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At least 1,153 records · Page 64
All sourcesNASA NTRSDOE OSTI
DOE OSTI2019

Coherent order parameter dynamics in SmTe 3

We present ultrafast optical pump-probe and ultrafast x-ray diffraction measurements of the charge density wave dynamics in SmTe3 at 300 K. We performed ultrafast x-ray diffraction measurements at the Linac Coherent Light Source to directly probe the dynamics of the finite-wave-vector order parameter. The dynamics reveal coherent oscillations at ~1.6 THz that become overdamped with increasing fluence. We identify this oscillation with the lattice component of the amplitude mode. Furthermore, our data allow for a clear identification of the amplitude mode frequency in the optical pump-probe data. In both measurements, the system reaches the symmetric phase at high fluence, where the order parameter vanishes and the response (reflectivity and x-ray intensity) is quadratic in the order parameter. This is observed in the x-ray diffraction as a small overdamped modulation near zero intensity. Similar overdamped features are observed in the optical reflectivity at high fluence. In conclusion, a time-dependent Ginzburg-Landau model captures qualitatively the essential features of the experimental observations.

36 MATERIALS SCIENCE↗
DOE OSTI2016

Evolution of the substructure of a novel 12% Cr steel under creep conditions

In this work we study the microstruture evolution of a newly developed 12% Cr martensitic/ferritic steel in as-received condition and after creep at 650 °C under 130 MPa and 80 MPa. The microstructure is described as consisting of mobile dislocations, dipole dislocations, boundary dislocations, precipitates, lath boundaries, block boundaries, packet boundaries and prior austenitic grain boundaries. The material is characterized employing light optical microscopy (LOM), scanning electron microscopy (SEM), transmission electron microscopy (TEM), X-ray diffraction (XRD) and electron backscatter diffraction (EBSD). TEM is used to characterize the dislocations (mobile + dipole) inside the subgrains and XRD measurements are used to the characterize mobile dislocations. Based on the subgrain boundary misorientations obtained from EBSD measurements, the boundary dislocation density is estimated. The total dislocation density is estimated for the as-received and crept conditions adding the mobile, boundary and dipole dislocation densities. Additionally, the subgrain size is estimated from the EBSD measurements. In this publication we propose the use of three characterization techniques TEM, XRD and EBSD as necessary to characterize all type of dislocations and quantify the total dislocation densty in martensitic/ferritic steels. - Highlights: • Creep properties of a novel 12% Cr steel alloyed with Ta • Experimental characterization of different types of dislocations: mobile, dipole and boundary • Characterization and interpretation of the substructure evolution using unique combination of TEM, XRD and EBSD.

36 MATERIALS SCIENCE↗
NASA NTRS1982

Tolerance analysis of optical telescopes using coherent addition of wavefront errors

A near diffraction-limited telescope requires that tolerance analysis be done on the basis of system wavefront error. One method of analyzing the wavefront error is to represent the wavefront error function in terms of its Zernike polynomial expansion. A Ramsey-Korsch ray trace package, a computer program that simulates the tracing of rays through an optical telescope system, was expanded to include the Zernike polynomial expansion up through the fifth-order spherical term. An option to determine a 3 dimensional plot of the wavefront error function was also included in the Ramsey-Korsch package. Several assimulation runs were analyzed to determine the particular set of coefficients in the Zernike expansion that are effected by various errors such as tilt, decenter and despace. A 3 dimensional plot of each error up through the fifth-order spherical term was also included in the study. Tolerance analysis data are presented.

Davenport, J. W.↗
DOE OSTI2019

Co doping effect on structural and optical properties of nickel oxide (NiO) thin films via spray pyrolysis

Undoped and cobalt doped nickel oxide thin films (Co:NiO) at different doping concentrations were deposited on a glass substrate at constant substrate temperature by spray pyrolysis. The doping percentage increased from 0 to 10% and the effects of doping content on structural, morphological and optical properties were explored by X-ray diffraction, atomic force microscopy and UV–visible spectroscopy, respectively. X-ray diffraction configurations proved the NiO thin films were polycrystalline in nature having a cubic crystal structure. The regularly used parameters such as crystallite size, micro-strain, dislocation density and texture coefficient are presented from structural data. The average crystallite size is found between 10 and 14 nm with cobalt doping (Co) concentration. The band gap energies were increased with the effect of Co doping concentration in the range between 2.10 and 2.50 eV. The various optical constants as a function of photon energy are modified with Co doping concentration.

