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At least 1,135 records · Page 63
All sourcesNASA NTRSDOE OSTI
DOE OSTI2024

Towards Construction of a Novel Nanometer-Resolution MeV-STEM for Imaging Thick Frozen Biological Samples

Driven by life-science applications, a mega-electron-volt Scanning Transmission Electron Microscope (MeV-STEM) has been proposed here to image thick frozen biological samples as a conventional Transmission Electron Microscope (TEM) may not be suitable to image samples thicker than 300–500 nm and various volume electron microscopy (EM) techniques either suffering from low resolution, or low speed. The high penetration of inelastic scattering signals of MeV electrons could make the MeV-STEM an appropriate microscope for biological samples as thick as 10 μm or more with a nanoscale resolution, considering the effect of electron energy, beam broadening, and low-dose limit on resolution. The best resolution is inversely related to the sample thickness and changes from 6 nm to 24 nm when the sample thickness increases from 1 μm to 10 μm. To achieve such a resolution in STEM, the imaging electrons must be focused on the specimen with a nm size and an mrad semi-convergence angle. This requires an electron beam emittance of a few picometers, which is ~1000 times smaller than the presently achieved nm emittance, in conjunction with less than 10 -4 energy spread and 1 nA current. We numerically simulated two different approaches that are potentially applicable to build a compact MeV-STEM instrument: (1) DC (Direct Current) gun, aperture, superconducting radio-frequency (SRF) cavities, and STEM column; (2) SRF gun, aperture, SRF cavities, and STEM column. Beam dynamic simulations show promising results, which meet the needs of an MeV-STEM, a few-picometer emittance, less than 10 -4 energy spread, and 0.1–1 nA current from both options. Also, we designed a compact STEM column based on permanent quadrupole quintuplet, not only to demagnify the beam size from 1 μm at the source point to 2 nm at the specimen but also to provide the freedom of changing the magnifications at the specimen and a scanning system to raster the electron beam across the sample with a step size of 2 nm and the repetition rate of 1 MHz. This makes it possible to build a compact MeV-STEM and use it to study thick, large-volume samples in cell biology.

36 MATERIALS SCIENCE↗
DOE OSTI2016

A Keck adaptive optics survey of a representative sample of gravitationally lensed star-forming galaxies: High spatial resolution studies of kinematics and metallicity gradients

We discuss spatially resolved emission line spectroscopy secured for a total sample of 15 gravitationally lensed star-forming galaxies at a mean redshift of z≃2 based on Keck laser-assisted adaptive optics observations undertaken with the recently improved OSIRIS integral field unit (IFU) spectrograph. By exploiting gravitationally lensed sources drawn primarily from the CASSOWARY survey, we sample these sub-L{sup ∗} galaxies with source-plane resolutions of a few hundred parsecs ensuring well-sampled 2D velocity data and resolved variations in the gas-phase metallicity. Such high spatial resolution data offer a critical check on the structural properties of larger samples derived with coarser sampling using multiple-IFU instruments. We demonstrate how kinematic complexities essential to understanding the maturity of an early star-forming galaxy can often only be revealed with better sampled data. Although we include four sources from our earlier work, the present study provides a more representative sample unbiased with respect to emission line strength. Contrary to earlier suggestions, our data indicate a more diverse range of kinematic and metal gradient behavior inconsistent with a simple picture of well-ordered rotation developing concurrently with established steep metal gradients in all but merging systems. Comparing our observations with the predictions of hydrodynamical simulations suggests that gas and metals have been mixed by outflows or other strong feedback processes, flattening the metal gradients in early star-forming galaxies.

79 ASTRONOMY AND ASTROPHYSICS↗
DOE OSTI2016

ROTATION–ACTIVITY CORRELATIONS IN K AND M DWARFS. I. STELLAR PARAMETERS AND COMPILATIONS OF v sin i AND P /sin i FOR A LARGE SAMPLE OF LATE-K AND M DWARFS

The reliable determination of rotation–activity correlations (RACs) depends on precise measurements of the following stellar parameters: T {sub eff}, parallax, radius, metallicity, and rotational speed v sin i . In this paper, our goal is to focus on the determination of these parameters for a sample of K and M dwarfs. In a future paper (Paper II), we will combine our rotational data with activity data in order to construct RACs. Here, we report on a determination of effective temperatures based on the ( R – I ){sub C} color from the calibrations of Mann et al. and Kenyon and Hartmann for four samples of late-K, dM2, dM3, and dM4 stars. We also determine stellar parameters ( T {sub eff}, log( g ), and [M/H]) using the principal component analysis–based inversion technique for a sample of 105 late-K dwarfs. We compile all effective temperatures from the literature for this sample. We determine empirical radius–[M/H] correlations in our stellar samples. This allows us to propose new effective temperatures, stellar radii, and metallicities for a large sample of 612 late-K and M dwarfs. Our mean radii agree well with those of Boyajian et al. We analyze HARPS and SOPHIE spectra of 105 late-K dwarfs, and we have detected v sin i in 92 stars. In combination with our previous v sin i measurements in M and K dwarfs, we now derive P /sin i measures for a sample of 418 K and M dwarfs. We investigate the distributions of P /sin i , and we show that they are different from one spectral subtype to another at a 99.9% confidence level.

