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Search indexed NASA NTRS and DOE OSTI research on propulsion, heat transfer, battery materials and energy systems. Follow report and document links to the original sources.

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At least 1,117 records · Page 62
All sourcesNASA NTRSDOE OSTI
DOE OSTI2015

Investigation of precipitate refinement in Mg alloys by an analytical composite failure model

An analytical model is developed to simulate precipitate refinement in second phase strengthened magnesium alloys. The model is developed based on determination of the stress fields inside elliptical precipitates embedded in a rate dependent inelastic matrix. The stress fields are utilized to determine the failure mode that governs the refinement behavior. Using an AZ31 Mg alloy as an example, the effects the applied load, aspect ratio and orientation of the particle is studied on the macroscopic failure of a single α-Mg17Al12 precipitate. Additionally, a temperature dependent version of the corresponding constitutive law is used to incorporate the effects of temperature. In plane strain compression, an extensional failure mode always fragments the precipitates. The critical strain rate at which the precipitates start to fail strongly depends on the orientation of the precipitate with respect to loading direction. The results show that the higher the aspect ratio is, the easier the precipitate fractures. Precipitate shape is another factor influencing the failure response. In contrast to elliptical precipitates with high aspect ratio, spherical precipitates are strongly resistant to sectioning. In pure shear loading, in addition to the extensional mode of precipitate failure, a shearing mode may get activated depending on orientation and aspect ratio of the precipitate. The effect of temperature in relation to strain rate was also verified for plane strain compression and pure shear loading cases.

Tabei, Ali↗
DOE OSTI2023

Flexible tape-drive target system for secondary high-intensity laser-driven sources

Here, we present the development of a flexible tape-drive target system to generate and control secondary high-intensity laser-plasma sources. Its adjustable design permits the generation of relativistic MeV particles and x rays at high-intensity (i.e., ≥1 × 10 18 W cm —2 ) laser facilities, at high repetition rates (>1 Hz). The compact and robust structure shows good mechanical stability and a high target placement accuracy (<4 μm RMS). Its compact and flexible design allows for mounting in both the horizontal and vertical planes, which makes it practical for use in cluttered laser-plasma experimental setups. The design permits ~170° of access on the laser-driver side and 120° of diagnostic access at the rear. A range of adapted apertures have been designed and tested to be easily implemented to the targetry system. The design and performance testing of the tape-drive system in the context of two experiments performed at the COMET laser facility at the Lawrence Livermore National Laboratory and at the Advanced Lasers and Extreme Photonics (ALEPH) facility at Colorado State University are discussed. Experimental data showing that the designed prototype is also able to both generate and focus high-intensity laser-driven protons at high repetition rates are also presented.

70 PLASMA PHYSICS AND FUSION TECHNOLOGY↗
DOE OSTI2023

Ultrahigh supercurrent density in a two-dimensional topological material

Ongoing advances in superconductors continue to revolutionize technology thanks to the increasingly versatile and robust availability of lossless supercurrents. In particular, high supercurrent density can lead to more efficient and compact power transmission lines, high-field magnets, as well as high-performance nanoscale radiation detectors and superconducting spintronics. In this work, we report the discovery of an unprecedentedly high superconducting critical current density (17 MA / cm 2 at 0 T and 7 MA / cm 2 at 8 T) in 1T'–WS 2 , exceeding those of all reported two-dimensional superconductors to date. 1T'–WS 2 features a strongly anisotropic (both in- and out-of-plane) superconducting state that violates the Pauli paramagnetic limit signaling the presence of unconventional superconductivity. Spectroscopic imaging of the vortices further substantiates the anisotropic nature of the superconducting state. More intriguingly, the normal state of 1T'–WS 2 carries topological properties. The band structure obtained via angle-resolved photoemission spectroscopy and first-principles calculations points to a Z 2 topological invariant. The concomitance of topology and superconductivity in 1T'–WS 2 establishes it as a topological superconductor candidate, which is promising for the development of quantum computing technology.

