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At least 1,153 records · Page 64
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NASA NTRS1977

Drop dynamics in space

Experiments to study the dynamics of liquid drops are being planned to be performed in the weightless environment of Spacelab. The liquids will range from superfluid helium through ordinary liquid to molten metals and glasses. The experiments will be conducted in a chamber now being developed which utilizes the forces and torques produced by acoustic waves excited within the chamber. None of the currently available facilities (drop towers, sounding rockets, or zero-g aircraft flights) can provide a sustained weightless environment, since the resulting zero-g periods are from 3 sec to 5 min. Spaceflight, however, will provide weightlessness for periods of one week, or more, allowing truly laboratory-like experiments to be conducted on free liquid drops and bubbles. In this paper we discuss both the drop dynamics experiments proposed for Spacelab and the acoustic chamber: its operation and current testing for these and other experiments.

Wang, T. G.↗
NASA NTRS1981

Combustion experiments in a zero-gravity laboratory

One of the payloads that the Shuttle will carry into low-earth orbit is the Spacelab, a laboratory designed by a European consortium which will enable scientist-astronauts to conduct research in a shirt-sleeve environment. The typical flight of seven days will permit numerous experiments to be conducted that take advantage of long-term reduced gravity. A description is presented of plans for the conduction of Spacelab experiments which are related to the study of combustion, taking into account also investigations performed in the preparation of such experiments. Attention is given to an overview study of combustion experiments in a space laboratory, droplet burning, flammability limits in a standard tube, the combustion of particle clouds, smoldering combustion in porous fuels, liquid pool burning, and combustion experimentation aboard the space transportation system.

Cochran, T. H.↗
NASA NTRSDate not supplied

Performance of a broad-band, high-resolution, transition-edge sensor spectrometer for x-ray astrophysics

Future x-ray astrophysics experiments require multiplexed readout of high-fill-factor, kilo-pixel arrays of transition-edge sensors (TESs), with very high spectral resolution over a broad range of energies. In this paper we report on a prototype kilo pixel array of Mo/Au TESs read out with 8-column by 32-row time-division multiplexing (TDM). This system is being used to demonstrate the critical detector and readout technology for ESA’s Athena X-IFU, and when complete will used to laboratory astrophysics experiments. Our array and TDM readout has demonstrated a combined energy resolution, including > 200 pixels, of: 1.95 eV for Ti-K (4.5 keV), 1.97 eV for Mn-K (5.9 keV), 2.16 eV for Co-Kα (6.9 keV), 2.33 eV for Cu-Kα (8 keV), 3.26 eV for Br-Kα (11.9 keV). The 1 sigma error is  0.01 eV for all spectra. These results meet the broad-band resolution requirements for X-IFU.

Stephen J. Smith↗
NASA NTRS2021

Performance of a broad-band, high-resolution, transition-edge sensor spectrometer for X-ray astrophysics

Future X-ray astrophysics experiments require multiplexed readout of high fill-factor, kilo-pixel arrays of transition-edge sensors (TESs), with very high spectral resolution over a broad range of energies. In this paper we report on a prototype kilo-pixel array of Mo/Au TESs readout with 8-column by 32-row time-division multiplexing (TDM). This system is being used to demonstrate the critical detector and readout technology for ESA’s Athena X-IFU, and when complete will be used in laboratory astrophysics experiments. Our array and TDM readout have demonstrated a combined full-width-at-half-maximum energy resolution, including >200 pixels, of:1.95 eV for Ti-Ka(4.5 keV), 1.97eV for Mn-Ka(5.9 keV), 2.16 eV for Co-Kα(6.9 keV),2.33 eV for Cu-Kα(8 keV), 3.26 eV for Br-Kα(11.9 keV). The 1 sigma statistical errorsare£0.01 eV for all spectra. These results meet the broad-band resolution requirements for X-IFU with margin.

