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Search indexed NASA NTRS and DOE OSTI research on propulsion, heat transfer, battery materials and energy systems. Follow report and document links to the original sources.

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At least 1,171 records · Page 65
All sourcesNASA NTRSDOE OSTI
DOE OSTI2017

Generation of Ramped Current Profiles in Relativistic Electron Beams Using Wakefields in Dielectric Structures

We show that temporal pulse tailoring of charged-particle beams is essential to optimize efficiency in collinear wakefield acceleration schemes. In this Letter, we demonstrate a novel phase space manipulation method that employs a beam wakefield interaction in a dielectric structure, followed by bunch compression in a permanent magnet chicane, to longitudinally tailor the pulse shape of an electron beam. This compact, passive, approach was used to generate a nearly linearly ramped current profile in a relativistic electron beam experiment carried out at the Brookhaven National Laboratory Accelerator Test Facility. Here, we report on these experimental results including beam and wakefield diagnostics and pulse profile reconstruction techniques.

43 PARTICLE ACCELERATORS↗
DOE OSTI2017

Impact of Monoenergetic Photon Sources on Nonproliferation Applications Final Report

Near-monoenergetic photon sources (MPSs) have the potential to improve sensitivity at greatly reduced dose in existing applications and enable new capabilities in other applications, particularly where passive signatures do not penetrate or are insufficiently accurate. MPS advantages include the ability to select energy, energy spread, flux, and pulse structures to deliver only the photons needed for the application, while suppressing extraneous dose and background. Some MPSs also offer narrow angular divergence photon beams which can target dose and/or mitigate scattering contributions to image contrast degradation. Current bremsstrahlung photon sources (e.g., linacs and betatrons) produce photons over a broad range of energies, thus delivering unnecessary dose that in some cases also interferes with the signature to be detected and/or restricts operations. Current sources must be collimated (reducing flux) to generate narrow divergence beams. While MPSs can in principle resolve these issues, they remain at relatively low TRL status. Candidate MPS technologies for nonproliferation applications are now being developed, each of which has different properties (e.g. broad vs. narrow angular divergence). Within each technology, source parameters trade off against one another (e.g. flux vs. energy spread), representing a large operation space. This report describes a broad survey of potential applications, identification of high priority applications, and detailed simulations addressing those priority applications. Requirements were derived for each application, and analysis and simulations were conducted to define MPS parameters that deliver benefit. The results can inform targeting of MPS development to deliver strong impact relative to current systems.

73 NUCLEAR PHYSICS AND RADIATION PHYSICS↗
DOE OSTI2016

DISCOVERY OF A GALAXY CLUSTER WITH A VIOLENTLY STARBURSTING CORE AT z = 2.506

We report the discovery of a remarkable concentration of massive galaxies with extended X-ray emission at z {sub spec} = 2.506, which contains 11 massive (M {sub *} ≳ 10{sup 11} M {sub ⊙}) galaxies in the central 80 kpc region (11.6 σ overdensity). We have spectroscopically confirmed 17 member galaxies with 11 from CO and the remaining ones from H α . The X-ray luminosity, stellar mass content, and velocity dispersion all point to a collapsed, cluster-sized dark matter halo with mass M {sub 200} {sub c} = 10{sup 13.9±0.2} M {sub ⊙}, making it the most distant X-ray-detected cluster known to date. Unlike other clusters discovered so far, this structure is dominated by star-forming galaxies (SFGs) in the core with only 2 out of the 11 massive galaxies classified as quiescent. The star formation rate (SFR) in the 80 kpc core reaches ∼3400 M {sub ⊙} yr{sup −1} with a gas depletion time of ∼200 Myr, suggesting that we caught this cluster in rapid build-up of a dense core. The high SFR is driven by both a high abundance of SFGs and a higher starburst fraction (∼25%, compared to 3%–5% in the field). The presence of both a collapsed, cluster-sized halo and a predominant population of massive SFGs suggests that this structure could represent an important transition phase between protoclusters and mature clusters. It provides evidence that the main phase of massive galaxy passivization will take place after galaxies accrete onto the cluster, providing new insights into massive cluster formation at early epochs. The large integrated stellar mass at such high redshift challenges our understanding of massive cluster formation.

