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Pfleger-Lab/Metabolic-Modeling---Yield-Analysis-of-PhaG

Microbial lipid metabolism is an attractive route for producing oleochemicals. The predominant strategy centers on heterologous thioesterases to synthesize desired chain-length fatty acids. To convert acids to oleochemicals (e.g., fatty alcohols, ketones), the narrowed fatty acid pool needs to be reactivated as coenzyme A thioesters at cost of one ATP per reactivation – an expense that could be saved if the acyl-chain was directly transferred from ACP- to CoA-thioester. Here, we demonstrate such an alternative acyl-transferase strategy by heterologous expression of PhaG, an enzyme first identified in Pseudomonads, that transfers 3-hydroxy acyl-chains between acyl-carrier protein and coenzyme A thioester forms for creating polyhydroxyalkanoate monomers. We use it to create a pool of acyl-CoA’s that can be redirected to oleochemical products. Through bioprospecting, mutagenesis, and metabolic engineering, we develop three strains of Escherichia coli capable of producing over 1 g/L of medium-chain free fatty acids, fatty alcohols, and methyl ketones.

Yan, Qiang↗

Exploring Causes of Beam Loss at CEBAF

At Jefferson Lab, the Continuous Electron Beam Accelerator (CEBAF) features a unique design with two linear accelerators and two arc sections allowing for multiple turns of the electron beam, as well as four experimental end stations. This topology leads to increased beam losses, especially in the spreader and recombiner regions connecting the arcs to the linacs and in the extraction regions connecting the experimental end stations to the accelerator. These losses result in equipment activation and operational interruptions. Recent upgrades to the facility’s diagnostic systems, including the addition of xenon ion chambers, have provided higher-resolution data regarding these loss events. Building on this improved observational capability, we are developing a simulation framework using optics codes and the Geant4-based BDSIM to model beam extinction and halo formation in these regions. This work aims to correlate simulation results with experimental data to isolate the causes of beam loss and inform future machine tuning strategies. We present a summary of conclusions drawn from recent operational studies and outline a plan to model the beam loss and validate the simulations.

Matthews, C. [Old Dominion Univ., Norfolk, VA (Uni↗

A commentary on thallium radiochemistry in conjunction with OPEX23

Thallium radiochemistry was developed as a routine analytical capability at Los Alamos, dating from some of its earliest history after WWII. The first post-war compilation of radiochemical procedures published by the Radiochemistry Group J-11 is dated February 1953 as Los Alamos report LA-1566. The thallium radiochemistry procedure was authored by René J. Prestwood, and the details of the method as documented in 1953 are nearly identical to the thallium procedure contained in the most recent Collected Radiochemical and Geochemical Procedures (Fifth Edition) contained in Los Alamos report LA-1721 issued May 1990. René was a talented and well-respected member of the Radiochemistry Group. He first came to the lab in 1943 as an undergraduate student from UC Berkeley to join the Manhattan Project. After the war, René earned his PhD in Nuclear Chemistry with Art Wahl at Washington University in St. Louis. He then returned to Los Alamos as a technical staff member and retired in 1984. René passed away at the age of 92 on December 21, 2012.

38 RADIATION CHEMISTRY, RADIOCHEMISTRY, AND NUCLEA↗

Additional Development and Systems Analyses of Pneumatic Technology for High Speed Civil Transport Aircraft

In the Task I portion of this NASA research grant, configuration development and experimental investigations have been conducted on a series of pneumatic high-lift and control surface devices applied to a generic High Speed Civil Transport (HSCT) model configuration to determine their potential for improved aerodynamic performance, plus stability and control of higher performance aircraft. These investigations were intended to optimize pneumatic lift and drag performance; provide adequate control and longitudinal stability; reduce separation flowfields at high angle of attack; increase takeoff/climbout lift-to-drag ratios; and reduce system complexity and weight. Experimental aerodynamic evaluations were performed on a semi-span HSCT generic model with improved fuselage fineness ratio and with interchangeable plain flaps, blown flaps, pneumatic Circulation Control Wing (CCW) high-lift configurations, plain and blown canards, a novel Circulation Control (CC) cylinder blown canard, and a clean cruise wing for reference. Conventional tail power was also investigated for longitudinal trim capability. Also evaluated was unsteady pulsed blowing of the wing high-lift system to determine if reduced pulsed mass flow rates and blowing requirements could be made to yield the same lift as that resulting from steady-state blowing. Depending on the pulsing frequency applied, reduced mass flow rates were indeed found able to provide lift augmentation at lesser blowing values than for the steady conditions. Significant improvements in the aerodynamic characteristics leading to improved performance and stability/control were identified, and the various components were compared to evaluate the pneumatic potential of each. Aerodynamic results were provided to the Georgia Tech Aerospace System Design Lab. to conduct the companion system analyses and feasibility study (Task 2) of theses concepts applied to an operational advanced HSCT aircraft. Results and conclusions from these experimental evaluations are presented herein, as are recommendations for further development and follow-on investigations. Also provided as an Appendix for reference are the basic results from the previous pneumatic HSCT investigations.

