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NASA NTRS2005

A Shape Memory Alloy Based Cryogenic Thermal Conduction Switch

Shape memory alloys (SMAs) can produce large strains when deformed (e.g., up to 8%). Heating results in a phase transformation and associated recovery of all the accumulated strain. This strain recovery can occur against large forces, resulting in their use as actuators. Thus an SMA element can integrate both sensory and actuation functions, by inherently sensing a change in temperature and actuating by undergoing a shape change as a result of a temperature-induced phase transformation. Two aspects of our work on cryogenic SMAs are addressed here. First - a shape memory alloy based cryogenic thermal conduction switch for operation between dewars of liquid methane and liquid oxygen in a common bulkhead arrangement is discussed. Such a switch integrates the sensor element and the actuator element and can be used to create a variable thermal sink to other cryogenic tanks for liquefaction, densification, and zero boil-off systems for advanced spaceport applications. Second - fabrication via arc-melting and subsequent materials testing of SMAs with cryogenic transformation temperatures for use in the aforementioned switch is discussed.

Notardonato, W. U.↗

NASA NTRS1982

Large Prandtl number finite-amplitude thermal convection with Maxwell viscoelasticity

It has long been known that the earth behaves viscoelastically. Viscoelasticity may be of importance in two aspects of mantle convection, including time-dependent behavior and local storage of recoverable work. The present investigation makes use of thermal convection in a box as a prototype of mantle flow. It is demonstrated that recoverable work can be important to the local mechanical energy balance in the descending lithosphere. It is shown that, even when assuming large viscoelastic parameters, an inherent time-dependence of viscoelastic convection appears only in local exchanges of mechanical energy. There is no strong exchange between buoyant potential energy and recoverable strain energy in the Rayleigh number range investigated. The investigation is mainly concerned with viscoelastic effects occurring on a buoyant time scale. It is found that viscoelastic effects have a negligible influence on the long term thermal energetics of mantle convection.

Ivins, E. R.↗

NASA NTRS1984

Elevated temperature compressive steady state deformation and failure in the oxide dispersion strengthened alloy MA 6000E

The compressive flow strength-strain rate behavior of the oxide-dispersion-strengthened alloy MA 6000E has been studied in the temperature range 1144-1366 K, with strain rates ranging from 2.1 x 10 to the -5th to 2.1 x 10 to the -7th per s. It is found that the inherent strength of the alloy is essentially the same in all test directions and that the low strength observed in tensile tests results from the inability of grain boundaries to support high tensile stresses. The failure of MA 6000E under high-temperature, slow plastic flow conditions is shown to be the result of concentrated slip. Slow plastic deformation in MA 6000E can be described by a threshold stress model of creep where threshold stresses are calculated from relatively fast testing procedures and the effective stress exponent for creep is assumed to be 3.5.

Whittenberger, J. D.↗

NASA NTRS1989

Novel applications of optical techniques to the study of buried semiconductor interfaces

Detailed electronic and structural information about buried semiconductor interfaces obtained through application of optical techniques is discussed. The measurements described include the determination of band discontinuities, strain, and disorder associated with semiconductor heterointerfaces. The contactless and nondestructive nature of these optical techniques is particularly important for the study of heterointerfaces which are inherently inaccessible to direct electrical or physical contact.

Wilson, Barbara A.↗

DOE OSTI2022

In-situ synchrotron X-ray diffraction investigation on deformation behavior of Nb/NiTi composite during pre-straining process

The mechanisms responsible for deformation behavior in Nb/NiTi composite during pre-straining were investigated systematically using in-situ synchrotron X-ray diffraction, transmission electron microscopy and tensile test. It is shown that upon loading, the composite experiences elastic elongation and slight plastic deformation of B19', B2 and β-Nb phases, together with the forward stress-induced martensitic (SIM) transformation from B2 to B19'. Upon unloading, the deformation mechanisms of the composite mainly involve elastic recovery of B19', B2 and β-Nb phases, compression deformation of β-Nb phase and incomplete B19'→B2 reverse SIM transformation. In the tensile loading-unloading procedure, besides the inherent elastic deformation and SIM transformation, the (001) compound twins in B19' martensite can also be conducive to the elastic deformation occurring in B19'-phase of the composite. Therefore, this composite can exhibit a large recoverable strain after unloading owing to the elastic deformation, and the partially reversible and consecutive SIM transformation together with the (001) compound twins.