79 ASTRONOMY AND ASTROPHYSICS↗
DOE OSTI2025

Fabrication of 4H-SiC Low Gain Avalanche Detectors (LGADs)

Low gain avalanche detectors (LGADs) offer high temporal resolution for high energy particle detection, which is critical for next generation experiments in hadron colliders. While silicon LGADs (Si-LGADs) have rapidly matured in the last decade, research into silicon carbide (SiC) LGADs has only recently begun. By accounting for fundamental differences in material properties and fabrication processes, we present a prototype device design and process flow for 4H-SiC LGADs with etch-based isolation. Critical steps of the process flow and their results are discussed, including plasma etching, passivation, and the formation of low resistivity contacts. Electrical characterization (I-V, C-V) shows sufficient depletion of the device structure to demonstrate low-gain charge carrier multiplication.

High Energy Physics↗
NASA NTRS1978

Power train analysis for the DOE/NASA 100-kW wind turbine generator

Progress in explaining variations of power experienced in the on-line operation of a 100 kW experimental wind turbine-generator is reported. Data are presented that show the oscillations tend to be characteristic of a wind-driven synchronous generator because of low torsional damping in the power train, resonances of its large structure, and excitation by unsteady and nonuniform wind flow. The report includes dynamic analysis of the drive-train torsion, the generator, passive driveline damping, and active pitch control as well as correlation with experimental recordings. The analysis assumes one machine on an infinite bus with constant generator-field excitation.

Seidel, R. C.↗
NASA NTRS1992

Some results of the oxidation investigation of copper and silver samples flown on LDEF

The Long Duration Exposure Facility (LDEF) Mission provides a unique opportunity to study the long term effects of the space environment on materials. The LDEF has been deployed in orbit on 7 April 1984 by the shuttle Challenger in an almost circular orbit with a mean altitude of 477 km and an inclination of 28.5 degrees. It was retrieved from its decayed orbit of 335 km by the shuttle Columbia on 12 January 1990 after almost 6 years in space. The LDEF is a 12-sided, 4.267 m diameter, and 9.144 m long structure. The experiments, placed on trays, are attached to the twelve sides and the two ends of the spacecraft. The LDEF was passively stabilized with one end of the spacecraft always pointing towards the earth center and one of the sides (row 9) always facing the flight direction. The materials investigated originate from the Ultra-Heavy Cosmic Ray Experiment (UHCRE). The main objective is a detailed study of the charge spectra of ultraheavy cosmic-ray nuclei from zinc to uranium and beyond, using solid-state track detectors. Besides the aluminium alloy used for the experiment, UHCRE comprises several other materials. The results of space exposure for two of them, the copper grounding strips and the thermal covers (FEP Teflon/Ag/Inconel) painted black on the inner side (Chemglaze Z306), are presented.

Derooij, A.↗
NASA NTRS1993

CSI flight experiment projects of the Naval Research Laboratory

The Naval Research Laboratory (NRL) is involved in an active program of CSI flight experiments. The first CSI flight experiment of the Naval Research Laboratory, the Low Power Atmospheric Compensation Experiment (LACE) dynamics experiment, has successfully measured vibrations of an orbiting satellite with a ground-based laser radar. The observations, made on January 7, 8 and 10, 1991, represent the first ever measurements of this type. In the tests, a narrowband heterodyne CO2 laser radar, operating at a wavelength of 10.6 microns, detected vibration induced differential-Doppler signatures of the LACE satellite. Power spectral densities of forced oscillations and modal frequencies and damping rates of free-damped vibrations were obtained and compared with finite element structural models of the LACE system. Another manifested flight experiment is the Advanced Controls Technology Experiment (ACTEX) designed to demonstrate active and passive damping with piezo-electric (PZT) sensors and actuators. This experiment was developed under the management of the Air Force Phillips Laboratory with integration of the experiment at NRL. It is to ride as a secondary, or 'piggyback,' experiment on a future Navy satellite.