S J Smith↗
NASA NTRS2016

Performing Mineral Hydration Experiments in the CheMin Diffractometer on Mars

Laboratory work is the cornerstone of experimental planetary geochemistry, mineralogy, and petrology, but much is to be gained by "experiments" while on a planet surface. Earth-bound experiments are often limited in ability to control multiple conditions relevant to planetary bodies (e.g. cycles in temperature and vapor pressure of water), but observations on-planet provide a unique opportunity where conditions are native to the planet and those affected by sampling and analysis can be constrained. The CheMin XRD instrument on Mars Science Laboratory has been able to test mineral hydration in samples held for up to 300 Mars days (sols). Clay minerals sampled at Yellowknife Bay early in the mission had both collapsed (10 Å) and expanded (13.2 Å) basal spacing. Collapsed interlayers were expected, but larger spacing was not; it was uncertain whether larger basal spacing would collapse on prolonged exposure to warmer conditions inside CheMin. Observation over several hundred sols showed no collapse, with the conclusion that expanded interlayer spacing was due to partial intercalation by metal-hydroxyl groups that resist dehydration. More recently, a sample of the Murray Formation, Oudam, provided the first XRD detection of gypsum and a chance to observe gypsum stability. Laboratory work suggests gypsum should be stable at Mars surface conditions, and indeed gypsum has been observed from orbit at higher latitudes and in thick veins at Yellowknife Bay by Mastcam reflectance spectra. Laboratory experiments have shown that on dehydration the gypsum would not become X-ray amorphous but would rather transform to a water-deficient bassanite structure. Over a period of 37 sols, it was observed that the Oudam sample in CheMin transformed from an assemblage of gypsum+anhydrite, to gypsum+bassanite+anhydrite, and finally to bassanite+anhydrite. Mg-sulfates were also anticipated but have not been observed in CheMin despite chemical evidence for their presence. Unlike gypsum, hydrated Mg-sulfates can transition to an X-ray amorphous form. Crystalline Mg-sulfates are expected higher in the section on Mount Sharp, where it should be possible to determine whether they persist or are destabilized after sampling, providing further insight into hydrous mineral stability at Mars near-equatorial conditions.

Vaniman, D. T.↗
NASA NTRS2018

Photochemical Haze Formation in the Atmospheres of Super-Earths and Mini-Neptunes

UV (ultraviolet) radiation can induce photochemical processes in the atmospheres of exoplanet and produce haze particles. Recent transmission spectra of super-Earths and mini-Neptunes have demonstrated the possibility that exoplanets have haze/cloud layers at high altitudes in their atmospheres. Haze particles play an important role in planetary atmospheres because they affect the chemistry, dynamics, and radiation flux in planetary atmospheres, and may provide a source of organic material to the surface which may impact the origin or evolution of life. However, very little information is known about photochemical processes in cool, high-metallicity exoplanetary atmospheres. We present here photochemical haze formation in laboratory simulation experiments with UV radiation; we explored temperatures ranging from 300 to 600 degrees Kelvin and a range of atmospheric metallicities (100 times, 1000 times, and 10000 times solar metallicity). We find that photochemical hazes are generated in all simulated atmospheres, but the haze production rates appear to be temperature dependent: the particles produced in each metallicity group decrease as the temperature increases. The images taken with an atomic force microscope (AFM) show that the particle size (15 nanometers to 190 nanometers) varies with temperature and metallicity. Our results provide useful laboratory data on the photochemical haze formation and particle properties, which can serve as critical inputs for exoplanet atmosphere modeling, and guide future observations of exoplanets with the Transiting Exoplanet Survey Satellite (TESS), the James Webb Space Telescope (JWST), and the Wide-Field Infrared Survey Telescope (WFIRST).