77 NANOSCIENCE AND NANOTECHNOLOGY↗
DOE OSTI2016

Direct and real time probe of photoinduced structure transition in colossal magnetoresistive material

Here, we report a direct and real time measurement of photoinduced structure phase transition in single crystal La 0.84 Sr 0.16 MnO 3 using femtosecond electron diffraction. The melting of orthorhombic lattice ordering under femtosecond optical excitation is found involving two distinct processes with different time scales, an initial fast melting of orthorhombic phase in about 4 ps and a subsequent slower transformation in 90 ps and longer timescales. Furthermore, the fast process is designated as the initial melting of orthorhombic phase induced by the Mn-O bond change that is most likely driven by the quenching of the dynamic Jahn-Teller distortion following the photo-excitation. We attribute the slow process to the growing of newly formed structure domain from the photo-excited sites to the neighboring non-excited orthorhombic sites.

75 CONDENSED MATTER PHYSICS, SUPERCONDUCTIVITY AND↗
DOE OSTI2015

C ion-implanted TiO{sub 2} thin film for photocatalytic applications

Third-generation TiO{sub 2} photocatalysts were prepared by implantation of C{sup +} ions into 110 nm thick TiO{sub 2} films. An accurate structural investigation was performed by Rutherford backscattering spectrometry, secondary ion mass spectrometry, X-ray diffraction, Raman-luminescence spectroscopy, and UV/VIS optical characterization. The C doping locally modified the TiO{sub 2} pure films, lowering the band-gap energy from 3.3 eV to a value of 1.8 eV, making the material sensitive to visible light. The synthesized materials are photocatalytically active in the degradation of organic compounds in water under both UV and visible light irradiation, without the help of any additional thermal treatment. These results increase the understanding of the C-doped titanium dioxide, helpful for future environmental applications.

36 MATERIALS SCIENCE↗
DOE OSTI2019

Measurement Error of Interferometers with Diffraction Reference Wave

An experimental setup and results on aberration of sources of a reference spherical wave (SRSW) based on a single-mode optical fiber with a subwavelength output aperture obtained with the aid of an optical part of recording system (OPRS) are presented. SRSW and OPRS are developed for referenceless interferometer with diffraction reference wave. Methods for minimization of the measurement error are proposed. The SRSW and OPRS provide subnanometer measurement accuracy for optics. An increase in the measurement accuracy of the interferometer to a picometer level is discussed.

46 INSTRUMENTATION RELATED TO NUCLEAR SCIENCE AND ↗
DOE OSTI2014

Observation of mid-infrared intersubband absorption in non-polar m-plane AlGaN/GaN multiple quantum wells

Mid-infrared (4.20–4.84 μm) intersubband absorption in non-polar m-plane Al{sub 0.5}Ga{sub 0.5}N/GaN multiple-quantum wells is observed at room temperature. 10 period Al{sub 0.5}Ga{sub 0.5}N/GaN multiple-quantum wells were grown on free-standing m-plane GaN substrates by metalorganic chemical vapor deposition (MOCVD), and the high-quality structural and optical properties are revealed by x-ray diffraction and photoluminescence studies. Through this we have demonstrated that MOCVD grown non-polar m-plane AlGaN/GaN quantum wells are a promising material for mid-infrared intersubband devices.

