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DOE OSTI2022

Analysis of the Source Physics Experiment Dry Alluvium Geology Ball Drop Sources

Two balls were dropped approximately 150 m down an open borehole as part of an investigation into the aftershocks from a 51 ton TNT-equivalent chemical explosion. The ball drop sources, a concrete-filled basketball and a bowling ball, were intended to mimic falling debris within an underground explosion borehole and cavity. Falling debris or sloughing of the borehole and cavity walls is thought to be one of the sources of explosion aftershocks. The signals from the ball drop sources were recorded by the same seismic network that monitored the aftershocks of the chemical explosion, so the ball drop recordings were used as templates to search through the continuous stream of aftershocks and detect correlated signals as a proportion of all aftershocks. The search resulted in only four similar event recordings out of the thousands of detected aftershocks. A synthetic test showed that the small, high-frequency ball drop templates were limited to producing highly correlated detections for events occurring in a small region around the impact location at 150 m depth. The high-frequency templates were necessary since the small ball drop signals were only above the noise at frequencies greater than 10 Hz. Unfortunately, the impact location is where the borehole was filled with sand in preparation for the subsequent chemical explosion in the test series, making it 150 m above the explosion created cavity centered at 300 m depth. This puts the ball drop templates 150 m away from the cavity, where many more events from falling debris would be expected. Further synthetic tests confirmed events emanating from the cavity 150 m below the impact site would have correlated with the lower frequency template and been detected had the template been usable below 10 Hz. Therefore, we conclude that the four detected events were most probably falling debris within the open borehole that impacted the floor at 150 m depth just as the ball drop sources had, and that this type of explosion aftershock mechanism comprises less than 1% of all explosion aftershocks.

58 GEOSCIENCES↗

DOE OSTI2022

Computed Tomography Scanning and Geophysical Measurements of the Enhanced Geothermal Systems (EGS) Collab SURF Core

The computed tomography (CT) facilities and the Multi-Sensor Core Logger (MSCL) at the National Energy Technology Laboratory (NETL) in Morgantown, West Virginia were used to characterize core from 8 wells from the Enhanced Geothermal Systems (EGS) Collab project located in the Sanford Underground Research Facility’s (SURF) 4850 level. The work in this report falls in Experiment 1 in a three-phase experiment, with the primary purpose to increase understanding of hydraulic fracturing. The primary impetus of this work is a collaboration between U.S. Department of Energy (DOE) and the EGS Collab. The resultant datasets are presented in this report and can be accessed from NETL's Energy Data eXchange (EDX) online system using the following link: https://edx.netl.doe.gov/dataset/surf-collab-core. All equipment and techniques used were non-destructive, enabling future examinations and analyses to be performed on these cores. None of the equipment used was suitable for direct visualization of the pore space in the core, although fractures and discontinuities were detectable with the methods tested. Low resolution CT imagery with the NETL medical CT scanner was performed on the entire core. Qualitative analysis of the medical CT images, coupled with X-ray fluorescence (XRF), P-wave, and magnetic susceptibility measurements from the MSCL were useful in identifying zones of interest for more detailed analysis as well as fractured zones. The ability to quickly identify key areas for more detailed study with higher resolution will save time and resources in future studies. The combination of methods used provides a multi-scale analysis of the core; the resulting macro and micro descriptions are relevant to many subsurface energy related examinations traditionally performed at NETL.

47 OTHER INSTRUMENTATION↗

DOE OSTI2022

Bayesian Seismoacoustic Source Location: Acoustic Approach

Seismic waves and infrasound are key technologies in the International Monitoring System (IMS) to monitor explosive events in the solid Earth and atmosphere. Energetic man-made or natural events (e.g., chemical/nuclear explosions, volcanic eruptions, and earthquakes) near the Earth’s surface produce both ground motion and atmospheric pressure disturbances which propagate as seismic waves and infrasound, respectively. Seismic waves have been generally used to detect and identify underground and near-surface events (Myers, et. al., 2007), and infrasound are sensitive to events near the surface or in the atmosphere (Modrak et. al., 2010). Due to their different sensitivities to events, they can complement to each other to improve the event detection and discrimination. The framework of joint seismoacoustic event location has recently reviewed by theoretical research (Koch and Arrowsmith, 2019). Although the early applications showed promising results to improve the accuracy of event location, their application were still limited to a small set of events selected to prove the concepts, and practical capability of the method for operational purpose is not fully evaluated with data. Our final goal is to apply the method of seismoacoustic event location to a larger set of events and evaluate its applicability for operational event location in practice. To that end, we focus on developing and verifying acoustic source location method in this study.

