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At least 1,189 records · Page 66

Evaluation of selected thermal control coatings for long-life space structures

Graphite-reinforced resin matrix composites are being considered for spacecraft structural applications because of their light weight, high stiffness, and lower thermal expansion. Thin protective coatings with stable optical properties and the proper ratio of solar absorption (alpha sub s) to thermal emittance (epsilon) minimize orbital thermal extremes and protect these materials against space environment degradation. Sputtered coatings applied directly to graphite/epoxy composite surfaces and anodized coatings applied to thin aluminum foil were studied for use both as an atomic oxygen barrier and as thermal control coatings. Additional effort was made to develop nickel-based coatings which could be applied directly to composites. These coating systems were selected because their inherent tenacity made them potentially more reliable than commercial white paints for long-life space missions. Results indicate that anodized aluminum foil coatings are suitable for tubular and flat composite structures on large platforms in low Earth orbit. Anodized foil provides protection against some elements of the natural space environment (atomic oxygen, ultraviolet, and particulate radiation) and offers a broad range of tailored alpha sub s/epsilon. The foil is readily available and can be produced in large quantities, while the anodizing process is a routine commercial technique.

Teichman, Louis A.↗

Evaluation of Surlyn 8920 as PHE Visor Material and Evaluations of New Adhesives for Improving Bonding Between Teflon and Stainless Steel at Cryogenic Temperature

Two studies are presented, and in the first study, Surlyn 8920 (an ionic and amorphous low density polyethylene made by Dupont) was evaluated as a possible replacement of Plexyglass G as PHE visor material. Four formulations of the polymer were made by adding different amounts of UV stabilizer, energy quencher, and antioxident in a Brabender Plasticorder. The formulated polymers were molded in the form of sheets in a compression molder. Cut samples from the molded sheets were exposed in a weatherometer and tested on Instron Tensile Tester for strength and elongation. Specially molded samples of the formulated polymers were subjected to Charpy Impact Tests. In the second study, preliminary evaluations of adhesives for improvement of bonding between Teflon and stainless steel (SS) were performed. Kapton, a high temperature polyimide made by Dupont, and a rubber based adhesive made by Potter Paint Co., were evaluated against industrial quality epoxy, the current material used to bond Teflon and SS. The degreased surfaces of the SS discs were etched mechanically, with a few of these etched chemically. The surfaces of the SS discs were etched mechanically, with a few of these etched chemically. Bonding strengths were evaluated using lap shear tests on the Instron Tensile Tester for the samples bonded by Kapton and industrial quality epoxy. Bond strengths were also evaluated using a pull test on the Instron for the samples bonded by Potter adhesive (CWL-152) and industrial quality epoxy. Based on limited lap shear data, Kapton gave bond strength favorable compared to that of industrial epoxy. Based on limited pull test data, Kapton bonded and CWL-152 bonded samples showed poor strength compared to epoxy bonded sample.

Ray, Asit K.↗

Flow studies in close-coupled ventral nozzles for STOVL aircraft

Flow in a generic ventral nozzle system was studied experimentally and analytically with the PARC3D computational fluid dynamics program in order to evaluate the program's ability to predict system performance and internal flow patterns. A generic model of a tailpipe with a rectangular ventral nozzle, about 1/3 of full size, was tested with unheated air at steady state pressure ratios up to 4.0. The end of the tailpipe was closed to simulate a blocked exhaust nozzle. Flow behavior into and through the ventral duct is discussed and illustrated with paint streak flow visualization photographs. PARC3D graphic images are shown for comparison with the experimental photographs. The program successfully predicted internal flow patterns; it also computed thrust and discharge coefficients within 1 pct. of measured values.

Mcardle, Jack G.↗

Multi-colored layers for visualizing aerodynamic flow effects

A method is provided for visualizing aerodynamic flow effects on a test surface. First, discrete quantities of a sublimating chemical such as naphthalene are distinctively colored via appropriate dyes or paints. Next, a uniform layer of the sublimating chemical having a particular color is applied to the test surface. This layer is covered with a second uniform layer of a different colored sublimating chemical, and so on until a composite of multi-colored layers is formed having a discrete thickness. Friction caused by an airflow results in the distinctly colored layers being removed in proportion to such aerodynamic flow characteristics as velocity and temperature, resulting in a multi-colored portrait which approximates the air flow on the underlying test surface.

