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Search indexed NASA NTRS and DOE OSTI research on propulsion, heat transfer, battery materials and energy systems. Follow report and document links to the original sources.

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At least 1,099 records · Page 61
All sourcesNASA NTRSDOE OSTI
DOE OSTI2024

Controlling Bond Scission Pathways of Isopropanol on Fe- and Pt-Modified Mo 2 N Model Surfaces and Powder Catalysts

Biomass valorization can be used to produce value-added chemicals and fuels from renewable biomass resources by upgrading them via selective bond scission while retaining certain functional groups. Specifically, upgrading biomass through the dehydrogenation of alcohols to carbonyl compounds has gained interest as a method of utilizing biomass-derived alcohols while additionally producing H 2 . In this work, isopropanol was used as a probe molecule to control bond scission selectivity over Fe- and Pt-modified molybdenum nitride (Mo 2 N) model surfaces and powder catalysts. Trends in the selectivity toward dehydration and dehydrogenation were dependent on both the type and coverage of the metal overlayer on model surfaces. These results were then extended to the corresponding powder catalysts to demonstrate how model surface studies can inform the design of supported catalysts. Density functional theory calculations provided insights into controlling the dehydration and dehydrogenation pathways. In conclusion, this work shows that a fundamental understanding of the reactivity and intermediates on Mo 2 N-based model surfaces can be applied to understand the catalytic performance of metal-modified Mo 2 N powder catalysts, and also demonstrates that Mo 2 N-based catalysts are potentially promising materials for upgrading biomass-derived oxygenates.

09 BIOMASS FUELS↗
DOE OSTI2025

Multimodal Ambient Pressure Sample Environment for the HIPPIE Solid-Gas Endstation at MAX IV Laboratory

The HIPPIE APXPS instruments have undergone several major upgrades, such as developing a dedicated solid gas endstation to specialize in multimodal ambient pressure sample environments centered around X-ray photoelectron spectroscopy. Herein, the technical specifications of the HIPPIE solid gas endstation are detailed; upgrades to the laser heating and gas systems, as well as the addition of an offline 1 bar reactor, are introduced. To demonstrate how the endstation is currently being utilized, scientific examples of all upgrades are presented, as well as science cases using infrared reflection-adsorption spectroscopy. The HIPPIE solid gas endstation is maturing into an instrument offering bespoke sample environments aimed at pushing experimental capabilities, especially in the time-resolved domain.

37 INORGANIC, ORGANIC, PHYSICAL, AND ANALYTICAL CH↗
DOE OSTI2024

Opening pathways for the conversion of woody biomass into sustainable aviation fuel via catalytic fast pyrolysis and hydrotreating

Meeting aggressive decarbonization targets set by the International Civil Aviation Organization (ICAO) will require the rapid development of technologies to produce sustainable aviation fuel (SAF). Catalytic fast pyrolysis (CFP) can support these efforts by opening pathways for the conversion of woody biomass into an upgraded biogenic oil that can be further processed to SAF and other fuels. However, the absence of end-to-end experimental data for the process leads to uncertainty in the yield, product quality, costs, and sustainability of the pathway. The research presented here serves to address these needs through a series of integrated experimental campaigns in which real biomass feedstocks are converted to a final SAF product using large bench-scale continuous reactor systems. For these campaigns, the degree of catalytic upgrading during CFP was varied to produce CFP-oils with oxygen contents of 17 and 20 wt% on a dry basis. The CFP-oils were then hydrotreated and distilled into gasoline, diesel, and SAF fractions. Detailed yield and compositional data were obtained for each step of the process to inform technoeconomic and lifecycle analyses, and the fuel properties of the SAF fraction were evaluated to provide first-of-its-kind insight into the quality of the final product. This research reveals opportunities to optimize process carbon efficiency by tuning the degree of catalytic upgrading during the CFP step and highlights routes to produce a high-quality cycloalkane-rich SAF with 85–92% reduction in greenhouse gas emissions compared to fossil-based pathways.