58 GEOSCIENCES↗

DOE OSTI2022

Strategic Petroleum Reserve Cavern Leaching Monitoring CY21

Th e U.S. Strategic Petroleum Reserve (SPR) is a crude oil storage system administered by the U.S. Department of Energy. The reserve consists of 60 active storage caverns located in underground salt domes spread across four sites in Louisiana and Texas, near the Gulf of Mexico. Beginning in 2016, the SPR started executing C ongressionally mandated oil sales. The configuration of the reserve, with a total capacity of greater than 700 million barrels ( MMB ) , re quires that unsaturated water (referred to herein as ?raw? water) is injected into the storage caverns to displace oil for sales , exchanges, and drawdowns . As such, oil sales will produce cavern growth to the extent that raw water contacts the salt cavern walls and dissolves (leaches) the surrounding salt before reaching brine saturation. SPR injected a total of over 45 MMB of raw water into twenty - six caverns as part of oil sales in CY21 . Leaching effects were monitored in these caverns to understand how the sales operations may impact the long - term integrity of the caverns. While frequent sonars are the most direct means to monitor changes in cavern shape, they can be resource intensive for the number of caverns involved in sales and exchanges. An interm ediate option is to model the leaching effects and see if any concerning features develop. The leaching effects were modeled here using the Sandia Solution Mining Code , SANSMIC . The modeling results indicate that leaching - induced features do not raise co ncern for the majority of the caverns, 15 of 26. Eleven caverns, BH - 107, BH - 110, BH - 112, BH - 113, BM - 109, WH - 11, WH - 112, WH - 114, BC - 17, BC - 18, and BC - 19 have features that may grow with additional leaching and should be monitored as leaching continues in th ose caverns. Additionally, BH - 114, BM - 4, and BM - 106 were identified in previous leaching reports for recommendation of monitoring. Nine caverns had pre - and post - leach sonars that were compared with SANSMIC results. Overall, SANSMIC was able to capture the leaching well. A deviation in the SANSMIC and sonar cavern shapes was observed near the cavern floor in caverns with significant floor rise, a process not captured by SANSMIC. These results validate that SANSMIC continues to serve as a useful tool for mon itoring changes in cavern shape due to leaching effects related to sales and exchanges.

02 PETROLEUM↗

DOE OSTI2022

Report on the LLNL Global Seismic Waveform Tomography Modeling Project

Earth models have important applications for seismic event monitoring including the location and characterization of potential underground nuclear tests. Seismic waves generated by earthquakes and man-made events are altered by variations in Earth’s subsurface properties; and these distortions effect the arrival times of energy packets (phases) and obscure the characteristics of the original energy source (event mechanism). Three-dimensional models of Earth’s seismic properties can help explain and predict the distortions to the seismic wavefield and reveal the properties of a source that generated the waves, including the event location using the model-predicted timing of the phases and source mechanism using the modelpredicted waveform characteristics.

58 GEOSCIENCES↗

DOE OSTI2022

M4 Summary of EBS International

Thermal-Hydrologic-Mechanical (THM) modeling of DECOVALEX 2023, Task C has continued. In FY2022 the simulations have progressed to Step 1, which is on 3-D modeling of the full-scale emplacement experiment at the Mont Terri Underground Rock Laboratory (Nagra, 2019). This report summarizes progress in Thermal-Hydrologic (TH) modeling of Step 1. THM modeling will be documented in future reports.

