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NASA NTRS2009

Geologic Mapping of the Lunar South Pole, Quadrangle LQ-30: Volcanic History and Stratigraphy of Schroedinger Basin

In this study we use recent images and topographic data to map the geology and geomorphology of the lunar South Pole quadrangle (LQ-30) at 1:2.5M scale [1-4] in accordance with the Lunar Geologic Mapping Program. Mapping of LQ-30 began during Mest's postdoctoral appointment and has continued under the PG&G Program, from which funding became available in February 2009. Preliminary map-ping and analyses have been done using base materials compiled by Mest, but properly mosaicked and spatially registered base materials are being compiled by the USGS and should be received by the end of June 2009. The overall objective of this research is to constrain the geologic evolution of the lunar South Pole (LQ-30: 60deg -90deg S, 0deg - +/-180deg ) with specific emphasis on evaluation of a) the regional effects of basin formation on the structure and composition of the crust and b) the spatial distribution of ejecta, in particular resulting from formation of the South Pole-Aitken (SPA) basin and other large basins. Key scientific objectives include: 1) Constraining the geologic history of the lunar South Pole and examining the spatial and temporal variability of geologic processes within the map area. 2) Constraining the vertical and lateral structure of the lunar regolith and crust, assessing the distribution of impact-generated materials, and determining the timing and effects of major basin-forming impacts on crustal structure and stratigraphy in the map area. And 3) assessing the distribution of resources (e.g., H, Fe, Th) and their relationships with surface materials.

Mest, S. C.↗

NASA NTRSDate not supplied

Data Fusion and Mining Techniques to Map Water Use and Drought across Spatial and Temporal Scales

As the world’s water resources come under increasing tension due to dual stressors of climate change and population growth, accurate knowledge of water consumption through evapotranspiration (ET) over a range in spatial scales will be critical in developing adaptation strategies. Remote sensing methods for monitoring consumptive water use (e.g, ET) are becoming increasingly important, especially in areas of significant water and food insecurity. One method to estimate ET from satellite-based methods, the Atmosphere Land Exchange Inverse (ALEXI) model uses the change in mid-morning land surface temperature to estimate the partitioning of sensible and latent heat fluxes which are then used to estimate daily ET. This presentation will outline several recent enhancements to the ALEXI modeling system, with a focus on global ET and drought monitoring. Until recently, ALEXI has been limited to areas with high resolution temporal sampling of geostationary sensors. The use of geostationary sensors makes global mapping a complicated process, especially for real-time applications, as data from as many as five different sensors are required to be ingested and harmonized to create a global mosaic. However, our research team has developed a new and novel method of using twice-daily observations from polar-orbiting sensors such as MODIS and VIIRS to estimate the mid-morning rise in LST that is used to drive the energy balance estimations within ALEXI. This allows the method to be applied globally using a single sensor (in this case, initially MODIS with a planned transition to VIIRS) rather than a global compositing of all available geostationary data. Other advantages of this new method include the higher spatial resolution provided by MODIS and VIIRS and the increased sampling at high latitudes where oblique view angles limit the utility of geostationary sensors. This presentation will focus on global applications for mapping water use and drought using data mining and data fusion across spatial scales extending from 5-km to 30-m “field-scale” estimates.

Christopher Hain↗

NASA NTRS2014

Bunburra Rockhole: Exploring the Geology of a New Differentiated Basaltic Asteroid

Bunburra Rockhole (BR) is the first recovered meteorite of the Desert Fireball Network. It was initially classified as a basaltic eucrite, based on texture, mineralogy, and mineral chemistry but subsequent O isotopic analyses showed that BR's composition lies significantly far away from the HED group of meteorites. This suggested that BR was not a piece of the HED parent body (4 Vesta), but other explanations could also account for the observed oxygen signatures. Possible scenarios include contamination by components from other bodies (chondrites or other achondrites) or that 4 Vesta may not be as equilibrated as hypothesized. After examining multiple pieces with different instruments (CT scans and x-ray maps), no obvious evidence of contamination was found. If BR is not from Vesta, a conundrum exists as no unusual features were found in mineral and bulk trace element chemistry as exist for other anomalous basaltic achondrites such as Ibitira or Asuka 881394. These meteorites have distinct petrological and geochemical characteristics, in addition to their anomalous O isotope compositions, that set them apart from eucrites. Thus, early results provided a somewhat ambiguous picture of BR's petrogenesis and parentage. To clarify the nature of the relationship, if any, between BR and eucrites, we have performed a correlated stable isotope and bulk chemical study of several lithologic fragments.