36 MATERIALS SCIENCE↗

NASA NTRS1987

Strain energy release rates of composite interlaminar end-notch and mixed-mode fracture: A sublaminate/ply level analysis and a computer code

A computer code is presented for the sublaminate/ply level analysis of composite structures. This code is useful for obtaining stresses in regions affected by delaminations, transverse cracks, and discontinuities related to inherent fabrication anomalies, geometric configurations, and loading conditions. Particular attention is focussed on those layers or groups of layers (sublaminates) which are immediately affected by the inherent flaws. These layers are analyzed as homogeneous bodies in equilibrium and in isolation from the rest of the laminate. The theoretical model used to analyze the individual layers allows the relevant stresses and displacements near discontinuities to be represented in the form of pure exponential-decay-type functions which are selected to eliminate the exponential-precision-related difficulties in sublaminate/ply level analysis. Thus, sublaminate analysis can be conducted without any restriction on the maximum number of layers, delaminations, transverse cracks, or other types of discontinuities. In conjunction with the strain energy release rate (SERR) concept and composite micromechanics, this computational procedure is used to model select cases of end-notch and mixed-mode fracture specimens. The computed stresses are in good agreement with those from a three-dimensional finite element analysis. Also, SERRs compare well with limited available experimental data.

Valisetty, R. R.↗

NASA NTRS1995

Mechanical Properties of Aerogels

Aerogels are extremely low density solids that are characterized by a high porosity and pore sizes on the order of nanometers. Their low thermal conductivity and sometimes transparent appearance make them desirable for applications such as insulation in cryogenic vessels and between double paned glass in solar architecture. An understanding of the mechanical properties of aerogels is necessary before aerogels can be used in load bearing applications. In the present study, the mechanical behavior of various types of fiber-reinforced silica aerogels was investigated with hardness, compression, tension and shear tests. Particular attention was paid to the effects of processing parameters, testing conditions, storage environment, and age on the aerogels' mechanical response. The results indicate that the addition of fibers to the aerogel matrix generally resulted in softer, weaker materials with smaller elastic moduli. Furthermore, the testing environment significantly affected compression results. Tests in ethanol show an appreciable amount of scatter, and are not consistent with results for tests in air. In fact, the compression specimens appeared to crack and begin to dissolve upon exposure to the ethanol solution. This is consistent with the inherent hydrophobic nature of these aerogels. In addition, the aging process affected the aerogels' mechanical behavior by increasing their compressive strength and elastic moduli while decreasing their strain at fracture. However, desiccation of the specimens did not appreciably affect the mechanical properties, even though it reduced the aerogel density by removing trapped moisture. Finally, tension and shear test results indicate that the shear strength of the aerogels exceeds the tensile strength. This is consistent with the response of brittle materials. Future work should concentrate on mechanical testing at cryogenic temperatures, and should involve more extensive tensile tests. Moreover, before the mechanical response of reinforced aerogels can be fully understood, more tests of unreinforced aerogels are necessary. Unreinforced aerogels are of particular use because their birefringent nature allows for visual determination of stress fields during mechanical testing. The success of any future tests depends on the availability of a large supply of quality specimens with well-documented preparation and storage histories.

Parmenter, Kelly E.↗

NASA NTRS2001

Finite Element Analysis of Active and Sensory Thermopiezoelectric Composite Materials

Analytical formulations are developed to account for the coupled mechanical, electrical, and thermal response of piezoelectric composite materials. The coupled response is captured at the material level through the thermopiezoelectric constitutive equations and leads to the inherent capability to model both the sensory and active responses of piezoelectric materials. A layerwise laminate theory is incorporated to provide more accurate analysis of the displacements, strains, stresses, electric fields, and thermal fields through-the-thickness. Thermal effects which arise from coefficient of thermal expansion mismatch, pyroelectric effects, and temperature dependent material properties are explicitly accounted for in the formulation. Corresponding finite element formulations are developed for piezoelectric beam, plate, and shell elements to provide a more generalized capability for the analysis of arbitrary piezoelectric composite structures. The accuracy of the current formulation is verified with comparisons from published experimental data and other analytical models. Additional numerical studies are also conducted to demonstrate additional capabilities of the formulation to represent the sensory and active behaviors. A future plan of experimental studies is provided to characterize the high temperature dynamic response of piezoelectric composite materials.

