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NASA NTRS2016

Development of X-Ray Microcalorimeter Imaging Spectrometers for the X-Ray Surveyor Mission Concept

Four astrophysics missions are currently being studied by NASA as candidate large missions to be chosen inthe 2020 astrophysics decadal survey.1 One of these missions is the X-Ray Surveyor (XRS), and possibleconfigurations of this mission are currently under study by a science and technology definition team (STDT). Oneof the key instruments under study is an X-ray microcalorimeter, and the requirements for such an instrument arecurrently under discussion. In this paper we review some different detector options that exist for this instrument,and discuss what array formats might be possible. We have developed one design option that utilizes eithertransition-edge sensor (TES) or magnetically coupled calorimeters (MCC) in pixel array-sizes approaching 100kilo-pixels. To reduce the number of sensors read out to a plausible scale, we have assumed detector geometriesin which a thermal sensor such a TES or MCC can read out a sub-array of 20-25 individual 1 pixels. In thispaper we describe the development status of these detectors, and also discuss the different options that exist forreading out the very large number of pixels.

multiplexing↗
NASA NTRS2016

Dios: The Dark Baryon Exploring Mission

DIOS (Diffuse Intergalactic Oxygen Surveyor) is a small satellite aiming for a launch around 2022 with JAXA's Epsilon rocket. Its main aim is a search for warm-hot intergalactic medium with high-resolution X-ray spectroscopy of redshifted emission lines from OVII and OVIII ions. The superior energy resolution of TES microcalorimeters combined with a wide field of view (30 diameter) will enable us to look into gas dynamics of cosmic plasmas in a wide range of spatial scales from Earths magnetosphere to unvirialized regions of clusters of galaxies. Mechanical and thermal design of the spacecraft and development of the TES calorimeter system are described. Employing an enlarged X-ray telescope with a focal length of 1.2 m and fast repointing capability, DIOS can observe absorption features from X-ray afterglows of distant gamma-ray bursts.

X-ray telescope↗
NASA NTRS2016

Characterization of an Atomic Hydrogen Source for Charge Exchange Experiments

We characterized the dissociation fraction of a thermal dissociation atomic hydrogen source byinjecting the mixed atomic and molecular output of the source into an electron beam ion trapcontaining highly charged ions and recording the x-ray spectrum generated by charge exchangeusing a high-resolution x-ray calorimeter spectrometer. We exploit the fact that the charge exchangestate-selective capture cross sections are very different for atomic and molecular hydrogen incidenton the same ions, enabling a clear spectroscopic diagnostic of the neutral species.

issociationX-ray spectrometersX-ray spectraMolecul↗
NASA NTRS2016

First Peek of ASTRO-H Soft X-Ray Telescope (SXT) In-Orbit Performance

ASTRO-H (Hitomi) is a Japanese X-ray astrophysics satellite just launched in February, 2016, from Tanegashima, Japan by a JAXA's H-IIA launch vehicle. It has two Soft X-ray Telescopes (SXTs), among other instruments, that were developed by the NASA Goddard Space Flight Center in collaboration with ISAS/JAXA and Nagoya University. One is for an X-ray micro-calorimeter instrument (Soft X-ray Spectrometer, SXS) and the other for an X-ray CCD camera (Soft X-ray Imager, SXI), both covering the X-ray energy band up to 15 keV. The two SXTs were fully characterized at the 30-m X-ray beam line at ISAS/JAXA. The combined SXT+SXS system effective area is about 250 and 300 cm(exp 2) at 1 and 6 keV, respectively, although observations were performed with the gate valve at the dewar entrance closed, which blocks most of low energy X-rays and some of high energy ones. The angular resolution for SXS is 1.2 arcmin (Half Power Diameter, HPD). The combined SXT+SXI system effective area is about 370 and 350 cm (exp 2) at 1 and 6 keV, respectively. The angular resolution for SXI is 1.3 arcmin (HPD). The both SXTs have a field of view of about 16 arcmin (FWHM of their vignetting functions).The SXT+SXS field of view is limited to 3 x 3 arcmin by the SXS array size. In-flight data available to the SXT team was limited at the time of this conference and a point-like source data is not available for the SXT+SXS. Although due to lack of attitude information we were unable to reconstruct a point spread function of SXT+SXI, according to RXJ1856.5-3754 data, the SXT seems to be working as expected in terms of imaging capability. As for the overall effective area response for both SXT+SXS and SXT+SXI, consistent spectral model fitting parameters with the previous measurements were obtained for Crab and G21.5-0.9 data. On the other hand, their 2-10 keV fluxes differ by about 20% at this point. Calibration work is still under progress. The SXT is the latest version of the aluminum foil X-ray mirror, which is extremely light-weight and very low cost, yet produces large effective area over a wide energy-band. Its area-mass ratio is the largest, 16 cm(exp 2)/kg, among ASTRO-H, Chandra, and XMM-Newton mirrors. The aluminum foil mirror is a still compelling technology depending on the mission science goal.

