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NASA NTRSDate not supplied

First in-situ Nitrogen Isotope Measurements in Martian Meteorites

The origin and timing of the accretion of volatile elements on the terrestrial planets remains a subject of controversy. Nitrogen and hydrogen isotopes are powerful tools to constrain the source(s) of primordial volatiles accreted by planetary bodies because their isotope ratios (15N/14N; D/H) differ significantly between different solar system reservoirs (e.g., solar, chondritic, cometary). Hf-W data of martian samples indicate that Mars accreted very rapidly in the inner solar system and reached half ofits size in 1.8 Myr [1]. Therefore, martian samples are key to understand the distribution of volatile elements in the inner solar system during the early stages of planetary formation. Since no space missions have yet returned samples from Mars, martian meteorites (Shergottites, Nakhlites, Chassignites) are unique samples to constrain the source(s) of volatiles present in the martian mantle. The goal of this study was to target pristine phases(e.g., melt inclusions, mesostasis) for in-situ measurements of their nitrogen content and isotopic ratios to access the most primitive melt of the Chassignites and Nakhlites reservoirs. Five different Nakhlites (Nakhla, NWA 998, MIL 03346, Y 000593,NWA 6148) and Chassigny were analysed [2] using a recent high-resolution analytical technique that allows constraining the nitrogen composition of both carbon-bearing and carbon-free phases in natural and synthetic samples. Nitrogen was measured in the form of 14N16O- and 15N16O- with the CAMECA 1280-HR2 at the CRPG [3]. A significant amount of nitrogen was detected in melt inclusions in Chassigny and in the mesostasis of Nakhla, Y000593, MIL 03346, and NWA 6148. Nitrogen isotope signatures of Chassigny and Nakhlites exhibit a heavy isotope enrichment compared to Earth's mantle, and are consistent with a carbonaceous chondrite-like source [4]. This suggests that Earth and Mars accreted nitrogen from different chondritic sources. Overall, our in-situ technique is a unique and powerful tool to characterize the nitrogen abundance and isotopic composition of natural samples.

C Deligny↗
NASA NTRS2000

Performance of Adsorption - Based CO2 Acquisition Hardware for Mars ISRU

Chemical processing of the dusty, low-pressure Martian atmosphere typically requires conditioning and compression of the gases as first steps. A temperature-swing adsorption process can perform these tasks using nearly solid-state hardware and with relatively low power consumption compared to alternative processes. In addition, the process can separate the atmospheric constituents, producing both pressurized CO2 and a buffer gas mixture of nitrogen and argon. To date we have developed and tested adsorption compressors at scales appropriate for the near-term robotic missions that will lead the way to ISRU-based human exploration missions. In this talk we describe the characteristics, testing, and performance of these devices. We also discuss scale-up issues associated with meeting the processing demands of sample return and human missions.

Finn, John E.↗
NASA NTRSDate not supplied

Venus Sample Return Using In-situ Propellant

This project will pioneer a new approach to return a sample from the surface of Venus. At 450°C and 92 bar pressure, the Venus surface is the most hostile environment in the solar system. This project merges an innovative carbon monoxide rocket concept using propellant made from the Venus atmosphere with innovations in high-temperature technology and solar aircraft. We turn an ambitious mission into a reality. The mission will return a sample from the scorching surface of Venus, using a novel multi-step approach incorporating new technology. The high-temperature solar aircraft collects the sample from the surface and carries it above the main cloud deck to a balloon platform with a launch vehicle & propellant manufacturing plant. The carbon monoxide/oxygen monopropellant is manufactured from the Venus atmosphere.

Venus↗
NASA NTRS1974

Mineralogy, petrology, and chemistry of basalt fragments returned by Luna 16

Mineralogical, petrological, and chemical analyses, along with Rb-Sr age and Ar-40/Ar-39 measurements, were carried out with the B-1 sample returned from the Luna 16 mission. The sample, weighing 62 mg, is a fine-grain basalt of ophitic structure. It differs from the Apollo samples in that the pyroxene and plagioclass contents are almost identical, and the ilmenite content (7%) lies between those of the Apollo-11 and Apollo-12 samples. Chemically, it is characterized by a high Sr content and a high K/U ratio.