36 MATERIALS SCIENCE↗
DOE OSTI2017

A Full-Height Axial P 3 Solver for the 2D/1D Method in MPACT

This report encompasses the efforts to complete L3:RTM.PRT.P15.04, which relates to improvements to the axial solvers in MPACT. Over the past few years, a number of convergence issues have been encountered throughout the 2D/1D calculation. While many of these were related to transport-corrected stability, which has been much improved through the development of multigroup MOC kernels, there are still some instabilities that are more directly related to the 1D axial nodal solvers. The primary focus of this milestone is on the development of a full-height P 3 solver, which solves for a single linear system for the entire rod, compared to the one- and two-node solvers previously available in MPACT. To provide an efficient full-height solver, the SuperLU direct linear solver was leveraged and an alternative rod decomposition scheme is used in favor over the typically employed axial decomposition. In addition to the full-height solver, a number of stability observations are discussed pertaining to (1) cases with thin planes in the axial reflectors, (2) quadratic radial leakage interpolation, (3) the reset sol capability, which reinitializes the solution before continuing the calculation, and (4) the flux threshold used in the radial transverse leakage splitting logic. The last of these was improved by identifying an acceptable threshold, which greatly help provide stability to the default one-node P 3 solver approach. Results demonstrating the full-height solver are presented for (1) a single assembly case from the AP1000 reactor design, (2) VERA Progression Problem 5a, and (3) a Watts Bar Unit 1, Cycle 1 case that demonstrated convergence issues due to thin planes in the axial reflector. In total, the full-height solver appears to be 3–5× slower for the nodal solve time, yield a roughly 10–20% increase in total problem run time, and requires ~5% more memory. However, these increases may be justifiable if the solver is proven to be more stable than the current default. Additionally, the VERA Progression Problem 4a case with the 252-group library is shown for the one-node P 3 solver with the updated threshold for radial transverse leakage splitting. This case also previous failed very early in the calculation, but is now able to run to completion. Brief details are also included related to the refactoring the nodal sweeper design. Previously, all nodal sweeper options were available in one large module, which was cumbersome and difficult to extend. Before the work here began, the design was refactored to include a number of abstract and extended types, which will help make future extensions easier. All-in-all, this milestone successfully implemented a new axial solver and improved the stability of the current default axial solver. However, additional testing will be necessary on new cases that demonstrate convergence issues before a decision can be made to change the current default in MPACT.

97 MATHEMATICS AND COMPUTING↗
DOE OSTI2016

Development of attenuation and diffraction corrections for linear and nonlinear Rayleigh surface waves radiating from a uniform line source

In recent studies with nonlinear Rayleigh surface waves, harmonic generation measurements have been successfully employed to characterize material damage and microstructural changes, and found to be sensitive to early stages of damage process. A nonlinearity parameter of Rayleigh surface waves was derived and frequently measured to quantify the level of damage. The accurate measurement of the nonlinearity parameter generally requires making corrections for beam diffraction and medium attenuation. These effects are not generally known for nonlinear Rayleigh waves, and therefore not properly considered in most of previous studies. In this paper, the nonlinearity parameter for a Rayleigh surface wave is defined from the plane wave displacement solutions. We explicitly define the attenuation and diffraction corrections for fundamental and second harmonic Rayleigh wave beams radiated from a uniform line source. Attenuation corrections are obtained from the quasilinear theory of plane Rayleigh wave equations. To obtain closed-form expressions for diffraction corrections, multi-Gaussian beam (MGB) models are employed to represent the integral solutions derived from the quasilinear theory of the full two-dimensional wave equation without parabolic approximation. Diffraction corrections are presented for a couple of transmitter-receiver geometries, and the effects of making attenuation and diffraction corrections are examined through the simulation of nonlinearity parameter determination in a solid sample.

71 CLASSICAL AND QUANTUM MECHANICS, GENERAL PHYSIC↗
DOE OSTI2025

Epitaxial Growth of 2D Core‐Crown SnS 2 /SnSe 2 Heterostructure Through Interfacial Modification with Polyvinylpyrrolidone

Abstract Developing generalized strategies for controlled synthesis of 2D heterostructures remains a significant challenge because the existing approaches often suffer from poor reproducibility and scalability. In this study, a solution synthesis approach for epitaxial core‐crown heterostructures with controlled band alignment, that overcomes these challenges is reported. Polyvinylpyrrolidone (PVP) is used as a structure‐directing agent to reduce lattice mismatch between SnS 2 and SnSe 2 (10‐10) surfaces and direct epitaxial growth of SnSe 2 crown on SnS 2 seed. Additionally, PVP adsorption to the basal plane prevents van der Waals stacking and stabilizes 2D heterostructures during synthesis. Driven by interfacial thermodynamics, the formation of the core‐crown heterostructure is highly reproducible and the size of the 2D heterostructure and relative areas of the core and the crown can be precisely controlled in a two‐step process by varying synthesis times for the seed and the crown. The identified growth pathway for 2D heterostructures can be generalized to other combinations of van der Waals materials to provide a platform for synthesizing micron‐size epitaxial heterostructures with a desired electronic structure for catalysis and microelectronics.