X-rays↗
NASA NTRS2016

The ASTRO-H SXT Performance to the Large Off-Set Angles

The X-ray astronomy satellite ASTRO-H, which is the 6th Japanese X-ray astronomy satellite and is renamed Hitomi after launch, is designed to observe celestial X-ray objects in a wide energy band from a few hundred eV to 600 keV. The Soft X-ray Telescopes (SXTs) onboard ASTRO-H play a role of collecting and imaging X-rays up to approximately 12 keV. Although the field of view of the SXT is approximately 15' (FWHM), due to the thin-foil-nested Wolter-I type optics adopted in the SXTs, X-rays out of the field of view can reach the focal plane without experiencing a normal double reflection. This component is referred to as 'stray light'. Owing to investigation of the stray light so far, 'secondary reflection' is now identified as the main component of the stray light, which is composed of X-rays reflected only by secondary reflectors. In order to cut the secondary reflections, a 'pre-collimator' is equipped on top of the SXTs. However, we cannot cut all the stray lights with the pre-collimator in some off-axis angle domain. In this study, we measure the brightness of the stray light of the SXTs at some representative off-axis angles by using the ISAS X-ray beam line. ASTRO-H is equipped with two modules of the SXT; one is for the Soft X-ray Spectrometer (SXS), an X-ray calorimeter, and the other is for the Soft X-ray Imager (SXI), an X-ray CCD camera. These SXT modules are called SXT-S and SXT-I, respectively. Of the two detector systems, the SXI has a large field of view, a square with 38' on a side. To cope with this, we have made a mosaic mapping of the stray light at a representative off-axis angle of 30' in the X-ray beam line at the Institute of Space and Astronautical Science. The effective area of the brightest secondary reflection is found of order approximately 0.1% of the on-axis effective area at the energy of 1.49 keV. The other components are not so bright (less than 5 x 10(exp -4) times smaller than the on-axis effective area). On the other hand, we have found that the effective area of the stray light in the SXS field of view (approximately 3' x 3') at large off-axis angles (greater than 15') are approximately 1(exp -4) times smaller than the on-axis effective area (approximately 590 sq cm at 1.49 keV).

X-rays↗
NASA NTRS2016

In-Flight Performance of the Soft X-Ray Spectrometer Detector System on ASTRO-H

The SXS instrument was launched aboard the Astro-H observatory on February 17, 2016. The SXS spectrometer is based on a high sensitivity x-ray calorimeter detector system that has been successfully deployed in many ground and sub-orbital spectrometers. The instrument was to provide essential diagnostics for nearly every class of x-ray emitting objects from the atmosphere of Jupiter to the outskirts of galaxy clusters, without degradation for spatially extended objects. The SXS detector system consisted of a 36-pixel cryogenic microcalorimeter array operated at a heat sink temperature of 50 mK. In pre-flight testing, the detector system demonstrated a resolving power of better than 1300 at 6 keV with a simultaneous band-pass from below 0.3 keV to above 12 keV with a timing precision better than 100 microsecond. In addition, a solid-state anti-coincidence detector was placed directly behind the detector array for background suppression. The detector error budget included the measured interference from the SXS cooling system and the spacecraft. Additional margin for on-orbit gain-stability, and on-orbit spacecraft interference were also included predicting an on-orbit performance that meets or exceeds the 7 eV FWHM at 6 keV requirement. The actual on-orbit spectral resolution was better than 5 eV FWHM at 6 keV, easily satisfying the instrument requirement. Here we discuss the actual on-orbit performance of the SXS detector system and compare this to performance in pre-flight testing and the on-orbit predictions. We will also discuss the on-orbit gain stability, additional on-orbit interference, and measurements of the on-orbit background.