Benedix, G.K.↗

DOE OSTI2025

Basin-Size Mapping: Prediction of Metastable Polymorph Synthesizability Across TaC–TaN Alloys

The sizes of the basins of attraction on the potential energy surface are helpful indicators in determining the experimental synthesizability of metastable phases. In principle, these basins can be controlled with changes in thermodynamic conditions such as composition, pressure, and surface energy. Herein, we use random structure sampling to computationally study how alloying smoothly perturbs basin of attraction sizes. The TaC 1-x N x pseudobinary is an ideal test system given the structural and polymorphic contrast of its parent compounds and their technological relevance as epitaxial substrates for Al 1-x Ga x N. While we find limited thermodynamic stability across all computationally observed phases, random structure sampling shows a significant composition region where the rocksalt basin dominates. As such, we predict the potential for the nonequilibrium synthesis of metastable rocksalt TaC 1-x N x alloys as substrates for Al 1-x Ga x N. At higher nitrogen concentrations, other low-energy metastable polymorphs emerge that continue to retain the hexagonal close packing suitable for III-N growth. Confidence in these trends was established through uncertainty quantification of the basin sizes and energy distributions; such analysis utilized the Beta and Dirichlet distributions. In conclusion, we also find (a) polymorph basin sizes can be rationalized in terms of energetic preferences for different coordination environments; and (b) basin sizes universally shrink with increasing nitrogen content, making the system more prone to amorphous growth.

36 MATERIALS SCIENCE↗

DOE OSTI2021

Accelerated optimization of pure metal and ligand compositions for light-driven hydrogen production

Photocatalytic hydrogen production is a promising alternative to traditional hydrogen production. To implement photocatalytic hydrogen production the development of efficient, sustainable, and stable catalysts is necessary, and overcoming the current challenges surrounding high dimensional search spaces requires both computational and experimental efforts. Utilizing photo driven processes, stable colloidal metal catalysts can be formed in situ for efficient hydrogen production from water. When considering colloidal catalysts, stability is typically a concern solved through the addition of supports or ligands. In this work, poly(ethylene glycol) methyl ether thiol acts as a stabilizing ligand eliminating the need for catalyst supports while providing stable and active nanoparticle catalysts for more than 45 hours of reaction time and illumination. These systems utilize molecular photosensitizers, water reduction catalysts, stabilizing ligands, water, a sacrificial reductant, and organic solvents, posing new challenges pertaining to the optimization of multi-variable systems. Design of experiments (DOE) is applied to accelerate the understanding of variable interactions and is used as a tool to rapidly optimize the compositions of Au, Cu, Ni, and Fe containing systems. Through a collaboration leveraging computation and experimentation (both high throughput and characterizations), optimized performance peaks were obtained for each of these metals alongside distinct mapping of expected activity associated with photosensitizer, metal, and ligand concentration variations. With the highly digitized workflow, this study allowed for comparative generalizations to be made regarding photo driven hydrogen production for all four metals.

08 HYDROGEN↗

DOE OSTI2021

Expanding standards in viromics: in silico evaluation of dsDNA viral genome identification, classification, and auxiliary metabolic gene curation

Viruses influence global patterns of microbial diversity and nutrient cycles. Though viral metagenomics (viromics), specifically targeting dsDNA viruses, has been critical for revealing viral roles across diverse ecosystems, its analyses differ in many ways from those used for microbes. To date, viromics benchmarking has covered read pre-processing, assembly, relative abundance, read mapping thresholds and diversity estimation, but other steps would benefit from benchmarking and standardization. Here we use in silico-generated datasets and an extensive literature survey to evaluate and highlight how dataset composition (i.e., viromes vs bulk metagenomes) and assembly fragmentation impact (i) viral contig identification tool, (ii) virus taxonomic classification, and (iii) identification and curation of auxiliary metabolic genes (AMGs). The in silico benchmarking of five commonly used virus identification tools show that gene-content-based tools consistently performed well for long (≥3 kbp) contigs, while k -mer- and blast-based tools were uniquely able to detect viruses from short (≤3 kbp) contigs. Notably, however, the performance increase of k -mer- and blast-based tools for short contigs was obtained at the cost of increased false positives (sometimes up to ~5% for virome and ~75% bulk samples), particularly when eukaryotic or mobile genetic element sequences were included in the test datasets. Furthermore, for viral classification, variously sized genome fragments were assessed using gene-sharing network analytics to quantify drop-offs in taxonomic assignments, which revealed correct assignations ranging from ~95% (whole genomes) down to ~80% (3 kbp sized genome fragments). A similar trend was also observed for other viral classification tools such as VPF-class, ViPTree and VIRIDIC, suggesting that caution is warranted when classifying short genome fragments and not full genomes. Finally, we highlight how fragmented assemblies can lead to erroneous identification of AMGs and outline a best-practices workflow to curate candidate AMGs in viral genomes assembled from metagenomes. Together, these benchmarking experiments and annotation guidelines should aid researchers seeking to best detect, classify, and characterize the myriad viruses ‘hidden’ in diverse sequence datasets.