Liu, Lili [Physical and Computational Sciences Dir↗
DOE OSTI2016

Facile synthesis of one dimensional ZnO nanostructures for DSSC applications

Development of zinc oxide (ZnO) nanostructure based third generation dye sensitized solar cell is interesting compared to conventional silicon solar cells. ZnO nanostructured thin films were electrochemically deposited onto fluorine doped tin oxide (FTO) glass substrate. The effect of ethylene-diamine-tetra-acetic acid (EDTA) on structural, morphological and optical properties is investigated using X-ray diffraction (XRD) meter, field emission scanning electron microscope (FE-SEM) and micro Raman spectroscopy. XRD patterns reveal that the prepared nanostructures are hexagonal wutrzite structures with (101) plane orientation, the nanostructure prepared using EDTA exhibits better crystallinity. FE-SEM images illustrate that the morphological changes are observed from nanorod structure to cauliflower like structure as EDTA is added. Micro Raman spectra predict that cauliflower like structure possesses a higher crystalline nature with less atomic defects compared to nanorod structures. Dye sensitized solar cell (DSSC) is constructed for the optimized cauliflower structure, and open circuit voltage, short circuit density, fill factor and efficiency are estimated from the J-V curve.

77 NANOSCIENCE AND NANOTECHNOLOGY↗
DOE OSTI2022

Three-dimensional hot-spot x-ray emission tomography from cryogenic deuterium–tritium direct-drive implosions on OMEGA

A three-dimensional model of the hot-spot x-ray emission has been developed and applied to the study of low-mode drive asymmetries in direct-drive inertial confinement fusion implosions on OMEGA with cryogenic deuterium–tritium targets. Here, the steady-state model assumes an optically thin plasma and the data from four x-ray diagnostics along quasi-orthogonal lines of sight are used to obtain a tomographic reconstruction of the hot spot. A quantitative analysis of the hot-spot shape is achieved by projecting the x-ray emission into the diagnostic planes and comparing this projection to the measurements. The model was validated with radiation-hydrodynamic simulations assuming a mode-2 laser illumination perturbation resulting in an elliptically shaped hot spot, which was accurately reconstructed by the model using synthetic x-ray images. This technique was applied to experimental data from implosions in polar-direct-drive illumination geometry with a deliberate laser-drive asymmetry, and the hot-spot emission was reconstructed using spherical-harmonic modes of up to ℓ = 3. A 10% stronger drive on the equator relative to that on the poles resulted in a prolate-shaped hot spot at stagnation with a large negative A 2,0 coefficient of A 2,0 = –0.47 ± 0.03, directly connecting the modal contribution of the hot-spot shape with the modal contribution in laser-drive asymmetry.

70 PLASMA PHYSICS AND FUSION TECHNOLOGY↗
DOE OSTI2025

Higher-order symmetry plane correlations in Pb-Pb collisions at $\sqrt{s_{NN}}$ = 5.02 TeV

The correlations between event-by-event fluctuations of symmetry planes are measured in Pb-Pb collisions at a center-of-mass energy per nucleon pair $\sqrt{s_{NN}}$ = 5.02 TeV recorded by the ALICE detector at the Large Hadron Collider. This analysis is conducted using the Gaussian estimator technique, which is insensitive to biases from correlations between different flow amplitudes. The study presents, for the first time, the centrality dependence of correlations involving up to five different symmetry planes. The correlation strength varies depending on the harmonic order of the symmetry plane and the collision centrality. Comparisons with measurements from lower energies indicate no significant differences within uncertainties. Additionally, the results are compared with hydrodynamic model calculations. Although the model predictions provide a qualitative explanation of the experimental results, they overestimate the data for some observables. This is particularly true for correlators that are sensitive to the nonlinear response of the medium to initial-state anisotropies in the collision system. As these new correlators provide unique information—independent of flow amplitudes—their usage in future model developments can further constrain the properties of the strongly interacting matter created in ultrarelativistic heavy-ion collisions.

