Estimation of Effective Elastic Properties of General Carbon-Carbon Honeycomb Structures Using a Unit Cell Method
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T. Krishnamurthy↗
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Results for “Structural properties”
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Properties of Periodic Arrays of Symmetric Complementary Structures and their Application to Grid Amplifiers
Deschamps's theorem for n-terminal complementary structures is reviewed. An extension to Deschamps's theorem for a class of 3-terminal bounded structures with one axis of symmetry is presented.
grid↗
Wavenumber Imaging For Damage Detection and Measurement
This paper presents a method for analyzing ultrasonic wavefield data using the Continuous Wavelet Transform (CWT) applied in the spatial domain. Unlike data obtained by sparse arrays of transducers, full wavefield data contains information local to the structure and can be used to obtain more detailed measurements of damage type, location, size, etc. By calculating the CWT of the wavefield in the spatial domain, the wavenumber spectrum is determined for the inspected locations. Because wavenumber is affected by the local geometry and material properties of the structure through which Lamb waves propagate, the wavenumber spectrum can be analyzed to assess the location, severity, and size of damage. The technique is first applied to experimental wavefield data obtained using a laser Doppler vibrometer and automated positioning stage. The out-of-plane velocity along the length of a composite stringer was measured to detect the presence of delaminations within the composite overwrap. Next, simulated corrosion is detected and measured within an aluminum plate using the two dimensional CWT. The experimental results show the usefulness of the technique for vehicle structure inspection applications.
Rogge, Matthew D.↗
Preparation and properties of superconducting thin films of beta-tungsten structure compounds
Superconducting thin films of beta-tungsten structure Nb-Al-Ge compound, discussing high purity sputtering preparation techniques and properties in magnetic fields
Gavaler, J. R.↗
Kinetics of graphitization. I - The high-temperature structural transformation in pyrolytic carbons
Crystal structure transformations and physical property changes in pyrolytic graphite at high temperatures - kinetics of graphitization
KINETICS↗
Effects Of Irradiation By Electrons On Two Polyimides
Polyimides of new class, known as polyetherimides, used for composites and castings. Study undertaken to compare effects of electron radiation, in doses expected for 30-year missions in geosynchronous orbit, on molecular structures and tensile properties of two commercially available polyimides: polypyromellitimide and polyetherimide. Findings helpful in development of new polymers that endure radiation, leading to synthesis of polymers not having methyl groups or other moieties that are sources of hydrogen, inhibiting self-mending. Significance of study for polymer industry relating to structures in outer space considerable.
Long, Edward R., Jr.↗
Finite Element Simulation of the Direct Energy Deposition using Comsol Multiphysics
Direct Energy Deposition (DED) is an emerging technology extensively employed in metal Additive Manufacturing (AM). Despite its widespread industrial application, mathematical modeling in this domain remains challenging. This complexity arises from the intricate nature of the modeling approach and the nonlinear behavior of material parameters across a broad temperature range. Consequently, experimentalists often resort to a trial-and-error method to achieve structures with desired properties. However, this approach can be time-consuming and may not always yield parts with the requisite characteristics, highlighting the necessity for mathematical modeling to enhance manufacturing success. This study focuses on thin-walled manufacturing with a single bead thickness, adjusting laser parameters to produce such structures. The laser cladding speed, typical for DED manufacturing, is considered to be on the order of centimeters per second. The various wall thicknesses and heights are explored to discern the general characteristics of walls manufactured via this DED approach. Our modeling approach diverges from the conventional DED modeling based on activation-deactivation of predefined mesh domains, commonly implemented in many finite element codes. Instead, a method is proposed that effectively models layer cladding and melt pool dynamics, enabling predictions of the microstructure in the resulting structures. The formation mechanisms of cellular, dendritic columnar, and stray (equiaxed) grains, which arise from the interplay between nucleation and growth from the surface is analyzed. The study also examines the feasibility of microstructure formation to demonstrate the various thermal characteristics inherent in wall manufacturing. Our results illustrate how different process parameters influence the temperature gradient and cooling rate of the molten pool, subsequently affecting the primary dendrite arm spacing (PDAS). This modeling technique allows for the investigation of diverse thermal conditions, facilitating the prediction of microstructure and residual stresses in the manufactured parts.