Fisher, Shalom↗
NASA NTRS1995

Product Assurance for Spaceflight Hardware

This report contains information about the tasks I have completed and the valuable experience I have gained at NASA. The report is divided into two different sections followed by a program summary sheet. The first section describes the two reports I have completed for the Office of Mission Assurance (OMA). I describe the approach and the resources and facilities used to complete each report. The second section describes my experience working in the Receipt Inspection/Quality Assurance Lab (RI/QA). The first report described is a Product Assurance Plan for the Gas Permeable Polymer Materials (GPPM) mission. The purpose of the Product Assurance Plan is to define the various requirements which are to be met through completion of the GPPM mission. The GPPM experiment is a space payload which will be flown in the shuttle's SPACEHAB module. The experiment will use microgravity to enable production of complex polymeric gas permeable materials. The second report described in the first section is a Fracture Analysis for the Mir Environmental Effects Payload (MEEP). The Fracture Analysis report is a summary of the fracture control classifications for all structural elements of the MEEP. The MEEP hardware consists of four experiment carriers, each of which contains an experiment container holding a passive experiment. The MEEP hardware will be attached to the cargo bay of the space shuttle. It will be transferred by Extravehicular Activity and mounted on the Mir space station. The second section of this report describes my experiences in the RVQA lab. I listed the different equipment I used at the lab and their functions. I described the extensive inspection process that must be completed for spaceflight hardware. Included, at the end of this section, are pictures of most of the equipment used in the lab. There is a summary sheet located at the end of this report. It briefly describes the valuable experience I have gained at NASA this summer and what I will be able to take with me as I return to college. I briefly discuss the experiences I mentioned in the previous three paragraphs along with training classes I attended and courses I completed at the Learning Lab.

Monroe, Mike↗
NASA NTRS2003

Use of GTE, Mozaic, Sonex, and UARS-MLS Data in Understanding Tropospheric Processes Critical to Model Development

During the first year we focused on the analysis of data collected on over 7600 commercial aircraft flights (the MOZAIC program). The aim was to further our understanding of the fundamental dynamical processes that drive mesoscale phenomena in the upper troposphere and lower stratosphere, and their effects on the advection of passive scalars. Through these studies we made the following findings. 2001]: We derived the Kolmogorov equation for the third-order velocity structure function on an f-plane. We showed how the sign of the function yields the direction of the energy cascade. The remarkable linearity of the measured off diagonal third-order structure function was studied. We suggested that the Coriolis term, which appears explicitly in this equation, may be crucial in understanding the observed kinetic energy spectra at scales larger than 100 km, instead of the nonlinear advection term as previously assumed. Also, we showed that decreases with latitude for mid- to high-latitudes, and tabulated the values. Ozone concentration structure functions were calculated by restricting the data points to approximately isentropic pairings. In this way we were able to make comparisons with scalar advection theories. We found that, at even the largest scales, there was no evidence for the simple scaling predicted for smooth advection/diffusion.

Newell, Reginald E.↗
NASA NTRS2003

AMS-02 Cryocooler Baseline Configuration and Engineering Model Qualification Test Results

Four Sunpower M87N Stirling-cycle cryocoolers will be used to extend the lifetime of the Alpha Magnetic Spectrometer-02 (AMS-02) experiment. The cryocoolers will be mounted to the AMS-02 vacuum case using a structure that will thermally and mechanically decouple the cryocooler from the vacuum case while providing compliance to allow force attenuation using a passive balancer system. The cryocooler drive is implemented using a 60Hz pulse duration modulated square wave. Details of the testing program, mounting assembly and drive scheme will be presented. AMS-02 is a state-of-the-art particle physics detector containing a large superfluid helium-cooled superconducting magnet. Highly sensitive detector plates inside the magnet measure a particle s speed, momentum, charge, and path. The AMS-02 experiment, which will be flown as an attached payload on the International Space Station, will study the properties and origin of cosmic particles and nuclei including antimatter and dark matter. Two engineering model cryocoolers have been under test at NASA Goddard since November 2001. Qualification testing of the engineering model cryocooler bracket assembly is near completion. Delivery of the flight cryocoolers to Goddard is scheduled for September 2003.

