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At least 1,117 records · Page 62

Material characterization of superplastically formed titanium (Ti-6Al-2Sn-4Zr-2Mo) sheet

The aerospace industry has focused considerable interest on the near-alpha titanium alloy Ti-6Al-2Sn-4Zr-2Mo (Ti-6242) because of both its high-temperature properties and its superplastic forming (SPF) capabilities. This paper describes current research to characterize selected mechanical properties of Ti-6242 sheet in the SPF-strained condition, both with and without heat treatment, and compares the results with those obtained on as-received material. Tensile and creep tests were conducted, and metallographic analysis was performed to show the effect of 100 to 700 percent SPF strain on titanium properties. Analysis shows that as a result of SPF processing, both tensile and yield strengths, as well as elongation, are moderately reduced. Creep tests at 800 F and 1000 F show that the SPF processed material displays superior creep resistance compared with the as-received material. A post-SPF duplex-anneal heat treatment had no beneficial effect on tensile and creep properties.

Ossa, William A.↗

A review of tin oxide-based catalytic systems: Preparation, characterization and catalytic behavior

This paper reviews the important aspects of the preparation, characterization and catalytic behavior of tin oxide-based catalytic systems including doped tin oxide, mixed oxides which contain tin oxide, Pt supported on tin oxide and Pt/Sn supported on alumina. These systems have a broad range of applications and are continually increasing in importance. However, due to their complex nature, much remains to be understood concerning how they function catalytically.

Hoflund, Gar B.↗

Characterization of Pt/SnO2 catalysts for CO oxidation

Results are presented of surface characterization of 2% and 1% (w/w) Pt on SnO2 catalysts which are being used in promoting the oxidation of CO in pulsed CO2 lasers. The N2 adsorption BET surface area for both catalysts is 6.9 sq m/g. The CO chemisorbed area at 313K is 0.17 sq m/g and 0.062 sq m/g for the 2% and 1% catalysts, respectively. Monitoring the reaction between CO and O2 by the same technique, at the same temperature yields a turn-over frequency (TOF) for the 2% catalyst of 2.7 x 100 molecules of CO2/site/s and for the 1% catalyst a value of 1.2 x 100. The ratio of the TOFs for the two catalysts is 2.2 which is approximately the ratio of the Pt loading.

Brown, K. G.↗

General purpose algorithms for characterization of slow and fast phase nystagmus

In the overall aim for a better understanding of the vestibular and optokinetic systems and their roles in space motion sickness, the eye movement responses to various dynamic stimuli are measured. The vestibulo-ocular reflex (VOR) and the optokinetic response, as the eye movement responses are known, consist of slow phase and fast phase nystagmus. The specific objective is to develop software programs necessary to characterize the vestibulo-ocular and optokinetic responses by distinguishing between the two phases of nystagmus. The overall program is to handle large volumes of highly variable data with minimum operator interaction. The programs include digital filters, differentiation, identification of fast phases, and reconstruction of the slow phase with a least squares fit such that sinusoidal or psuedorandom data may be processed with accurate results. The resultant waveform, slow phase velocity eye movements, serves as input data to the spectral analysis programs previously developed for NASA to analyze nystagmus responses to pseudorandom angular velocity inputs.

Lessard, Charles S.↗

Microwave characterization and modeling of GaAs/AlGaAs heterojunction bipolar transistors

The characterization and modeling of a microwave GaAs/AlGaAs heterojunction Bipolar Transistor (HBT) are discussed. The de-embedded scattering parameters are used to derive a small signal lumped element equivalent circuit model using EEsof's Touchstone software package. Each element in the equivalent circuit model is shown to have its origin within the device. The model shows good agreement between the measured and modeled scattering parameters over a wide range of bias currents. Further, the MAG (maximum available power gain) and the h sub 21 (current gain) calculated from the measured data and those predicted by the model are also in good agreement. Consequently, the model should also be capable of predicting the f sub max and the f sub T of other HBTs.

Simons, Rainee N.↗

Acousto-ultrasonic input-output characterization of unidirectional fiber composite plate by SH waves

A unidirectional fiberglass epoxy composite plate specimen is modelled as a homogeneous transversely isotropic continuum plate medium. Acousto-ultrasonic non-contact input-output characterization by tracing SH waves in the continuum is studied theoretically with a transmitting and receiving transducer located on the same face of the plate. It is found that the directional dependence of the phase velocity of the SH waves travelling in the transversely isotropic medium has a significant effect on the delay time as opposed to the phase velocity of the SH wave travelling in an isotropic medium.

