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At least 109 records · Page 6

Prolonged 500 C Operation of 100+ Transistor Silicon Carbide Integrated Circuits

This report describes more than 5000 hours of successful 500 C operation of semiconductor integrated circuits (ICs) with more than 100 transistors. Multiple packaged chips with two different 4H-SiC junction field effect transistor (JFET) technology demonstrator circuits have surpassed thousands of hours of oven-testing at 500 C. After 100 hours of 500 C burn-in, the circuits (except for 2 failures) exhibit less than 10% change in output characteristics for the remainder of 500 C testing. We also describe the observation of important differences in IC materials durability when subjected to the first nine constituents of Venus-surface atmosphere at 9.4 MPa and 460 C in comparison to what is observed for Earth-atmosphere oven testing at 500 C.

Spry, David J.↗

Lunar Advanced Volatile Analysis Integration and Testing

The Regolith and Environment Science Oxygen and Lunar Volatile Extraction (RESOLVE) payload is part of Resource Prospector (RP) along with a rover and a lander that are expected to launch in 2020. RP will identify volatile elements that may be combined and collected to be used for fuel, air, and water in order to enable deeper space exploration. The Resource Prospector mission is a key part of In-Situ Resource Utilization (ISRU). The demand for this method of utilizing resources at the site of exploration is increasing due to the cost of resupply missions and deep space exploration goals. The RESOLVE payload includes the Lunar Advanced Volatile Analysis (LAVA) subsystem. The main instrument used to identify the volatiles evolved from the lunar regolith is the Gas Chromatograph-Mass Spectrometer (GC-MS). LAVA analyzes the volatiles emitted from the Oxygen and Volatile Extraction Node (OVEN) Subsystem. The objective of OVEN is to obtain, weigh, heat and transfer evolved gases to LAVA through the connection between the two subsystems called the LOVEN line. This paper highlights the work completed during a ten week internship that involved the integration, testing, data analysis, and procedure documentation of two candidate mass spectrometers for the LAVA subsystem in order to aid in determining which model to use for flight. Additionally, the examination of data from the integrated Resource Prospector '15 (RP' 15) field test will be presented in order to characterize the amount of water detected from water doped regolith samples.

In-Situ Resource Utilization↗

Sulfur-bearing Phases Detected by Evolved Gas Analysis of the Rocknest Aeolian Deposit, Gale Crater, Mars

The Sample Analysis at Mars (SAM) instrument suite detected SO2, H2S, OCS, and CS2 from ~450 to 800degC during evolved gas analysis (EGA) of materials from the Rocknest aeolian deposit in Gale Crater, Mars. This was the first detection of evolved sulfur species from a Martian surface sample during in situ EGA. SO2 (~3-22 μmol) is consistent with the thermal decomposition of Fe sulfates or Ca sulfites, or evolution/desorption from sulfur-bearing amorphous phases. Reactions between reduced sulfur phases such as sulfides and evolved O2 or H2O in the SAM oven are another candidate SO2 source. H2S (~41-109 nmol) is consistent with interactions of H2O, H2 and/or HCl with reduced sulfur phases and/or SO2 in the SAM oven. OCS (~1-5nmol) and CS2 (~0.2-1 nmol) are likely derived from reactions between carbon-bearing compounds and reduced sulfur. Sulfates and sulfites indicate some aqueous interactions, although not necessarily at the Rocknest site; Fe sulfates imply interaction with acid solutions whereas Ca sulfites can form from acidic to near-neutral solutions. Sulfides in the Rocknest materials suggest input from materials originally deposited in a reducing environment or from detrital sulfides from an igneous source. The presence of sulfides also suggests that the materials have not been extensively altered by oxidative aqueous weathering. The possibility of both reduced and oxidized sulfur compounds in the deposit indicates a nonequilibrium assemblage. Understanding the sulfur mineralogy in Rocknest materials, which exhibit chemical similarities to basaltic fines analyzed elsewhere on Mars, can provide insight in to the origin and alteration history of Martian surface materials.