modeling↗
Observations and Parameterizations of Particle Size Distributions in Deep Tropical Cirrus and Stratiform Precipitation Clouds: Results from In-Situ Observations in TRMM Field Campaigns
In this study, we report on the evolution of particle size distributions (PSDs) and habits as measured during slow, Lagrangian-type spiral descents through deep subtropical and tropical cloud layers in Florida, Brazil, and Kwajalein, Marshall Islands, most of which were precipitating. The objective of the flight patterns was to learn more about how the PSDs evolved in the vertical and to obtain information of the vertical structure of microphysical properties. New instrumentation yielding better information on the concentrations of particles in the size (D) range between 0.2 and 2 cm, as well as improved particle imagery, produced more comprehensive observations for tropical stratiform precipitation regions and anvils than have been available previously. Collocated radar observations provided additional information on the vertical structure of the cloud layers sampled. Most of the spirals began at cloud top, with temperatures (T) as low as -50 C, and ended at cloud base or below the melting layer (ML). The PSDs broadened from cloud top towards cloud base, with the largest particles increasing in size from several millimeters at cloud top to one centimeter or larger towards cloud base. Some continued growth was noted in the upper part of the ML. Concentrations of particles less than 1 mm in size decreased with decreasing height. The result was a consistent change in the PSDs in the vertical. Similarly, systematic changes in the size dependence of the particle cross-sectional area was noted with decreasing height. Aggregation-as ascertained from both the changes in the PSDs and evolution of particle habits as observed in high detail with the cloud particle imager (CPI) probe-was responsible for these trends. The PSDs were generally well-represented by gamma distributions of the form N = N0 gamma D microns e- lambda gamma D that were fitted to the PSDs over 1-km horizontal intervals throughout the spirals. The intercept (N0 gamma), slope (lambda gamma), and dispersion (microns) values were derived for each PSD. Exponential curves (N = N0e- lambdaD; micron = 0) were also fitted to the distributions. The lambda gamma values for given spirals varied systematically with temperature as did the values of lambda (exponential), and the data generally conformed to values found in previous studies involving exponential fits to size distributions in mid-latitude frontal and cirrus layers. Considerable variability often noted in the PSD properties during the loops of individual spirals was manifested primarily in large changes in N0 gamma and N0, but micron, lambda gamma and lambda remained fairly stable. Temperature is not found to be the sole factor controlling lambda gamma or lambda but is a primary one. Direct relationships were found between lambda gamma and N0 gamma or lambda gamma and micron for the gamma distributions and lambda and N0 for the exponential. The latter relationship was not found as distinctly in earlier studies; observed PSDs in this study had better fidelity with less scatter. The micron values changed monotonically with T over the range of temperatures and were directly related to N0 gamma or lambda gamma, thereby reducing the number of variables in the PSD functional equation to two. In the upper part of the ML, N0 and lambda continued to decrease, and in the lower part these values began to increase as the largest particles melted. We developed general expressions relating various bulk microphysical, radar, and radiative transfer-related variables to N0 gamma and lambda gamma, useful for both tropical and mid-latitude clouds. These relationships facilitate the specification of a number of bulk properties in cloud and climate models. The results presented in this paper apply best to temperatures between 0 and -40 C, for which the measured radar reflectivities fall in the range of 0 to 25 dBZe.
Heymsfield, Andrew J.↗
Determinants of Market Structure and the Airline Industry
The general economic determinants of market structure are outlined with special reference to the airline industry. Included are the following facets: absolute size of firms; distributions of firms by size; concentration; entry barriers; product and service differentiation; diversification; degrees of competition; vertical integration; market boundaries; and economies of scale. Also examined are the static and dynamic properties of market structure in terms of mergers, government policies, and economic growth conditions.
Raduchel, W.↗
A revised version of the transfer matrix method to analyze one-dimensional structures
A new and general method to analyze both free and forced vibration characteristics of one-dimensional structures is discussed in this paper. This scheme links for the first time the classical transfer matrix method with the recently developed integrating matrix technique to integrate systems of differential equations. Two alternative approaches to the problem are presented. The first is based upon the lumped parameter model to account for the inertia properties of the structure. The second releases that constraint allowing a more precise description of the physical system. The free vibration of a straight uniform beam under different support conditions is analyzed to test the accuracy of the two models. Finally some results for the free vibration of a 12th order system representing a curved, rotating beam prove that the present method is conveniently extended to more complicated structural dynamics problems.