Albee, A. L.↗
NASA NTRS2000

JSC Stardust Curation Team

STARDUST, a NASA Discovery-class mission, is the first to return samples from a comet. Grains from comet Wild 2's coma-the gas and dust envelope that surrounds the nucleus-will be collected as well as interstellar dust. The mission which launched on February 7, 1999 will encounter the comet on January 10, 2004. As the spacecraft passes through the coma, a tray of silica aerogel will be exposed, and coma grains will impact there and become captured. Following the collection, the aerogel tray is closed for return to Earth in 2006. A dust impact mass spectrometer on board the STARDUST spacecraft will be used to gather spectra. of dust during the entire mission, including the coma passage. This instrument will be the best chance to obtain data on volatile grains, which will not be well-collected in the aerogel. The dust impact mass spectrometer will also be used to study the composition of interstellar grains. In the past 5 years, analysis of data from dust detectors aboard the Ulysses and Galileo spacecraft have revealed that there is a stream of interstellar dust flowing through our solar system. These grains will be captured during the cruise phase of the STARDUST mission, as the spacecraft travels toward the comet. The sample return capsule will parachute to Earth in February 2006, and will land in western Utah. Once on y the ground, the sample return capsule will be placed into a dry nitrogen environment and flown to the curation lab at JSC.

Zolensky, Michael E.↗
NASA NTRSDate not supplied

Overview of the Capture, Containment, and Return System (CCRS)

The Mars Sample Return (MSR) campaign is one of the most ambitious and complex planetary exploration missions currently underway. With the participation of NASA, ESA, and a large number of industry partners, MSR aims to bring Martian soil, rock, and atmospheric samples back to Earth, in order to answer key questions about Mars’ biological evolution. To accomplish this goal the campaign relies on four coordinated missions, each fulfilling a fundamental role to bring the samples to Earth. The Mars Perseverance rover, the first of the four missions, landed safely on Mars on February 18, 2021 and has already acquired candidate samples for Earth return. A selection of the samples of Martian soil and atmosphere that Perseverance has captured during its mission will be recovered, launched into Mars orbit, and transported back to Earth. The Sample Fetch Rover and Mars Ascent System, both parts of the Sample Return Lander project, perform the Mars surface missions to retrieve the collected samples and launch them into Mars orbit. NASA’s Capture, Containment, and Return System (CCRS), hosted on ESA’s Earth Return Orbiter (ERO), brings the samples back to Earth from Mars orbit. These retrieval and return missions are currently in the planning and design stages of development. The NASA-provided CCRS is the payload of the ESA ERO and is the focus of this presentation. ERO will enter Mars orbit and provide communication relay to Earth for the other MSR elements. The Sample Return Lander systems will fetch the sample tubes and integrate them into a protective vessel – the Orbiting Sample (OS) system – which is then launched into low Mars orbit. ERO will perform rendezvous maneuvers, allowing its CCRS payload to capture the OS, contain it, and perform the first automated in-space assembly of a spacecraft, the Earth Entry System (EES), while in Mars orbit. ERO will then begin its journey back to Earth, with CCRS and its assembled EES spacecraft. Three days prior to arrival, CCRS will release the EES on an Earth entry trajectory from a distance beyond the orbit of the Moon. The passive EES spacecraft will then enter Earth’s atmosphere, flying on a ballistic trajectory, followed by a terminal descent (without a parachute) and landing at the Utah Test and Training Range (UTTR). This presentation will show the current design of the CCRS system and its concept of operations. ERO and CCRS will perform several firsts in planetary exploration: (a) orbital rendezvous and capture in Mars orbit, (b) in-space sterilization and containment, (c) on-orbit spacecraft assembly at Mars, and (d) fully-passive entry, descent, and landing sequence for sample return.