He, Chao↗
NASA NTRS1989

Solution growth of Triglycine Sulfate (TGS) crystals on the International Microgravity Laboratory (IML-1)

An experiment was planned for the International Microgravity Laboratory (IML-1) to be launched around Feb. 1991. Crystals of triglycine sulfate (TGS) will be grown by low temperature solution crystal growth technique using a multiuser facility called Fluid Experiment System (FES). A special cooled sting technique of solution crystal growth will be used where heat is extracted from the seed crystal through a semi-insulating sting, thereby creating the desired supersaturation near the growing crystal. Also, a holocamera will be used to provide tomography of the three dimensional flow field and particle image displacement velocimetry to monitor the convective flows.

Lal, Ravi B.↗
NASA NTRS2019

Coordinated Analysis of an Experimentally Space Weathered Carbonaceous Chondrite

The surfaces of airless bodies experience solar wind irradiation and micrometeorite impacts, a process collectively known as space weathering. These mechanisms alter the chemical composition, microstructure, and optical properties of surface materials and considerable work has been done to understand this phenomenon in lunar and ordinary chondritic materials. However, ongoing sample return missions Hayabusa2 to asteroid Ryugu and OSIRIS-REx to asteroid Bennu have prompted the need to study the effects of space weathering on hydrated, organic-rich materials, especially in the context of early results. Understanding space weathering of these samples is critical for properly interpreting remote sensing data during asteroid encounters, for sample site selection, and for the eventual study of returned samples. We can better understand space weathering of carbonaceous materials by simulating these processes in the laboratory. Recent experiments have shown that the changes in spectral characteristics of carbonaceous chondrites are not consistent among experiments, suggesting additional work is needed before these results can inform our understanding of spectral variations on asteroidal surfaces. Similarly, substantial work remains to characterize the chemical and microstructural effects of these processes in order to correlate these features with spectral changes. Here, we build on our previous work, presenting new results of the pulsed laser irradiation of the Murchison (CM2) meteorite to simulate micrometeorite impacts and the progressive space weathering of carbonaceous surfaces.

Thompson, M. S.↗
NASA NTRS2017

Influence of Oxychlorine Phases During the Pyrolysis of Organic Molecules: Implications for the Quest of Organics on Mars with the SAM Experiment Onboard the Curiosity Rover

One among the main objectives of the Sample Analysis at Mars (SAM) experiment is the in situ molecular analysis of gases evolving from solid samples heated up to approximately 850 degrees Centigrade, and collected by Curiosity on Mars surface/sub-surface in Gale crater. With this aim, SAM uses a gas-chromatograph coupled to a quadrupole mass spectrometer (GC-QMS) devoted to separate, detect and identify both volatile inorganic and organic compounds. SAM detected chlorinated organic molecules produced in evolved gas analysis (EGA) experiments. Several of these were also detected by the Viking experiments in 1976. SAM also detected oxychlorine compounds that were present at the Phoenix landing site. The oxychlorines may be prevelant over much of the martian surface. The C1 to C3 aliphatic chlorohydrocarbons (chloromethane and di- and trichloromethane) detected by SAM were attributed to reaction products occurring between the oxychlorines phases and the organic compounds coming from SAM instrument background. But SAM also showed the presence of a large excess of chlorobenzene and C2 to C4 dichloroalkanes among the volatile species released by the Cumberland sample of the Sheepbed mudstone. For the first time in the history of the Mars exploration, this proved the presence of Mars indigenous organic material at the Mars' surface. However, the identification of the precursor organic compounds of these chlorohydrocarbons is difficult due to the complexity of the reactions occurring during the sample pyrolysis. Laboratory pyrolysis experiments have demonstrated that oxychlorines phases such as perchlorates and chlorates, decomposed into dioxygen and volatile chlorine bearing molecules (HCl and/or Cl2) during the pyrolysis. These chemical species can then react with the organic molecules present in the martian solid samples through oxidation, chlorination and oxychlorination processes.