Williams, James H., Jr.↗

Electro-optical characterization of GaAs solar cells

The electro-optical characterization of gallium arsenide p/n solar cells is discussed. The objective is to identify and understand basic mechanisms which limit the performance of high efficiency gallium arsenide solar cells. The approach involves conducting photoresponse and temperature dependent current-voltage measurements, and interpretation of the data in terms of theory to determine key device parameters. Depth concentration profiles are also utilized in formulating a model to explain device performance.

Olsen, Larry C.↗

Spectral characterization of Martian soil analogues

As previously reported, reflectance spectra of iron oxide precipitated as ultrafine particles, unlike ordinary fine grained hematite, have significant similarities to reflectance spectra from the bright regions of Mars. These particles were characterized according to composition, magnetic properties, and particle size distribution. Mossbauer, magnetic susceptibility, and optical data were obtained for samples with a range of concentrations of iron oxide in silica gel of varying pore diameters. To analyze the Mossbauer spectra, a versatile fitting program was enhanced to provide user friendly screen input and theoretical models appropriate for the superparamagnetic spectra obtained.

Agresti, David G.↗

APS-Workshop on Characterization of MMIC (Monolithic Microwave Integrated Circuit) Devices for Array Antenna

The IEEE AP-S ADCOM is attempting to expand its educational, tutorial and information exchange activities as a further benefit to all members. To this end, ADCOM will be forming specialized workshops on topics of interest to its members. The first such workshop on Characterization and Packaging of MMIC Devices for Array Antennas was conceived. The workshop took place on June 13, 1986 as part of the 1986 International Symposium sponsored by IEEE AP-S and URSI in Philadelphia, PA, June 9-13, 1986. The workshop was formed to foster the interchange of ideas among MMIC device users and to provide a forum to collect and focus information among engineers experienced and interested in the topic. After brief presentations by the panelists and comments from attendees on several subtopics, the group was divided into working committees. Each committee evaluated and made recommendations on one of the subtopics.

Smetana, Jerry↗

FTIR characterization of advanced materials

This paper surveys the application of Fourier transform infrared spectroscopy to the characterization of advanced materials. FTIR sampling techniques including internal and external reflectance and photoacoustic spectroscopy are discussed. Representative examples from the literature of the analysis of resins, fibers, prepregs and composites are reviewed. A discussion of several promising specialized FTIR techniques is also presented.

Young, P. R.↗

Sintering, microstructural, radiographic, and strength characterization of a high-purity Si3N4-based composition

A commercially available high purity alpha-Si3N4 powder (UBE SN-E10) was characterized, milled with additives, and sintered in a high-pressure nitrogen atmosphere at temperatures ranging from 1750 to 2140 C. The composition selected for this study has been previously examined using a different alpha-Si3N4 powder. Densification behavior, microstructure characteristics, X-radiographic appearance, room- and high-temperatures flexural strength, and fracture-initiating flaw sites were determined. The high-temperature flexural strengths significantly exceeded those observed in the earlier studies using an identical composition (different alpha-Si3N4 powder) and similar processing techniques.

Kiser, J. D.↗

Three-dimensional nearfield characterization of a VSTOL jet in turbulent crossflow

This paper documents the measurement and prediction of the near-field evolution of the steady, subsonic, turbulent three-dimensional external aerodynamic flow-field associated with a high speed jet issued from an orifice perpendicular to an imposed crossflow velocity field. A parabolic Navier-Stokes CFD solver is employed, utilizing a Kappa-epsilon closure system with algebraic Reynolds stress equation, in concert with suitably defined porous far-field boundary conditions and a virtual source initial condition procedure. The CFD results correlate well with NASA generated near-field LDA experimental data on mean velocity and rms fluctuation velocity (interpolated to turbulent kinetic energy) distributions. The numerical results in the farther field predict the vortex roll-up and jet deflection/entrainment characterization verified by pitot-static mean velocity experimental data. Detailed results are presented for a circular jet for velocity ratios ranging 4 to 8.