77 NANOSCIENCE AND NANOTECHNOLOGY↗
DOE OSTI2019

Preparation and Studies of Thin Films of Cu-doped GdSr{sub 2}RuCu{sub 2}O{sub 8}

Preparation of superconducting thin films of the Cu-doped Ruthenocuprate superconductor GdSr{sub 2}Ru{sub 0.9}Cu{sub 2.1}O{sub 8} has been attempted by pulsed laser deposition method. Thin films were deposited on different substrates employing different laser ablation parameters with the idea of obtaining good-quality films which exhibit superconductivity. The crystal structure and morphology of the thin films were characterized by X-ray diffraction and scanning electron microscopy measurements and optical characteristics by Raman scattering measurements. High-temperature ex situ oxygen annealing led to the formation of homogeneous films with the occurrence of an onset of superconductivity, traced by electrical resistivity measurements. Increasing the annealing time has led to a systematic improvement in the sample quality and the physical properties. However, prolonged high-temperature annealing seems to cause deterioration in properties as seen from electrical resistivity and Raman scattering measurements. The studies reveal the importance of an optimal high-temperature oxygen annealing procedure to induce superconductivity in thin films of this Ruthenocuprate system.

75 CONDENSED MATTER PHYSICS, SUPERCONDUCTIVITY AND↗
NASA NTRS2016

High-Performance Reaction Wheel Optimization for Fine-Pointing Space Platforms: Minimizing Induced Vibration Effects on Jitter Performance plus Lessons Learned from Hubble Space Telescope for Current and Future Spacecraft Applications

The Hubble Space Telescope (HST) applies large-diameter optics (2.5-m primary mirror) for diffraction-limited resolution spanning an extended wavelength range (approx. 100-2500 nm). Its Pointing Control System (PCS) Reaction Wheel Assemblies (RWAs), in the Support Systems Module (SSM), acquired an unprecedented set of high-sensitivity Induced Vibration (IV) data for 5 flight-certified RWAs: dwelling at set rotation rates. Focused on 4 key ratios, force and moment harmonic values (in 3 local principal directions) are extracted in the RWA operating range (0-3000 RPM). The IV test data, obtained under ambient lab conditions, are investigated in detail, evaluated, compiled, and curve-fitted; variational trends, core causes, and unforeseen anomalies are addressed. In aggregate, these values constitute a statistically-valid basis to quantify ground test-to-test variations and facilitate extrapolations to on-orbit conditions. Accumulated knowledge of bearing-rotor vibrational sources, corresponding harmonic contributions, and salient elements of IV key variability factors are discussed. An evolved methodology is presented for absolute assessments and relative comparisons of macro-level IV signal magnitude due to micro-level construction-assembly geometric details/imperfections stemming from both electrical drive and primary bearing design parameters. Based upon studies of same-size/similar-design momentum wheels' IV changes, upper estimates due to transitions from ground tests to orbital conditions are derived. Recommended HST RWA choices are discussed relative to system optimization/tradeoffs of Line-Of-Sight (LOS) vector-pointing focal-plane error driven by higher IV transmissibilities through low-damped structural dynamics that stimulate optical elements. Unique analytical disturbance results for orbital HST accelerations are described applicable to microgravity efforts. Conclusions, lessons learned, historical context/insights, and perspectives on future applications are given; these previously unpublished data and findings represents a valuable resource for fine-pointing spacecraft or space-based platforms using RWAs, Control Moment Gyros (CMGs), Momentum Wheels, or other ball-bearing-based rotational units.

Hasha, Martin D.↗
DOE OSTI2019

Microstructural, optical and electrical properties of CdS thin films grown by spray pyrolysis technique as a function of substrate temperature

In this research, nanocrystalline cadmium sulfide thin films were produced by the spray pyrolysis technique on glass substrates. The effects of substrate temperature in the range 400–550 °C on the structural, morphological, optical, and electrical properties of the thin films were investigated. The thin films have been characterized by investigating their X-ray diffraction, field emission scanning electron microscope (FE-SEM), and optical absorption (UV–Vis) measurements. X-ray analysis revealed that thin films were a polycrystalline structure with the hexagonal phase in all cases and by increasing in substrate temperature, crystallite size decreases, and dislocation density increases. The FE-SEM images showed that the surface of the thin films is uniform, homogeneous and without cracks. The average sizes of the grains are at the range of 210–235 nm. The obtained values for optical band gap have been in the range of 2.18–2.41 eV, where the value of optical band gap for the thin films decreases by increasing substrate temperature. The Urbach energies of the thin films increase as the substrate temperature is increased. When substrate temperature increased from 400 to 550 °C, electrical resistivity increased from 531 to 2817 Ω cm, carrier concentration decreased from 15.96 × 10{sup 14} to 3.71 × 10{sup 14} cm{sup −3}, Hall mobility decreased from 7.37 to 5.98 cm{sup 2}/V s. Hall effect analysis indicated that the thin films exhibited n-type conductivity.

