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At least 1,081 records · Page 60

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DOE OSTI2021

Quantification of manganese for ChemCam Mars and laboratory spectra using a multivariate model

In this work, we report a new calibration model for manganese using the laser-induced breakdown spectroscopy instrument that is part of the ChemCam instrument suite onboard the NASA Curiosity rover. The model has been trained using an expanded set of 523 manganese-bearing rock, mineral, metal ore, and synthetic standards. The optimal calibration model uses the Partial Least Squares (PLS) and Least Absolute Shrinkage and Selection Operator (LASSO) multivariate techniques, with a novel “double blending” technique. We determined the detection limit for manganese is 82 ppm using a method blank procedure and is possibly as low as 27 ppm based on visual inspection of the spectra. Based on a representative test set consisting of measurements on 93 standards, the double blended multivariate model shows a Root Mean Squared Error of Prediction (RMSEP) accuracy of 1.39 wt% MnO for the full blended model. Employing a local RMSEP estimate where the model performance is evaluated based on nearby test samples, the accuracy is 0.03 wt% at the quantification limit (0.05 wt% MnO), 0.4 wt% accuracy at 1.0 wt% MnO, and 4.4 wt% accuracy at 100 wt% MnO. Precision is estimated using the standard deviation of the test set measurements, and is ±0.01 wt% MnO at the quantification limit, ±0.09 wt% MnO at 1.0 wt% MnO, and ± 2.1 wt% MnO at 100 wt% MnO (all 1 standard deviation). This new calibration is important for understanding the variation of manganese in the bedrock with the Curiosity rover on Mars, which provides insight into past redox conditions on Mars.

37 INORGANIC, ORGANIC, PHYSICAL, AND ANALYTICAL CH↗

NASA NTRS1995

(abstract) The 1994 Laboratory Calibration Of TIMS

This summary describes the spatial, spectral, and radiometric calibration of TIMS performed at the JPL Thermal Infrared Calibration Facility (TIRCAL) between May and August 1994. The 1994 calibration of TIMS was the first to make use of the new EXABYTE (8mm helical-scan tape) recording system. With the new recorder, the TIMS data tapes may be read directly on any computer system that has an EXABYTE tape drive. We analyzed the calibration data sets using image processing procedures written in IDL (Research Systems, Inc., Boulder, CO 80303).

TIMS↗

DOE OSTI2020

Ubiquitous Traffic Volume Estimation through Machine-Learning Procedure

Traffic volume data is one of the most important metrics for accurate assessment of the performance of a transportation system. Quality volume data is required to effectively assess extent of delay and congestion, detect real-time perturbations to the network, and understand traffic patterns during major weather events. Traffic volume on freeways are typically collected through continuous count stations installed by state DOTs, while there is lack of traffic volume observability on off-freeway roads. The National Renewable Energy Laboratory (NREL), in Collaboration with the I-95 Corridor Coalition and the University of Maryland, extended its research into estimating volumes anywhere anytime from industry probe based data for off-freeway roads. NREL combined vehicle probe count data with several other data sets (speed, whether, roadway geometry, time-of-day, day-of-week, etc.) to estimate hourly volumes as well as AADTs. The research validated and demonstrated the machine learning model, namely XGBoost, using data collected from Pennsylvania, North Carolina, and Tennessee.

47 OTHER INSTRUMENTATION↗

DOE OSTI2026

Robust and High Throughput Tools for Characterization of Wet Cellulosic Biogas Feedstocks and Co-Products: Cooperative Research and Development Final Report, CRADA Number CRD-21-21472

This project will develop standardized analytical procedures to support understanding of the chemical composition of wet manure feedstocks, and the digestate formed following anaerobic digestion of organic waste to produce renewable natural gas (RNG). The developed methods will be validated to improve component mass closure, eliminate ambiguities around key constituents, and document the precision and accuracy of the methods. Following validation of the analytical laboratory methods for characterization of wet organic waste feedstocks and digestate, NLR will use the same samples to build and validate near-infrared (NIR) models for high throughput analysis, potentially deployable at commercial facilities, enabling increased production of low carbon intensity RNG from wet organic wastes.