Carlie H. Zumwalt↗
NASA NTRS1985

The geologic history of quartz-normative and olivine-normative basalts in the vicinity of Hadley Rille (Apollo 15)

The geologic history of the quartz normative (QNB) and olivine normative (ONB) basalt types at Hadley Rille are discussed. A model for the geology of the mare basalts was constructed from a combination of field observations, sample chemistry, sample petrology and personal bias from terrestrial experience. The model proposes that the QNBs are the only mare lava type that is present as outcrop in the area traversed by the astronauts during the Apollo 15 mission. The returned QNB samples formed during a single eruptive phase of the Hadley Rille lava tube system. The ONB lavas are an exotic component transported to the site by a cratering event, or the ONBs are samples excavated from older are bedrock that was partly covered by the QNB lavas.

Grove, T. L.↗
NASA NTRSDate not supplied

Atmosphere Modeling and Performance Sensitivity for the Mars Sample Return Earth Entry System

The Capture, Containment, and Return System (CCRS) mission is a key element of the joint NASA-European Space Agency (ESA) planned Mars Sample Return (MSR) Campaign. The CCRS assembled Earth Entry System (EES) will enter the mission’s final segment in its Approach, Entry, Descent, and Landing (AEDL) Phase. The EES AEDL aims to deliver a highly reliable, safe, and accurate return while maintaining strict containment assurance targets established by the campaign. As currently designed, the EES would be the first fully passive sample return capsule with no parachute or onboard control system, prompting a significant effort in Earth atmosphere characterization and modeling. Earth’s atmosphere, specifically winds, have a strong influence on EES flight mechanics and landing footprint during its free fall landing. This paper describes Earth atmosphere modeling, atmosphere characterization, and performance sensitivities incorporated into the teams’s efforts to ensure AEDL success. By utilizing high resolution balloon radiosondes, analyzing wind structural and distributional compositions, and investigating flight mechanics sensitivities, the AEDL atmosphere team has been able to better understand and simulate local wind conditions at the Utah Test and Training Range (UTTR). Utilizing tools such as horizontal turbulent kinetic energy, vertical wind shear, or integrated wind, the team have been able to reveal valuable information about wind profiles in a deeper context than previously conducted, ultimately improving understanding of AEDL flight mechanics sensitivity and EES design.

Kaustubh Ray↗
NASA NTRS2004

Acquisition of a High-resolution Inductively Coupled Plasma Mass Spectrometer for Cosmochemical and Geochemical Research

The primary goal of our research in this program is to develop new techniques for the analysis of volatile trace elements in very small samples using inductively coupled plasma mass spectrometry (ICP-MS) in preparation for samples returned by the Stardust mission. The instrument that will serve as the basis of our experiments is the ELEMENT2 high-resolution ICP-MS. We have spent the past year designing the laboratory to house this instrument as well as space to store and prepare samples returned by the Stardust mission. Unfortunately, the location that we had initially selected for the instrument turned out to be insufficient for our needs. This was determined almost eight months into the first year of our funding cycle, after extensive work including the production of engineering drawings. However, during this time the Lunar and Planetary Laboratory was selected to lead Phoenix, the first Mars Scout mission. As a result of this award LPL purchased a new, 50,000 square foot building. We have acquired 1400 square feet of laboratory space in this new facility. Four-hundred square feet will be used for a class-100 clean room. This area is designated for storage and preparation of extraterrestrial materials. The additional 1000 square feet will house the ELEMENT2 ICP-MS and peripheral devices. This is an enormous amount of space for this instrument, but it provides plenty of room for expansion in the future. The ICP-MS and the clean room facilities have been purchased. The instrument has been delivered. The startup time for this instrument is relatively short and we expect to be collecting our first data by mid-summer.

Lauretta, D. S.↗
NASA NTRS2019

The CAESAR New Frontiers Mission: 1. Expected Nature of the Returned Comet Sample

Comets are time capsules from the birth of our Solar System that record pre-solar history, the initial stages of planet formation, and the sources of prebiotic organics and volatiles for the origin of life. These capsules can only be opened in laboratories on Earth. CAESAR (Comet Astrobiology Exploration Sample Return)’s sample analysis objectives are to understand the nature of Solar System starting materials and how these components came together to form planets and give rise to life. Examination of these comet nucleus surface samples in laboratories around the world will also provide ground truth to remote observations of the innumerable icy bodies of the Solar System.