Banks, Stuart↗
NASA NTRS2005

Study of a 30-M Boom For Solar Sail-Craft: Model Extendibility and Control Strategy

Space travel propelled by solar sails is motivated by the fact that the momentum exchange that occurs when photons are reflected and/or absorbed by a large solar sail generates a small but constant acceleration. This acceleration can induce a constant thrust in very large sails that is sufficient to maintain a polar observing satellite in a constant position relative to the Sun or Earth. For long distance propulsion, square sails (with side length greater than 150 meters) can reach Jupiter in two years and Pluto in less than ten years. Converting such design concepts to real-world systems will require accurate analytical models and model parameters. This requires extensive structural dynamics tests. However, the low mass and high flexibility of large and light weight structures such as solar sails makes them unsuitable for ground testing. As a result, validating analytical models is an extremely difficult problem. On the other hand, a fundamental question can be asked. That is whether an analytical model that represents a small-scale version of a solar-sail boom can be extended to much larger versions of the same boom. To answer this question, we considered a long deployable boom that will be used to support the solar sails of the sail-craft. The length of fully deployed booms of the actual solar sail-craft will exceed 100 meters. However, the test-bed we used in our study is a 30 meter retractable boom at MSFC. We first develop analytical models based on Lagrange s equations and the standard Euler-Bernoulli beam. Then the response of the models will be compared with test data of the 30 meter boom at various deployed lengths. For this stage of study, our analysis was limited to experimental data obtained at 12ft and 18ft deployment lengths. The comparison results are positive but speculative. To observe properly validate the analytic model, experiments at longer deployment lengths, up to the full 30 meter, have been requested. We expect the study to answer the extendibility question of the analytical models. In operation, rapid temperature changes can be induced in solar sails as they transition from day to night and vice versa. This generates time dependent thermally induced forces, which may in turn create oscillation in structural members such as booms. Such oscillations have an adverse effect on system operations, precise pointing of instruments and antennas and can lead to self excited vibrations of increasing amplitude. The latter phenomenon is known as thermal flutter and can lead to the catastrophic failure of structural systems. To remedy this problem, an active vibration suppression system has been developed. It was shown that piezoelectric actuators used in conjunction with a Proportional Feedback Control (PFC) law (or Velocity Feedback Control (VFC) law) can induce moments that can suppress structural vibrations and prevent flutter instability in spacecraft booms. In this study, we will investigate control strategies using piezoelectric transducers in active, passive, and/or hybrid control configurations. Advantages and disadvantages of each configuration will be studied and experiments to determine their capabilities and limitations will be planned. In particular, special attention will be given to the hybrid control, also known as energy recycling, configuration due to its unique characteristics.

Keel, Leehyun↗
NASA NTRS2010

MISSE 6 Polymer Film Tensile Experiment

The Polymer Film Tensile Experiment (PFTE) was flown as part of Materials International Space Station Experiment 6 (MISSE 6). The purpose of the experiment was to expose a variety of polymer films to the low Earth orbital environment under both relaxed and tension conditions. The polymers selected are those commonly used for spacecraft thermal control and those under consideration for use in spacecraft applications such as sunshields, solar sails, and inflatable and deployable structures. The dog-bone shaped samples of polymers that were flown were exposed on both the side of the MISSE 6 Passive Experiment Container (PEC) that was facing into the ram direction (receiving atomic oxygen, ultraviolet (UV) radiation, ionizing radiation, and thermal cycling) and the wake facing side (which was supposed to have experienced predominantly the same environmental effects except for atomic oxygen which was present due to reorientation of the International Space Station). A few of the tensile samples were coated with vapor deposited aluminum on the back and wired to determine the point in the flight when the tensile sample broke as recorded by a change in voltage that was stored on battery powered data loggers for post flight retrieval and analysis. The data returned on the data loggers was not usable. However, post retrieval observation and analysis of the samples was performed. This paper describes the preliminary analysis and observations of the polymers exposed on the MISSE 6 PFTE.