09 BIOMASS FUELS↗
DOE OSTI2020

40 MHz Level-1 Trigger Scouting for CMS

The CMS experiment will be upgraded for operation at the HighLuminosity LHC to maintain and extend its physics performance under extreme pileup conditions. Upgrades will include an entirely new tracking system, supplemented by a track finder processor providing tracks at Level-1, as well as a high-granularity calorimeter in the endcap region. New front-end and back-end electronics will also provide the Level-1 trigger with high-resolution information from the barrel calorimeter and the muon systems. The upgraded Level-1 processors, based on powerful FPGAs, will be able to carry out sophisticated feature searches with resolutions often similar to the offline ones, while keeping pileup effects under control. In this paper, we discuss the feasibility of a system capturing Level-1 intermediate data at the beam-crossing rate of 40 MHz and carrying out online analyzes based on these limited-resolution data. This 40 MHz scouting system would provide fast and virtually unlimited statistics for detector diagnostics, alternative luminosity measurements and, in some cases, calibrations. It has the potential to enable the study of otherwise inaccessible signatures, either too common to fit in the Level-1 accept budget, or with requirements which are orthogonal to “mainstream” physics, such as long-lived particles. We discuss the requirements and possible architecture of a 40 MHz scouting system, as well as some of the physics potential, and results from a demonstrator operated at the end of Run-2 using the Global Muon Trigger data from CMS. Plans for further demonstrators envisaged for Run-3 are also discussed.

46 INSTRUMENTATION RELATED TO NUCLEAR SCIENCE AND ↗
DOE OSTI2020

W-band system-on-chip electron cyclotron emission imaging system on DIII-D

Monolithic, millimeter wave “system-on-chip” (SoC) technology has been employed in heterodyne receiver integrated circuit radiometers in a newly developed Electron Cyclotron Emission Imaging (ECEI) system on the DIII-D tokamak for 2D electron temperature profile and fluctuation evolution diagnostics. Here, a prototype module operating in E-band (72-80 GHz) was first employed in a 2 x 10 element array that demonstrated significant improvements over the previous quasi-optical Schottky diode mixer arrays during the 2018 operational campaign of the DIII-D tokamak. For compatibility with International Thermonuclear Experimental Reactor (ITER) relevant scenarios on DIII-D, the SoC ECEI system was upgraded with 20 horn-waveguide receiver modules. Each individual module contains a University of California at Davis designed W-band (75 -110 GHz) receiver die that integrates a broadband low noise amplifier (LNA), a double balanced down-converting mixer, and a x4 multiplier on the local oscillator (LO) chain. A x2 multiplier and two IF amplifiers are packaged and selected to further boost the signal strength as well as downconvert the signal frequency. The upgraded W-band array exhibits > 30 dB additional gain and 20x improvement in noise temperature comparing with the previous Schottky diode radio frequency (RF) mixer input systems; an internal 8 times multiplier chain is used to bring down the LO frequency below 12 GHz, thereby obviating the need for a large aperture for quasi-optical LO coupling and replacing it with coaxial connectors. The horn-waveguide shielding housing avoids out-of-band noise interference on each individual module. The upgraded ECEI system plays an important role for absolute electron temperature evolution and fluctuation measurements for edge and core region transport physics studies.

70 PLASMA PHYSICS AND FUSION TECHNOLOGY↗
DOE OSTI2024

Implementation of low temperature spectrometers for the JET high resolution Thomson scattering diagnostic for disruption plasma measurements

This work presents a system upgrade of the High Resolution Thomson Scattering (HRTS) diagnostic on JET that allows it to measure low temperature (1–500 eV) plasma pre- and post-Thermal quench (TQ), which would help us further understand the Shattered Pellet Injection (SPI) physics. The upgrade was done by connecting optic fibers from the original HRTS system to four spectrometers specialized in measuring low temperature plasmas. The upgraded system allows for the measurement of low temperature plasma at up to 12 spatial points, which can be flexibly distributed throughout the JET outer midplane profile during the dedicated SPI experiments. In other JET experiments, four previously unused groups of fibers were used to measure the central plasma to provide disruption data without changing the standard HRTS system. The low temperature Thomson scattering system was installed, commissioned, and cross-calibrated against the standard HRTS diagnostic in a calibration pulse. The system worked reliably during the JET experiments and provided electron density and temperature profiles for pre- and post-TQ low temperature plasmas in the SPI campaign.