77 NANOSCIENCE AND NANOTECHNOLOGY↗
NASA NTRS2015

Prototype Imaging Spectrograph for Coronagraphic Exoplanet Studies (PISCES) for WFIRST-AFTA

Prototype Imaging Spectrograph for Coronagraphic Exoplanet Studies (PISCES) is a lenslet array based integral field spectrometer (IFS) designed for high contrast imaging of extrasolar planets. PISCES will be used to advance the technology readiness of the high contrast IFS baselined on the Wide-Field InfraRed Survey Telescope/Astrophysics Focused Telescope Assets (WFIRST-AFTA) coronagraph instrument. PISCES will be integrated into the high contrast imaging testbed (HCIT) at the Jet Propulsion Laboratory (JPL) and will work with both the Hybrid Lyot Coronagraph (HLC) and the Shaped Pupil Coronagraph (SPC) configurations. We discuss why the lenslet array based IFS was selected for PISCES. We present the PISCES optical design, including the similarities and differences of lenslet based IFSs to normal spectrometers, the trade-off between a refractive design and reflective design, as well as the specific function of our pinhole mask on the back surface of the lenslet array to reduce the diffraction from the edge of the lenslets. The optical analysis, alignment plan, and mechanical design of the instrument will be discussed.

Wide-Field InfraRed Survey Telescope Astrophysics ↗
DOE OSTI2022

Super-resolution image display using diffractive decoders

High-resolution image projection over a large field of view (FOV) is hindered by the restricted space-bandwidth product (SBP) of wavefront modulators. We report a deep learning–enabled diffractive display based on a jointly trained pair of an electronic encoder and a diffractive decoder to synthesize/project super-resolved images using low-resolution wavefront modulators. The digital encoder rapidly preprocesses the high-resolution images so that their spatial information is encoded into low-resolution patterns, projected via a low SBP wavefront modulator. The diffractive decoder processes these low-resolution patterns using transmissive layers structured using deep learning to all-optically synthesize/project super-resolved images at its output FOV. This diffractive image display can achieve a super-resolution factor of ~4, increasing the SBP by ~16-fold. We experimentally validate its success using 3D-printed diffractive decoders that operate at the terahertz spectrum. This diffractive image decoder can be scaled to operate at visible wavelengths and used to design large SBP displays that are compact, low power, and computationally efficient.

36 MATERIALS SCIENCE↗
NASA NTRS1993

HiRES - High Resolution Extreme Ultraviolet Spectroheliometer toroidal diffraction grating performance evaluation

The ray-tracing results presented characterize the theoretically achievable EUV performance of the HiRES instrument. The effects of optical system misalignment on spectrograph images, and the laboratory results for two f/15 toroidal diffraction gratings that employ a multianode microchannel array, are also presented. Interferometric studies of toroidal figure accuracy, as well as optical and electron microscopy investigations of surface quality, are discussed. While the current toroidal gratings are noted to furnish good imaging across a wide wavelength range, they exhibit excessive EUV scatter, as well as spectral ghosting.

Berger, Thomas E.↗
DOE OSTI2018

Structural and Mechanical Properties of Zr-Si-N Coatings Deposited by Arc Evaporation at Different Substrate Bias Voltages

ZrN and Zr-Si-N coatings were formed using vacuum-arc plasma fluxes deposition system at the substrate bias voltage (U{sub B}) ranged from − 50 to − 220 V on HS6-5-2 steel substrates. The structural, mechanical and tribological properties were characterized using x-ray diffraction, atomic force microscopy, scanning electron microscopy, optical microscopy, nanoindentation and ball-on-disk test. The surface roughness parameter Ra of ZrN coatings is lower than Zr-Si-N coatings. Both roughness Ra of Zr-Si-N coatings and the number of surface defects with mainly small dimensions to 1 µm decrease with increasing negative substrate bias voltage. The addition of silicon to ZrN significantly reduces the crystallite size, from about 18.3 nm for ZrN coating to 6.4 nm for Zr-Si-N coating both deposited at the same U{sub B} = − 100 V and 7.8 nm for U{sub B} = − 150 V. The hardness of Zr-Si-N coatings increases to about 30 GPa with the increase in negative substrate bias voltage (U{sub B} = − 220 V). Adhesion of the coatings tested is high, and critical load is above 80 N and reduces with U{sub B} increase. Coefficient of friction determined using AFM shows similar trend as surface roughness in microscale.