Jensen, Ronald N.↗

Plastic superconductor bearings any size-any shape: 77 K and up

'Friction free' bearings at 77 K or higher are possible using the high T(sub c) copper oxide ceramic superconductors. The conventional method for making such bearings is to use a sintered ceramic monolith. This puts great restraints on size, shape, and postforming machining. The material is hard and abrasive. It is possible to grind up ceramic superconductors and suspend the granules in a suitable matrix. Mechanical properties improve and are largely dependent on the binder. The Meissner effect is confined to individual grains containing electron vortices. Tracks, rails, levitation areas, and bearings can be made this way with conventional plastic molding and extruding machines or by painting. The parts are easily machined. The sacrifice is in bulk electrical conductivity. A percolating wick feed for LN2 is used to cool remote superconductors and large areas quite effectively. A hollow spheroid or cylinder of superconductor material is molded with the internal surfaces shielded by the Meissner effect. It can be thought of as the DC magnetic analog of the Faraday cage and the inside is the 'Meissner space'. It is selective. The AC fields are transmitted with minor attenuation. Particle size and distribution have a profound effect on final magnetic and electrical characteristics.

Reick, Franklin G.↗

Molecular films associated with LDEF

The molecular films deposited on the surface of the Long Duration Exposure Facility (LDEF) originated from the paints and room-temperature-vulcanized (RTV) silicone materials intentionally used on the satellite and not from residual contaminants. The high silicone content of most of the films and the uniformity of the films indicates a homogenization process in the molecular deposition and suggests a chemically most favored composition for the final film. The deposition on interior surfaces and vents indicated multiple bounce trajectories or repeated deposition-reemission cycles. Exterior surface deposits indicated a significant return flux. Ultraviolet light exposure was required to fix the deposited film as is indicated by the distribution of the films on interior surfaces and the thickness of films at the vent locations. Thermal conditions at the time of exposure to ultraviolet light seems to be an important factor in the thickness of the deposit. Sunrise facing (ram direction) surfaces always had the thicker film. These were the coldest surfaces at the time of their exposure to ultraviolet light. The films have a layered structure suggesting cyclic deposition. As many as 34 distinct layers were seen in the films. The cyclic nature of the deposition and the chemical uniformity of the film one layer to the next suggest an early deposition of the films though there is evidence for the deposition of molecular films throughout the nearly six year exposure of the satellite. A final 'spray' of an organic material associated with water soluble salts occurred very late in the mission. This may have been the result of one of the shuttle dump activities.

Crutcher, E. R.↗

M and D SIG progress report: Laboratory simulations of LDEF impact features

Laboratory impact experiments are needed to understand the relationship between a measured penetration hole diameter and associated projectile dimension in the thermal blankets of experiment A0178, which occupied some 16 sq. m. These blankets are composed of 125 micron thick Teflon that has an Ag/enconel second mirror surface, backed by organic binder and Chemglaze paint for a total thickness of some 170 microns. While dedicated experiments are required to understand the penetration behavior of this compound target in detail, we report here on impact simulations sponsored by other projects into pure Teflon and aluminum targets. These experiments will allow first order interpretations of impact features on the Long Duration Exposure Facility (LDEF), and they will serve as guides for dedicated experiments that employ the real LDEF blankets, both exposed and unexposed, for a refined understanding of the LDEF's collisional environment. We employed a light gas gun to launch soda-lime glass spheres from 50 to 3200 microns in diameter that impacted targets of variable thickness. Penetration measurements are given.

Horz, Friedrich↗

The electrical conductivities of the DSS-13 beam-waveguide antenna shroud material and other antenna reflector surface materials

A significant amount of noise temperature can potentially be generated by currently unknown dissipative losses in the beam waveguide (BWG) shroud. The amount of noise temperature contribution from this source is currently being studied. In conjunction with this study, electrical conductivity measurements were made on samples of the DSS-13 BWG shroud material at 8.420 GHz. The effective conductivities of unpainted and painted samples of the BWG shroud were measured to be 0.01 x 10(exp 7) and 0.0036 x 10(exp 7) mhos/m, respectively. This value may be compared with 5.66 x 10(exp 7) mhos/m for high conductivity copper.

Otoshi, T. Y.↗

Preliminary findings of the LDEF Materials Special Investigation Group

The retrieval of NASA's LDEF from low Earth orbit provided an opportunity for the study of long duration space environmental effects on materials. The five year, nine month flight of the LDEF greatly enhanced the potential value of most LDEF materials. NASA recognized this potential by forming the LDEF Space Environmental Effects on Materials Special Investigation Group (MSIG). Its goal is to explore the expanded materials analysis opportunities available in the LDEF structure and on experiment trays. The charter and scope of MSIG activities is presented, followed by an overview of the preliminary MSIG observations. These observations of low Earth orbit environmental effects on materials were made in-space during LDEF retrieval and during LDEF tray disintegration. Also presented are initial findings of lab analyses of LDEF materials. Included are effects of individual environmental parameters: atomic oxygen, ultraviolet radiation, meteoroid and debris impacts, thermal cycling, vacuum, and contamination, plus combined effects of these parameters. Materials considered include anodized aluminum, polymer matrix composites, polymer films, silvered Teflon thermal blankets, and a white thermal control paint.