Englar, Robert J.↗

NASA’s Progress Toward Commercial Space Communications—SATCOM Demonstrations and Wideband Multilingual Terminal Development

The National Aeronautics and Space Administration (NASA) Space Communications and Navigation (SCaN) Program is continuing to forge a path toward programmatic and operational transformation enabling commercialization of communications and navigation services to the greatest extent possible for near Earth users. National Space Policy is driving government agencies to incorporate commercial offerings and services to the maximum extent possible. As such, NASA has no plans to build or deploy Tracking and Data Relay Satellites, but will seek to fill NASA mission space-relay capability needs using commercial satellite communications (SATCOM) providers and services. The goal is to support an approach that is both flexible to commercial service constructs and provides continuity of support with current assets as long as required. Progress toward commercialization is advancing in two key areas: (1) awards have been made for demonstrations of SATCOM services, and (2) development of wideband and multilingual user terminals has advanced to the flight demonstration phase. The Communications Services Project (CSP) at Glenn Research Center (GRC), has awarded Funded Space Act Agreements (FSAA) to six industry vendors. Inmarsat Government Inc., Kuiper Government Solutions (KGS) LLC, SES Government Solutions, Space Exploration Technologies, Telesat U.S. Services LLC, and Viasat Incorporated received a combined $278.5 million to complete technology development and in-space demonstrations over the next several years. The end-to-end service capabilities being targeted are based on existing NASA mission operational needs. Accordingly, each company has proposed a technical approach to lower costs, increase flexibility, and improve performance for a broad range of missions. In the current market, industry vendors operate at a range of different frequencies and use variable, sometime proprietary, coding and modulations schemes. As NASA strives for a network comprised of services provided by multiple distinct suppliers, interoperability is a fitting solution to unify the network. Wideband and multi-lingual user terminals are being developed to bridge differences in industry services. Building on ground demonstrations completed in 2021, the Johns Hopkins Applied Physics Lab (APL) will be flight testing a multi-lingual wideband terminal (payload) and demonstrating connectivity to both government and commercial relay services. This paper provides a discussion of the progress toward NASA’s commercial space communications goals and consideration of key challenges and next steps.

space communications↗

NASA's Progress Toward Commercial Space Communications — SATCOM Demonstrations and Wideband Multilingual Terminal Development

The National Aeronautics and Space Administration (NASA) Space Communications and Navigation (SCaN) Program is continuing to forge a path toward programmatic and operational transformation enabling commercialization of communications and navigation services to the greatest extent possible for near Earth users. U.S. National Space Policy is driving government agencies to incorporate commercial offerings and services to the maximum extent possible. As such, NASA has no plans to build or deploy additional Tracking and Data Relay Satellites (TDRS), but will seek to fill NASA mission space-relay capability needs using commercial satellite communications (SATCOM) providers and services. The goal is to support an approach that is both flexible to commercial service constructs and provides continuity of support with current assets as long as required. Progress toward commercial services is advancing in two key areas: (1) awards have been made for demonstrations of SATCOM services, and (2) development of wideband and multilingual user terminals has advanced to the flight demonstration phase. The Communications Services Project (CSP) at Glenn Research Center (GRC), has awarded Funded Space Act Agreements (FSAA) to six industry vendors. Inmarsat Government Inc., Kuiper Government Solutions (KGS) LLC, SES Government Solutions, Space Exploration Technologies, Telesat U.S. Services LLC, and Viasat Incorporated will receive a combined $278.5 million to complete technology development and in-space demonstrations over the next several years. The end-to-end service capabilities being targeted are based on existing NASA mission operational needs. Accordingly, each company has proposed a technical approach to lower costs, increase flexibility, and improve performance for a broad range of missions. In the current market, industry vendors operate at a range of different frequencies and use variable, sometimes proprietary, coding and modulations schemes. As NASA strives for a network comprised of services provided by multiple distinct suppliers, interoperability is a fitting solution to unify the network. Wideband and multi-lingual user terminals are being developed to bridge differences in industry services. Building on ground demonstrations completed in 2021, the Johns Hopkins Applied Physics Lab (APL) will be flight testing a multi-lingual wideband terminal (payload) and demonstrating connectivity to both government and commercial relay services. This paper provides a discussion of the progress toward NASA’s commercial space communications goals and consideration of key challenges and next steps.