79 ASTRONOMY AND ASTROPHYSICS↗
DOE OSTI2017

The Fraction of Cool-core Clusters in X-Ray versus SZ Samples Using Chandra Observations

We derive and compare the fractions of cool-core clusters in the Planck Early Sunyaev–Zel’dovich sample of 164 clusters with z⩽0.35 and in a flux-limited X-ray sample of 100 clusters with z⩽0.30, using Chandra observations. We use four metrics to identify cool-core clusters: (1) the concentration parameter, which is the ratio of the integrated emissivity profile within 0.15 r {sub 500} to that within r {sub 500}; (2) the ratio of the integrated emissivity profile within 40 kpc to that within 400 kpc; (3) the cuspiness of the gas density profile, which is the negative of the logarithmic derivative of the gas density with respect to the radius, measured at 0.04 r {sub 500}; and (4) the central gas density, measured at 0.01 r {sub 500}. We find that the sample of X-ray-selected clusters, as characterized by each of these metrics, contains a significantly larger fraction of cool-core clusters compared to the sample of SZ-selected clusters (44% ± 7% versus 28% ± 4% using the concentration parameter in the 0.15–1.0 r {sub 500} range, 61% ± 8% versus 36% ± 5% using the concentration parameter in the 40–400 kpc range, 64% ± 8% versus 38% ± 5% using the cuspiness, and 53% ± 7% versus 39 ± 5% using the central gas density). Qualitatively, cool-core clusters are more X-ray luminous at fixed mass. Hence, our X-ray, flux-limited sample, compared to the approximately mass-limited SZ sample, is overrepresented with cool-core clusters. We describe a simple quantitative model that uses the excess luminosity of cool-core clusters compared to non-cool-core clusters at fixed mass to successfully predict the observed fraction of cool-core clusters in X-ray-selected samples.

79 ASTRONOMY AND ASTROPHYSICS↗
DOE OSTI2022

The Solar System calcium isotopic composition inferred from Ryugu samples

The Hayabusa2 spacecraft has returned samples from the Cb-type asteroid (162173) Ryugu to Earth. Previous petrological and chemical analyses support a close link between Ryugu and CI chondrites that are presumed to be chemically the most primitive meteorites with a solar-like composition. However, Ryugu samples are highly enriched in Ca compared to typical CI chondrites. To identify the cause of this discrepancy, here we report stable Ca isotopic data (expressed as δ 44/40 Ca SRM915a ) for returned Ryugu samples collected from two sites. We found that samples from both sites have similar δ 44/40 Ca SRM915a (0.58 ± 0.03 ‰ and 0.55 ± 0.08 ‰, 2 s.d.) that fall within the range defined by CIs. This isotopic similarity suggests that the Ca budget of CIs and Ryugu samples is dominated by carbonates, and the variably higher Ca contents in Ryugu samples are due to the abundant carbonates. Precipitation of carbonates on Ryugu likely coincided with a major episode of aqueous activity dated to have occurred ~5 Myr after Solar System formation. Based on the pristine Ryugu samples, the average δ 44/40 Ca SRM915a of the Solar System is defined to be 0.57 ± 0.04 ‰ (2 s.d.).

79 ASTRONOMY AND ASTROPHYSICS↗
NASA NTRS1971

Description of core samples returned by Apollo 12

Three core samples were collected by the Apollo 12 astronauts. Two are single cores, one of which (sample 12026) was collected close to the lunar module during the first extravehicular activity period and is 19.3 centimeters long. The second core (sample 12027) was collected at Sharp Crater during the second extravehicular activity period and is 17.4 centimeters long. The third sample is a double core (samples 12025 and 12028), which was collected near Halo Crater during the second extravehicular activity period. Unlike the other cores, the double-drive-tube core sample has complex layering with at least 10 clearly defined stratigraphic units. This core sample is approximately 41 centimeters long.