09 BIOMASS FUELS↗

NASA NTRS1975

Fracture control method for composite tanks with load sharing liners

The experimental program was based on the premise that the plastic sizing cycle, which each pressure vessel is subjected to prior to operation, acts as an effective proof test of the liner, screening out all flaws or cracks larger than a critical size. In doing so, flaw growth potential is available for cyclic operation at pressures less than the sizing pressure. Static fracture and cyclic life tests, involving laboratory type specimens and filament overwrapped tanks, were conducted on three liner materials: (1) 2219-T62 aluminum, (2) Inconel X750 STA, and (3) cryoformed 301 stainless steel. Variables included material condition, thickness, flaw size, flaw shape, temperature, sizing stress level, operating stress level and minimum-to-maximum operating stress ratio. From the empirical data base obtained, a procedure was established by which the service life of composite tanks with load sharing liners could be guaranteed with a high degree of confidence.

Bixler, W. D.↗

NASA NTRS1989

Low temperature measurement of the vapor pressures of planetary molecules

Interpretation of planetary observations and proper modeling of planetary atmospheres are critically upon accurate laboratory data for the chemical and physical properties of the constitutes of the atmospheres. It is important that these data are taken over the appropriate range of parameters such as temperature, pressure, and composition. Availability of accurate, laboratory data for vapor pressures and equilibrium constants of condensed species at low temperatures is essential for photochemical and cloud models of the atmospheres of the outer planets. In the absence of such data, modelers have no choice but to assume values based on an educated guess. In those cases where higher temperature data are available, a standard procedure is to extrapolate these points to the lower temperatures using the Clausius-Clapeyron equation. Last summer the vapor pressures of acetylene (C2H2) hydrogen cyanide (HCN), and cyanoacetylene (HC3N) was measured using two different methods. At the higher temperatures 1 torr and 10 torr capacitance manometers were used. To measure very low pressures, a technique was used which is based on the infrared absorption of thin film (TFIR). This summer the vapor pressure of acetylene was measured the TFIR method. The vapor pressure of hydrogen sulfide (H2S) was measured using capacitance manometers. Results for H2O agree with literature data over the common range of temperature. At the lower temperatures the data lie slightly below the values predicted by extrapolation of the Clausius-Clapeyron equation. Thin film infrared (TFIR) data for acetylene lie significantly below the values predicted by extrapolation. It is hoped to bridge the gap between the low end of the CM data and the upper end of the TFIR data in the future using a new spinning rotor gauge.

Kraus, George F.↗

NASA NTRS1995

Results of the 1995 JPL balloon flight solar cell calibration program

The Jet Propulsion Laboratory (JPL) solar cell calibration program was conceived to produce reference standards for the purpose of accurately setting solar simulator intensities. The concept was to fly solar cells on a high-altitude balloon, to measure their output at altitudes near 120,000 ft (36.6 km), to recover the cells, and to use them as reference standards. The procedure is simple. The reference cell is placed in the simulator beam, and the beam intensity is adjusted until the reference cell reads the same as it read on the balloon. As long as the reference cell has the same spectral response as the cells or panels to be measured, this is a very accurate method of setting the intensity. But as solar cell technology changes, the spectral response of the solar cells changes also, and reference standards using the new technology must be built and calibrated. Until the summer of 1985, there had always been a question as to how much the atmosphere above the balloon modified the solar spectrum. If the modification was significant, the reference cells might not have the required accuracy. Solar cells made in recent years have increasingly higher blue responses, and if the atmosphere has any effect at all, it would be expected to modify the calibration of these newer blue cells much more so than for cells made in the past. JPL has been flying calibration standards on high-altitude balloons since 1963 and continues to organize a calibration balloon flight at least once a year. The 1995 flight was the 48th flight in this series. The 1995 flight incorporated 46 solar cell modules from 7 different participants. The payload included Si, amorphous Si, GaAs, GaAs/Ge, dual junction cells, top and bottom sections of dual junction cells, and a triple junction cell. A new data acquisition system was built for the balloon flights and flown for the first time on the 1995 flight. This system allows the measurement of current-voltage (I-V) curves for 20 modules in addition to measurement of modules with fixed loads as had been done in the past.

Anspaugh, B. E.↗

NASA NTRS1996

Engineering strategies for the design of plant nutrient delivery systems for use in space: approaches to countering microbiological contamination

Microbiological contamination of crops within space-based plant growth research chambers has been postulated as a potentially significant problem. Microbial infestations; fouling of Nutrient Delivery System (NDS) fluid loops; and the formation of biofilms have been suggested as the most obvious and important manifestations of the problem. Strict sanitation and quarantine procedures will reduce, but not eliminate, microbial species introduced into plant growth systems in space habitats. Microorganisms transported into space most likely will occur as surface contaminants on spacecraft components, equipment, the crew, and plant-propagative materials. Illustrations of the potential magnitude of the microbiological contamination issue will be drawn from the literature and from documentation of laboratory and commercial field experience. Engineering strategies for limiting contamination and for the development of countermeasures will be described. Microbiological control technologies and NDS hardware will be discussed. Configurations appropriate for microgravity research facilities, as well as anticipated bio-regenerative life support system implementations, will be explored. An efficiently designed NDS, capable of adequately meeting the environmental needs of crop plants in space, is considered to be critical in both the research and operational domains. Recommended experiments, tests, and technology developments, structured to allow the development of prudent engineering solutions also will be presented.