commercialization↗

National Nuclear Security Administration Strategic Vision Strengthening our Nation through Nuclear Security

The National Nuclear Security Administration’s enduring mission is to protect our nation by maintaining a safe, secure, and effective nuclear weapons stockpile, reducing global nuclear threats, and providing our submarines and aircraft carriers with militarily effective nuclear propulsion. Although we have numerous strategic partners that enable, contribute to, and benefit from our efforts, no other organization, government or civilian, can accomplish our unique mission on behalf of the American people. In this area, we stand alone. This strategic vision pursues urgent change at a significant scale to develop creative approaches, make sustained investments, and be disciplined in our approach to develop a nuclear capability for our time and for the foreseeable future. It is incumbent on us to anticipate our future security challenges and ensure our country is ready to meet them. Not doing so would have far-reaching consequences. Failure to meet our vital mission objectives will erode confidence in the security that the United States strategic deterrent umbrella provides. In assessing the current mission environment in NNSA, we can count on one thing—change: The geopolitical environment for our deterrent is ever-changing Threats from rogue states and terrorists are evolving Our nuclear weapons and the infrastructure that supports them are aging Science and technology continue to move forward at an ever-increasing pace In this dynamic environment, it is not sufficient to remedy today’s situation and meet our current mission requirements. We must lean forward in the development, planning, and execution of programs that address our current challenges while developing the workforce, infrastructure, tools, and governance systems that will enable us to meet our deterrence, non-proliferation, and naval propulsion mission requirements for the next 50 years. We must embrace a next-generation enterprise that is flexible enough to respond to future challenges. With decades of stagnation following the end of the Cold War, we find ourselves in the unenviable position of implementing near-term fixes while using those lessons learned to better prepare for the future. Without sustained and predictable investments to restore and modernize our infrastructure, we will rapidly lose our ability to deliver on our promise of a safe and reliable nuclear weapons stockpile, which will degrade our deterrent capability and render legacy weapon systems irrelevant to the defense of our nation. We must not and will not allow the next generation of our nuclear security enterprise to simply maintain the status quo. We have a storied past that guides us. For 75 years our enterprise has overcome every challenge, led the country in incredible scientific and engineering endeavors and discoveries, and successfully ensured constant vigilance in maintaining an effective deterrent, reducing global nuclear threats, and powering our nuclear navy. Now is the time for us to take decisive action in forging the enterprise of the future. As I have traveled to all of our labs, plants, and sites and met with people across our complex, I have been left with one overwhelming impression: the incredible workforce that makes up our nuclear security enterprise is up to all of the challenges we have before us. Together we can and will ensure that those in the future workforce have the resources and the responsive, agile infrastructure they need to maintain the systems of today and to design and field the systems of tomorrow.

Source record↗

Hybrid network via instantaneous photoradiation: High efficient design of 100% bio-based thermosets with remoldable and recyclable capabilities after UV curing

Conventional thermoset materials cannot be remolded and recycled due to the covalent bonds existing in the network. The reversible nature of secondary interactions between monomeric units renders supramolecular structure reconfigurable abilities upon exposure to appropriate stimuli. This feature is quite useful in the design of novel thermoset materials with remoldability and recyclability, but its widespread adoption is limited due to the low strength and high cost of supramolecular structure. Here, we present a new class of thermoset with a distinct recycling mechanism and structural design. It is strong, transparent, recyclable, 100% biorenewable, creep resistance after thermal treatment, and produced in a ultrafast, scalable and cost-effective manner. These characteristics come from a purpose-designed hybrid network via a ultraviolet radiation in seconds. As a result, this technology provides a new way to obtain thermosets with remoldability and recyclability. It is green and efficient, not limited in lab, and can be scaled up for industry.

