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Search indexed NASA NTRS and DOE OSTI research on propulsion, heat transfer, battery materials and energy systems. Follow report and document links to the original sources.

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At least 109 records · Page 6
All sourcesNASA NTRSDOE OSTI
DOE OSTI2022

Probing charge density in materials with atomic resolution in real space

The charge distribution in materials at the nanoscale can often explain the origin of macroscopic properties such as localized conductivity or the plasmonic response and illuminate more fundamental changes in the microscopic structure such as changes in chemical bonding characteristics. Previously, direct visualization of the charge density with high spatial resolution was often a missing link in the formation of structure–property relationships, especially in heterogeneous materials systems. Furthermore, recent advancements in microscopy technology have enabled researchers to visualize the charge distribution in materials down to subatomic length scales. In this Technical Review, we discuss the developments in high-resolution real-space charge distribution imaging using diffraction techniques and electron microscopy, with a focus on the recent advancement of four-dimensional scanning transmission electron microscopy, electron holography, and applications to materials interfaces.

Electronic properties and materials↗
DOE OSTI2016

Real-time monitoring of calcification process by Sporosarcina pasteurii biofilm

Sporosarcina pasteurii is known to produce calcite or biocement in the presence of urea and Ca 2+ . Herein, we report the use of novel ultramicrosensors such as pH, Ca 2+ , and redox sensors, along with a scanning electrochemical microscope (SECM), to monitor a real-time, bacteria-mediated urea hydrolysis process and subsequent changes in morphology due to CaCO 3 precipitation. We report that the surface pH of a live biofilm changed rapidly from 7.4 to 9.2 within 2 min, whereas similar fast depletion (10 min) of Ca 2+ was observed from 85 mM to 10 mM in the presence of a high urea (10 g L -1 ) brine solution at 23 °C. Both the pH and the Ca 2+ concentration profiles were extended up to 600 μm from the biofilm surface, whereas the bulk chemical composition of the brine solution remained constant over the entire 4 h of SECM experiments. In addition, we observed a change in biofilm surface morphology and an increase in overall biofilm height of 50 μm after 4 h of precipitation. Electron microscopy confirmed the changes in surface morphology and formation of CaCO 3 crystals. Development of the Ca 2+ profile took 10 min, whereas that of the pH profile took 2 min. This finding indicates that the initial urea hydrolysis process is fast and limited by urease or number of bacteria, whereas later CaCO 3 formation and growth of crystals is a slow chemical process. The ultramicrosensors and approaches employed here are capable of accurately characterizing bioremediation on temporal and spatial scales pertinent to the microbial communities and the processes they mediate.

59 BASIC BIOLOGICAL SCIENCES↗
DOE OSTI2018

Twinning and Dislocation Evolution during Shock Compression and Release of Single Crystals: Real-Time X-Ray Diffraction

Determining the temporal evolution of twinning and/or dislocation slip, in real time (nanoseconds), in single crystals subjected to plane shock wave loading is a long-standing scientific need. Non-cubic crystals pose special challenges because they have many competing slip and twinning systems. Here, we report on time-resolved, in situ, synchrotron Laue x-ray diffraction measurements during shock compression and release of magnesium single crystals that are subjected to compression along the c-axis. Significant twinning was observed directly during stress release following shock compression; during compression, only dislocation slip was observed. Our measurements unambiguously distinguish between twinning and dislocation slip on nanosecond timescales in a shocked hexagonal-close-packed metal.

36 MATERIALS SCIENCE↗
DOE OSTI2015

Real-time x-ray studies of indium island growth kinetics

The authors have investigated the early stages of indium island formation and growth by vapor phase deposition on room temperature sapphire using real-time grazing incidence small angle x-ray scattering (GISAXS), followed by ex-situ atomic force microscopy and scanning electron microscopy. The results are consistent with the formation and coalescence of hemispherical islands, as described by Family and Meakin. Monte Carlo simulations of systems of coalescing islands were used to supplement and quantify the results of GISAXS, and a good agreement is seen between the data and the simulations.

42 ENGINEERING↗
DOE OSTI2024

Get Non-Real: Randomized Sketching for High-Dimensional Non-Real Valued Data (Final Report)

In our final report for DE-C0022186, we describe the work we did on this grant towards the goals we proposed. Our first goal was characterizing fundamental limits for sketching of discrete high-dimensional matrices with low-dimensional structures. Our second main goal was designing algorithms for data reconstruction from sketches. We focus on approaches that are either specifically designed for non-real-valued data (binary, finite field) or that will translate more readily to that setting.