59 BASIC BIOLOGICAL SCIENCES↗

NASA NTRS1981

Use of LANDSAT data to define soil boundaries in Carroll County, Missouri

Bands 4, 5 and 7 false color composite photographs were prepared using data from LANDSAT scenes acquired during April 1977 and April 1981 on computer compatible tapes, and these color composites were compared with band 7 black and white photographs prepared for the entire county. Delineations of soil boundaries at the soil association level were achieved using LANDSAT spectral reflectance data and slope maps for a portion of Carroll County, Missouri. Forty two spectral reflectance classes from April 1977 LANDSAT data were overlaid on digitized slope maps of nine USGS 7.5 minute series topographic quadrangle slope maps to achieve boundary delineations of the soil associations.

Davidson, S. E.↗

NASA NTRS1983

MAGSAT investigation of crustal magnetic anomalies in the eastern Indian Ocean

Crustal magnetic anomalies in a region of the eastern Indian Ocean were studied using data from NASA's MAGSAT mission. The investigation region (0 deg to 50 deg South, 75 to 125 deg East) contains several important tectonic features, including the Broken Ridge, Java Trench, Ninetyeast Ridge, and Southeast Indian Ridge. A large positive magnetic anomaly is associated with the Broken Ridge and smaller positive anomalies correlate with the Ninetyeast Ridge and western Australia. Individual profiles of scalar data (computed from vector components) were considered to determine the overall data quality and resolution capability. A set of MAGSAT ""Quiet-Time'' data was used to compute an equivalent source crustal magnetic anomaly map of the study region. Maps of crustal magnetization and magnetic susceptibility were computed from the equivalent source dipoles. Gravity data were used to help interpretation, and a map of the ratio of magnetization to density contrasts was computed using Poisson's relation. The results are consistent with the hypothesis of induced magnetization of a crustal layer having varying thickness and composition.

Sailor, R. V.↗

NASA NTRS1984

The Mars Geoscience/Climatology Orbiter 1990 mission

The fundamental objectives of the Mars Geoscience/Climatology Orbiter (MGCO) 1990 mission are related to the determination of the surface composition and topography of the planet Mars, its gravitational and intrinsic magnetic fields, and the seasonal behavior of volatiles, dust, and the atmosphere of Mars. These objectives would be achieved through a global mapping of the planet over a Martian year. For the baseline mission, a single spacecraft would be launched in August 1990, arrive at Mars in August 1991, and map the planet from a Sun-synchronous, near-circular, polar orbit for one Martian year. Attention is given to a science rationale and objectives, a mission description, the flight system, and mission operations.

Low, G. D.↗

NASA NTRS1985

The Pioneer Venus extended mission

A history of the Pioneer Venus Orbiter is given, as well as a presentation of the ongoing and future missions (through reentry in 1992). General characteristics of Venus including atmospheric and ionospheric data are reviewed. Development of the Pioneer program and studies including comet detection, gamma ray bursts, composition and structure of the atmosphere, ionosphere, clouds, and solar wind are discussed. Planned observations of Halley's Comet in 1986 and of past observations of the Comet Enke are examined in detail. Maps and diagrams illustrate the studies and observations of this extended mission. Specification of the spacecraft as well as details of its orbits are given.

Craig, R. A.↗

NASA NTRS1987

Abundance and distribution of ultramafic microbreccia in Moses Rock dike - Quantitative application of mapping spectroscopy

Data from the Airborne Imaging Spectrometer were used to map the distribution and abundance of the serpentized ultramafic microbreccia (SUM) component in the Moses Rock dike, which is a Tertiary diatreme located on the Colorado Plateau in Utah. The geologic setting and composition of Moses Rock dike are discussed together with its texture and the relationship to the bedrock of surface materials. These observations along with laboratory spectroscopic data are used to interpret surface mineralogy of the dike and the surrounding regions from the imaging spectometer data. The spatial distribution and the abundance of the primary surface components were calculated using a nonlinear model for the mixing of spectra from multicomponent surfaces. The derived SUM distribution and abundance data support McGetchin's (1968) model for the emplacement of Moses Rock dike as a fluidized system.