Stein, Bland A.↗

Unusual materials effects observed on the thermal control surfaces experiment (S0069)

A number of unusual effects were observed on the Thermal Control Surfaces Experiment (TCSE) test samples, front cover, and structural components. These effects include atomic oxygen (AO) texturing of the exposed surface of the silver Teflon (Ag/FEP) thermal control material, 'brownish' discoloration of the Ag/FEP material, changes in fluorescence of thermal control paint samples, and meteoroid/debris impact effects on silver Teflon.

Zwiener, James M.↗

Spacecraft thermal control coatings

The Experiment AO 138-6 was located on the trailing edge of the Long Duration Exposure Facility as part of the French Cooperative Payload (FRECOPA) Experiment. It was purely passive in nature: material specimens 2 x 2 cm, independently mounted in sample-holders, with their surface in the same reference plane, were exposed to space. Thirty samples were set in a vacuum-tight canister which was opened in space a few days after LDEF deployment and closed while still in orbit ten months later; twenty-four samples were directly exposed to space for the total flight duration (preflight handling, shuttle bay environment, separation from shuttle, shuttle environment, LEO environment, docking, descent, transfer to KSC). Materials included paints (conductive or nonconductive), SSM's, polymeric films, surface coatings, composite materials, and metals. After sample retrieving, inspection and measurements were carried out in atmospheric laboratory conditions on each sample: observation with binocular lenses and scanning electron microscopy, spectral relectance and transmittance using an integrating sphere in the wavelength range 280-2300 nm, emissivity by the means of a Gier & Dunkle portable reflectometer, electron spectroscopy for chemical analysis-x-ray photoelectron spectroscopy (ESCA-XPS), and Rutherford backscattering spectroscopy (RBS) measurements on some selected samples. The results obtained from flight were compared to laboratory data obtained in UV-irradiation tests when these data were available. As a general statement a good spectral concordance is observed for all samples not in the canister so long as air recoveries are taken into account. For one material, the degradation is more important for the sample in the canister than for those of the same material mounted at the surface of the tray; for most samples in the canister the degradation is slightly higher than the one which can be predicted from laboratory standard irradiations. Contamination problems having been ruled out, the higher temperature experience by the samples on the inside of canister probably explains these phenomena.

Guillaumon, Jean-Claude↗

NASA technology applications team. Applications of aerospace technology

Discussed here are the activities of the Research Triangle Institute (RTI) Technology Applications Team for the period 1 October 1990 through 30 September 1991. Topics researched include automated data acquisition and analysis of highway pavement cracking, thermal insulation for refrigerators, the containment of paint removed from steel structures, improved technologies for Kuwait oil well control, sprayed zinc coatings for corrosion control of reinforcing steel in bridges, and the monitoring and life support of medically fragile children in the educational setting.

Source record↗

An overview of the first results on the solar array materials passive LDEF experiment (sample), A0171

Power degradation in the solar cells was consistent with the exposure environment and appears to be produced principally by the radiation and atomic oxygen environments. Atomic oxygen erosion was generally as expected; atomic oxygen effects dominated for the most part in materials that were both atomic oxygen and ultraviolet vulnerable. Silicone coatings appear to protect Kapton, and adhesive systems contained under photon opaque materials were surprisingly environmentally resistant. A high density of small micro-meteroid/space debris impacts were observed on mirrors, protective coatings, paints, and composites. New synergistic effects of the space environment were noted in the interaction of atomic oxygen and copious amounts of contamination and in the induced luminescence of many materials.

Ann F Whitaker↗

LDEF active optical system components experiment

A preliminary report on the Active Optical System Components Experiment is presented. This experiment contained 136 components in a six inch deep tray including lasers, infrared detectors and arrays, ultraviolet light detectors, light-emitting diodes, a light modulator, flash lamps, optical filters, glasses, and samples of surface finishes. Thermal, mechanical, and structural considerations leading to the design of the tray hardware are discussed. In general, changes in the retested component characteristics appear as much related to the passage of time as to the effects of the space environment, but organic materials, multilayer optical interference filters, and extreme-infrared reflectivity of black paints show unexpected changes.