Miller, Sharon K. R.↗
DOE OSTI2016

Implementation of Enhanced Attenuation at the DOE Mound Site OU-1 Landfill: Accelerating Progress and Reducing Costs - 16270

A field demonstration of enhanced attenuation (EA) was initiated in 2014 to expedite the remediation of industrial solvents in the groundwater impacted by the former landfill Operable Unit 1 (OU-1) at the US Department of Energy (DOE) Mound, Ohio, Site. EA uses active engineering solutions to alter the target site so that the contaminant plume will passively stabilize and shrink. For OU-1, the EA was implemented by targeted injection of an electron donor (vegetable oil) to create 'structured geochemical zones'. Volatile organic compounds (VOCs) in the altered subsurface system encounter alternating anaerobic and aerobic environments along the plume flow path. The effect of these structured geochemical zones is effective and rapid degradation of parent compounds such as trichloroethene (TCE) and tetrachloroethene (PCE), and daughter compounds such as cis-1,2-dichloroethene and vinyl chloride. EA at Mound OU-1 provides a transition to natural attenuation and is an alternative to the baseline pump-and-treat (P and T) system. Industrial solvents (primarily TCE) and other VOCs that originated from the former solid-waste landfill contaminated the groundwater in the Buried Valley Aquifer beneath the Mound site. A groundwater P and T system was initiated in 1996 to control the plume, and a soil vapor extraction system was installed and operated from 1997 to 2003 to remove the bulk of the VOC sources from the vadose zone. Physical removal of the landfill waste and contaminated soil was performed between 2006 and 2010. Approximately 76,100 cubic meters (99,500 cubic yards) of material were removed from the OU-1 landfill area. Operation of the groundwater P and T system continued throughout this period. The principles and technical basis of the ongoing EA field demonstration were developed by the Interstate Technology and Regulatory Council. The goal of the EA implementation is to provide a bridge between active groundwater treatments and monitored natural attenuation. EA relies on understanding and manipulating the contaminant mass balance. Technologies are applied to sustainably reduce the contaminant loading from the source and/or increase the rate of natural attenuation processes within the plume. In 2014, a core team that included DOE, the US Environmental Protection Agency (EPA), the Ohio EPA, and technical support organizations evaluated remedial options for OU-1. During the 2014 evaluation, the team projected a cleanup time frame for the baseline P and T system of 26 additional years and a cleanup time frame for the EA remedy of 13 years. On the basis of that evaluation, EPA approved the implementation of the EA remedy that required the shutdown of the P and T system. The combination of technologies implemented for OU-1 EA included (a) neat vegetable oil in the vadose zone in the former landfill and (b) emulsified vegetable oil within the footprint of the groundwater plume. In the first part of the deployment, neat oil spreads laterally and forms a thin layer on the water table beneath residual soil sources to intercept and reduce future VOC loading and to reduce oxygen inputs to the local groundwater. In the second part of the deployment, emulsified oil forms active bioremediation anaerobic treatment zones within the plume footprint to degrade existing groundwater contaminants (via reductive dechlorination, co-metabolism, or both) and stimulates long-term attenuation capacity in the down-gradient aerobic plume (via co-metabolism). The results from the first year of the field demonstration indicate that the dissolved TCE and PCE plumes have decreased in size and mass. Statistical tests indicate that the VOC concentrations in the majority of the source-area wells are decreasing. The VOC concentrations throughout the plume are projected to be below the target maximum contaminant level of 2 to 5 μg/L within 5 to 10 years-sooner than the design projection of 13 years. The biogeochemistry and microbial community within the structured geochemical zones are consistent with the design and appear to be stable. At Mound OU-1, EA has accelerated progress toward the remedial action objectives and reduced costs. Ongoing monitoring will determine whether the EA remedy has transitioned the site into monitored natural attenuation status and whether the EA will continue to be effective, timely, and sustainable. (authors)