NASA Discipline Number 61-10↗

NASA NTRS2003

Progress on Updating the 1961-1990 National Solar Radiation Database

The 1961-1990 National Solar Radiation Data Base (NSRDB) provides a 30-year climate summary and solar characterization of 239 locations throughout the United States. Over the past several years, the National Renewable Energy Laboratory (NREL) has received numerous inquiries from a range of constituents as to whether an update of the database to include the 1990s will be developed. However, there are formidable challenges to creating an update of the serially complete station-specific database for the 1971-2000 period. During the 1990s, the National Weather Service changed its observational procedures from a human-based to an automated system, resulting in the loss of important input variables to the model used to complete the 1961-1990 NSRDB. As a result, alternative techniques are required for an update that covers the 1990s. This paper examines several alternative approaches for creating this update and describes preliminary NREL plans for implementing the update.

Data bases↗

NASA NTRS2005

SAFER Inspection of Space Shuttle Thermal Protection System

In the aftermath of the space shuttle Columbia accident, it quickly became clear that new methods would need to be developed that would provide the capability to inspect and repair the shuttle's thermal protection system (TPS). A boom extension to the Remote Manipulator System (RMS) with a laser topography sensor package was identified as the primary means for measuring the damage depth in acreage tile as well as scanning Reinforced Carbon- Carbon (RCC) surfaces. However, concern over the system's fault tolerance made it prudent to investigate alternate means of acquiring close range photographs and contour depth measurements in the event of a failure. One method that was identified early was to use the Simplified Aid For EVA Rescue (SAFER) propulsion system to allow EVA access to damaged areas of concern. Several issues were identified as potential hazards to SAFER use for this operation. First, the ability of an astronaut to maintain controlled flight depends upon efficient technique and hardware reliability. If either of these is insufficient during flight operations, a safety tether must be used to rescue the crewmember. This operation can jeopardize the integrity of the Extra-vehicular Mobility Unit (EMU) or delicate TPS materials. Controls were developed to prevent the likelihood of requiring a tether rescue, and procedures were written to maximize the chances for success if it cannot be avoided. Crewmember ability to manage tether cable tension during nominal flight also had to be evaluated to ensure it would not negatively affect propellant consumption. Second, although propellant consumption, flight control, orbital dynamics, and flight complexity can all be accurately evaluated in Virtual Reality (VR) Laboratory at Johnson Space Center, there are some shortcomings. As a crewmember's hand is extended to simulate measurement of tile damage, it will pass through the vehicle without resistance. In reality, this force will push the crewmember away from the vehicle, and could induce a moment which, if strong enough, could saturate the attitude control system in SAFER. This raises the concern that additional propellant will be consumed to maintain controlled flight. To account for this, the fidelity of the Virtual Reality simulation was improved to include the effect of crewmember contact with the vehicle during SAFER flight. In addition, while participating in VR simulations, the subject is in shirt sleeves and sits in a chair. This does not provide a flight-like representation of body position awareness. To prevent inadvertent contact with tile or RCC, other facilities were utilized to establish crew preferences for body attitude and tool configuration. Finally, a study was performed to determine if attitude constraints are needed for the Space shuttle and International Space Station to reduce SAFER flight difficulty.