Lee, Ho-Jun↗

NASA NTRS2004

Linear and Nonlinear Analyses of a Wind-Tunnel Balance

The NASA Langley Research Center (LaRC) has been designing strain-gauge balances for utilization in wind tunnels since its inception. The utilization of balances span a wide variety of aerodynamic tests. A force balance is an inherently critically stressed component due to the requirements of measurement sensitivity. Force balance stress analysis and acceptance criteria are under review due to LaRC wind tunnel operational safety requirements. This paper presents some of the analyses done at NASA LaRC. Research and analyses were performed in order to investigate the structural integrity of the balances and better understand their performance. The analyses presented in this paper are helpful in understanding the overall behavior of an existing balance and can also be used in design of new balances to enhance their performance. As a first step, maximum load combination is used for linear structural analysis. When nonlinear effects are encountered, the analysis is extended to include the nonlinearities. Balance 1621 is typical for LaRC designed balances and was chosen for this study due to its traditional high load capacity, Figure 1. Maximum loading occurs when all 6 components are applied simultaneously with their maximum value allowed (limit load). This circumstance normally will not occur in the wind tunnel. However, if it occurs, is the balance capable of handling the loads with an acceptable factor of safety? Preliminary analysis using Pro/Mechanica indicated that this balance might experience nonlinearity. It was decided to analyze this balance by using NASTRAN so that a nonlinear analysis could be conducted. Balance 1621 was modeled and meshed in PATRAN for analysis in NASTRAN. The model from PATRAN/NASTRAN is compared to the one from Pro/Mechanica. For a complete analysis, it is necessary to consider all the load cases as well as use a dense mesh near all the edges. Because of computer limitations, it is not feasible to analyze model with the dense mesh near all edges. In the present study, the dense mesh is limited to the surface on the end of the axial sections.

Karkehabadi, R.↗

NASA NTRS2020

Controlled Environmental Effects on Creep Test Data of Woven Fabric Webbings for Inflatable Space Modules

eveloping technologies for proposed lunar and Mars space exploration missions. Enhanced habitation sy g studied as potential habitats due to their inherent low mass and small launch volume. One goal of inflatable module research is quantification of the safe-life and end-of-life creep-strain spectrum. Full-scale pressurized inflatable modules are large, costly, and difficult to experimentally study. Therefore, material subcomponents are often studied as an alternative. An experimental thermally controlled long-term creep study of VectranTM webbings for application to inflatable modules is presented. Vectran fibers have high strength and low creep properties. High strength webbing materials are desirable for the load bearing restraint layer of inflatable modules because they are strong, flexible, and lightweight. Characterization of the creep behavior, safe-life, and end-of- life of webbing specimens will help quantify comparable life properties for inflatable modules. Several experimental multiple-year creep studies of webbing specimens in uncontrolled thermal environments have been conducted at NASA Langley Research Center. Experimental data obtained exhibits the classic creep-strain curve due to load, coupled with unique sinusoidal variation due to variation in temperature and humidity over daily and annual time periods. Results also have indicated that specimens fail within a year if the applied load is greater than 50 percent of the rated load. The primary goal of this study is to eliminate thermal effects from the creep data for a group of webbing specimens, and to allow uncontrolled thermal effects to influence the creep data of a second group of webbing specimens. Comparison of both sets of data will define how temperature influences creep data. A unique creep test facility was fabricated to facilitate the generation and comparison of the two sets of data. The facility consists of five creep test stands with an integrated heating and cooling system, and four creep test stands exposed to external environmental or ambient conditions. The facility contains displacement, temperature, humidity, and load sensors. Test specimens consist of one- inch wide, 48-inch long Vectran webbings rated at 12,500 pounds-per-inch. Experimental thermally controlled creep-strain data has been generated for two groups of webbing specimens. Applied load for all test stands was above 9000 lbs and greater than 50 percent of the rated load. Temperatures varied between 58˚F and 83˚F for the four test stands exposed to ambient conditions. Associated creep data exhibited the classic creep- strain profiles. The temperature was set to 72˚F for the five test stands in the controlled temperature environment. Creep data for tests with temperature control also exhibited the classic strain profiles. Data indicated that if the load is greater n thermal effects do not manifest. Therefore, creep tests with loads less than 50 percent of the rated load are planned for in the near future.