Lindsay, J. F.↗
NASA NTRS1972

Documentation of Apollo 15 samples

A catalog is presented of the documentation of Apollo 15 samples using photographs and verbal descriptions returned from the lunar surface. Almost all of the Apollo 15 samples were correlated with lunar surface photographs, descriptions, and traverse locations. Where possible, the lunar orientations of rock samples were reconstructed in the lunar receiving laboratory, using a collimated light source to reproduce illumination and shadow characteristics of the same samples shown in lunar photographs. In several cases, samples were not recognized in lunar surface photographs, and their approximate locations are known only by association with numbered sample bags used during their collection. Tables, photographs, and maps included in this report are designed to aid in the understanding of the lunar setting of the Apollo 15 samples.

Sutton, R. L.↗
NASA NTRS1973

Chemical composition of Apollo 15, 16, and 17 samples

The authors analyzed 22 Apollo 15 samples, 21 Apollo 16 samples, 4 Luna 20 samples, and 6 Apollo 17 samples for 26 to 30 major, minor, and trace elements by instrumental neutron activation analysis (INAA). Major attention is given to Apollo 16 results and recent Apollo 17 data. The roster of elements via INAA has been extended to include Nd, Ni, Ir, and Au in the Apollo 16 and 17 samples. The latter three elements are highly abundant in these samples. Sample preparation, activation conditions, and the detailed INAA analytical procedure are essentially the same as reported by Laul and Schmitt (1973).

Laul, J. C.↗
NASA NTRS1974

Digital redesign of continuous systems by matching of states at multiple sampling periods

This paper presents a method of digital approximation of a continuous-data system by the matching of states at multiple sampling periods. Two alternate methods are presented; one method samples the states every sampling period, and alters the forward and feedback gains, so as to match the states of the two systems at the end of N sampling periods. The second method requires the sampling of the states every N sampling periods, with the change of gains at each sampling period. An illustrative example using the one-axis dynamics of the Skylab Satellite is presented.

Yackel, R. A.↗
NASA NTRS1975

Stability of multirate sampled-data systems

Current adaptive sampling schemes that can be used in sampled-data systems with variable rate sampling does not guarantee the stability of the resulting closed-loop system. A study was undertaken with the objective of finding a stable control law for multirate sampled-data systems. The problem is formulated such that the sampling interval is selected from a set of fixed number of sample intervals. A necessary and sufficient condition under which these types of systems can be stabilized is given. For a certain subclass of these types of systems, a sampling selection algorithm is given which results in a stable closed-loop system.

Stanford, D. P.↗
NASA NTRS1974

Preservation of lunar core samples - Preparation and interpretation of three-dimensional stratigraphic sections

Preservation and analysis of core samples collected from the lunar regolith are discussed. The objectives of core sampling are described together with the core-sampling equipment used in the Apollo program. The effects of disaggregation in core samples are summarized, and ways to preserve the stratigraphy in these samples are reviewed, particularly partial impregnation of samples with polybutyl methacrylate. It is shown that stratigraphic sections preserved in this way reveal individual fragments of the regolith in their original positions, primary and secondary depositional structures related to lunar processes, and the nature and extent of deformations caused by sampling equipment. It is concluded that since the core sedimentary structures indicate complex three-dimensional variations in the regolith, quantitative models of regolith evolution must allow for distinctive local histories as well as irregular reworking and deposition events due to impact processes.

Fryxell, R.↗
NASA NTRS1971

Plural output optimetric sample cell and analysis system

An apparatus suitable for receiving a sample for optimetric analysis includes a sample cell comprising an opaque hollow tube. Several apertures are defined in the wall of the tubing and a lens barrel which extends beyond to opposite surfaces of the wall is supported within at least one of the apertures. A housing is provided with one channel for receiving the sample cell and a series of channels extending from the exterior housing to the sample cell apertures. A filter element is housed in each of these latter channels. These channels slidingly receive an excitation light source for a photodetector cell to permit selective focusing. A sample cell containing at least three apertures in the walls can be mounted for rotation relative to a light source or photoconduction means for simultaneous or alternative optimetric determination of the components of a single sample. The sample cell is fabricated by supporting a lens barrel within the aperture. A molten portion of glass is deposited in the lens barrel and cooled while in a horizontal position to form a lens having an acceptable angle.

Haley, F. C.↗
NASA NTRS1979

Recovering the spectrum of a narrow-band process from syncopated samples

A nonuniform sampling strategy, phase quadrature sampling, in which a process of bandwith B is sampled at rate B in each of two channels where the two channels are pi/2 out of phase at frequency B is described. Phase quadrature sampling is a special case of sampling, where the phase between channels is fixed but arbitrary. A simple method for recovering the spectrum of the input process from syncopated samples is derived. The derivation indicates what values of phase between channels result in lossless sampling.