Scoville, Zebulon C.↗

NASA NTRS2007

Effects of Hind Limb Unloading on Pharmacokinetics of Procainamide in Mice

The pharmacokinetics (PK) of medications administered to astronauts could be altered by the conditions in space. It is prudent to expect that low gravity and free floating (and associated hemodynamic changes) could affect the absorption, distribution, metabolism and excretion of the drugs. Knowledge of these alterations is essential for adjusting the dosage and the regimen of drug administration. Among the medications of special interest are the cardiovascular drugs, especially the antiarrhythmic agents. In this study we used hind limb unloaded (HLU) mice as a model to investigate possible changes in the PK of a common antiarrhythmic drug procainamide (PA). Prior to drug administration the experimental animals were tail suspended for 24 hours and the control animals were kept free. PA (150-250 mg per kg) was given orally by a gavage procedure. After that the experimental mice were kept suspended for additional 1, 2, 3 and 6 hours. At these time points the serum concentration of PA and N-acetyl-procainamide (NAPA), an active metabolite which is formed by N-acetyltransferase in the liver, were measured by the fluorescence polarization immunoassay (FPIA) on the AxSYM autoanalyzer (Abbott Laboratories, Abbott Park, IL). The serum level of PA in HLU mice at 1 hour after administration was almost 40% lower than in controls. At 2-3 hours the difference still maintained, however, it was not statistically significant; at 6 hours no difference was detected. The level of NAPA in HLU mice was slightly lower at 1 and 2 hours but the difference did not reach statistical significance. The estimated PA half-life time in HLU mice was almost 55% longer than in control animals. These results confirm that hind limb unloading and related hemodynamic changes significantly alter the PK of PA. The effects are most likely primarily associated with a decrease in the drug absorption, especially within the first two hours after administration. At the same time prolongation of the PA half-life time in the HLU mice points towards slower drug elimination from the circulation.

Risin, Semyon A.↗

NASA NTRS2014

Comparison of Spectral Radiance Calibration Techniques Used for Backscatter Ultraviolet Satellite Instruments

Methods for determining the absolute radiometric calibration sensitivities of backscatter ultraviolet (BUV) satellite instruments are compared as part of an effort to minimize pre-launch calibration errors. An internally illuminated integrating sphere source has been used for the Shuttle Solar BUV (SSBUV), Total Ozone Mapping Spectrometer (TOMS), Ozone Mapping Instrument (OMI), and Global Ozone Monitoring Experiment 2 (GOME-2) using standardized procedures traceable to national standards. These sphere-based sensitivities agree to within three percent [k equals 2] relative to calibrations performed using an external diffuser illuminated by standard irradiance sources, the customary radiance calibration method for BUV instruments. The uncertainty for these calibration techniques as implemented at the NASA Goddard Space Flight Centers Radiometric Calibration and Development Laboratory is shown to be 4 percent at 250nm [k equals 2] when using a single traceable calibration standard. Significant reduction in the uncertainty of nearly 1 percent is demonstrated when multiple calibration standards are used.

residual errors↗

NASA NTRS2019

TURBOMAT: A Probabilistic Turbomachinery Aeroelastic Analysis Tool

An integration of aeroelastic analysis procedures with probabilistic analysis methods enables us to design safe reliable engines with quantified reliability. Towards this goal, a graphical user interface (GUI) based tool that integrates the codes Aeroelastic analysis of propfans (ASTROP2) and Numerical Evaluation of Stochastic Structures Under Stress (NESSUS) is developed. The tool entitled TURBOMachinery Aeroelastic Analysis Tool (TURBOMAT), is developed utilizing the MATrix Laboratory (Matlab) Guide (Graphical User Interface Development) tool box. TURBOMAT provides a user friendly computational environment for rapid assessment of Turbomachinery blades flutter characteristics, subjected to uncertain loading conditions with variability in material and aerodynamic properties. The tool is seen as an education tool for new students and young engineers starting their careers in structural Aeroelasticity who want to learn and understand aeroelastic aspects of turbomachinery components, fans, compressors and turbines, including uncertainties in loading and material properties.A typical fan blade configuration geometry was chosen to demonstrate the tool. The results are presented in the form of probabilistic density function (PDF), the cumulative distribution function (CDF) and sensitivity factors. Both first order fast probability integration (FPI) and the Monto Carlo (MC) techniques are used in the analysis and compared. The tool enabled us to quantify blade flutter reliability as well as the ranking of uncertain variables and their importance to blade flutter response.

Aeroelastic Analysis↗

DOE OSTI2021

LiDAR-Based Point Cloud Data Processing

The presentation includes the procedures of utilizing LiDAR-based point cloud data in WebGL applications, such as capturing data, processing data, importing point cloud into Unity software, and improving application performance. It uses IRC BLD 603 Lab B-12 as an example. It'll be presented at Viz n Learn workshop which is a collaboration series between INL's Applied Visualization Laboratory (AVL) and University of Wyoming (UW)'s Shell 3D Visualization center. Each session will highlight 2 projects from each institution monthly, followed by discussion on areas of collaborative interest and action.