Millan, M.↗
NASA NTRS2003

Properties of Cusp Diamagnetic Cavities

Progress can be reported in two areas related to characterizing the properties of cusp diamagnetic cavities. Laboratory terrella experiments have been conducted for the purpose of using neutral gas excitation as a tracer of trapped electron populations in the presence of two dipoles that are used to develop a magnetic cusp topology. Figure 1 and 2 show top and side views of two configurations. Dipole trapped electron populations appear as the two luminous annular rings. Other populations are the most intense regions are shown. Interspersed between these regions are narrow regions that represent the topological cusps in these configurations. That they contain luminous gas is evidence for cusp trapping similar to what we believe exists in the terrestrial magnetosphere. The asymmetry of these cusp regions as seen in Figure 1 is the result of a relative tilt between the two dipoles suggestive of what would be expected in space. It is in these regions that particle observations were sought, so as to validate the realization of proposed and laboratory achieved trapping in a diamagnetic cusp. Figure 3 shows particle trajectories in a modeled cusp magnetic topology for three particle energies. Blue, green, and red traces correspond to increasing energies. Due to factors discussed outside of this final report, a thorough exploration of relevant satellite observations have not been achieved.

Sheldon, Robert B.↗
NASA NTRS1979

Laboratory simulations of the pyrolytic release experiments - An interim report

During its operation on Mars the pyrolytic release experiment (PR) detected the fixation of small amounts of CO2 and/or CO. Laboratory simulations of the experimental conditions were made in an attempt to substantiate the previous conclusion that these reactions were chemical rather than biological. After pretreatment and incubation under various conditions, pyrolytic analysis was used to indicate the extent of surface catalyzed conversion of (C-14)O2 or (C-14)O to (C-14)-organic compounds. This abiotic synthesis was detected in experiments with three iron oxides, viz. hematite, magnetite and maghemite. When the incubation atmosphere was supplemented with water vapor, the levels of synthesis were in a range comparable to that detected in the Viking PR tests. An abiotic synthesis was also detected in experiments with a mixture of clays and minerals (Mars analog soil) or with montmorillonite artificially enriched in iron. With either substratum the reaction appeared to be the result of a photocatalytic synthesis of (C-14)-organics from (C-14)O and surface hydroxyl groups. This process was not dependent on the presence of water vapor in the incubation atmosphere. Although a duplication of the Viking data has not been achieved, these findings support the abiotic interpretation of the PR results.

Hubbard, J. S.↗
NASA NTRS2013

Evidence for Perchlorates and the Origin of Chlorinated Hydrocarbons Detected by SAM at the Rocknest Aeolian Deposit in Gale Crater

A single scoop of the Rocknest aeolian deposit was sieved (less than 150 micrometers), and four separate sample portions, each with a mass of approximately 50 mg, were delivered to individual cups inside the Sample Analysis at Mars (SAM) instrument by the Mars Science Laboratory rover's sample acquisition system. The samples were analyzed separately by the SAM pyrolysis evolved gas and gas chromatograph mass spectrometer analysis modes. Several chlorinated hydrocarbons including chloromethane, dichloromethane, trichloromethane, a chloromethylpropene, and chlorobenzene were identified by SAM above background levels with abundances of approximately 0.01 to 2.3 nmol. The evolution of the chloromethanes observed during pyrolysis is coincident with the increase in O2 released from the Rocknest sample and the decomposition of a product of N-methyl-N-(tert-butyldimethylsilyl)-trifluoroacetamide (MTBSTFA), a chemical whose vapors were released from a derivatization cup inside SAM. The best candidate for the oxychlorine compounds in Rocknest is a hydrated calcium perchlorate (Ca(ClO4)2·nH2O), based on the temperature release of O2 that correlates with the release of the chlorinated hydrocarbons measured by SAM, although other chlorine-bearing phases are being considered. Laboratory analog experiments suggest that the reaction of Martian chlorine from perchlorate decomposition with terrestrial organic carbon from MTBSTFA during pyrolysis can explain the presence of three chloromethanes and a chloromethylpropene detected by SAM. Chlorobenzene may be attributed to reactions of Martian chlorine released during pyrolysis with terrestrial benzene or toluene derived from 2,6-diphenylphenylene oxide (Tenax) on the SAM hydrocarbon trap. At this time we do not have definitive evidence to support a nonterrestrial carbon source for these chlorinated hydrocarbons, nor do we exclude the possibility that future SAM analyses will reveal the presence of organic compounds native to the Martian regolith.