Lauretta, D. S.↗
NASA NTRS1990

Lunar Polar Coring Lander

Plans to build a lunar base are presently being studied with a number of considerations. One of the most important considerations is qualifying the presence of water on the Moon. The existence of water on the Moon implies that future lunar settlements may be able to use this resource to produce things such as drinking water and rocket fuel. Due to the very high cost of transporting these materials to the Moon, in situ production could save billions of dollars in operating costs of the lunar base. Scientists have suggested that the polar regions of the Moon may contain some amounts of water ice in the regolith. Six possible mission scenarios are suggested which would allow lunar polar soil samples to be collected for analysis. The options presented are: remote sensing satellite, two unmanned robotic lunar coring missions (one is a sample return and one is a data return only), two combined manned and robotic polar coring missions, and one fully manned core retrieval mission. One of the combined manned and robotic missions has been singled out for detailed analysis. This mission proposes sending at least three unmanned robotic landers to the lunar pole to take core samples as deep as 15 meters. Upon successful completion of the coring operations, a manned mission would be sent to retrieve the samples and perform extensive experiments of the polar region. Man's first step in returning to the Moon is recommended to investigate the issue of lunar polar water. The potential benefits of lunar water more than warrant sending either astronauts, robots or both to the Moon before any permanent facility is constructed.

Angell, David↗
NASA NTRS2013

Advanced Aerogel Technology

The JPL Aerogel Laboratory has made aerogels for NASA flight missions, e.g., Stardust, 2003 Mars Exploration Rovers and the 2011 Mars Science Laboratory, as well as NASA research projects for the past 14 years. During that time it has produced aerogels of a range of shapes, sizes, densities and compositions. Research is ongoing in the development of aerogels for future sample capture and return missions and for thermal insulation for both spacecraft and scientific instruments. For the past several years, the JPL Aerogel Laboratory has been developing, producing and testing a new composite material for use as the high temperature thermal insulation in the Advanced Sterling Radioisotope Generator (ASRG) being developed by Lockheed Martin and NASA. The composite is made up of a glass fiber felt, silica aerogel, Titania powder, and silica powder. The oxide powders are included to reduce irradiative heat transport at elevated temperatures. These materials have thermal conductivity values that are the same as the best commercially produced high temperature insulation materials, and yet are 40% lighter. By greatly reducing the amount of oxide powder in the composite, the density, and therefore for the value of the thermal conductivity, would be reduced. The JPL Aerogel Laboratory has experimented with using glass fiber felt, expanded glass fiber felt and loose fibers to add structural integrity to silica aerogels. However, this work has been directed toward high temperature applications. By conducting a brief investigation of the optimal combination of fiber reinforcement and aerogel density, a durable, extremely efficient thermal insulation material for ambient temperature applications would be produced. If a transparent thermal insulation is desired, then aerogel is an excellent candidate material. At typical ambient temperatures, silica aerogel prevents the transport of heat via convection and conduction due to its highly porous nature. To prevent irradiative thermal transport, silica aerogel can be used in conjunction with a transparent polymeric material that blocks infrared radiation. The transparency of silica aerogel is typically greater than 90% for visible wavelengths from 500 nm to 900 nm for a 5 mm long path length.