73 NUCLEAR PHYSICS AND RADIATION PHYSICS↗
DOE OSTI2020

X-ray free-electron laser wavefront sensing using the fractional Talbot effect

Wavefront sensing at X-ray free-electron lasers is important for quantitatively understanding the fundamental properties of the laser, for aligning X-ray instruments and for conducting scientific experimental analysis. A fractional Talbot wavefront sensor has been developed. This wavefront sensor enables measurements over a wide range of energies, as is common on X-ray instruments, with simplified mechanical requirements and is compatible with the high average power pulses expected in upcoming X-ray free-electron laser upgrades. Single-shot measurements were performed at 500 eV, 1000 eV and 1500 eV at the Linac Coherent Light Source. These measurements were applied to study both mirror alignment and the effects of undulator tapering schemes on source properties. The beamline focal plane position was tracked to an uncertainty of 0.12 mm, and the source location for various undulator tapering schemes to an uncertainty of 1m, demonstrating excellent sensitivity. These findings pave the way to use the fractional Talbot wavefront sensor as a routine, robust and sensitive tool at X-ray free-electron lasers as well as other high-brightness X-ray sources.

73 NUCLEAR PHYSICS AND RADIATION PHYSICS↗
DOE OSTI2025

Measuring Local Turbulence Along the Optical Path: Multi-Beam Optical Seeing Sensor

Deflection of light along the optical path is a major source of image degradation for ground-based telescopes. Methods have been developed to measure upper atmospheric seeing based on models of the turbulence in the atmosphere, but due to boundary conditions, transmission within telescope enclosures is more complex. The Multi-beam Optical Seeing Sensor (MOSS) directly measures the component of the image quality degradation from inhomogeneity of the index of refraction within the telescope dome. MOSS outputs four near-parallel beams of light that travel along the optical path and are imaged by the telescope’s detector, landing like starlight on the telescope’s focal plane. By using a strobed light source, we can ‘freeze’ the instantaneous index variations transverse to the optical path. This system captures both ‘dome’ and ‘mirror’ seeing. Through plotting the standard deviation of differential motion between pairs of beams, MOSS enables characterization of the length scale of turbulence within the dome. The temporal coherence of temperature gradients can be probed with different pulse lengths, and the spatial coherence by comparing pairs at different separations across the aperture of the telescope. Optical path turbulence measurements, alongside other telemetry metrics, will guide thermal and airflow management to optimize image quality. A MOSS prototype was installed in the 1.2[Formula: see text]m Auxiliary Telescope (AuxTel) at the Vera C. Rubin Observatory in Chile, and preliminary data constrain the optical path turbulence with a lower bound of 1.4 arcsec. The optical path turbulence varied throughout the night of observing.

Astronomical seeing↗
DOE OSTI2021

Eddy Current Model of a Coil Over An Infinite Perfectly Electrical Conductor (PEC) Half-Plane

Eddy current sensors measure the lift-off or distance between the sensor and a conducting surface. They operate on the principle of an alternating current in a conduction coil inducing a magnetic field within the surface. An eddy current is set up in the surface to counter the incident magnetic field which, in turn, sets up a magnetic field which counters that of the coil. This changes the coil impedance which is a function of the lift-off. As the lift-off increases, the effect of the eddy current magnetic field on the coil magnetic field weakens, resulting in a higher inductance and lower resistance. Thus, the lift-off may be derived from an impedance measurement. Dodd and Deeds developed an analytic model for an eddy current sensor coil impedance with an air core which has been implemented in MATLAB. LLNL assembled an eddy current sensor with a mu-metal core for which there is no analytic model. Rather than derive an analytic model which includes the mu-metal core, analytic empirically based functions are derived to map the Dodd and Deeds model to measured inductance and resistance.

