximately equal to 50 MHz, and the thickness of the resonator in the area of mode localization was 30 microns. In the experiment, laser power of 9 mW was coupled into the resonator with an efficiency of 75 percent, and the laser was scanned over a frequency band 9 GHz wide at a nominal wavelength of approximately equal to 780 nm. Resonance frequencies were measured as functions of time during several hours of exposure to the laser light. The results of these measurements, plotted in the figure, show a pronounced collective frequency drift of the resonator modes. The size of the drift has been estimated to correspond to a change of 8.5 x 10(exp -5) in the effective ordinary index of refraction of the resonator material.

Matsko, Andrey↗
NASA NTRS2019

Common Habitat for Long Duration Transit and Surface Operations

This concept is based on the Skylab II concept, which proposes using a SLS propellant tank as the primary structure of a habitat. Common Habitat takes this a step further, proposing an interior architecture that is equally viable as a lunar surface hab, transit hab, and Mars surface hab, thus enabling a single development to support all three long duration habitat roles. Common Habitat has been pursued by the PI and co-investigators at MSFC and other centers in a spare time / funding available basis, often with heavy student intern support. Student resources have developed preliminary concepts, but these models must be refined to reflect accurate vehicle subsystems, utilities, stowage, workstations, and other crew systems. This investigation applies NASA civil servant and contractor expertise to correct errors in the most recent student concepts in order to prepare them for future human-in-the-loop evaluations to determine the most viable configuration for a Common Habitat. In prior studies there was never an opportunity to trade both crew size and internal orientation. Prior work has been a series of point designs with inconsistent design constraints, making apples to apples comparisons impossible. The most recent student work produced CAD models of four habitat variants for future use in a trade study, but the student products contain model construction and geometry errors, inaccurate subsystems design and placement, and unrealistic structural elements and outfitting. These must be corrected before the models can be moved into a VR environment for humanin- the-loop testing. Through consultation with SMEs throughout the Agency, the fidelity of these designs will be upgraded to a level of quality sufficient to make a comparative analysis of crew size sensitivity and internal orientation. The product of this activity is four upgraded CAD models, each reflecting a different configuration of the Common Habitat. One is a horizontal configuration using the full length of the SLS LOX tank. One is a vertical configuration using the same tank dimensions. The third is a horizontal configuration using a truncated SLS LOX tank (half the barrel length). The fourth is a vertical configuration of the half-length SLS LOX tank.

Howard, Robert L.↗
DOE OSTI2016

Unparticles and anomalous dimensions in the cuprates

Motivated by the overwhelming evidence some type of quantum criticality underlies the power-law for the optical conductivity and T-linear resistivity in the cuprates, we demonstrate here how a scale-invariant or unparticle sector can lead to a unifying description of the observed scaling forms. We adopt the continuous mass formalism or multi band (flavor) formalism of the unparticle sector by letting various microscopic parameters be mass-dependent. In particular, we show that an effective mass that varies with the flavor index as well as a running band edge and lifetime capture the AC and DC transport phenomenology of the cuprates. A key consequence of the running mass is that the effective dynamical exponent can differ from the underlying bare critical exponent, thereby providing a mechanism for realizing the fractional values of the dynamical exponent required in a previous analysis\cite{ Hartnoll:2015sea}. We also predict that regardless of the bare dynamical exponent, z, a non-zero anomalous dimension for the current is required. Physically, the anomalous dimension arises because the charge depends on the flavor, mass or energy. The equivalent phenomenon in a d+1 gravitational construction is the running of the charge along the radial direction. We find that the nature of the superconducting instability in the presence of scale invariant stuff shows that the transition temperature is not necessarily a monotonic function of the pairing interaction.

72 PHYSICS OF ELEMENTARY PARTICLES AND FIELDS↗