Milenkovic, P. H.↗
NASA NTRS1978

Luna 24: 90-150 micrometer fraction - Implications for remote sampling of regolith

An analysis of the mineral grains and glasses found in the 90 to 150 micron fraction of the Luna 24 core sample is presented and implications for the automatic collection of planetary and asteroidal regoliths are discussed. Electron microprobe analysis for pyroxene, olivine, plagioclase, opaque minerals and glass in samples at various depths indicate that polymineralic grains have compositions similar to those of gabbroic and basaltic fragments from coarser samples, while monomineralic grains contain an additional population of Mg-rich olivines and pyroxene. Most of the glasses are found to be related to mare basalts or local regolith, with nonmare material represented by glasses of highland basalt and low K Fra Mauro composition. It is concluded that as regards mineralogy and petrology, a single grab sample would have been as useful and a series of grab samples on a long traverse would have been more useful than the Luna 24 core sample, with the fine sample being more informative than the coarse.

Papp, H. A.↗
NASA NTRS1981

CCD correlated quadruple sampling processor

A correlated quadruple sampling processor for improved signal-to-noise ratio in the output of a charge-coupled device (CCD) is comprised of: switching means for momentarily clamping a CCD signal line at a first reference level A before a CCD data pulse and then obtaining a first data sample B with respect to the reference A during a CCD data pulse, and storing the positive sample B-A; switching means for momentarily clamping the CCD signal line a second time at the level C during the presence of the CCD data pulse and then obtaining a second data sample D with respect to the reference level C after the CCD data pulse, and storing the negative sample D-C; and means for obtaining the difference between the stored samples +(B-A) and -(D-C), thus increasing the net signal amplitude by a factor of about 2 while the noise would be increased by only a factor of square root of 2 since there will be no correlation in the noise between the double samples +(B-A) and -(D-C) effectively added.

Gaalema, S. D.↗
NASA NTRS1982

Studies with sample conductivity, insertion rates, and particle deflection in a continuous flow electrophoresis system

The continuous flow electrophoresis system makes electrophoresis possible in a free-flowing film of aqueous electrolyte medium. The sample continuously enters the electrolyte at the top of the chamber and is subjected to the action of a lateral dc field. This divides the sample into fractions since each component has a distinctive electrophoretic mobility. Tests were made using monodisperse polystyrene latex microspheres to determine optimum sample conductivity, insertion rates and optimum electric field applications as baseline data for future STS flight experiments. Optimum sample flow rates for the selected samples were determined to be approximately 26 micro-liters/min. Experiments with samples in deionized water yielded best results and voltages in the 20 V/cm to 30 V/cm range were optimum. Deflections of formaldehyde fixed turkey and bovine erythrocytes were determined using the continuous flow electrophoresis system. The effects of particle interactions on sample resolution and migration in the chamber was also evaluated.

Williams, G., Jr.↗
NASA NTRS1983

Influence of sampling rate on the calculated fidelity of an aircraft simulation

One of the factors that influences the fidelity of an aircraft digital simulation is the sampling rate. As the sampling rate is increased, the calculated response of the discrete representation tends to coincide with the response of the corresponding continuous system. Because of computer limitations, however, the sampling rate cannot be increased indefinitely. Moreover, real-time simulation requirements demand that a finite sampling rate be adopted. In view of these restrictions, a study was undertaken to determine the influence of sampling rate on the response characteristics of a simulated aircraft describing short-period oscillations. Changes in the calculated response characteristics of the simulated aircraft degrade the fidelity of the simulation. In the present context, fidelity degradation is defined as the percentage change in those characteristics that have the greatest influence on pilot opinion: short period frequency omega, short period damping ratio zeta, and the product omega zeta. To determine the influence of the sampling period on these characteristics, the equations describing the response of a DC-8 aircraft to elevator control inputs were used. The results indicate that if the sampling period is too large, the fidelity of the simulation can be degraded.

Howard, J. C.↗
NASA NTRS1984

Sampling system for wheat (Triticum aestivum L) area estimation using digital LANDSAT MSS data and aerial photographs

A procedure to estimate wheat (Triticum aestivum L) area using sampling technique based on aerial photographs and digital LANDSAT MSS data is developed. Aerial photographs covering 720 square km are visually analyzed. To estimate wheat area, a regression approach is applied using different sample sizes and various sampling units. As the size of sampling unit decreased, the percentage of sampled area required to obtain similar estimation performance also decreased. The lowest percentage of the area sampled for wheat estimation with relatively high precision and accuracy through regression estimation is 13.90% using 10 square km as the sampling unit. Wheat area estimation using only aerial photographs is less precise and accurate than those obtained by regression estimation.

Parada, N. D. J.↗