42 ENGINEERING↗
DOE OSTI2022

Expanding the Material Search Space for Multivalent Cathodes

Multivalent batteries are an energy storage technology with the potential to surpass lithium-ion batteries; however, their performance have been limited by the low voltages and poor solid-state ionic mobility of available cathodes. A computational screening approach to identify high-performance multivalent intercalation cathodes among materials that do not contain the working ion of interest has been developed, which greatly expands the search space that can be considered for material discovery. This approach has been applied to magnesium cathodes as a proof of concept, and four resulting candidate materials [NASICON V 2 (PO 4 ) 3 , birnessite NaMn 4 O 8 , tavorite MnPO 4 F, and spinel MnO 2 ] are discussed in further detail. In examining the ion migration environment and associated Mg 2+ migration energy in these materials, local energy maxima are found to correspond with pathway positions where Mg 2+ passes through a plane of anion atoms. While previous studies have established the influence of local coordination on multivalent ion mobility, these results suggest that considering both the type of the local bonding environment and available free volume for the mobile ion along its migration pathway can be significant for improving solid-state mobility.

25 ENERGY STORAGE↗
DOE OSTI2021

Isotropic Pauli-limited superconductivity in the infinite-layer nickelate Nd 0.775 Sr 0.225 NiO 2

The recent observation of superconductivity in thin-film infinite-layer nickelates offers a different angle from which to investigate superconductivity in layered oxides. A wide range of candidate models have been proposed, which emphasize single- or multi-orbital electronic structure, Kondo or Hund’s coupling and analogies to cuprates. Further experimental characterization of the superconducting state is needed to develop a full understanding of the nickelates. Here we use magnetotransport measurements to probe the superconducting anisotropy in Nd 0.775 Sr 0.225 NiO 2 . Here, we find that the upper critical field is surprisingly isotropic at low temperatures despite the layered crystal structure. In a magnetic field, the superconductivity is strongly Pauli-limited, such that the paramagnetic effect dominates over orbital de-pairing. Underlying this isotropic response is a substantial anisotropy in the superconducting coherence length, which is at least four times longer in-plane than out-of-plane. A prominent low-temperature upturn in the upper critical field indicates the presence of an unconventional ground state.

75 CONDENSED MATTER PHYSICS, SUPERCONDUCTIVITY AND↗
DOE OSTI2015

Lattice model of linear telechelic polymer melts. II. Influence of chain stiffness on basic thermodynamic properties

The lattice cluster theory (LCT) for semiflexible linear telechelic melts, developed in Paper I, is applied to examine the influence of chain stiffness on the average degree of self-assembly and the basic thermodynamic properties of linear telechelic polymer melts. Our calculations imply that chain stiffness promotes self-assembly of linear telechelic polymer melts that assemble on cooling when either polymer volume fraction ϕ or temperature T is high, but opposes self-assembly when both ϕ and T are sufficiently low. This allows us to identify a boundary line in the ϕ-T plane that separates two regions of qualitatively different influence of chain stiffness on self-assembly. The enthalpy and entropy of self-assembly are usually treated as adjustable parameters in classical Flory-Huggins type theories for the equilibrium self-assembly of polymers, but they are demonstrated here to strongly depend on chain stiffness. Moreover, illustrative calculations for the dependence of the entropy density of linear telechelic polymer melts on chain stiffness demonstrate the importance of including semiflexibility within the LCT when exploring the nature of glass formation in models of linear telechelic polymer melts.