M D Blue↗

Contamination of optical surfaces in Earth orbit

Glass and glass ceramic samples exposed to the low earth orbit environment for approximately 5.5 years on the Long Duration Exposure Facility (LDEF) were found to display limited degradation in optical transmission. Commercial optical quality fused silica samples display decreases in transmission in the 200 to 400 nm wavelength region, and this degradation appears to be a consequence of surface contamination. The contamination, found only on internal surfaces of samples, was measured by medium energy backscattering spectrometry and found to be primarily carbon. Additional thin film contamination by a species with atomic mass near 64, which was present at the level of about 8 x 10 exp 14/sq. cm has not been identified. These observations are consistent with the interpretation that organic binders used in the black absorbing paint (Chem Glaze Z-306) inside the sample holding tray were concentrated in the vicinity of the samples and photolytically cracked by solar UV radiation. The resulting decomposition products were deposited on the interior sample surface and gave rise to the optical transmission loss. No detectable contamination was observed on the external or space exposed surface of the samples. No measurable damage was detected which could be attributed to the direct action of gamma or UV radiation on the glass samples. These results emphasize the need for special precautions in the preparation of spacecraft carrying precision optical components on long duration missions.

Donald L Kinser↗

Detailed examination of LDEF's frame and the A0178 thermal blankets by the meteoroid and debris special investigations group

A responsibility of the group is to define the hypervelocity particle environment encountered by LDEF during its stay in low Earth orbit. LDEF's 6061-T6 aluminum frame and the 'Teflon silver-inconel paint' thermal blankets represent large surface areas that were widely distributed around the spacecraft. The results are reported of high resolution scans of approx. 0.36 and approx. 0.31 sq m for the intercostals and thermal blankets, respectively. The findings are in qualitative agreement with existing model predictions that suggest high differential bombardment histories for surfaces pointing into specific directions relative to the velocity vector of a non-spinning platform in LEO. The production rate for craters greater than or = 50 microns in diameter in aluminum and penetration holes greater than or = 100 microns in diameter in thin foil materials differ by more than a factor of 10 between forward and rearward facing surfaces. These are substantial differences that must be considered during the design of future long duration space platforms in LEO.

See, Thomas H.↗

Hypervelocity impact facility for simulating materials exposure to impact by space debris

The Space Power Institute at Auburn University has constructed an electromagnetically driven particle accelerator for simulating the effects of space debris on the materials for use in advanced spacecraft. The facility consists of a capacitively driven accelerator section, a drift tube and a specimen impact chamber. The drift tube is sufficiently long that all electrical activity has ceased prior to impact in the specimen chamber. The impact chamber is large enough to allow a wide range of specimen geometries, ranging from small coupons to active portions of advanced spacecraft. The electric drive for the accelerator consists of a 67 kJ, 50 k capacitor bank arranged in a low inductance configuration. The bank is discharged through an aluminum armature/plastic ablator plate/projectile load in roughly 1.2 microsec. The evaporation of the ablaitor plate produces an expanding gas slug, mostly H2, traveling at a velocity of some 60 km/sec. Because of the pressure and local density, the expanding gas cloud accelerates projectiles due to plasma drag. To date, we have utilized projectiles consisting of 100 micron SiC, 100 and 400 micron Al2O3, 100 and 145 micron olivines. Since many particles are accelerated in a given experiment, there is a range of velocities for each shot as well as some particle breakup. Advanced diagnostics techniques allow determination of impact coordinates, velocity, and approximate size for as many as 50 individual impacts in a given experiment. We routinely measure velocities in the range 1-15 km/sec. We have used this facility to study a variety of impact generated phenomena on coated surfaces, both paint and plastic, thermal blanket material, solar cell arrays, and optical materials such as glass and quartz lenses. The operating characteristics of the gun, the advanced diagnostic scheme, and the results of studies of crater morphology are described in detail. Projectile residue analysis, as a function of impact velocity for the materials listed above, is also discussed. Wherever possible, these results are compared to those obtained by LDEF investigators and future experiments suggested which could help to explain unique features associated with LDEF impacts.

Rose, M. Frank↗

Databases for LDEF results

One of the objectives of the team supporting the LDEF Systems and Materials Special Investigative Groups is to develop databases of experimental findings. These databases identify the hardware flown, summarize results and conclusions, and provide a system for acknowledging investigators, tracing sources of data, and future design suggestions. To date, databases covering the optical experiments, and thermal control materials (chromic acid anodized aluminum, silverized Teflon blankets, and paints) have been developed at Boeing. We used the Filemaker Pro software, the database manager for the Macintosh computer produced by the Claris Corporation. It is a flat, text-retrievable database that provides access to the data via an intuitive user interface, without tedious programming. Though this software is available only for the Macintosh computer at this time, copies of the databases can be saved to a format that is readable on a personal computer as well. Further, the data can be exported to more powerful relational databases, capabilities, and use of the LDEF databases and describe how to get copies of the database for your own research.

Bohnhoff-Hlavacek, Gail↗