reduce irradiative heat transport↗
NASA NTRS2014

GeoLab: A Geological Workstation for Future Missions

The GeoLab glovebox was, until November 2012, fully integrated into NASA's Deep Space Habitat (DSH) Analog Testbed. The conceptual design for GeoLab came from several sources, including current research instruments (Microgravity Science Glovebox) used on the International Space Station, existing Astromaterials Curation Laboratory hardware and clean room procedures, and mission scenarios developed for earlier programs. GeoLab allowed NASA scientists to test science operations related to contained sample examination during simulated exploration missions. The team demonstrated science operations that enhance theThe GeoLab glovebox was, until November 2012, fully integrated into NASA's Deep Space Habitat (DSH) Analog Testbed. The conceptual design for GeoLab came from several sources, including current research instruments (Microgravity Science Glovebox) used on the International Space Station, existing Astromaterials Curation Laboratory hardware and clean room procedures, and mission scenarios developed for earlier programs. GeoLab allowed NASA scientists to test science operations related to contained sample examination during simulated exploration missions. The team demonstrated science operations that enhance the early scientific returns from future missions and ensure that the best samples are selected for Earth return. The facility was also designed to foster the development of instrument technology. Since 2009, when GeoLab design and construction began, the GeoLab team [a group of scientists from the Astromaterials Acquisition and Curation Office within the Astromaterials Research and Exploration Science (ARES) Directorate at JSC] has progressively developed and reconfigured the GeoLab hardware and software interfaces and developed test objectives, which were to 1) determine requirements and strategies for sample handling and prioritization for geological operations on other planetary surfaces, 2) assess the scientific contribution of selective in-situ sample characterization for mission planning, operations, and sample prioritization, 3) evaluate analytical instruments and tools for providing efficient and meaningful data in advance of sample return and 4) identify science operations that leverage human presence with robotic tools. In the first year of tests (2010), GeoLab examined basic glovebox operations performed by one and two crewmembers and science operations performed by a remote science team. The 2010 tests also examined the efficacy of basic sample characterization [descriptions, microscopic imagery, X-ray fluorescence (XRF) analyses] and feedback to the science team. In year 2 (2011), the GeoLab team tested enhanced software and interfaces for the crew and science team (including Web-based and mobile device displays) and demonstrated laboratory configurability with a new diagnostic instrument (the Multispectral Microscopic Imager from the JPL and Arizona State University). In year 3 (2012), the GeoLab team installed and tested a robotic sample manipulator and evaluated robotic-human interfaces for science operations.

Evans, Cynthia↗
NASA NTRS1993

Operations concepts for Mars missions with multiple mobile spacecraft

Missions are being proposed which involve landing a varying number (anywhere from one to 24) of small mobile spacecraft on Mars. Mission proposals include sample returns, in situ geochemistry and geology, and instrument deployment functions. This paper discusses changes needed in traditional space operations methods for support of rover operations. Relevant differences include more frequent commanding, higher risk acceptance, streamlined procedures, and reliance on additional spacecraft autonomy, advanced fault protection, and prenegotiated decisions. New methods are especially important for missions with several Mars rovers operating concurrently against time limits. This paper also discusses likely mission design limits imposed by operations constraints .

Dias, William C.↗
NASA NTRSDate not supplied

Ballistic Lunar Return Trajectories for Sustainable Cargo Return and Entry System Technology Development

As part of the sustained approach for the lunar Gateway and Artemis program as a whole, NASA is extending the logistics supply chain beyond low Earth orbit and to the Moon. This supply chain includes the possibility of lunar sample and cargo return. To enable these future return missions, the possibility for incorporating demonstration payloads including various entry, descent, and landing technologies is examined. Possible implementations include deployable entry vehicles, high speed sample return capsules, aeroassist technologies, and control technologies for guided hypersonic flight. The mission concepts utilize the secondary payload capabilities provided on a relatively low-cost logistic module. The logistic module may perform close Earth flyby, pointing, and release of return systems prior to disposal, with reentry velocities for payloads on the order of 11.5 km/sec. In this paper, we study the various return mission architectures available during the Artemis program to define the range of mission possibilities. Potential options include a reusable logistics module using a hypersonic inflatable aerodynamic decelerator, externally mounted entry system vehicle technologies, and a reusable sample return vehicle using a similar inflatable architecture with a feathered configuration with applied aerodynamic control. In these cases, the use of a ballistic lunar return trajectory is assumed, and a sensitivity analysis of midcourse corrections and the possibility of a lunar gravity assist for refining Earth entry interface points is provided. Furthermore, a novel controller for controlling a vehicle during reentry imposing heating limitations is introduced.