37 INORGANIC, ORGANIC, PHYSICAL, AND ANALYTICAL CH↗
DOE OSTI2016

Spray Foam Exterior Insulation with Stand-Off Furring - New York

IBACOS and Green Homes America 1 (GHA) collaborated with the New York State Energy Research and Development Authority (NYSERDA) Advanced Buildings Program to research a variation of a commercial curtain wall assembly for residential construction as part of a comprehensive whole-house deep energy retrofit (DER) package. The advantages of this strategy include minimizing the physical connections to each individual existing wall stud, using closedcell spray foam to encapsulate existing siding materials including lead paint, and creating a vented rain screen assembly to promote drying. As Moore (2011) states, "Closed-cell foam acts as air-sealing, insulation, and secondary drainage plane..." Field installations on a limited number of houses indicate that the incremental cost when installed as part of a typical siding and window replacement job adds approximately $10/ft2 of wall area. 2 x 4 framing members were attached to the wall at band joists and top plates using "L" clips, and spray foam was used to insulate the wall after the framing was installed. Windows were installed as the framing was put up, including extension jambs. Key lessons learned include the following: (1) The installed cost of the spray foam system was comparable to the installed cost of the rigid foam and furring strips. (2) Spray foam should be applied in such a way that it locks the framing members in place before the remaining foam is installed in the field of the wall. The spray foam has a tendency to move the new wall framing as it expands. Best practice is to "picture frame" the wall framing with spray foam and then apply the spray foam in the field of each bay. (3) Variations in the existing siding conditions must be accounted for when attaching the ledger boards and wall framing. A best practice is to uniformly shim the ledger boards off the walls so the new framing is a uniform distance from the ledger boards and the inside surface of the interior framing. This is important primarily for window and door installation and the associated extension jambs and trim. (4) From a sequencing perspective, it is advantageous to replace the windows at the same time as the exterior walls are being built. This requires a crew that can perform a number of different tasks (e.g., framing, flashing, window install, trim carpentry) and does not lend itself to subcontracting this approach piecemeal (e.g., framing subcontractor, window installer, drainage plane installer, trim carpenter). (5) Application of the brackets and associated fastener screws was more time consuming than anticipated. (6) It is important for the spray foam contractor to perform all preparatory work, which in this case included placing plastic over the windows and exposed foundation to minimize or eliminate the possibility of damage due to overspray.

Array↗
DOE OSTI2021

Two Year Cosmology Large Angular Scale Surveyor (CLASS) Observations: Long Timescale Stability Achieved with a Front-end Variable-delay Polarization Modulator at 40 GHz

The Cosmology Large Angular Scale Surveyor (CLASS) is a four-telescope array observing the largest angular scales (2≲ ℓ ≲ 200) of the cosmic microwave background (CMB) polarization. These scales encode information about reionization and inflation during the early universe. The instrument stability necessary to observe these angular scales from the ground is achieved through the use of a variable-delay polarization modulator as the first optical element in each of the CLASS telescopes. Here, we develop a demodulation scheme used to extract the polarization timestreams from the CLASS data and apply this method to selected data from the first 2 yr of observations by the 40 GHz CLASS telescope. These timestreams are used to measure the 1/f noise and temperature-to-polarization (T → P) leakage present in the CLASS data. We find a median knee frequency for the pair-differenced demodulated linear polarization of 15.12 mHz and a T → P leakage of <3.8 × 10 -4 (95% confidence) across the focal plane. We examine the sources of 1/f noise present in the data and find the component of 1/f due to atmospheric precipitable water vapor (PWV) has an amplitude of 203 ± 12 µK RJ $\sqrt{{s}}$ for 1 mm of PWV when evaluated at 10 mHz; accounting for ~17% of the 1/f noise in the central pixels of the focal plane. In conclusion, the low levels of T → P leakage and 1/f noise achieved through the use of a front-end polarization modulator are requirements for observing of the largest angular scales of the CMB polarization by the CLASS telescopes.

79 ASTRONOMY AND ASTROPHYSICS↗
DOE OSTI2015

Comparison of growth texture in round Bi2212 and flat Bi2223 wires and its relation to high critical current density development

Why Bi₂Sr₂CaCu₂O x (Bi2212) allows high critical current density J c in round wires rather than only in the anisotropic tape form demanded by all other high temperature superconductors is important for future magnet applications. Here we compare the local texture of state-of-the-art Bi2212 and Bi2223 ((Bi,Pb)₂Sr₂Ca₂Cu₃O₁₀), finding that round wire Bi2212 generates a dominant a-axis growth texture that also enforces a local biaxial texture (FWHM <15°) while simultaneously allowing the c-axes of its polycrystals to rotate azimuthally along and about the filament axis so as to generate macroscopically isotropic behavior. By contrast Bi2223 shows only a uniaxial (FWHM <15°) c-axis texture perpendicular to the tape plane without any in-plane texture. Consistent with these observations, a marked, field-increasing, field-decreasing J c (H) hysteresis characteristic of weak-linked systems appears in Bi2223 but is absent in Bi2212 round wire. Growth-induced texture on cooling from the melt step of the Bi2212 J c optimization process appears to be the key step in generating this highly desirable microstructure.

Kametani, F.↗