46 INSTRUMENTATION RELATED TO NUCLEAR SCIENCE AND ↗
DOE OSTI2020

Characterization of alkylguaiacol-degrading cytochromes P450 for the biocatalytic valorization of lignin

Upgrading lignin, an underutilized component of biomass, is essential for the sustainability of biorefineries. Biocatalysis has considerable potential for upgrading lignin, but our lack of knowledge of relevant enzymes and pathways has limited its application. Herein, we describe a microbial pathway responsible for catabolizing alkylguaiacols, a major component of several industrial lignin streams. Catabolism is initiated by a cytochrome P450, with related P450s catalyzing the O-demethylation of different lignin-derived guaiacols and subsequent catabolism depending on the substitution pattern of the guaiacol. Importantly, the alkylguaiacol catabolic pathway enables bacterial growth on corn stover lignin produced by reductive catalytic fractionation. Overall, these insights greatly facilitate the engineering of P450s and bacteria to biocatalytically upgrade lignin.

59 BASIC BIOLOGICAL SCIENCES↗
DOE OSTI2022

An Integrated Risk Assessment Process of Safety-Related Digital I&C Systems in Nuclear Power Plants

Upgrading the existing analog instrumentation and control (I&C) systems to state-of-the-art digital I&C (DI&C) systems will greatly benefit existing light water reactors. However, the issue of software common cause failure (CCF) remains an obstacle in terms of qualification for digital technologies. Existing analyses of CCFs in I&C systems mainly focus on hardware failures. With the application and upgrading of new DI&C systems, design flaws could cause software CCFs to become a potential threat to plant safety, considering that most redundancy designs use similar digital platforms or software in their operating and application systems. With complex multilayer redundancy designs to meet the single failure criterion, these I&C safety systems are of particular concern in U.S. Nuclear Regulatory Commission licensing procedures. In Fiscal Year 2019, the Risk-Informed Systems Analysis (RISA) Pathway of the U.S. Department of Energy’s Light Water Reactor Sustainability Program initiated a project to develop a risk assessment strategy for delivering a strong technical basis to support effective, licensable, and secure DI&C technologies for digital upgrades and designs. An integrated risk assessment for the DI&C process was proposed for this strategy to identify potential key digital-induced failures, implement reliability analyses of related digital safety I&C systems, and evaluate the unanalyzed sequences introduced by these failures (particularly software CCFs) at the plant level. Here this paper summarizes these RISA efforts in the risk analysis of safety-related DI&C systems at Idaho National Laboratory.

22 GENERAL STUDIES OF NUCLEAR REACTORS↗
DOE OSTI2025

Design and Implementation of Surface Eroding Thermocouples for Stage-One Modular Divertor Integration at the DIII-D Tokamak

The DIII-D has upgraded its upper divertor to a modular system using copper alloy pedestals to alter the divertor geometry without changing the vessel structure. Six new graphite tiles were designed for the shape and volume rise (SVR) divertor. Here, these new SVR tiles facilitated the formation of a poloidal array of 27 surface eroding thermocouples (SETCs) in the upper divertor region. At one location, a specialized recessed SETC, paired with a standard flush SETC, was installed in one of the ceiling tiles to provide comprehensive heat flux measurements, distinguishing between charged and noncharged particle contributions. Upgrades were made to the SETC system in the small-angle slot (SAS) divertor to improve overall performance. These upgrades included optimizing the feedthrough system to double the thermocouple cable capacity and reallocating cables from the SAS area to the SVR divertor. A compact isolation amplifier system with a fixed gain of 41 was employed to improve the signal level and minimize interference. Additionally, two analog-to-analog fiber systems were implemented for transmitting thermocouple signals over a single fiber, significantly reducing both noise levels and costs. The newly installed SETCs in the SVR divertor successfully completed initial commissioning testing. The SETCs captured the in-out asymmetry in the power distribution between the inner and outer strike points and demonstrated the dependency of the heat flux profile on the outer strike point location. During divertor detachment, heat flux mitigation was noted at the outer strike point location, while significant heat flux contributions from neutral particles were measured in the SVR divertor.