42 ENGINEERING↗

DOE OSTI2022

Elementary Particle Interactions (Final Technical Report)

Neutrinos provide a promising window to probe a wide range of fundamental physics. The past two decades have brought several remarkable neutrino-related discoveries indicating that one may answer the most sought after question of our matter dominated universe from within the neutrino sector. The global neutrino physics program is currently focused on studying neutrino oscillations, and to understand the implications of this phenomena on the evolution of the universe. Addressing all of these open questions and completing the story of neutrino oscillations requires technological advances in neutrino detection. Liquid argon time projection chambers (LArTPCs) are imaging detectors that offer fine-grained tracking, calorimetry and scalability, and are increasingly favored for the next generation of large neutrino detectors. Through leading technical and scientific roles on MicroBooNE, Short-Baseline Near Detector (SBND) and the Deep Underground Neutrino Experiment (DUNE) LArTPC neutrino experiments, the research program supported through this funding has significantly advanced the understanding of neutrino properties along with technical development of LArTPCs for both short- and long-baseline neutrino oscillations physics.

72 PHYSICS OF ELEMENTARY PARTICLES AND FIELDS↗

DOE OSTI2022

Organic Evaporation and Oxidation Testing in Support of Hanford Sample-and-Send

The Hanford site has approximately 56 million gallons of radioactive mixed waste stored in 177 underground storage tanks. The Hanford Waste Treatment and Immobilization Plant (WTP) is being built to treat and immobilize the tank waste. The baseline method for immobilization of Low Activity Waste (LAW) through the WTP is vitrification, but additional immobilization capacity is needed to supplement the initial LAW melters. An alternative cementitious waste form is being investigated for that future immobilization method to supplement vitrification. However, one impediment to a cementitious waste form is the presence of Land Disposal Restricted (LDR) organic chemicals in tank waste. This work evaluates potential avenues to eliminate that impediment to permit possible use of a cementitious waste form and work towards a decision whether additional LDR organic pretreatment would be required. Savannah River National Laboratory (SRNL) performed testing using simulants to examine evaporation as a method to remove some prevalent organics from LAW. Spiking the caustic LAW simulant with selected regulated organic chemicals found one that clearly decomposes because of caustic instability. Oxidation testing of other organic chemicals found some LDR organics degrade as desired and others are stable in the presence of peroxide and permanganate. In addition to studies with simulants, a literature review was performed to evaluate radiological stability of LDR organics. Descriptions of the experimental details, equipment, and results are included in this report. Evaporation testing consisted of preparing the LAW simulant, spiking that simulant with organic chemicals, and evaporating the mixture via differential distillation. The apparatus was a laboratory-scale vacuum evaporator operated at 60 ±5 torr absolute (vacuum evaporation) and also at atmospheric pressure. The LAW simulant represented the liquid expected to be retrieved from the Hanford tank farms at approximately 4.0 M [Na + ] total sodium ion concentration. The concentration of the organic chemicals added was significantly higher than typically found in the tank waste samples since the higher levels were necessary to assist in analytical measurement and tracking of the spiked species. Organic chemicals were chosen for the work with a consideration of how their volatility compares with that of methanol. This was done by comparing the ratio of the pure water Henry’s law coefficient (K h ) of methanol to that of the compound in question (hereafter termed the K h ratio), where ratios above unity indicated less volatility than methanol. Methanol was chosen because it is a common regulated chemical with relatively low volatility but which has been removed by evaporation in previous laboratory work. While organic separation results depend on evaporator design, laboratory experiments verified that organic partitioning to the overhead condensate stream by evaporation is a practical process. The work reported here found difficulties in quantitative analysis of the organic chemicals in aqueous samples. Most of the time there was insufficient analysis to close a mass balance for evaporator runs, but qualitative evidence of carryover was obtained. The methods were also able to show whether organic chemicals were susceptible or resistant to solution oxidation in permanganate or hydrogen peroxide tests.