Nitzsche, F.↗
SWICS/Ulysses and MASS/wind observations of solar wind sulfur charge states
As Ulysses journeys from the southern to the northern solar pole, the newly launched Wind spacecraft is monitoring the solar wind near 1 AU, slightly upstream of the Earth. Different solar wind structures pass over both spacecraft as coronal holes and other features rotate in and out of view. Ulysses and Wind are presently on opposing sides of the sun allowing us to monitor these streams for extended periods of time. Composition measurements made by instruments on both spacecraft provide information concerning the evolution and properties of these structures. We have combined data from the Solar Wind Ion Composition Spectrometer (SWICS) on Ulysses and the high mass resolution spectrometer (MASS) on Wind to determine the charge state distribution of sulfur in the solar wind. Both instruments employ electrostatic deflection with time-of-flight measurement. The high mass resolution of the MASS instrument (M/Delta-M approximately 100) allows sulfur to be isolated easily while the stepping energy/charge selection provides charge state information. SWICS measurements allow the unique identification of heavy ions by their mass and mass/charge with resolutions of M/Delta-M approximately 3 and M/q/Delta(M/q) approximately 20. The two instruments complement each other nicely in that MASS has the greater mass resolution while SWICS has the better mass/charge resolution and better statistics.
Cohen, C. M. S.↗
Site- and compartment-specific changes in bone with hindlimb unloading in mature adult rats
The purpose of this study was to examine site- and compartment-specific changes in bone induced by hindlimb unloading (HU) in the mature adult male rat (6 months old). Tibiae, femora, and humeri were removed after 14, 21, and 28 days of HU for determination of bone mineral density (BMD) and geometry by peripheral quantitative computed tomography (pQCT), mechanical properties, and bone formation rate (BFR), and compared with baseline (0 day) and aging (28 day) controls. HU resulted in 20%-21% declines in cancellous BMD at the proximal tibia and femoral neck after 28 day HU vs. 0 day controls (CON). Cortical shell BMD at these sites was greater (by 4%-6%) in both 28 day HU and 28 day CON vs. 0 day CON animals, and nearly identical to that gain seen in the weight-bearing humerus. Mechanical properties at the proximal tibia exhibited a nonsignificant decline after HU vs. those of 0 day CON rats. At the femoral neck, a 10% decrement was noted in ultimate load in 28 day HU rats vs. 28 day CON animals. Middiaphyseal tibial bone increased slightly in density and area during HU; no differences in structural and material properties between 28 day HU and 28 day CON rats were noted. BFR at the tibial midshaft was significantly lower (by 90%) after 21 day HU vs. 0 day CON; this decline was maintained throughout 28 day HU. These results suggest there are compartment-specific differences in the mature adult skeletal response to hindlimb unloading, and that the major impact over 28 days of unloading is on cancellous bone sites. Given the sharp decline in BFR for midshaft cortical bone, it appears likely that deficits in BMD, area, or mechanical properties would develop with longer duration unloading.
Non-NASA Center↗
Ionic Polyimides: New High Performance Polymers for Additive Manufacturing
There is currently a very limited set of engineering polymers that have been demonstrated as viable for use in 3-D printing. Additive manufacturing of custom components will require a much larger array of polymers, especially those with physical, thermal, chemical, and mechanical properties that can be tailor-made. The development of ‘Ionic Polyimides’ offers a solution to this shortage by combining the well understood and widely accepted properties of conventional polyimides, with a new approach to polymer synthesis. Polyimides and polymeric ionic liquids (poly(ILs)) are at the forefront of advanced polymer materials, each with their own set of advantages and disadvantages. While it is clear that more types of polymer materials are needed for fused deposition modeling (FDM) additive manufacturing, there is a need to explore these classes of materials. The synthesis process developed by the Bara Research Group at the University of Alabama allows full control over polymer structure, nanostructure, thermal, electrical, and physical properties making them a prime candidate for use in the additive manufacturing process. Furthermore, the new process allows us to tailor-make a high strength polymer that can be used to fabricate filament feedstock instead of pellets for 3D printing. The primary objective of this proposal is to determine the relationship between molecular structure, physical properties, and performance of ionic polyimides. Further, we seek to determine their utility as materials suitable for additive manufacturing of components used in aerospace vehicles, with an emphasis on characterizing and simulating their thermal behaviors and properties. This proposal addresses the need for fundamental research on a customizable polymer filament feedstock for 3-D printing with tailor-made properties potentially making it superior to the commercial blends offered in industry today. The deliverables for this project are the creation of a database that will detail the relationships between the molecular structure and physical properties for the ionic polyimide of interest (e.g. Tg/Tm (Glass Transition Temperature divided by Melting Point)) relative to different ionic polyimide structures). This new database will provide a “road map” to the development of the first generation of materials and ultimately proof-of-concept.