Gale Crater↗

The 2008 Mars Phoenix Lander Thermal and Evolved Gas Analyzer (TEGA) Dataset: Placing Easily Interpretable Evolved Gas Data on the Planetary Data System (PDS)

The Phoenix Scout Lander mission investigated the north polar region of Mars in 2008 with the goal to study the history of water, assess the past/present Martian climate, search for organics, and evaluate the potential for past/present microbial habit-ability on Mars. To accomplish this goal, the Phoenix Lander’s Thermal and Evolved-Gas Analyzer (TEGA) instrument assessed the gas composition of the Martian atmosphere and evaluated the mineralogy of the Martian regolith. The TEGA instrument consisted of eight small ovens connected to a 4 channel magnetic sector mass spectrometer. The ovens heated soil samples from ambient to 1000°C where the gases (e.g., H2O, CO2, etc.) evolved from thermal decomposition of mineral phases were analyzed by the mass spectrometer. Minerals thermally decomposed at characteristic temperatures and the evolving gases indicated the presence of perchlorate, carbonate, and hydrated phases in the Phoenix landing site soils.

Garcia, A. H.↗

Percentage of Water Retained in Icy Lunar Regolith Simulant During Transfer into a Sample Container

We now know that water ice exists on the lunar surface thanks to the findings of multiple lunar missions such as LRO and LCROSS. However, before we develop systems that can utilize this precious resource at a useful scale, we need to acquire more data about the concentration of water in the lunar regolith and how it may vary by depth and location. The OVEN (Optimized Volatile Extraction Node) system is designed to determine the concentration of water as part of an instrument called WAVE (Water Analysis & Volatile Extraction) which can be deployed during a lunar resource prospecting mission. Experiments were carried out at the Johnson Space Center in order to better understand the potential losses of water that may occur during a prospecting mission when a sample is transferred from a drill to the OVEN. A description of the experiment as well as the results will be presented here.

ISRU↗

Experimental Study on Mitigation of Lifetime-Limiting Dielectric Cracking in Extreme Temperature 4H-SiC JFET Integrated Circuits

While NASA Glenn Research Center's "Generation 10" 4H-SiC Junction Field Effect Transistor (JFET) integrated circuits (ICs) have uniquely demonstrated 500 °C electrical operation for durations of over a year, this experimental work has also revealed that physical cracking of chip dielectric passivation layers ultimately limits extreme-environment operating lifetime [1-3]. The prevention of such dielectric passivation cracks should therefore improve IC high temperature durability and yield, leading to more beneficial technology adoption into aerospace, automotive, and energy systems. This report describes Generation 10.2, 11.1, and 11.2 die tested under unbiased and unpackaged accelerated age testing at 500 °C, 600 °C, 720 °C, and 800 °C in air-atmosphere ovens for 100- and 200-hour duration. Additional samples were separately subjected to 10 thermal cycles between the same high temperatures (with 10-hour high-temperature soak each cycle) and 50 °C. It is shown that having two stoichiometric Si3N4 layers in the interconnect dielectric stack substantially decreases the amount of dielectric cracking observed following these oven tests.

Spry, D. J.↗

Design of an Automated Ultrasonic Scanning System for In-Situ Composite Cure Monitoring and Defect Detection

The preliminary design and development of an automated ultrasonic scanning system for in-situ composite cure monitoring and defect detection in the high temperature environment of an oven was completed. This preliminary design is a stepping stone to deployment in the high temperature and high pressure environment of an autoclave, the primary cure method of aerospace grade thermoset composites. Cure monitoring with real-time defect detection during the process could determine when defects form and how they move. In addition, real-time defect detection during cure could assist validating physics-based process models for predicting defects at all stages of the cure cycle. A physics-based process model for predicting porosity and fiber waviness originating during cure is currently under development by the NASA Advanced Composites Project (ACP). For the design, an ultrasonic contact scanner is enclosed in an insulating box that is placed inside an oven during cure. Throughout the cure cycle, the box is nitrogen-cooled to approximately room temperature to maintain a standard operating environment for the scanner. The composite part is mounted on the outside of the box in a vacuum bag on the build/tool plate. The build plate is attached to the bottom surface of the box. The scanner inspects the composite panel through the build plate, tracking the movement of defects introduced during layup and searching for new defects that may form during cure. The focus of this paper is the evaluation and selection of the build plate material and thickness. The selection was based on the required operating temperature of the scanner, the cure temperature of the composite material, thermal conductivity models of the candidate build plates, and a series of ultrasonic attenuation tests. This analysis led to the determination that a 63.5 mm thick build plate of borosilicate glass would be utilized for the system. The borosilicate glass plate was selected as the build plate material due to the low ultrasonic attenuation it demonstrated, its ability to efficiently insulate the scanner while supporting an elevated temperature on the part side of the plate, and the availability of a 63.5 mm thick plate without the need for lamination.