Mustard, John F.↗

NASA NTRS1998

Numerical Simulation of THM Growth of CdTe in Presence of Rotating Magnetic Fields

The influence of rotating magnetic fields (RMF) on the flow pattern and compositional uniformity in the solution zone of a traveling heater method (THM) system for growth of CdTe is numerically investigated. The analysis is conducted at the 10(exp -6) and 10(exp -1) g(sub 0) as representative of space and ground processing conditions. It is shown that under microgravity conditions, application of RMF can be used to overwhelm residual buoyancy-induced convection and to control the uniformity of solution-zone composition at the growth front without appreciable modification of the growth interface shape. At high gravity levels, RMF is found not to be able to completely dominate buoyancy-induced convection. In this regime, for the range of field strengths studied, RMF is found to result in a) complex flow structures in the solution zone, b) enhancement of compositional non-uniformities at the growth front, and c) increased convexity of the growth interface. A scaling analysis of convection in the solution zone is used to generate a non-dimensional map delineating the RMF- and gravity-dominated flow regimes.

Ghaddar, Chahid K.↗

NASA NTRS1999

Novel Method Used to Inspect Curved and Tubular Structural Materials

At the NASA Lewis Research Center, a technique for the ultrasonic characterization of plates has been extended to tubes and to curved structures in general. In this technique, one performs measurements that yield a thickness-independent value of the local through-the-thickness speed of sound in a specimen. From such measurements at numerous locations across the specimen, one can construct a map of velocity as a function of location. The gradients of velocity indicated by such a map indicate local through-the-thickness-averaged microstructural parameters that affect the speed of sound. Such parameters include the pore volume fraction, mass density, fiber volume fraction (in the case of a composite material), and chemical composition. Apparatus was designed to apply the technique to tubular and other curved specimens.

Roth, Don J.↗

NASA NTRS2006

Cassini Observations of Saturn's Dawn-Magnetotail Region and their Relation to Models of Saturn's Aurora: Preliminary Results

Using Cassini plasma and magnetic field observations from the dawn meridian of Saturn s outer magnetosphere to Saturn s magnetotail region, we investigate the applicability of the centrifugal instability model by Sittler et al. [2006] for Saturn s auroral response to the solar wind, versus the reconnection model of Saturn s aurora by Cowley et al. [2005]. We use Cassini Plasma Spectrometer (CAPS) Ion Mass Spectrometer (IMS) and Electron Plasma Spectrometer (ELS) observations to characterize the plasma environment. ELS and magnetometer observations are used to map out the morphology of the outer magnetosphere from dawn to midnight local time. IMS observations are used to measure plasma flow velocities from which one can infer rotation versus convective flows. IMS composition measurements are used to trace the source of plasma from the inner magnetosphere (protons, H2 and water group ions) versus an external solar wind source (protons and Heff ions). A critical parameter for both models is the strength of the convection electric field with respect to the rotational electric field for the large scale magnetosphere. Is there a significant return flow from the magnetotail? Pitch angle distributions also play an important role as a discriminator. If the magnetosphere tends to conserve angular momentum as suggested by Sittler et al. [2006], then we expect to see an anti-correlation between rotational flow component and radial flow velocities. All will be investigated.

Sittler, E. C.↗

NASA NTRS2005

The Space Shuttle Columbia Accident Investigation and Reconstruction: Two Years Later

The Space Shuttle Columbia was lost during re-entry over two years ago. Since the release of the official materials-related findings in August of 2003, additional testing and analysis of select pieces of debris has continued. Microanalytical techniques, including EMPA, ESCA, and x-ray elemental dot mapping, were employed during the initial investigation; the results related the microstructural characteristics of deposit layers to the breach location in the leading edge of the left wing. Such characteristics included deposition order, composition, and distribution. Subsequent to the original efforts, new analytical data and information, not available at the time of the primary investigation, has been generated. This data was obtained via a low-vacuum SEM, fitted not only with a light-element EDS detector, but an XRF tube as well. Essentially, for elements up to sodium, classic EDS was utilized; above sodium, XRF was used. Predominantly, the elements of interest were aluminum, titanium, chromium, iron, nickel, and copper. The findings of both old and new data are compared, and their application to the overall accident investigation detailed.