Jackson, Enrique↗
Molecular Dynamics Studies of Structure and Functions of Water-Membrane Interfaces
A large number of essential cellular processes occur at the interfaces between water and membranes. The selectivity and dynamics of these processes are largely determined by the structural and electrical properties of the water-membrane interface. We investigate these properties by the molecular dynamics method. Over the time scales of the simulations, the membrane undergoes fluctuations described by the capillary wave model. These fluctuations produce occasional thinning defects in the membrane which provide effective pathways for passive transport of ions and small molecules across the membrane. Ions moving through the membrane markedly disrupt its structure and allow for significant water penetration into the membrane interior. Selectivity of transport, with respect to ionic charge, is determined by the interfacial electrostatic potential. Many small molecules. of potential significance in catalysis, bioenergetics and pharmacology, are shown to bind to the interface. The energetics and dynamics of this process will be discussed.
Pohorille, Andrew↗
TPSAS-NF1676L-13664-DND
The safety of aerospace vehicles is largely dependent on the ability of modern non-destructive evaluation (NDE) tools to accurately detect structural damage before a critical flaw size is reached. However, existing NDE technologies are inherently limited by the physical response of the materials being inspected making the detection of small cracks or pre-crack damage difficult. One innovative solution to this problem is to create a multifunctional metallic material that can be used in structural applications and contains second phase sensory particles that significantly enhance the ability of conventional NDE techniques to detect incipient damage during use and at regularly scheduled inspections. Ferromagnetic shape-memory alloys (FSMAs) are an ideal material for use as this second phase material as they undergo a uniform and repeatable change in both magnetic properties and crystallographic structure when strained. These changes are more readily detected than small cracks, thereby, allowing for enhanced detection of damage by conventional NDE techniques. In this study, a multifunctional metallic material was produced by embedding the sensory material particles within an aluminum alloy to form a sensory alloy. The NDE response of the FSMA and the sensory alloy during tension/compression and fatigue loading have been investigated. These results suggest that sensory alloys can be utilized for improved on-board structural health monitoring and to improve the accuracy and reduce time for ground-based inspection.
T. A. Wallace↗
Synthesis of ZnO:As Films Using Off-Axis Sputtering Deposition
As a novel oxide semiconductor material, ZnO is interesting for use in many applications. For fabricating electronic devices, it is important to have n- and p- type ZnO materials. Arsenic has been proven to be one of the p-type dopants for ZnO materials. However, information in studying the ZnAsO ternary compound films has been scarce. In order to investigate the morphology, structure and electrical properties of ZnAsO ternary compounds, ZnO:As films have been synthesized using off-axis sputtering deposition on various substrates including (100) Si and (0001) sapphire crystals. Films are grown under various growth conditions. ZnO:As targets with the atomic weight ratios of arsenic to zinc from 0.01 to 0.10 are used for film synthesis. The growth temperatures and pressures range from 350 to 550C and 5 to 150 mTorr, respectively. Argon to oxygen gas ratio for film growth is varied to examine the film quality as well. Film surface morphology, crystal structure, and compositions, are characterized using atomic force microscopy, x-ray diffraction, and energy dispersive spectroscopy, respectively. The compositions of target material and ZnO:As films grown under various conditions are then assessed. The electrical properties were also measured. The detail of these measurements will be discussed in the presentation.
Zhu, Shen↗
Survey of long-term durability of fiberglass reinforced plastic structures
Included are fluid containment vessels, marine structures, and aircraft components with up to 19 years of service. Correlations were obtained for the variation of static fatigue strength, cyclic fatigue strength, and residual burst strength for pressure vessels. In addition, data are presented for the effects of moisture on strength retention. Data variations were analyzed, and relationships and implications for testing are discussed. Change in strength properties for complete structures was examined for indications of the effects of environmental conditions such as moisture and outdoor exposure (ultraviolet radiation, weathering) on long term durability.
Lieblein, S.↗
Development of Metallic Sensory Alloys
Existing nondestructive evaluation (NDE) technologies are inherently limited by the physical response of the structural material being inspected and are therefore not generally effective at the identification of small discontinuities, making the detection of incipient damage extremely difficult. One innovative solution to this problem is to enhance or complement the NDE signature of structural materials to dramatically improve the ability of existing NDE tools to detect damage. To address this need, a multifunctional metallic material has been developed that can be used in structural applications. The material is processed to contain second phase sensory particles that significantly improve the NDE response, enhancing the ability of conventional NDE techniques to detect incipient damage both during and after flight. Ferromagnetic shape-memory alloys (FSMAs) are an ideal material for these sensory particles as they undergo a uniform and repeatable change in both magnetic properties and crystallographic structure (martensitic transformation) when subjected to strain and/or temperature changes which can be detected using conventional NDE techniques. In this study, the use of a ferromagnetic shape memory alloy (FSMA) as the sensory particles was investigated.
Wallace Terryl A.↗