X-ray astrophysics↗
NASA NTRS2016

Vibration Isolation System for Cryocoolers of Soft X-Ray Spectrometer (SXS) Onboard ASTRO-H (Hitomi)

Soft X-ray Spectrometer (SXS) onboard ASTRO-H (named Hitomi after launch) is a micro-calorimeter-type spectrometer, installed in a dewar to be cooled at 50 mK. The energy resolution of the SXS engineering model suffered from micro-vibration from cryocoolers mounted on the dewar. This is mitigated for the flight model by introducing vibration isolation systems between the cryocoolers and the dewar. The detector performance of the flight model was verified before launch of the spacecraft in both ambient condition and thermal-vac condition, showing no detectable degradation in energy resolution. The in-orbit performance was also consistent with that on ground, indicating that the cryocoolers were not damaged by launch environment. The design and performance of the vibration isolation system along with the mechanism of how the micro-vibration could degrade the cryogenic detector is shown.

Microcalorimeter↗
NASA NTRS2017

Design and Optimization of Multi-Pixel Transition-Edge Sensors for X-Ray Astronomy Applications

Multi-pixel transition-edge sensors (TESs), commonly referred to as 'hydras', are a type of position sensitive micro-calorimeter that enables very large format arrays to be designed without commensurate increase in the number of readout channels and associated wiring. In the hydra design, a single TES is coupled to discrete absorbers via varied thermal links. The links act as low pass thermal filters that are tuned to give a different characteristic pulse shape for x-ray photons absorbed in each of the hydra sub pixels. In this contribution we report on the experimental results from hydras consisting of up to 20 pixels per TES. We discuss the design trade-offs between energy resolution, position discrimination and number of pixels and investigate future design optimizations specifically targeted at meeting the readout technology considered for Lynx.

Smith, Stephen J.↗
NASA NTRS2017

Heat Loads Due to Small Penetrations in Multilayer Insulation Blankets

The main penetrations (supports and piping) through multilayer insulation systems for cryogenic tanks have been previously addressed by heat flow measurements. Smaller penetrations due to fasteners and attachments are now experimentally investigated. The use of small pins or plastic garment tag fasteners to each the handling and construction of multilayer insulation (MLI) blankets goes back many years. While it has long been understood that penetrations and other discontinuities degrade the performance of the MLI blanket, quantification of this degradation has generally been lumped into gross performance multipliers (often called degradation factors or scale factors). Small penetrations contribute both solid conduction and radiation heat transfer paths through the blanket. The conduction is down the stem of the structural element itself while the radiation is through the hole formed during installation of the pin or fastener. Analytical models were developed in conjunction with MLI perforation theory and Fouriers Law. Results of the analytical models are compared to experimental testing performed on a 10 layer MLI blanket with approximately 50 small plastic pins penetrating the test specimen. The pins were installed at 76-mm spacing inches in both directions to minimize the compounding of thermal effects due to localized compression or lateral heat transfer. The testing was performed using a liquid nitrogen boil-off calorimeter (Cryostat-100) with the standard boundary temperatures of 293 K and 78 K. Results show that the added radiation through the holes is much more significant than the conduction down the fastener. The results are shown to be in agreement with radiation theory for perforated films.

Structural attachments↗
NASA NTRS2016

Examining the Angular Resolution of the Astro-H's Soft X-Ray Telescopes

The international x-ray observatory ASTRO-H was renamed Hitomi after launch. It covers a wide energy range from a few hundred eV to 600 keV. It is equipped with two soft x-ray telescopes (SXTs: SXT-I and SXT-S) for imaging the soft x-ray sky up to 12 keV, which focus an image onto the respective focal-plane detectors: CCD camera (SXI) and a calorimeter (SXS). The SXTs are fabricated in a quadrant unit. The angular resolution in half-power diameter (HPD) of each quadrant of the SXTs ranges between 1.1 and 1.4 arc min at 4.51 keV. It was also found that one quadrant has an energy dependence on the HPD. We examine the angular resolution with spot scan measurements. In order to understand the cause of imaging capability deterioration and to reflect it to the future telescope development, we carried out spot scan measurements, in which we illuminate all over the aperture of each quadrant with a square beam 8 mm on a side. Based on the scan results, we made maps of image blurring and a focus position. The former and the latter reflect figure error and positioning error, respectively, of the foils that are within the incident 8 mm x 8 mm beam. As a result, we estimated those errors in a quadrant to be approx. 0.9 to 1.0 and approx. 0.6 to 0.9 arc min, respectively. We found that the larger the positioning error in a quadrant is, the larger its HPD is. The HPD map, which manifests the local image blurring, is very similar from quadrant to quadrant, but the map of the focus position is different from location to location in each telescope. It is also found that the difference in local performance causes energy dependence of the HPD.