Matthew M. Wittal↗
NASA NTRSDate not supplied

Overview of Micrometeoroid and Orbital Debris Analysis Process for Mars Sample Return Earth Entry System

Introduction: Micrometeoroid and orbital debris (MMOD) risk analyses for the Mars Sample Return (MSR) Earth Entry System (EES) have been significantly more rigorous than previously flown missions because of its categorization as a Class V restricted return mission. This means the returned samples present significant concern for biogenic contamination. These analyses seek to determine if a micrometeoroid or orbital debris strike would result in loss of containment assurance and are summarized in the flowchart in Fig. 1. Methodology: The mission is considered in two MMOD phases: a pre-release phase where the EES is protected by a Micrometeoroid Protection System (MMPS) and a post-release phase called “free-flight” where the EES is exposed directly to the MMOD environment. These phases correspond to interplanetary cruise and imminent re-entry, respectively. To inform the MMPS design, a 30-shot high velocity impact testing (HVIT) series on candidate configurations at NASA White Sands Test Facility was completed in the summer of 2022. Sample post-shot images are shown in Fig 2 [1]. These data are used to baseline the MMPS design and to tune the hydrocode simulations. ALE3D, CTH, and SPHC are the hydrocodes that simulate physics of high-speed impacts [2]. Results generated with these populate a penetration depth versus energy space beyond the testable velocity regime of HVIT (~7 km/s). The penetration depth versus energy space data are used to define a critical projectile diameter function called a Ballistic Limit Equation (BLE), where the projectile “criticality” is determined by zone dependent failure criteria defined a-priori [3]. For example, the nose of the heatshield has a failure criterion of 50% TPS penetration, assigned because the landing loads are concentrated on that region and no substructure damage is permitted. The BLEs for each vehicle material zone are input into the BUMPER 3 code, along with the vehicle surface mesh and the corresponding space environment model, to calculate a probability of penetration or number of penetrations. The environment models, MEM3 for MM and ORDEM 3.2 for OD, simulate the meteoroid environment from 0.2 to 2 au based on the Grün flux equation, and the debris environment up to 40,000 km altitude from Earth surface, respectively [4,5]. Presentation Focus: The presentation or poster will present the results to-date focusing on the full risk analysis process flow seen in Fig. 1. Details on the derivation of the failure criteria will be discussed, along with HVIT results and how these influenced the MMPS configuration baseline decision. Further, results of hydrocode simulations will be presented and the tuning to HVIT outputs will be described. Finally, the strategies that direct the BLE formulation will be reviewed, specifically, for the EES elements that are most exposed to the MMOD environment.

mmod↗
NASA NTRSDate not supplied

Shock-Induced Deformation Recorded in the Regolith Particles from C-Type Asteroid Ryugu

The Hayabusa 2 mission successfully returned with samples of C-type near-Earth asteroid (162173) Ryugu on December of 2020. Ryugu samples contain large quantities of volatiles such as water and noble gases. Studying Ryugu samples is a great opportunity to understand the shock metamorphism on water-bearing rubble-pile asteroids. In this study, we have examined shock metamorphism on sixteen coarse mm-sized particles recovered by the Hayabusa 2 mission.

M. Kikuiri↗
NASA NTRSDate not supplied

An Assessment of Turbulence Models for MSR Sample Retrieval Lander Aerothermal Design

Several cases from past entries in the T9 and T5 hypersonic test facilities are examined using various turbulence models and shock-layer thermochemistries with the objectives of verifying/validating turbulence models and determining appropriate multiplicative factors on predicted turbulent heating for use in aerothermal design of the heatshield of the Sample Retrieval Lander (SRL) of the Mars Sample Return (MSR) Flagship mission. The zero-equation turbulence models of Baldwin-Lomax and Cebeci-Smith are shown to replicate measurements to within experimental uncertainty for the T9 cases. For T5 cases, the zero-equation model of Baldwin-Lomax can also replicate measurements provided the shock-layer thermochemistry is modified. The modified thermochemistry resolves a dichotomy from past CFD that required different wall catalycity assumptions in the laminar and turbulent flow regimes. The present work shows that such assumptions are not necessary. Finally, an initial estimate for a multiplicative factor on turbulent heating is estimated for the SST turbulence model – the chosen model for SRL aerothermal design simulations.

Mars entry↗