36 MATERIALS SCIENCE↗

Lab-scale Lidar Sensing of Diesel Engines Exhausts

Combustion technology and its environmental concerns are being considered with increasing attention, not only for global-scale effects, but also for toxicological implications, particularly in the lift conditions of traffic-congested areas and industrial sites. Majority combustion by-products (CO, NO(sub x)) and unburned hydrocarbons (HC), are already subject to increasingly severe regulations; however other, non-regulated minority species, mainly soot and heavy aromatic molecules, involve higher health risks, as they are suspected to be agents of serious pathologies and even mutagenic effects. This is but one of the reasons why much research work is being carried out worldwide on the physical properties of these substances. Correspondingly, the need arises to detect their presence in urban environments, with as high a sensitivity as is required by their low concentrations, proper time- and space-resolutions, and 'real-time' capabilities. Lidar techniques are excellent candidates to this purpose, although severe constraints limit their applicability, eye-safety problems and aerosol Mie scattering uncertainties above all. At CNR's Istituto Motori in Napels, a Lidar-like diagnostic system is being developed, aimed primarily at monitoring the dynamic behavior of internal combustion engines, particularly diesel exhausts, and at exploring the feasibility of a so-called 'Downtown Lidar'.

Borghese, A.↗

Plasma Cleaning Research for Z

Z is a high-current pulsed-power generator located at Sandia National Laboratories. It is capable of delivering 100-ns, 30-MA current pulses to loads used for materials studies, weapons-effects simulation, and nuclear-fusion research. Under some conditions, a significant fraction of the current does not reach the load but is shunted across the inter-electrode vacuum gap that leads to the load. That undesirable current loss is thought to be due to excessive plasma generation and flow from the electrodes into the vacuum gap. Much past work suggests that this current loss may be reduced if contaminants on or near the surfaces of the electrodes are removed by plasma discharge cleaning. This report describes light-lab work performed in the past year to evaluate and understand plasma cleaning, and to develop the technology required for future tests on Z.

70 PLASMA PHYSICS AND FUSION TECHNOLOGY↗

Human and Robotic Space Mission Use Cases for High-Performance Spaceflight Computing

Spaceflight computing is a key resource in NASA space missions and a core determining factor of spacecraft capability, with ripple effects throughout the spacecraft, end-to-end system, and mission. Onboard computing can be aptly viewed as a "technology multiplier" in that advances provide direct dramatic improvements in flight functions and capabilities across the NASA mission classes, and enable new flight capabilities and mission scenarios, increasing science and exploration return. Space-qualified computing technology, however, has not advanced significantly in well over ten years and the current state of the practice fails to meet the near- to mid-term needs of NASA missions. Recognizing this gap, the NASA Game Changing Development Program (GCDP), under the auspices of the NASA Space Technology Mission Directorate, commissioned a study on space-based computing needs, looking out 15-20 years. The study resulted in a recommendation to pursue high-performance spaceflight computing (HPSC) for next-generation missions, and a decision to partner with the Air Force Research Lab (AFRL) in this development.

use cases↗

Qualification of Domestic Lyocell Based Phenolic Impregnated Carbon Ablator (PICA-D) for NASA Missions

Phenolic Impregnated Carbon Ablator (PICA) is a low-density ablator that has been used as the planetary entry heatshield for several NASA missions since the late 90’s. Its low density and efficient performance characteristics have proven effective for use from Discovery to Flag-ship class missions, from Sample Return missions such as Stardust, OSIRIS-REx to large Mars Lander missions such as Mars Science Lab (MSL) and Mars 2020. The rayon-based carbon precursor raw material used in PICA preform manufacturing has experienced multiple supply chain issues. The challenge involved in finding a replacement fiber source is in processing as well as in the final performance of the ablator. Each replacement necessitates the requalification of the PICA. This has happened at least twice in the past 25 years, and a third substitution is now needed. Due to the obsolescence of the input foreign rayon fiber source, a new variant of PICA has been developed using a domestic rayon-like fiber source, Lyocell. Due to its flight heritage and proven capability, PICA is baselined as the Thermal Protection System (TPS) for Dragonfly and Mars Sample Return Sample Retrieval Lander mission and is being considered for the backshell of the Mars Sample Return Earth Entry System. All three missions are due to be launched between 2026 and 2028. The challenge this time is to ensure the PICA made with domestic material is a suitable replacement to the heritage PICA used in MSL and Mars 2020 so that the design of the heatshield can be matured without much risk. Results are presented from the recent efforts of 22 PICA-D billets that were Lot Acceptance Tested. Thermal, mechanical, and representative environment arc-jet tests have been conducted. Testing of PICA-Domestic (PICA-D) indicates very comparable performance with respect to “heritage” PICA materials and thus PICA-D is expected to be a sustainable and nearly a “drop-in” replacement solution for future NASA missions.