Divertor↗
DOE OSTI2022

Influence of triangularity on the plasma response to resonant magnetic perturbations

The effect of the axisymmetric plasma shape on the non-axisymmetric plasma response to resonant magnetic perturbations is investigated in experiment and modeling for the DIII-D, EAST and ASDEX Upgrade tokamaks. Systematically modeling the effect of the triangularity, whilst keeping other equilibrium quantities largely unchanged, reveals that the plasma response is strongly suppressed at high triangularity compared to that at low triangularity. This is validated through targeted comparison with experiments at DIII-D, EAST, and ASDEX Upgrade. DIII-D and EAST magnetic measurements are used to validate simulations, while at ASDEX Upgrade the plasma edge displacement is measured. Both experiments and modeling find a reduced magnetic plasma response on the high-field side at high triangularity across devices. Multi-modal analysis of the simulation results extracts the mode structure and applied spectrum dependence of each mode. The amplitude of the dominant mode reveals similar trends with the edge resonance and radial displacement near the X-point, which suggests that the multi-mode plasma response provides another way to understand the edge localized mode (ELM) control physics. The plasma response is strongly reduced at high triangularity compared to that at low triangularity, which implies different ELM control effects as shaping is varied. Furthermore, these findings indicate that the plasma shape should be taken into consideration when designing an RMP-ELM control strategy in experiment, and that predictive plasma response calculations can be used to maximize access to RMP-ELM control in future devices by maximizing the coupling between coils and the plasma.

70 PLASMA PHYSICS AND FUSION TECHNOLOGY↗
DOE OSTI2020

Design and performance of an in-vacuum, magnetic field mapping system for the Muon g-2 experiment

The Muon g - 2 experiment at Fermilab (E989) aims to measure the anomalous magnetic moment, a μ , of the muon with a precision of 140 parts-per-billion. This requires a precise measurement of both the anomalous spin precession frequency, ω α , of muons stored in a magnetic field of 1.45 T, and a precise measurement of that magnetic field in terms of the shielded proton Larmor frequency, ω' ρ . The measurement of ω' ρ with a total systematic uncertainty of 70 parts-perbillion involves a combination of various nuclear magnetic resonance (NMR) probes. There are 378 probes mounted in fixed locations that constantly monitor field drifts. A water-based, cylindrical calibration probe provides the calibration in terms of the shielded proton Larmor frequency. A crucial element for the multi-step measurement of ω' ρ is the regular mapping of the magnetic field over the muon storage region. The former experiment at Brookhaven National Laboratory (BNL) employed an in-vacuum field mapping system equipped with 17 NMR probes, which was developed by the University of Heidelberg. We have refurbished and upgraded this system with new probes and electronics. The upgrades include the addition of 16-bit, 1 MSPS digitization of the NMR signals, which replaced the hardware-implemented zero-crossing counting of the system at Brookhaven. The digitized signals offer new capabilities in the NMR frequency analysis and its related systematic uncertainties. To sustain the higher data rates, a new communication scheme with time-division multiplexing was implemented to separate the important NMR reference clock from the data communication in order to reach the specifications for the accuracy and stability of the reference clock. A new barcode reader provides more precise azimuthal position determination during the measurement and calibration. While the mechanical systems that move the field mapper inside the storage ring have been mostly refurbished from BNL, the motion control system was completely replaced with a custom-built electronics centered around a commercial Galil motion controller. Both the field mapping NMR system and its motion control were successfully commissioned at Fermilab and have been in reliable operation during the first three data taking periods of the experiment at Fermilab. Finally, this article will provide the details of the upgrades of the field mapper and its performance.

47 OTHER INSTRUMENTATION↗
DOE OSTI2023

AugerPrime surface detector electronics

Operating since 2004, the Pierre Auger Observatory has led to major advances in our understanding of the ultra-high-energy cosmic rays. The latest findings have revealed new insights that led to the upgrade of the Observatory, with the primary goal of obtaining information on the primary mass of the most energetic cosmic rays on a shower-by-shower basis. In the framework of the upgrade, called AugerPrime, the 1660 water-Cherenkov detectors of the surface array are equipped with plastic scintillators and radio antennas, allowing us to enhance the composition sensitivity. To accommodate new detectors and to increase experimental capabilities, the electronics is also upgraded. This includes better timing with up-to-date GPS receivers, higher sampling frequency, increased dynamic range, and more powerful local processing of the data. In this paper, the design characteristics of the new electronics and the enhanced dynamic range will be described. The manufacturing and test processes will be outlined and the test results will be discussed. The calibration of the SD detector and various performance parameters obtained from the analysis of the first commissioning data will also be presented.