Kenner, Winfred S.↗

DOE OSTI2021

Elevated temperature ductility dip in an additively manufactured Al-Cu-Ce alloy

The deformation and failure mechanisms of Al-9Cu-6Ce (wt%) based alloys fabricated with laser powder bed fusion were investigated from room temperature to 400°C. The yield and ultimate tensile strengths decreased monotonically with increase in temperature, but the tensile elongation dipped unexpectedly at elevated temperatures and exhibited a minimum at 300°C. The dip in tensile elongation occurred with a concomitant dip in strain-rate sensitivity (SRS) of deformation. The as-fabricated alloy microstructure was heterogeneous, and the heat affected zone (HAZ) underneath the melt pool boundary was prone to strain localization. At 300 °C, the reduced SRS promoted the progression of strain localization in the HAZ leading to failure initiation and the dip in tensile elongation. Furthermore, a higher SRS or strain-hardening rate at other temperatures improved the tensile elongation by slowing the progression of strain localization in the HAZ such that failure initiated by other mechanisms elsewhere in the microstructure. Notably, the tensile elongation was limited by the defect structure only in a narrow temperature range (150 - 200 °C) while at other temperatures it was limited by the inherent microstructural features. This investigation exemplifies unexpected deformation and failure mechanisms possible in heterogeneous microstructures that result from additive manufacturing.

36 MATERIALS SCIENCE↗

NASA NTRS1977

Applications of laser speckles in a holographic nondestructive test system

The grainy or speckle phenomenon of laser light is caused by two inherent characteristics of the laser - the coherence and monochromaticity of the radiation. Recent development have shown that this phenomenon can be used to measure minute surface displacements, surface strains, or vibrations of a body. The present paper deals with two techniques employing the speckle effect. One is called speckle beam holographic interferometry, and the other speckle photographic interferometry. A major advantage of the first technique is the elimination of the stringent vibration isolation requirement in existing holographic nondestructive test systems. The advantage of the second technique is that the resulting photographic data are sensitive only to the in-plane components of the surface variations. The basic principles and practical limitations of these techniques are discussed.

Liu, H.-K.↗

NASA NTRS1990

Load biaxiality and fracture - Synthesis and summary

The question of load biaxiality strongly affecting almost all of the characteristics of brittle fracture behavior of a cracked body is investigated. Results of research published piecemeal over the years by the authors have shown that the stress and displacement fields, the elastic strain energy density, and the maximum shear stress near the crack tip are all altered by loads applied parallel to the crack, as are the angle of initial crack extension, the strain energy of the entire body, the fracture load, and the rate of fatigue crack growth. A synthesis and summary of this research is presented showing the shortcomings inherent in both Griffith's global energy rate theory for crack instability and Irwin's local crack-tip stress intensity theory for fracture toughness. In both theories only the tensile load perpendicular to the crack influences fracture behavior of the body.

Eftis, J.↗

NASA NTRS1995

Current loop signal conditioning: Practical applications

This paper describes a variety of practical application circuits based on the current loop signal conditioning paradigm. Equations defining the circuit response are also provided. The constant current loop is a fundamental signal conditioning circuit concept that can be implemented in a variety of configurations for resistance-based transducers, such as strain gages and resistance temperature detectors. The circuit features signal conditioning outputs which are unaffected by extremely large variations in lead wire resistance, direct current frequency response, and inherent linearity with respect to resistance change. Sensitivity of this circuit is double that of a Wheatstone bridge circuit. Electrical output is zero for resistance change equals zero. The same excitation and output sense wires can serve multiple transducers. More application arrangements are possible with constant current loop signal conditioning than with the Wheatstone bridge.