Astro-H/Hitomi; soft x-ray telescope; SXT; Wolter ↗
NASA NTRS2016

Flow Characterization Studies of the 10-MW TP3 Arc-Jet Facility: Probe Sweeps

This paper reports computational simulations and analysis in support of calibration and flow characterization tests in a high enthalpy arc-jet facility at NASA Ames Research Center. These tests were conducted in the NASA Ames 10-MW TP3 facility using flat-faced stagnation calorimeters at six conditions corresponding to the steps of a simulated flight heating profile. Data were obtained using a conical nozzle test configuration in which the models were placed in a free jet downstream of the nozzle. Experimental surveys of arc-jet test flow with pitot pressure and heat flux probes were also performed at these arc-heater conditions, providing assessment of the flow uniformity and valuable data for the flow characterization. Two different sets of pitot pressure and heat probes were used: 9.1-mm sphere-cone probes (nose radius of 4.57 mm or 0.18 in) with null-point heat flux gages, and 15.9-mm (0.625 in) diameter hemisphere probes with Gardon gages. The probe survey data clearly show that the test flow in the TP3 facility is not uniform at most conditions (not even axisymmetric at some conditions), and the extent of non-uniformity is highly dependent on various arc-jet parameters such as arc current, mass flow rate, and the amount of cold-gas injection at the arc-heater plenum. The present analysis comprises computational fluid dynamics simulations of the nonequilibrium flowfield in the facility nozzle and test box, including the models tested. Comparisons of computations with the experimental measurements show reasonably good agreement except at the extreme low pressure conditions of the facility envelope.

Goekcen, Tahir↗
NASA NTRS2018

Combining Fractional Calorimetry with Statistical Methods to Characterize Thermal Runaway

Thermal management systems designed to handle the impacts of thermal runaway (TR) are key to safe operation of lithium-ion (Li-ion) batteries. Critical factors for optimizing these systems include the total energy released and the fraction of the total energy that is released through the cell casing versus through the ejecta material. A unique calorimeter, designed to characterize said factors, was utilized to examine the TR behavior of a variety of 18650-format Li-ion cells. Statistical methods were implemented to interpret the data.

Walker, William↗
NASA NTRS2016

Flow Characterization Studies of the 10-MW TP3 Arc-Jet Facility: Probe Sweeps

This paper reports computational simulations and analysis in support of calibration and flow characterization tests in a high enthalpy arc-jet facility at NASA Ames Research Center. These tests were conducted in the NASA Ames 10-MW TP3 facility using flat-faced stagnation calorimeters at six conditions corresponding to the steps of a simulated flight heating profile. Data were obtained using a conical nozzle test configuration in which the models were placed in a free jet downstream of the nozzle. Experimental surveys of arc-jet test flow with pitot pressure and heat flux probes were also performed at these arc-heater conditions, providing assessment of the flow uniformity and valuable data for the flow characterization. Two different sets of pitot pressure and heat probes were used: 9.1-mm sphere-cone probes (nose radius of 4.57 mm or 0.18 in) with null-point heat flux gages, and 15.9-mm (0.625 in) diameter hemisphere probes with Gardon gages. The probe survey data clearly show that the test flow in the TP3 facility is not uniform at most conditions (not even axisymmetric at some conditions), and the extent of non-uniformity is highly dependent on various arc-jet parameters such as arc current, mass flow rate, and the amount of cold-gas injection at the arc-heater plenum. The present analysis comprises computational fluid dynamics simulations of the nonequilibrium flowfield in the facility nozzle and test box, including the models tested. Comparisons of computations with the experimental measurements show reasonably good agreement except at the extreme low pressure conditions of the facility envelope.

CFD↗
NASA NTRS2018

Coupling Fractional Thermal Runaway Calorimetry (FTRC) Results with Statistical Analysis Methods

Important factors to consider when optimizing Lithium-ion (Li-ion) battery thermal management systems, from a battery safety perspective, include the total energy released during a single cell thermal runaway (TR) event and the fraction of the total energy that is released through the cell casing versus through the ejecta material. A fractional thermal runaway calorimeter (FTRC) was used to examine the TR behavior of the following 18650-format Li-ion cells: (1) Molicel 18650-J, (2) LG 18650-HG2, (3) Samsung 18650-30Q, (4) 3.35 Ah LG 18650 test cell, (5) Sony 18650-VC7, and (6) LG 18650-MJ1. These cells were intentionally selected to represent a variety of manufacturers, chemistries, capacities, and safety features. Because of the large number of random and non-random variables associated with the FTRC results, a linear regression model, developed using engineering statistical methods, was utilized to provide final interpretation of the TR behavior for each cell type and design variable combination.