Matt Gasch↗

Qualification of Domestic Lyocell Based Phenolic Impregnated Carbon Ablator (PICA-D) for NASA Missions

Phenolic Impregnated Carbon Ablator (PICA) is a low-density ablator that has been used as the planetary entry heatshield for several NASA missions since the late 90’s. Its low density and efficient performance characteristics have proven effective for use from Discovery to Flag-ship class missions, from Sample Return missions such as Stardust, OSIRIS-REx to large Mars Lander missions such as Mars Science Lab (MSL) and Mars 2020. The rayon-based carbon precursor raw material used in PICA preform manufacturing has experienced multiple supply chain issues. The challenge involved in finding a replacement fiber source is in processing as well as in the final performance of the ablator. Each replacement necessitates the requalification of the PICA. This has happened at least twice in the past 25 years, and a third substitution is now needed. Due to the obsolescence of the input foreign rayon fiber source, a new variant of PICA has been developed using a domestic rayon-like fiber source, Lyocell. Due to its flight heritage and proven capability, PICA is baselined as the Thermal Protection System (TPS) for Dragonfly and Mars Sample Return Sample Retrieval Lander mission and is being considered for the backshell of the Mars Sample Return Earth Entry System. All three missions are due to be launched between 2026 and 2028. The challenge this time is to ensure the PICA made with domestic material is a suitable replacement to the heritage PICA used in MSL and Mars 2020 so that the design of the heatshield can be matured without much risk. Results are presented from the recent efforts of 22 PICA-D billets that were Lot Acceptance Tested. Thermal, mechanical, and representative environment arc-jet tests have been conducted. Testing of PICA-Domestic (PICA-D) indicates very comparable performance with respect to “heritage” PICA materials and thus PICA-D is expected to be a sustainable and nearly a “drop-in” replacement solution for future NASA missions.

PICA↗

X-ray photonic microsystems for the manipulation of synchrotron light

In this study, photonic microsystems played an essential role in the development of integrated photonic devices, thanks to their unique spatiotemporal control and spectral shaping capabilities. Similar capabilities to markedly control and manipulate X-ray radiation are highly desirable but practically impossible due to the massive size of the silicon single-crystal optics currently used. Here we show that micromechanical systems can be used as X-ray optics to create and preserve the spatial, temporal and spectral correlation of the X-rays. We demonstrate that, as X-ray reflective optics they can maintain the wavefront properties with nearly 100% reflectivity, and as a dynamic diffractive optics they can generate nanosecond time windows with over 100-kHz repetition rates. Since X-ray photonic microsystems can be easily incorporated into lab-based and next-generation synchrotron X-ray sources, they bring unprecedented design flexibility for future dynamic and miniature X-ray optics for focusing, wavefront manipulation, multicolour dispersion, and pulse slicing.

71 CLASSICAL AND QUANTUM MECHANICS, GENERAL PHYSIC↗

Simulation Studies on the Interactions of Electron Beam with Wastewater

The manufactured chemical pollutants, like 1,4 dioxane and PFAS (per- and polyfluroralkyl substances), found in the underground water and/or drinking water are challenging to be removed or biodegraded. Energetic electrons are capable of mediating and removing them. This paper utilizes FLUKA code to evaluate the beam-wastewater interaction effects with different energy, space and divergence distributions of the electron beam. With 8 MeV average energy, the electron beam exits from a 0.0127 cm thick titanium window, travels through a 4.3 cm distance air and a second 0.0127 cm thick stainless water container window with 2.43 cm radius, and finally is injected into the water area, where the volume of water is around 75 cubic cm. The distribution parameters of the electron beam are from the GPT (General Particle Tracer) simulations for UITF (Upgraded Injector Test Facility) in Jefferson lab. By varying the distributions, several measurements including the dose (or energy deposition) distribution, electron fluence, photon fluence are scored and compared. Taking the comparisons into consideration, this paper is aiming to find better electron beams for the wastewater irradiation.