Anderson, Karl F.↗

NASA NTRS2004

Structural Integrity of a Wind Tunnel Balance

The National Aeronautics and Space Administration (NASA) Langley Research Center (LaRC) has been designing strain-gage balances for utilization in wind tunnels since its inception. The utilization of balances span over a wide variety of aerodynamic tests. A force balance is an inherently critically stressed component due to the requirements of measurement sensitivity. Research and analyses are done in order to investigate the structural integrity of the balances as well as developing an understanding of their performance in order to enhance their capability. Maximum loading occurs when all 6 components of the loads are applied simultaneously with their maximum value allowed (limit load). This circumstance normally does not occur in the wind tunnel. However, if it occurs, is the balance capable of handling the loads with an acceptable factor of safety? LaRC Balance 1621 was modeled and meshed in PATRAN for analysis in NASTRAN. For a complete analysis, it is necessary to consider all the load cases as well as use dense mesh near all the edges. Because of computer limitations, it is not possible to have one model with the dense mesh near all edges. In the present study, a dense mesh is limited to the surface corners where the cage and axial sections meet. Four different load combinations are used for the current analysis. Linear analysis is performed for each load case. In the case where the stress value is above linear elastic region, it is necessary to perform nonlinear analysis. It is also important to investigate the variables limiting the structural integrity of the balances. In order to investigate the possibility of modifying the existing balances to enhance the structural integrity, some modifications are done on this balance. The structural integrity of the balance after modification is investigated.

Karkehabadi, R.↗

DOE OSTI2024

Factors Affecting the Electron Conductivity in Single Crystal Li 7 La 3 Zr 2 O 12 and Li 7 P 3 S 11

One of the serious challenges in all solid-state Li ion batteries is neutral Li intrusion into the solid-state electrolyte that can ultimately cause catastrophic failure. One possibility for this is due to n-type electron conductivity that induces the reaction Li + + e – → Li 0 at sites where the potential is less than the Li + /Li potential. This paper reports hybrid density functional theory calculations of the electronic conductivity in two prototype single crystalline solid-state electrolytes, cubic Li 7 La 3 Zr 2 O 12 (c-LLZO) and Li 7 P 3 S 11 (LPS). The formation energies of important point defects that can affect electron conductivity are determined, and we find that the mechanism of n-type electron conductivity for both solid-state electrolytes is via “small” electron polaron hopping, where the quotes signify that substantial Li ion rearrangement is associated with the polaron formation and its migration. In both electrolytes, the formation energies for the small polarons at the Fermi energy are too high to generate measurable electron conductivity at room temperature. For c-LLZO, the concentration of electron polarons necessary to ensure charge neutrality from positively charged oxygen vacancies formed in synthesis can be significantly higher. Hence, the electron conductivity could be significant when measured with ion-blocking metal electrodes, and we discuss how the synthesis conditions could affect this magnitude. However, in the solid-state battery, these polarons are replaced by negatively charged Li vacancies so that the electron conductivity should remain minimal. For LPS single crystals, the inherent minimal electron conductivity is independent of synthesis conditions. Here we also show that the cost of forming Li 0 in bulk c-LLZO is enormous due to strain effects so that it could only potentially form at voids, grain boundaries, or around vacancy defects which relax the lattice strain.

37 INORGANIC, ORGANIC, PHYSICAL, AND ANALYTICAL CH↗

NASA NTRS1985

Utilization of Mobile VLBI for Geodetic Measurements

Three mobile very long base interferometry (VLBI) systems were fabricated for the NASA Crustal Dynamics Project. These systems include the 9-meter-diameter MV-3 telescope. Since 1980, mobile systems operated in conjunction with several fixed base stations in the western United States as part of a geodetic survey program to determine relative motions and regional strain fields near the tectonic plate boundaries in California and Alaska. A description is given of the three mobile systems and the environment in which they must function. The inherent accuracy of mobile VLBI measurements is assessed, based on a consideration of major sources of error. Some recent results are presented which serve to illustrate various aspects of the error model and are of geodetic interest as they span the broad region surrounding the surface trace of the San Andreas Fault. These results indicate that baseline measurements utilizing the current mobile VLBI systems attained an accuracy of 2 cm or better in the horizontal plane. It is likely that crustal motions will be detected within the next few years, provided they are presently occurring at the geological rates.

Davidson, J. M.↗

NASA NTRS1985

Utilization of mobile VLBI for geodetic measurements

Davidson, J. M.↗