12 MANAGEMENT OF RADIOACTIVE AND NON-RADIOACTIVE W↗
DOE OSTI2024

Anode Upcycling via Tailored Solvent Treatment

To achieve a truly closed-loop direct recycling process for lithium-ion batteries, all component materials must be recovered. To date, direct recycling method development has primarily focused on the high-value transition-metal cathode materials, while the inherently lower-value graphite has been challenging to recover in a cost-effective manner. However, end-of-life graphite contains a unique engineered value due to the presence of the solid electrolyte interphase (SEI). Growth of the SEI during the cell's active lifetime stabilizes the electronically reactive graphite surface through an irreversible consumption of Li, and thus necessitates both excess lithiation of the cathode and a costly and time-intensive formation procedure during manufacturing. An optimized pre-formed SEI that capitalizes on existing SEI components from end-of-life batteries has the potential to significantly reduce cathode lithiation requirements and eliminate the critical bottleneck of formation cycling during cell remanufacturing. Further, retaining Li at the anode obviates the need for a separate Li leaching and recovery step, improving the overall efficiency of the direct recycling line. In this work, we present a novel approach to "upcycling" spent graphite through use of tailored chemical treatment to remove adverse (i.e., highly resistive and/or poorly passivating) SEI species while retaining beneficially passivating components. We have explored a rational set of solvents spanning a range of polarity, proticity, and molecular size to evaluate structure-property-performance relationships between applied solvent(s), removed and remaining SEI species, and electrochemical response of the resulting graphite product. Further, we have developed and optimized a robust and holistic analysis procedure that couples symmetric-cell electrochemical testing, multi-modal materials characterization, and advanced electrochemical modeling. These analysis results inform a set of correlative metrics for graphite performance relative to both solvent properties and upcycled SEI composition. We demonstrate effective tunability in the residual SEI composition by varying solvent identity and concentration, and report on several promising solvent systems that achieve comparable or performance to pristine graphite.

anode recycling↗
NASA NTRS2012

Aquarius Main Structure Configuration

The Aquarius/SAC-D Observatory is a joint US-Argentine mission to map the salinity at the ocean surface. This information is critical to improving our understanding of two major components of Earth's climate system - the water cycle and ocean circulation. By measuring ocean salinity from space, the Aquarius/SAC-D Mission will provide new insights into how the massive natural exchange of freshwater between the ocean, atmosphere and sea ice influences ocean circulation, weather and climate. Aquarius is the primary instrument on the SAC-D spacecraft. It consists of a Passive Microwave Radiometer to detect the surface emission that is used to obtain salinity and an Active Scatterometer to measure the ocean waves that affect the precision of the salinity measurement. The Aquarius Primary Structure houses instrument electronics, feed assemblies, and supports a deployable boom with a 2.5 m Reflector, and provides the structural interface to the SAC-D Spacecraft. The key challenge for the Aquarius main structure configuration is to satisfy the needs of component accommodations, ensuring that the instrument can meet all operational, pointing, environmental, and launch vehicle requirements. This paper describes the evolution of the Aquarius main structure configuration, the challenges of balancing the conflicting requirements, and the major configuration driving decisions and compromises.