3D↗

DOE OSTI2026

Performance of pumped counterflow virtual impactors to study aerosol interactions with laboratory generated warm clouds

Pumped Counterflow Virtual Impactors (PCVI) are designed to separate aerosols based on aerodynamic diameter, which is particularly useful for isolating cloud droplets and ice crystals from smaller particles. However, the PCVI transmission efficiency (TE) values reported in the literature show considerable variability, and little information is available on the TEs for cloud liquid droplets. Here, we determined the optimal flow conditions for PCVI sampling for different activation ratios from the MTU Pi-cloud chamber, highlighting the conditions that maximize droplet residual sampling while minimizing interstitial transmission. Even for a lower limit cloud activation ratio = 1:10, an add flow of 1.5 LPM achieves a residual fraction greater than 0.80, with a droplet TE of ∼15% for typical Pi-Chamber droplets with diameters between 3.5 to 10 µm. This framework can be adapted for field cloud measurements based on the cloud conditions of interest. TE for cloud droplets under flow conditions at which ∼99% of the unactivated submicron particles were removed was substantially lower between 8 and 16% than for supermicron dry particles (∼30 to 40% for 3 µm polystyrene latex spheres). In addition, we conducted a comparison of the performances of three similar PCVI units to assess repeatability for dry aerosols and cloud droplets. All three PCVIs performed similarly in rejecting submicron particles smaller than the desired cutoff diameter. One of the units showed lower TEs due to a misalignment of the internal orifice. We discuss a procedure that improved alignment and performance.

54 ENVIRONMENTAL SCIENCES↗

DOE OSTI2026

Activation of Thermal Insulation and Contamination Prevention

The goals of this paper are to enhance the understanding of the potential activation and contamination hazards from the use of insulating materials in the Molten Chloride Reactor Experiment and to foster safer work environments through informed decision-making and strategic planning. It was written to resolve a gating comment from the core heating system preliminary design review. The largest dose expected from the considered insulation materials is about 0.1 mrem per year from Pyrogel. Although Cerablanket stood out among the insulation materials for encouraging ALARA practices, it has a higher thermal conductivity. At low power levels, focusing on reducing the generation of dust from ERD activities may be more effective for reducing the potential spread of contamination than changing the insulating material type. However, regardless of the material chosen, PPE and safety conscious procedural practices can help reduce the production and spread of activated dust––thus minimizing the radiological hazard to workers.

21 - SPECIFIC NUCLEAR REACTORS AND ASSOCIATED PLAN↗

NASA NTRS2023

NASA Glenn Propulsion Systems Laboratory Customer Guide

This guide describes the Propulsion Systems Laboratory (PSL) at NASA Glenn Research Center (GRC) and was written to help customers utilizing the facility understand all the components of conducting a test program within the facility. The PSL complex supports two large engine test cells that simulate altitude flight conditions for a wide range of research and experimental tests. The test cells operate at altitudes up to 90,000 ft and speeds from subsonic to above supersonic. The way the facility sets test points at the engine or test article inlet, such as pressure, temperature, and Mach number is discussed. Support systems such as the heated and cooled combustion air system, the altitude exhaust system, the hydraulic system, the nitrogen, oxygen, and hydrogen systems, hydrogen burners, the engine exhaust gas-sampling system, and single- and multiple-axis thrust stands are addressed. Facility safety procedures, pre-test requirements, test operation standards are also stated in later sections. Past PSL tests and other capabilities are also discussed.

PSL Customer Guide↗

DOE OSTI2022

Interim Report on FY22 ORNL A709 Welding Research and Testing of Production Welds in Support of Developing ASME A709 Code Case Data Package

As part of the Alloy 709 ASME Code Case development effort under the Advanced Reactor Technologies (ART) Program, this work covers the development of the technical basis for weld fabrication and weld qualification of Alloy 709. This report summarizes the Alloy 709 welding research conducted at Oak Ridge National Laboratory (ORNL) in FY 2022. Two new production welds were fabricated on two commercial heats of Alloy 709 of different phosphorus (P) levels using Alloy 709 filler metal with P content less than 20 wppm with gas tungsten arc welding (GTAW). Both production welds successfully passed ASME Section IX weld qualification tests, and this concludes the Alloy 709 welding procedure development to scale up to 2-in thick plates. In FY 2022, we also demonstrated the success in welding of high P commercial Alloy 709 plates with weld wires having higher P content at 30 wppm. A test weld fabricated with the 30 wppm weld wire on the first commercial heat (140 wppm P) passed all weld qualification tests without issues. Additionally, experiment setup and testing procedure of the circular patch weldability test has been developed, for evaluating the P effect in weld wire on solidification cracking susceptibility of Alloy 709 weld, with the preliminary results summarized in this report. Research on further relaxing the P level restriction beyond 30 wppm are planned in FY 2023. The preliminary cross-weld creep tests results continue to show little or no creep strength reduction relative to the base metal.

36 MATERIALS SCIENCE↗