sample analysis at mars↗
NASA NTRS2018

Direct Probe of Dark Energy Interactions with a Solar System Laboratory: NASA Innovative Advanced Concepts (NIAC) - Phase 1 Final Report

In this NIAC (NASA Innovative Advanced Concepts) study, we embrace the challenge of direct detection of the galileon dark energy field in the Vainshtein model. We developed a mission concept to directly measure the galileon field using the solar system as a laboratory. The experiment scheme involves precise measurements of the trace of the total scalar force gradient tensor. A tetrahedral constellation off our spacecraft measures the "local" traces while orbiting about 1 AU (Astronomical Unit) away from the Sun and faraway from planets (Figure 1). The trace measurement is insensitive to the much stronger gravity field which satisfies the inverse square law and thus is traceless. Atomic test masses and atom interferometer measurement techniques are used as precise drag-free inertial references while laser ranging interferometers are employed to connect among atom interferometer pairs in spacecraft for the differential gradient force measurements. We conclude that such a mission is scientifically and technologically feasible. We show that a mission of 3-year measurement time would be able to provide high confidence statements (over 3 standard deviations) about the existence and strength of the cubic galileon field of the Sun. In addition, such a mission would also provide rich and diverse scientific data for testing any gravitational theory in general beyond the Newtonian gravity, hunting for ultra-light fields of dark matter, and detecting gravitational waves in the mid-frequency band between those of LIGO (Laser Interferometer Gravitational-Wave Observatory) and LISA (Laser Interferometer Space Antenna). For these reasons, we will term the mission concept Gravity Observation and Dark energy Detection Explorer in the Solar System (GODDESS).

Dark Energy↗
NASA NTRS1966

Sterilization facilities

Clean room assembly and sterilization laboratories for experiments on Voyager capsule, components and modules

STERILIZATION↗
NASA NTRS1972

The effect of phosphorus on the formation of the Widmanstaetten pattern in iron meteorites.

Use of a combination of a revised Fe-Ni-P phase diagram and laboratory cooling experiments on Fe-Ni-P alloys to determine the effect of P on the formation of the Widmanstaetten pattern. From the phase diagram results, two reaction paths were found for the formation of kamacite (1) gamma (taenite) yields alpha (kamacite) + gamma (taenite) and (2) gamma yields gamma + Ph /phosphide, (FeNi)3P/ yields alpha + gamma + Ph. The reaction path gamma yields alpha + gamma is preferred at low P contents, while at higher P contents and at Ni contents greater than 7.0 wt.%, the reaction path gamma yields gamma + Ph yields alpha + gamma + Ph controls the formation of kamacite. Above 7 wt.% Ni, the effect of P on the equilibrium nucleation temperature of kamacite is quite small, less than about plus or minus 30 C with respect to the Fe-Ni binary diagram. The addition of P (greater than 0.1 wt.%) to meteorites promotes nucleation of kamacite at higher temperatures and effectively lowers the amount of undercooling necessary to nucleate kamacite homogeneously. Ni has just the opposite effect, decreasing the temperature of nucleation and increasing the amount of undercooling. It is concluded that significant amounts of undercooling, 50 to 100 C, are necessary for the nucleation of the Widmanstaetten structure in meteorites, and that chemical equilibrium is maintained in the various phases of slowly cooled iron meteorites to 650 C and probably to 600 C.

Goldstein, J. I.↗