36 MATERIALS SCIENCE↗
NASA NTRS1974

Diffraction by a perfectly conducting rectangular cylinder which is illuminated by an array of line sources

The geometrical theory of diffraction (GTD) is employed to analyze the radiation from a perfectly-conducting rectangular cylinder illuminated by an array of line sources. The excitation of the cylinder by a single electric or magnetic current line source is considered first, and a solution which includes contributions from the geometrical optics rays and all singly- and doubly-diffracted rays is obtained. A new diffraction coefficient valid in the transition regions of the shadow and reflection boundaries is employed to obtain a continuous total field, except for negligible discontinuities in the doubly-diffracted field at its shadow boundaries. Patterns calculated by the GTD method are found to be in excellent agreement with those calculated from an integral equation formulation. Using superposition the solution for array or aperture excitation of the rectangular cylinder is obtained. A computer program for this solution is included.

Kouyoumjian, R. G.↗
NASA NTRS1994

A comparison between using incoherent or coherent sources to align and test an adaptive optical telescope

The concept in the initial alignment of the segmented mirror adaptive optics telescope called the phased array mirror extendable large aperture telescope (Pamela) is to produce an optical transfer function (OTF) which closely approximates the diffraction limited value which would correspond to a system pupil function that is unity over the aperture and zero outside. There are differences in the theory of intensity measurements between coherent and incoherent radiation. As a result, some of the classical quantities which describe the performance of an optical system for incoherent radiation can not be defined for a coherent field. The most important quantity describing the quality of an optical system is the OTF and for a coherent source the OTF is not defined. Instead a coherent transfer function (CTF) is defined. The main conclusion of the paper is that an incoherent collimated source and not a collimated laser source is preferred to calibrate the Hartmann wavefront sensor (WFS) of an aligned adaptive optical system. A distant laser source can be used with minimum problems to correct the system for atmospheric turbulence. The collimation of the HeNe laser alignment source can be improved by using a very small pin hole in the spatial filter so only the central portion of the beam is transmitted and the beam from the filter is nearly constant in amplitude. The size of this pin hole will be limited by the sensitivity of the lateral effect diode (LEDD) elements.

Anderson, Richard↗
DOE OSTI2016

DSC and optical studies on BaO-Li{sub 2}O-B{sub 2}O{sub 3}-CuO glass system

Glasses with composition 15BaO-25Li{sub 2}O-(60-x)B{sub 2}O{sub 3} -xCuO (x= 0, 0.2, 0.4, 0.6, 0.8 and 1 mol%) were prepared by the conventional melt quenching technique. These glasses were characterized using X-ray diffraction (XRD), differential scanning calorimetry (DSC) and density measurements. Optical absorption studies were carried out as a function of copper ion concentration. The optical absorption spectra of studied glasses containing copper oxide exhibit a single broad band around 761nm which has been assigned to the 2B{sub 1g}→2B{sub 2g} transition. From these studies, the variations in the values of glass transition temperature (T{sub g}) have been observed. The fundamental absorption edge has been determined from the optical absorption spectra. The values of optical band gap and Urbach energy were determined with increase in concentration of CuO. The variations in density, glass transition temperature, optical band gap and Urbach energy with CuO content have been discussed in terms of changes in the glass structure. The analysis of these results indicated that copper ions mostly exist in Cu{sup 2+} state in these glasses when the concentration of CuO ≤ 0.8 mol% and above this concentration copper ions seem to subsist in Cu{sup 1+} state.

75 CONDENSED MATTER PHYSICS, SUPERCONDUCTIVITY AND↗