12 MANAGEMENT OF RADIOACTIVE AND NON-RADIOACTIVE W↗

DOE OSTI2022

Hydrogen Blending into Natural Gas Pipeline Infrastructure: Review of the State of Technology

Hydrogen is an energy carrier that could play an important role in reducing emissions associated with difficult-to-decarbonize sectors including peaking and load-following electricity and industrial heating. Blending hydrogen into the natural gas pipelines has been proposed as an approach for achieving near-term emissions reductions and early-market access for hydrogen technologies such as electrolyzers. Numerous challenges and uncertainties complicate this approach to natural gas decarbonization, however, and this review summarizes current research on the material, economic, and operational factors that must be considered for hydrogen blending. First, this review explores previous research regarding the effects of blending hydrogen on gas mixture fluid and thermodynamic properties, pipeline materials and equipment performance within transmission and distribution networks, and supporting facilities such as underground storage and end-use hydrogen separation. We also investigate and summarize studies that developed mathematical models of natural gas pipeline networks with hydrogen blending, and the operational and techno-economic findings of these network studies. Finally, we discuss notable hydrogen blending demonstrations and their key outcomes. Many blending demonstrations internationally have proven that low hydrogen percentage blending is feasible under very specific scenarios with limited end-usage applications on both high-pressure transmission lines and low-pressure distribution lines. This report summarizes findings from literature into key areas of consensus and disagreement. Research gaps and disagreements between the literature are highlighted to provide directions for future hydrogen blending research.

03 NATURAL GAS↗

DOE OSTI2022

Modeling Flow and Transport in Fractured Rock using Machine Learning [Slides]

Fractured systems in the subsurface play a role in many natural and engineered applications such as geologic carbon sequestration, hydraulic fracturing and underground nuclear test detection. Structural information (fracture size, orientation, etc.) plays a key role in governing the dominant physics for these systems but can only be known statistically. Traditional modeling approaches either ignore or idealize structural information at these larger scales because we lack a computational framework that utilizes it in its entirety. The work presented here integrates computational physics, machine learning and graph theory to make a paradigm shift from computationally intensive high-fidelity models to coarse-scale graphs without loss of critical structural information. We exploit the underlying discrete structure of fracture networks in systems considering flow through fractures and fracture propagation. We demonstrate that compact graph representations require significantly fewer degrees of freedom (dof) to capture micro-fracture information and further accelerate these models with Machine Learning.

58 GEOSCIENCES↗

DOE OSTI2021

International Collaboration Activities in Geologic Disposal Research: FY2021 Progress

This report describes the FY21 status of international collaboration regarding geologic disposal research in the Spent Fuel and Waste Disposition (SFWD) Campaign. Since 2012, in an effort coordinated by Lawrence Berkeley National Laboratory, SFWD has advanced active collaboration with several international geologic disposal programs across the world. Such collaboration has allowed the SFWD Campaign to benefit from a deep knowledge base in regards to alternative repository environments developed over decades and has provided a framework for active peer-to-peer research participation in international groups which conduct, analyze, and model performance-relevant processes. Via international collaboration, the SFWD Campaign also benefits from substantial international investments in research facilities (such as underground research laboratory testing and modeling) and achieves cost savings via joint funding of expensive field experiments. To date, SFWD’s International Disposal R&D Program has established formal collaboration agreements with multiple international initiatives and various international partners, and national lab scientists associated with SFWD have conducted a large number of specific collaborative R&D activities that align well with its R&D priorities.

12 MANAGEMENT OF RADIOACTIVE AND NON-RADIOACTIVE W↗

DOE OSTI2022

DUNE Offline Computing Conceptual Design Report

This document describes Offline Software and Computing for the Deep Underground Neutrino Experiment (DUNE) experiment, in particular, the conceptual design of the offline computing needed to accomplish its physics goals. Our emphasis in this document is the development of the computing infrastructure needed to acquire, catalog, reconstruct, simulate and analyze the data from the DUNE experiment and its prototypes. In this effort, we concentrate on developing the tools and systems that facilitate the development and deployment of advanced algorithms. Rather than prescribing particular algorithms, our goal is to provide resources that are flexible and accessible enough to support creative software solutions as HEP computing evolves and to provide computing that achieves the physics goals of the DUNE experiment.

46 INSTRUMENTATION RELATED TO NUCLEAR SCIENCE AND ↗

DOE OSTI2022

Strategic Petroleum Reserve Enhanced Monitoring Compendium (FY 2022)

The Strategic Petroleum Reserve (SPR) is the world's largest supply of emergency crude oil. The reserve consists of four sites in Louisiana and Texas. Each site stores crude in deep, underground salt caverns. It is the mission of the SPR's Enhanced Monitoring Program to examine all available data to inform our understanding of each site. This report discusses the monitoring data, processes, and results for each of the four sites for fiscal year 2022.