97 MATHEMATICS AND COMPUTING↗
DOE OSTI2019

Feasibility Analysis of Taxi Fleet Electrification Using 4.9 Million Miles of Real-World Driving Data: Preprint

Ride hailing activity is rapidly increasing, largely due to the growth of transportation network companies such as Uber and Lyft. However, traditional taxi companies continue to represent an important mobility option for travelers. Columbus Yellow Cab, a taxi company in Columbus, Ohio, offers traditional line-of-sight hailing as well as digital hailing through a mobile app. Data from Columbus Yellow Cab was provided to the National Renewable Energy Laboratory to analyze the potential for taxi electrification. Columbus Yellow Cab data contained information describing both global positioning system trajectories and taxi meter information. The data spanned a period of 13 months, containing approximately 70 million global system positioning system points, 840 thousand trips, and 170 unique vehicles. A variety of scenarios were evaluated using Columbus Yellow Cab data and the Electric Vehicle Infrastructure Projection Tool (EVI-Pro) to understand challenges and opportunities associated with operating an electrified taxi fleet. Two main factors-access to home charging and vehicle specifications-are shown to be major variables affecting successful electric fleet operation. The analysis indicates that 95.7% of taxi travel days can be successfully completed by a 250-mile-range electric vehicle assuming access to overnight and public charging infrastructure. However, when no overnight access is available to fleet vehicles, only 39.9% of taxi travel days are possible with 250-mile range electric vehicles. An additional scenario, reducing the vehicle range from 250 miles to 100 miles (while controlling for infrastructure access and permitting overnight charging) resulted in only 34.4% of taxi travel days being completed.

33 ADVANCED PROPULSION SYSTEMS↗
DOE OSTI2017

Methods for multitasking among real-time embedded compute tasks running on the GPU: Methods for Multitasking Real-time Embedded GPU Computing Tasks

Here, we provide an extensive survey on wide spectrum of scheduling methods for multitasking among graphics processing unit (GPU) computing tasks. We then design several schedulers and explain in detail the selected methods we have developed to implement our scheduling strategies. Next, we compare the performance of schedulers on various workloads running on Fermi and Kepler architectures and arrive at the following major conclusions: (1) Small kernels benefit from running kernels concurrently. (2) The combination of small kernels, high-priority kernels with longer runtimes, and lower-priority kernels with shorter runtimes benefits from a CPU scheduler that dynamically changes kernel order on the Fermi architecture. (3) Because of limitations of existing GPU architectures, currently CPU schedulers outperform their GPU counterparts. We also provide results and observations obtained from implementing and evaluating our schedulers on the NVIDIA Jetson TX1 system-on-chip architecture. We observe that although TX1 has the newer Maxwell architecture, the mechanism used for scheduler timings behaves differently on TX1 compared to Kepler leading to incorrect timings. In this paper, we describe our methods that allow us to report correct timings for CPU schedulers running on TX1. Lastly, we propose new research directions involving the investigation of additional scheduling strategies.

97 MATHEMATICS AND COMPUTING↗
DOE OSTI2016

In situ growth, structure, and real-time chemical reactivity of well-defined CeO x -Ru(0001) model surfaces

Ceria is an important material for chemical conversion processes in catalysis. Its intrinsic properties as a reducible oxide can be exploited to achieve catalytic selectivity and activity. However, numerous phenomenological characteristics of ceria remain unknown and its active nature is ever slowly being unraveled. Well defined models of ceria (111) are an important way to systematically study these properties and take advantage of new in situ methods that require pristine materials that allow for the interrogation of the most fundamental traits of this material. The ceria-Ru(0001) model is now the most well studied model surface with numerous aspects of its preparation, atomic structure and reactivity studied by several groups. The preparation of CeO x structures oriented with a (111) surface termination can be achieved through molecular beam deposition, facilitating the growth of well-defined nanostructures, microparticles, and films on the Ru(0001) surface. The growth mechanism exploits the epitaxial relationship between CeOx and Ru to form a carpet mode of well oriented layers of Osingle bondCesingle bondO. These models can be studied to unravel the atomic structure and the oxidation state (Ce 4+ and Ce 3+ ), as prepared and under redox conditions (reduction/oxidation) or with reaction using reactants (e.g., H 2 , methanol). Here, we present a discussion of these most recent observations pertaining to the growth mode, arrangement of atoms on the surface, characteristic chemical state, and redox chemistry of the CeO x -Ru surface. As a result, with insights from these studies we propose new strategies to further unravel the chemistry of ceria.

37 INORGANIC, ORGANIC, PHYSICAL, AND ANALYTICAL CH↗