Walker, William↗
NASA NTRS2015

Design and Characterization of a New Nozzle in a NASA Arc-Jet

The design of a new 76 mm (3 inch) nozzle of the Interaction Heating Facility arc jet at NASA Ames Research Center is described. The computational efforts which were an integral part of the preliminary design and characterization of the nozzle are described as well. Details of heat flux measurements made in this new nozzle are provided. Apart from showing the flow characteristics of the nozzle, predictions of stagnation point heat flux are compared against measurements made with a nullpoint calorimeter; the agreement between computation and measurement is found to be good. Unfortunately, pressure measurements could not be made in the first round. The predicted stagnation point pressures and heat fluxes, with appropriate scaling for a 25 mm (1 inch) diameter iso-q geometry (reference geometry), are used to establish a provisional operating envelope for the new nozzle. The envelope is shown to enclose relevant heating portions of representative atmospheric trajectories at Venus and Saturn.

Arcjet↗
NASA NTRS2018

Design, Implementation, and Performance of the Astro-H Soft X-Ray Spectrometer Aperture Assembly and Blocking Filters

The calorimeter array of the JAXA Astro-H (renamed Hitomi) soft x-ray spectrometer (SXS) was designed to provide unprecedented spectral resolution of spatially extended cosmic x-ray sources and of all cosmic x-ray sources in the Fe-K band around 6 keV. The properties that made the SXS array a powerful x-ray spectrometer also made it sensitive to photons from the entire electromagnetic band as well as particles. If characterized as a bolometer, it would have had a noise equivalent power of <4 × 10(exp −18) W/((Hz)(exp 0.5)). Thus, it was imperative to shield the detector from thermal radiation from the instrument and optical and UV photons from the sky. In addition, it was necessary to shield the coldest stages of the instrument from the thermal radiation emanating from the warmer stages. These needs were addressed by a series of five thin-film radiation-blocking filters, anchored to the nested temperature stages, that blocked long-wavelength radiation while minimizing x-ray attenuation. The aperture assembly was a system of barriers, baffles, filter carriers, and filter mounts that supported the filters and inhibited their potential contamination. The three outer filters also had been equipped with thermometers and heaters for decontamination. We present the requirements, design, implementation, and performance of the SXS aperture assembly and blocking filters.

Kilbourne, Caroline A.↗
NASA NTRS2019

Enhancing Battery Safety with Fractional Thermal Runaway Calorimetry

Effective thermal management systems, designed to handle the impacts of thermal runaway (TR) and to prevent cell-to-cell propagation, are key to safe operation of lithium-ion (Li-ion) battery assemblies. Critical factors for optimising these systems include the total energy released during a single cell TR event and the fraction of the total energy that is released through the cell casing versus through the ejecta material. A unique fractional thermal runaway calorimeter (FTRC), designed to characterise said critical factors, was utilised to examine the TR behaviour of Li-ion cells). Delegates will be provided with an in-depth discussion on what fractional thermal runaway calorimetry is and how it benefits the development of safe and optimised battery assemblies that protect against thermal runaway. Delegates will see calorimetry data associated with a variety of Li-ion cells. Data presented is relevant to any industry that utilises high-energy Li-ion cells in closed environments and has a need to focus on safety.

Walker, William↗
NASA NTRS2019

Metallized Plastic Current Collectors

Metallized plastic current collectors are an innovation patented by the Soteria Battery Innovation Group with the promise of isolating active material involved in an internal short by vaporizing and isolating the short from the rest of the cell electrode jellyroll or stack. Partnering with NREL, UCL, Coulometrics, and Soteria, NASA is leading a research effort into demonstrating the merits and understanding the phenomena of this safety innovation using prototype 18650 cylindrical cells vs control cells with standard metal foil current collectors. Cells with and without the plastic collector, with and without the on-demand internal short circuit device, and with polymer or cellulose separators were made. Safety evaluations were done with driving cells into thermal runaway (TR) with thermal and nail penetration triggers while inside our TR calorimeter and with ultra high speed X-ray videography provided at Synchrotrons. Preliminary results suggests that the thermally unstable plastic current collector innovation has great promise for preventing TR or reducing the severity of the TR output.

Li-ion cell↗