Hudson, Tyler B.↗

Bubble Distribution in Fused Obsidian and Slide Glass: Research Report - 12

In this report we obtain further data about the distri­bution of bubbles in glass. It gives the results obtained from the microscopic study of obsidian samples heated with an oxyacetylene torch and from powdered microscopic slide glass re-fused in an electric oven. This report continues our earlier study of the distributions: Badri Aghassi, 1961, B.U. Tektite Project, Research Report No. 11.

Aghassi, Badri↗

Refractory metal shielding /insulation/ increases operating range of induction furnace

Thermal radiation shield contains escaping heat from an induction furnace. The shield consists of a sheet of refractory metal foil and a loosely packed mat of refractory metal fibers in a concentric pattern. This shielding technique can be used for high temperature ovens, high temperature fluid lines, and chemical reaction vessels.

Ebihara, B. T.↗

Assembly jig assures reliable solar cell modules

Assembly jig holds the components for a solar cell module in place as the assembly is soldered and bonded by the even heat of an oven. The jig is designed to the configuration of the planned module. It eliminates uneven thermal conditions caused by hand soldering methods.

Ofarrell, H. O.↗

Adjustable thermal ''tree''

Tree mounts 10 thermocouples on extensible arms to provide a reliable heat profile of conditions within heat treating devices, such as ovens and autoclaves, and within environmental test chambers.

Appel, B. H.↗

A traverse gravimeter for the lunar surface

A semi-automatic, self-levelling lunar gravimeter was designed for the purpose of measuring gravity at predetermined stops along the route of a lunar rover vehicle to obtain a gravity profile. The traverse gravimeter is completely self-contained and is powered by an internal battery. The gravity sensor is a vibrating string accelerometer (VSA) which is enclosed in a precision oven. Gravity data are obtained by initiating a measurement. After the gravimeter has levelled, the VSA difference frequency is counted down and a gate is generated to enable a crystal-controlled clock to a BCD counter. The BCD counter stores the data which are a measurement of gravity. These data, displayed upon command by the astronaut, are transmitted by voice back to earth. It is expected that the accuracy of the gravimeter will be better than one milligal. Low power, light weight, reliability, and simplicity of operation are major considerations in the design of the gravimeter.

Mamon, G.↗

Development of self extinguishing Durette and/or Nomex fabric

A treatment was developed for Nomex or Durette fabric which renders it self-extinguishing in a 70% oxygen, 30% nitrogen atmosphere at 5 psia. The treatment does not degrade the physical and textile properties of the fabric excessively and does not outgas or have an objectional odor. The treatment is permanent and does not lose its fire protecting qualities after laundering. The treatment utilizes a mixture of formaldehyde, phosphorous acid, and tri-methyl phosphate in methanol. The cloth to be treated is held in a boiling solution of the above reagents for 24 hours, removed, air dried, and then heated to 120 C in a circulating air oven for 90 minutes. The treatment turns Nomex a pale yellow but does not have an appreciable effect on drape or hand. One inch wide strips of treated cloth failed in tension at 192 lbs, while untreated controls broke at 215 lbs. To remove any excess reagents, the cloth is processed in a home laundry through one wash and dry cycle without the use of any detergents. The thermal shrinkage of the treated material is 23% compared to a control of 40% for unwashed Stern Nomex HT 90-40.

Source record↗

In situ analysis of planetary surfaces for organic materials.

Discussion of the possibility of investigating the physical, chemical, and biological state of other planets in the hope of encountering one or more that is presently in a state prior to or just after the evolution of living systems. It may then be possible to observe the chemistry at and near the surface, evaluate the sources of energy available, and search for the presence or absence of living systems, and their degree of similarity to terrestrial ones. The mass spectrometry technique is considered to be the most appropriate. A system consisting of a series of sample ovens which can be consecutively attached to the gas stream of a small gas chromatograph which is in turn connected to a mass spectrometer via a carrier gas separator has been developed for the exploration of the surface of Mars.

Biemann, K.↗