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At least 1,099 records · Page 61

Collisions of Ir oxide nanoparticles with carbon nanopipettes: Experiments with one nanoparticle

Investigating the collisions of individual metal nanoparticles (NPs) with electrodes can provide new insights into their electrocatalytic behavior, mass transport, and interactions with surfaces. Here we report a new experimental setup for studying NP collisions based on the use of carbon nanopipettes to enable monitoring multiple collision events involving the same NP captured inside the pipet cavity. A patch clamp amplifier capable of measuring pA-range currents on the microsecond time scale with a very low noise and stable background was used to record the collision transients. The analysis of current transients produced by oxidation of hydrogen peroxide at one IrO x NP provided information about the origins of deactivation of catalytic NPs and the effects of various experimental conditions on the collision dynamics. Lastly, high-resolution TEM of carbon pipettes was used to attain better understanding of the NP capture and collisions.

36 MATERIALS SCIENCE↗

Measured Thermal and Fast Neutron Fluence Rates ATR Cycles 171A IR TMIST 3B

This report contains the thermal (2200 m/s) and fast (E>1MeV) neutron fluence rate data for ATR Cycle 171A which were measured by the Radiation Measurements Laboratory (RML) as requested by the Power Reactor Programs (ATR Experiments) Radiation Measurements Work Order. This report contains fluence rate values corresponding to the particular elevations (relative to the 80-ft. core elevation) where the measurements were taken. The data in this report consists of (1) a table of the ATR power history and distribution, (2) a listing of the calculated thermal and fast neutron fluence rates, and (3) plots of calculated both the thermal and fast neutron fluence rates. The fluence rates reported are for the average power levels given in the table of power history and distribution. During the irradiation of Cycle 152A, the RML performed additional flux measurements to assess core reconfiguration issues. Measurements using cadmium covered as well as bare neutron monitors in the Southwest, Southeast, and H positions of the Center lobe were performed to determine the division in neutron energy between epithermal and thermal neutrons. This is defined as the resonance correction defined in this report. It is used to quantify both thermal and fast neutron flux. For more information please refer to letter, “RADIATION MEASUREMENTS LABORATORY MEASUREMENTS OF IN CORE ATR PHYSICS TESTING DURING CYCLE 152A” dated January 24, 2013, to Casey Stengel from C. C. Jensen. The measured values documented in RML Procedure, “ACMM-3600, Flux Monitoring,” will be used indefinitely until further measurements supersede the current values.

11 NUCLEAR FUEL CYCLE AND FUEL MATERIALS↗

202508 HAIIC IR Images with Attitude Data at BNF

This campaign aims to collect infrared imagery using a custom data acquisition system to improve and validate a previously developed attitude estimation algorithm, with a focus on ensuring reliable performance at higher altitudes. The system integrates a Boson+320 infrared camera, a VN-200 IMU for recording attitude data synchronized with image acquisition, and a Raspberry Pi 4B+ for onboard processing and storage. Image orientation was controlled using a Gremsy T7 gimbal. The primary dataset spans roll angles from −40° to 40° and pitch angles from −20° to 40°, sampled at 1° increments. Additional, smaller datasets were also collected at 2.5° angular intervals.

Boson+320↗

NbN A/D Conversion of IR Focal Plane Sensor Signal at 10 K

We are implementing a 12 bit SFQ counting ADC with parallel-to-serial readout using our established 10 K NbN capability. This circuit provides a key element of the analog signal processor (ASP) used in large infrared focal plane arrays. The circuit processes the signal data stream from a Si:As BIB detector array. A 10 mega samples per second (MSPS) pixel data stream flows from the chip at a 120 megabit bit rate in a format that is compatible with other superconductive time dependent processor (TDP) circuits being developed. We will discuss our planned ASP demonstration, the circuit design, and test results.

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