46 INSTRUMENTATION RELATED TO NUCLEAR SCIENCE AND ↗
DOE OSTI2025

ECON-T and ECON-D: Endcap Concentrator ASICs for the CMS HGCAL

With over 6 million channels, the High Granularity Calorimeter (HGCAL) for the CMS HL-LHC Upgrade presents a unique data challenge. The ECON ASICs provide critical on-detector data reduction for the 40 MHz trigger path (ECON-T) and 750 kHz data acquisition path (ECON-D) of the HGCAL. The ASICs, fabricated in 65 nm CMOS, are rad-tolerant (600 Mrad) with low power consumption (<2.5 mW/channel). This presentation is the first comprehensive description of the ECON designs, first functionality and radiation tests for the ECON-T ASIC, and first results from the full production of 75k ECON-D and ECON-T ASICs.

Bergamin, G. [CERN] (ORCID:0000000285758704)↗
DOE OSTI2024

The Continuous Electron Beam Accelerator Facility at 12 GeV

This review paper describes the energy-upgraded Continuous Electron Beam Accelerator Facility (CEBAF) accelerator. This superconducting linac has achieved 12 GeV beam energy by adding 11 new high-performance cryomodules containing 88 superconducting cavities that have operated cw at an average accelerating gradient of 20 MV / m . After reviewing the attributes and performance of the previous 6 GeV CEBAF accelerator, we discuss the upgraded CEBAF accelerator system in detail with particular attention paid to the new beam acceleration systems. In addition to doubling the acceleration in each linac, the upgrade included improving the beam recirculation magnets, adding more helium cooling capacity to allow the newly installed modules to run cold, adding a new experimental hall, and improving numerous other accelerator components. We review several of the techniques deployed to operate and analyze the accelerator performance and document system operating experience and performance. In the final portion of the document, we present much of the current planning regarding projects to improve accelerator performance and enhance operating margins, and our plans for ensuring CEBAF operates reliably into the future. For the benefit of potential users of CEBAF, the performance and quality measures for the beam delivered to each of the experimental halls are summarized in the Appendix. Published by the American Physical Society 2024

43 PARTICLE ACCELERATORS↗
DOE OSTI2024

Virtual Tokamak for Test and Development of Plasma Control Applied to NSTX-U

Safe and efficient operation of tokamak experiments depends on shot preparation prior to the experiment to maximize performance and avoid issues that are predictable consequences of known physics. The General Atomics TokSys toolbox is used to test and develop the plasma control system (PCS) on numerous tokamaks around the world. Tokamaks that use a version of the DIII-D PCS can connect it to a TokSys simulation and control a virtual version of the tokamak with the real PCS. Recent upgrades to the simulation include more detailed profile and transport modeling to support design and implementation of optimized scenarios. The simulation combines a module called “Profiles” that simulates the 1D profiles of density, pressure, and current and a module called “GSevolve'' that evolves the 2D Grad-Shafranov equilibrium. The “Profiles'' module primarily uses simplified models for fueling, heating, and current. The TRANSP code provides precomputed diffusion coefficients and heating/current drive profiles from radio-frequency and neutral beam sources for the scenarios being simulated. The fidelity of a simulation can be enhanced by analyzing it with TRANSP and making corrections to the precomputed values and iterating until convergence. Simulations of the National Spherical Torus Upgrade (NSTX-U) are presented. It is shown that the simulation reproduces the experimental profile evolution. Here, the simulation has also been upgraded to reproduce the experimental outcome at points of bifurcation. This is demonstrated with a simulation of vertical displacement in NSTX-U.