02 PETROLEUM↗

DOE OSTI2021

Simulation Studies on the Interactions of Electron Beam with Wastewater

The manufactured chemical pollutants, like 1,4 dioxane and PFAS (per- and polyfluroralkyl substances), found in the underground water and/or drinking water are challenging to be removed or biodegraded. Energetic electrons are capable of mediating and removing them. This paper utilizes FLUKA code to evaluate the beam-wastewater interaction effects with different energy, space and divergence distributions of the electron beam. With 8 MeV average energy, the electron beam exits from a 0.0127 cm thick titanium window, travels through a 4.3 cm distance air and a second 0.0127 cm thick stainless water container window with 2.43 cm radius, and finally is injected into the water area, where the volume of water is around 75 cubic cm. The distribution parameters of the electron beam are from the GPT (General Particle Tracer) simulations for UITF (Upgraded Injector Test Facility) in Jefferson lab. By varying the distributions, several measurements including the dose (or energy deposition) distribution, electron fluence, photon fluence are scored and compared. Taking the comparisons into consideration, this paper is aiming to find better electron beams for the wastewater irradiation.

Li, X.↗

DOE OSTI2022

A Gaseous Argon-Based Near Detector for DUNE [Slides]

DUNE is the Deep Underground Neutrino Experiment. It is a comprehensive physics program whose focus is to search for the leptonic CP violation, determine mass ordering, precise measurements of neutrino mixing parameters, BSM searches, baryon number violation, and supernova neutrino observation. This presentation focus is on the argon-based near detector complex at DUNE.

43 PARTICLE ACCELERATORS↗

DOE OSTI2023

Follow-on Report of Analysis of Approaches to Supplemental Treatment of Low–Activity Waste at the Hanford Nuclear Reservation (Volumes I & II)

The Hanford Site, in southeast Washington State, is preparing to disposition approximately 56,000,000 gallons (56 Mgal) of radioactive and chemically hazardous wastes currently stored in underground tanks at the site. Tank wastes will be divided into a high-activity fraction and a low-activity fraction for subsequent treatment and disposition. A waste processing and treatment facility, the Waste Treatment and Immobilization Plant (WTP), will include the high-level waste (HLW) vitrification facility (WTP HLW Vitrification Facility) for immobilizing the high-activity fraction and a low-activity waste (LAW) vitrification facility (WTP LAW Vitrification Facility) for immobilizing the low-activity fraction. Both facilities will use vitrification technology to immobilize the Hanford tank wastes in a glass waste form.

12 MANAGEMENT OF RADIOACTIVE AND NON-RADIOACTIVE W↗

DOE OSTI2023

2022 Long-Term Hydrologic Monitoring Program Report for the Rio Blanco, Colorado Site

This report presents the monitoring data collected by the U.S. Department of Energy (DOE) Office of Legacy Management (LM) during the 2022 sampling event at the Rio Blanco, Colorado, Site, where an underground nuclear test was conducted in 1973. The test resulted in residual radionuclide contamination at the detonation depth. The 2022 sampling event included the collection of samples from onsite groundwater wells to monitor for any potential contamination that might be attributed to the Rio Blanco nuclear tests. This report summarizes the laboratory results obtained from the sampling along with the historical results since monitoring began in the 1970s. This annual report and previous reports are available on the LM public website at https://www.energy.gov/lm/rio-blanco-colorado-site. Data collected during this and previous monitoring events are available on the Geospatial Environmental Mapping System (GEMS) website at https://gems.lm.doe.gov/#site=RBL.

54 ENVIRONMENTAL SCIENCES↗

DOE OSTI2023

Follow-On Report of Analysis of Approaches to Supplemental Treatment of Low-Activity Waste at the Hanford Nuclear Reservation (Volumes I & II)

12 MANAGEMENT OF RADIOACTIVE AND NON-RADIOACTIVE W↗