Li, X.↗

Simulation Studies on the Interactions of Electron Beam with Wastewater

The manufactured chemical pollutants, like 1,4 dioxane and PFAS (per- and polyfluroralkyl substances), found in the underground water and/or drinking water are challenging to be removed or biodegraded. Energetic electrons are capable of mediating and removing them. This paper utilizes FLUKA code to evaluate the beam-wastewater interaction effects with different energy, space and divergence distributions of the electron beam. With 8 MeV average energy, the electron beam exits from a 0.0127 cm thick titanium window, travels through a 4.3 cm distance air and a second 0.0127 cm thick stainless water container window with 2.43 cm radius, and finally is injected into the water area, where the volume of water is around 75 cubic cm. The distribution parameters of the electron beam are from the GPT (General Particle Tracer) simulations for UITF (Upgraded Injector Test Facility) in Jefferson lab. By varying the distributions, several measurements including the dose (or energy deposition) distribution, electron fluence, photon fluence are scored and compared. Taking the comparisons into consideration, this paper is aiming to find better electron beams for the wastewater irradiation.

Li, X.↗

Automated Credibility Assessments of User Features in Scientific Software

Scientific software (SciSoft) is complex, often containing a mixture of production capabilities co-mingled with features under active research and development. Furthermore, SciSoft is often developed over decades by non-computer scientists who may not have a strong background in or prioritize software architecture design, testing, and quality (e.g., test coverage). These conditions lead to difficulty in understanding which software components or functions implement what user-facing features and therefore those features’ software quality pedigree. This lack of understanding poses challenges in assessing readiness and credibility of user features, and often relies on a SciSoft subject matter expert’s (SME) laborious investigation and assertion. This final report of a one-year Computing and Information Sciences Lab Directed Research and Development project presents a general framework for modeling SciSoft architecture as a direct relationship between user features and the software components/functions that implement them. Our approach leverages automated labeling of the SciSoft’s regression test suite and employs machine learning algorithms to construct the architecture model. We demonstrate this framework on the Solid Mechanics component of the SIERRA multi-physics engineering analysis suite developed at Sandia National Laboratories.

97 MATHEMATICS AND COMPUTING↗

FY23 Update: Aerosol Sampling for the Canister Deposition Field Demonstration

This report describes the results of preliminary testing of aerosol monitoring equipment that will be used to continuously monitor the aerosol source term for the multi-year Canister Deposition Field Demonstration (CDFD). These data are required inputs for the development and validation of models for the deposition of dust and potentially corrosive salts on the surface of spent nuclear fuel (SNF) dry storage canisters. Surface salt loads correlate with the extent of corrosion damage on a metal surface, and potentially to the likelihood and timing of initiation of stress corrosion cracks. Aerosols will be monitored at the CDFD site using three instruments. A Dekati ® ELPI+ cascade impactor will be used for real-time monitoring of aerosol particle sizes. It will also collect dust in 14 size bins on impactor targets that can be chemically analyzed to determine the soluble salts present as a function of particle size. However, this instrument can only measure dried aerosols, with a diameter of <10 µm. The second instrument is a Topas laser particle size spectrometer, which provides real-time monitoring of aerosol particle sizes up to ~40 µm in size. It monitors both the ambient (potentially deliquesced) aerosol particle size distributions required for the dust deposition models and the distributions of the equivalent dried particles, allowing correlation with the Dekati ® data. However, it does not discriminate between inert dust particles and salt aerosols, and it does not retain samples of the different particle sizes for later analysis. The third instrument that will monitor aerosols at the CDFD site is a Clean Air Status and Trends Network (CASTNET) tower, which uses a multiple canister system to collect weekly samples for analysis to total suspended aerosol particle compositions and atmospheric gas concentrations. This status report describes work in FY23 to develop the capabilities for using these tools. In two training exercises, the cascade impactor and laser particle sizer were deployed in two different testing environments, one indoor and one outdoor. For the cascade impactor, the tests provided opportunities for the operators to familiarize themselves with impactor substrate preparation, and post-test sample removal and analysis. For the laser particle sizer, the tests were used to evaluate different instrument parameters, to determine the most appropriate settings for capturing transient events. Data and samples were collected for weeks to months for each test, and the results are presented here. In addition to the preliminary testing, contracts were developed with WSP Analytical Labs for sample preparation and analysis of the cascade impactor samples. The impactor tower from outdoor test was delivered to WSP and used to train the staff there in disassembly, sample extraction, sample analysis, and tower reassembly with new target substrates. These are tasks that WSP will be performing routinely for the CDFD project. The CASTNET system cannot be purchased or tested until an actual site has been selected for the CDFD test. Work for this FY has been restricted to preparation of contracts for purchasing the CASTNET tower, and for sample analysis, once the tower is in operation.

11 NUCLEAR FUEL CYCLE AND FUEL MATERIALS↗