70 PLASMA PHYSICS AND FUSION TECHNOLOGY↗
DOE OSTI2022

Techno-economic assessment for the production of algal fuels and value-added products: opportunities for high-protein microalgae conversion

Abstract Background Microalgae possess numerous advantages for use as a feedstock in producing renewable fuels and products, with techno-economic analysis (TEA) frequently used to highlight the economic potential and technical challenges of utilizing this biomass in a biorefinery context. However, many historical TEA studies have focused on the conversion of biomass with elevated levels of carbohydrates and lipids and lower levels of protein, incurring substantial burdens on the ability to achieve high cultivation productivity rates relative to nutrient-replete, high-protein biomass. Given a strong dependence of algal biomass production costs on cultivation productivity, further TEA assessment is needed to understand the economic potential for utilizing potentially lower-cost but lower-quality, high-protein microalgae for biorefinery conversion. Results In this work, we conduct rigorous TEA modeling to assess the economic viability of two conceptual technology pathways for processing proteinaceous algae into a suite of fuels and products. One approach, termed mild oxidative treatment and upgrading (MOTU), makes use of a series of thermo-catalytic operations to upgrade solubilized proteins and carbohydrates to hydrocarbon fuels, while another alternative focuses on the biological conversion of those substrates to oxygenated fuels in the form of mixed alcohols (MA). Both pathways rely on the production of polyurethanes from unsaturated fatty acids and valorization of unconverted solids for use as a material for synthesizing bioplastics. The assessment found similar, albeit slightly higher fuel yields and lower costs for the MA pathway, translating to a residual solids selling price of $899/ton for MA versus $1033/ton for MOTU as would be required to support a $2.50/gallon gasoline equivalent (GGE) fuel selling price. A variation of the MA pathway including subsequent upgrading of the mixed alcohols to hydrocarbon fuels (MAU) reflected a required solids selling price of $975/ton. Conclusion The slight advantages observed for the MA pathway are partially attributed to a boundary that stops at oxygenated fuels versus fungible drop-in hydrocarbon fuels through a more complex MOTU configuration, with more comparable results obtained for the MAU scenario. In either case, it was shown that an integrated algal biorefinery can be economical through optimal strategies to utilize and valorize all fractions of the biomass.

09 BIOMASS FUELS↗
DOE OSTI2024

Permanent Magnet Resiliency in Jefferson Lab’s Radiation Environment: LDRD Grant Status and Plans

As the FFA@CEBAF energy upgrade study progresses, it is important to investigate the impact of radiation exposure on the permanent magnet materials to be used in the upgraded fixed field alternating gradient (FFA) arcs. To address this, Jefferson Lab has awarded a Laboratory Directed Research and Development (LDRD) grant to study the resiliency of several permanent magnet materials placed in a radiation environment similar to that in which they are expected to operate. Samples of NeFeB and SmCo are to be placed alongside appropriate dosimetry in a variety of radiation environments in the beam enclosure and experimental halls at CEBAF. The magnet degradation will be measured, and extrapolated to the higher energies expected during operations after the energy upgrade. This document will describe the current status of the LDRD study, as well as describe the upcoming plans. It will also direct the readers to other proceedings which further detail the work thus far.

Bodenstein, R.↗
DOE OSTI2024

First results of AUP Nb3Sn quadrupole horizontal tests

The Large Hadron Collider will soon undergo an upgrade to increase its luminosity by a factor of ~10 [1]. A crucial part of this upgrade will be replacement of the NbTi focusing magnets with Nb3Sn magnets that achieve a ~50% increase in the field strength. This will be the first ever large-scale implementation of Nb3Sn magnets in a particle accelerator. The High-Luminosity LHC Upgrade, HL-LHC is a CERN project with a world-wide collaboration. It is under construction and utilizes Nb3Sn Magnets (named MQXF) as key ingredients to increase tenfold the integrated luminosity delivered to the CMS and ATLAS experiments in the next decade. The HL-LHC AUP is the US effort to contribute approximately 50% of the low-beta focusing magnets and crab cavities for the HL-LHC. This paper will present the program to fabricate the Nb3Sn superconducting magnets. We are reporting the status of the HL-LHC AUP project present the results from horizontal tests of the first fully assembled cryo-assembly.

43 PARTICLE ACCELERATORS↗