Eremenko, Alexander↗
DOE OSTI2020

Controlling the corrosion resistance of multi-principal element alloys

Multi-principal element alloys (MPEAs) offer the possibility of many degrees of freedom in the choice of alloying elements to produce either single phase solid solutions or more complex multiphase microstructures. Large ranges of material properties have been observed for MPEAs and mastery of the selection of elements and their compositions can enable novel combinations of properties not possible in traditional alloys. From the aqueous corrosion perspective, optimization of phase stability, control of heterogeneities, passive film identity and its protectiveness, as well as substrate properties such as metal-metal bond strength and activation energy associated with dissolution, can all be controlling factors governed by alloy composition and structure. These factors can mediate the electrochemical reactions controlling spontaneous corrosion. The quest for superior properties based on well-informed element choice is suggested as a path forward guiding MPEA formulations for corrosion performance. However, gaps in fundamental knowledge exist regarding (a) the specific functions of each element, (b) the behavior of elements in unusual combinations, and (c) the formation of complex protective oxides. These issues currently hold back progress in optimization of corrosion properties.

Scully, John R.↗
NASA NTRS2010

Enhancements to the NASA/Goddard Space Flight Center (GSFC) Space Environment Simulator (SES) Facility to Support Cryogenic Testing of the James Webb Space Telescope (JWST) Integrated Science Instrument Module (ISIM)

NASA is the mission lead for the James Webb Space Telescope (JWST), the next of the "Great Observatories", scheduled for launch in 2014. It is directly responsible for the integration and test of the Integrated Science Instrument Module (ISIM), which includes a composite truss structure provided by NASA, and four science instruments sponsored and provided by NASA, the European Space Agency (ESA), the Canadian Space Agency (CSA), and the European Consortium (EC). Three of the four instruments are passively cooled and designed to operate at temperatures in the 36K to 40K range, and the fourth instrument is actively cooled to approximately 6K. The ISIM will undergo several performance tests at various levels of integration in the NASA Goddard Space Flight Center's (GSFC) Space Environment Simulator (SES), GSFC's largest thermal vacuum chamber. These activities range from Cryo-cycling the bare flight composite structure to thermal balance and performance testing of the full ISIM module. This paper describes the enhancements made to the SES chamber in order to support all cryogenic thermal vacuum testing of the ISIM. Upgrades discussed include: design and fabrication of a very large, removable and reconfigurable helium shroud; a new valve box permitting independent flow control of gaseous helium (GHe) to up to ten zones; and development of in-situ 3-dimensional photogrammetry capability in a cryogenic environment. Also presented will be select results from several facility tests already conducted to verify the chamber capabilities and optimize operational procedures, including the Helium Shroud -03 Configuration Acceptance Test, and the Helium Shroud -01 Configuration Chamber Certification Test.

Cleveland, Paul↗
DOE OSTI2018

Effect of Material Structure on Photoluminescence of ZnO/MgO Core-Shell Nanowires

Zinc oxide (ZnO) nanowires are widely studied for use in ultraviolet optoelectronic devices, such as nanolasers and sensors. Nanowires (NWs) with an MgO shell exhibit enhanced band-edge photoluminescence (PL), a result previously attributed to passivation of ZnO defects. However, we find that processing the ZnO NWs under low oxygen partial pressure leads to an MgO-thickness-dependent PL enhancement owing to the formation of optical cavity modes. Conversely, processing under higher oxygen partial pressure leads to NWs that support neither mode formation nor band-edge PL enhancement. High-resolution electron microscopy and density-functional calculations implicate the ZnO m-plane surface morphology as the key determinant of core-shell structure and cavity-mode optics. A ZnO surface with atomic steps along the m-plane in the c-axis direction stimulates the growth of a smooth MgO shell that supports guided-wave optical modes and enhanced UV PL. On the other hand, a smoother ZnO surface leads to nucleation of a rough cladding layer which supports neither enhanced UV PL nor optical cavity modes. Finite-element analysis shows a clear correlation between allowed Fabry-Perot and whispering gallery modes and enhanced UV-PL. Finally, these results point the way to fabricating ZnO/MgO core-shell nanowires for more efficient UV nanolasers, scintillators, and sensors.

77 NANOSCIENCE AND NANOTECHNOLOGY↗