Baker, A. J.↗

Characterization of crystalline LARC-TPI powder

LARC-TPI, a linear aromatic polyimide, developed by NASA Langley Research Center in the late 1970's had thermoplastic character, but its melt-flow properties were much lower than those of conventional thermoplastics. An imidized version of the LARC-TPI molding powder was submitted to NASA-Langley for evaluation. The initial broad melt of this material occurs in the 270 C range and reorders to higher melting forms, depending on the physical and thermal treatments. Rheological characterization of this polymer shows it to have a very low melt viscosity, which increases as the melted specie transforms to other crystalline forms with higher melting temperatures.

Burks, Harold D.↗

Characterization of InGaAs/AlGaAs pseudomorphic modulation-doped field-effect transistors

High-performance pseudomorphic In(y)Ga(1-y)As/Al0.15-Ga0.85As y = 0.05-0.2 MODFET's grown by MBE have been characterized at dc (300 and 77 K) and RF frequencies. Transconductances as high 310 and 380 mS/mm and drain currents as high as 290 and 310 mA/mm were obtained at 300 and 77 K, respectively, for 1-micron gate lengths and 3-micron source-drain spacing devices. Lack of persistent trapping effects, I-V collapse, and threshold voltage shifts observed with these devices are attributed to the use of low mole fraction Al(x)Ga(1-x)As while still maintaining two-dimensional electron gas concentrations of about 1.3 x to the 12th per sq cm. Detailed microwave S-parameter measurements indicate a current gain cut-off frequency of 24.5 GHz when y = 0.20, which is as much as 100 percent better than similar GaAs/AlGaAs MODFET structures, and a maximum frequency of oscillation of 40 GHz.

Ketterson, Andrew A.↗

Surface characterization of InP using photoluminescence

Photoluminescence (PL) measurements have been performed on InP samples in situ during various surface treatments including chemical etching, wet anodization, and low-pressure chemical vapor deposition. It was found, in agreement with previously published results, that the magnitude of the PL signal varies markedly with surface treatment due presumably to changes in either surface-state density, and/or surface potential. In an attempt to assess the effectiveness of this noninvasive method as a tool for characterizing and monitoring the progressive development of a semiconductor surface during processing, a number of experiments on InP have been performed. The results indicate that although some uncertainty may exist in assigning a mechanism for the PL change in any given experiment, the general trend appears to be that surface degradation results in a reduced signal. As a result, process steps which enhance the PL intensity are likely to be beneficial in the preparation of a high-quality interface.

Chang, R. R.↗

Performance characterization of a low power hydrazine arcjet

Hydrazine arcjets, which offer substantial performance advantages over alternatives in geosynchronous satellite stationkeeping applications, have undergone startup, materials compatibility, lifetime, and power conditioning unit design issues. Devices in the 1000-3000 W output range have been characterized for several different electrode configurations. Constrictor length and diameter, electrode gap setting, and vortex strength have been parametrically studied in order to ascertain the influence of each on specific impulse and efficiency; specific impulse levels greater than 700 sec have been achieved.

Knowles, S. C.↗

Mechanical and swelling behaviour of well characterized polybutadiene networks

Endlinking of hydroxyl-terminated polybutadiene with the appropriate isocyanate has been used to prepare well characterized networks. Two networks have been studied with molecular weights of the prepolymers being 6100 and 2400 g/mole by g.p.c. Cylindrical specimens were prepared and the derivatives of the stored energy function with respect to the stretch invariants were determined by torque and normal force measurements in torsion. From these data the Valanis-Landel (1967) stored energy function derivatives w-prime(lambda) were determined for both networks. The stored energy function for the junction constraint model of Flory (1953, 1977, 1979, 1985) which is a special form of the Valanis-Landel function, has been fitted to that determined from the experiments. The contributions to the stored energy function from the phantom network and from the junction constraints respectively do not agree with predictions from the topologies of the networks. In spite of this, the form of w-prime(lambda) for the junction constraint model gives an excellent 'curve fit' to the data. Comparison is also made with equilibrium swelling.

Mckenna, Gregory B.↗

Failure mechanism characterization of platinum alloy

This article describes procedures and results of testing performed on a platinum/10-percent rhodium, thin-wall tubular product. The purpose of the testing was to develop exemplar SEM fractographs to be used to characterize failures under various environmental conditions. Conditions evaluated for the platinum alloys included high temperature, hydrogen environment, braze metal contamination, and cyclic loading.

Rosen, J. M.↗