McDanels, Steven J.↗

DOE OSTI2026

Statistical White-Line Analysis in High-Throughput TXM-XANES for Chemical State Quantification

The transmission X-ray microscopy (TXM) based X-ray absorption near-edge structure (XANES) technique provides three-dimensional mapping of element-specific chemical states at nanometer-scale spatial resolution and micrometer-scale fields of view. However, compared to conventional volume-averaged XANES (VA-XANES) measurements, the inherently small voxel size in TXM-XANES leads to a lower signal-to-noise ratio, making full-spectrum analysis computationally demanding and less robust. Here, we present the structural and compositional conditions for a statistical white-line analysis framework under which chemical state information can be directly extracted from the white-line peak position in voxel spectra without the need for voxel-wise background subtraction or normalization, under well-defined structural and compositional conditions. The method is validated on layered oxide cathode materials, where low-order polynomial fitting accurately reproduces white-line features, and the extracted energy distributions correlate strongly with VA-XANES results. This statistical approach enables high-throughput, dose-efficient, and noise-robust chemical state quantification in TXM-XANES, offering broad applicability to functional materials requiring nanoscale oxidation-state mapping.

TXM↗

NASA NTRS2013

Selection of Hyperspectral Narrowbands (HNBs) and Composition of Hyperspectral Twoband Vegetation Indices (HVIs) for Biophysical Characterization and Discrimination of Crop Types Using Field Reflectance and Hyperion-EO-1 Data

The overarching goal of this study was to establish optimal hyperspectral vegetation indices (HVIs) and hyperspectral narrowbands (HNBs) that best characterize, classify, model, and map the world's main agricultural crops. The primary objectives were: (1) crop biophysical modeling through HNBs and HVIs, (2) accuracy assessment of crop type discrimination using Wilks' Lambda through a discriminant model, and (3) meta-analysis to select optimal HNBs and HVIs for applications related to agriculture. The study was conducted using two Earth Observing One (EO-1) Hyperion scenes and other surface hyperspectral data for the eight leading worldwide crops (wheat, corn, rice, barley, soybeans, pulses, cotton, and alfalfa) that occupy approx. 70% of all cropland areas globally. This study integrated data collected from multiple study areas in various agroecosystems of Africa, the Middle East, Central Asia, and India. Data were collected for the eight crop types in six distinct growth stages. These included (a) field spectroradiometer measurements (350-2500 nm) sampled at 1-nm discrete bandwidths, and (b) field biophysical variables (e.g., biomass, leaf area index) acquired to correspond with spectroradiometer measurements. The eight crops were described and classified using approx. 20 HNBs. The accuracy of classifying these 8 crops using HNBs was around 95%, which was approx. 25% better than the multi-spectral results possible from Landsat-7's Enhanced Thematic Mapper+ or EO-1's Advanced Land Imager. Further, based on this research and meta-analysis involving over 100 papers, the study established 33 optimal HNBs and an equal number of specific two-band normalized difference HVIs to best model and study specific biophysical and biochemical quantities of major agricultural crops of the world. Redundant bands identified in this study will help overcome the Hughes Phenomenon (or "the curse of high dimensionality") in hyperspectral data for a particular application (e.g., biophysical characterization of crops). The findings of this study will make a significant contribution to future hyperspectral missions such as NASA's HyspIRI. Index Terms-Hyperion, field reflectance, imaging spectroscopy, HyspIRI, biophysical parameters, hyperspectral vegetation indices, hyperspectral narrowbands, broadbands.

Vegetation↗

NASA NTRS1981

Some examples of the utility of HCMM data in geologic remote sensing

Examples of HCMM (Heat Capacity Mapping Mission) data in geologic remote sensing are presented, and the data set is composed of HCMM and aircraft digital scanner data and ground truth data from four western U.S. test sites. Data are used in the thermal model to test thermal data effectiveness, and changes in temperature with depth and time for dry soils are described by the model. It is found that the HCMM thermal inertia image is useful in the separability of bedrock and alluvium in Death Valley, and aa and pahoehoe flows in the Pisgah basalt flow. In a color composite of HCMM day temperature, night temperature, and day visible images of the Pisgah Crater test site, it is possible to distinguish alluvium, playa, aa and pahoehoe basalt flow, rhyolite intrusives, and other elements. Ground checking of units at a few points will extend capabilities to large areas and assist in creating telegeologic maps.

Kahle, A. B.↗