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NASA NTRS1988

Mars orbital tethered sample return: The feasibility and uses of obtaining entrained particulates from the atmosphere

By employing technology developed for the Tethered Satellite Program, it appears feasible to obtain Martian dust samples from the atmosphere using an orbiting spacecraft. If collected during an annual dust storm, such a sample would contain a global selection of windborne materials. Atmospheric dust sampling is of importance to the study of Martian surface geochemistry, soil mechanics, atmospheric dynamics, and atmospheric and radiative transfer. Tethered sample return offers two key advantages over a lander sample return: relative simplicity and low spacecraft weight. In another vein, the collection of atmospheric dust by a lander sample return mission is itself of scientific merit. By employing a mast and collection plate aboard a lander mission, it is possible to obtain dust from distant locations transported as entrained material in the local aeolian environment.

Stern, S. A.↗

NASA NTRS1992

Spacecraft thermal control coatings

The Experiment AO 138-6 was located on the trailing edge of the Long Duration Exposure Facility as part of the French Cooperative Payload (FRECOPA) Experiment. It was purely passive in nature: material specimens 2 x 2 cm, independently mounted in sample-holders, with their surface in the same reference plane, were exposed to space. Thirty samples were set in a vacuum-tight canister which was opened in space a few days after LDEF deployment and closed while still in orbit ten months later; twenty-four samples were directly exposed to space for the total flight duration (preflight handling, shuttle bay environment, separation from shuttle, shuttle environment, LEO environment, docking, descent, transfer to KSC). Materials included paints (conductive or nonconductive), SSM's, polymeric films, surface coatings, composite materials, and metals. After sample retrieving, inspection and measurements were carried out in atmospheric laboratory conditions on each sample: observation with binocular lenses and scanning electron microscopy, spectral relectance and transmittance using an integrating sphere in the wavelength range 280-2300 nm, emissivity by the means of a Gier & Dunkle portable reflectometer, electron spectroscopy for chemical analysis-x-ray photoelectron spectroscopy (ESCA-XPS), and Rutherford backscattering spectroscopy (RBS) measurements on some selected samples. The results obtained from flight were compared to laboratory data obtained in UV-irradiation tests when these data were available. As a general statement a good spectral concordance is observed for all samples not in the canister so long as air recoveries are taken into account. For one material, the degradation is more important for the sample in the canister than for those of the same material mounted at the surface of the tray; for most samples in the canister the degradation is slightly higher than the one which can be predicted from laboratory standard irradiations. Contamination problems having been ruled out, the higher temperature experience by the samples on the inside of canister probably explains these phenomena.

Guillaumon, Jean-Claude↗

NASA NTRS1987

Effect of control sampling rates on model-based manipulator control schemes

The effect of changing the control sampling period on the performance of the computed-torque and independent joint control schemes is discussed. While the former utilizes the complete dynamics model of the manipulator, the latter assumes a decoupled and linear model of the manipulator dynamics. Researchers discuss the design of controller gains for both the computed-torque and the independent joint control schemes and establish a framework for comparing their trajectory tracking performance. Experiments show that within each scheme the trajectory tracking accuracy varies slightly with the change of the sampling rate. However, at low sampling rates the computed-torque scheme outperforms the independent joint control scheme. Based on experimental results, researchers also conclusively establish the importance of high sampling rates as they result in an increased stiffness of the system.

Khosla, P. K.↗

NASA NTRS1976

Forestry applications project/timber resource. Sam Houston National forest inventory and development of a survey planning model

The Forestry Applications Project has been directed towards solving the problem of meeting informational needs of the resource managers utilizing remote sensing data sources including satellite data, conventional aerial photography, and direct measurement on the ground in such combinations as needed to best achieve these goals. It is recognized that sampling plays an important role in generating relevant information for managing large geographic populations. The central problem, therefore, is to define the kind and amount of sampling and the place of remote sensing data sources in that sampling system to do the best possible job of meeting the manager's informational needs.

Colwell, R. N.↗

NASA NTRS1989

Thermal histories of the samples of two KOSI comet nucleus simulation experiments

Temperatures recorded during two KOSI comet nucleus simulation experiments strongly suggest that heat transport by vapor flow into the interior of the sample is very important. Two comet nucleus simulation experiments have been done by the KOSI team in a big space simulator. The thermal evolution of the sample during insolation and the results of simplified thermal evolution calculations are discussed. The observed thermal histories cannot be explained by a simple model with heat transferred by heat conduction at a constant conductivity, so a coupled heat and mass transfer problem was considered. The porous ice matrix was assumed to have a constant thermal conductivity and to be in thermal equilibrium with vapor in the pores, the internal pressure being the vapor pressure. The vapor was modelled as an ideal gas because, at the temperatures relevant to the problem, the mean free path length of the vapor molecules is large in comparison with the pore dimensions. The heat capacity at constant volume per unit mass of the two phase mixture was also assumed constant. The vapor was allowed to flow and transfer heat in response to an internal pressure gradient.

Spohn, T.↗

NASA NTRS1989

The search for and identification of amino acids, nucleobases and nucleosides in samples returned from Mars

An investigation of the returned Mars samples for biologically important organic compounds, with emphasis on amino acid, the puring and pyrimidine bases, and nucleosides is proposed. These studies would be conducted on subsurface samples obtained by drilling past the surface oxidizing layer with emphasis on samples containing the larges quantities of organic carbon as determined by the rover gas chromatographic mass spectrometer (GCMS). Extraction of these molecules from the returned samples will be performed using the hydrothermal extraction technique described by Cheng and Ponnamperuma. More rigorous extraction methods will be developed and evaluated. For analysis of the extract for free amino acids or amino acids present in a bound or peptidic form, aliquots will be analyzed by capillary GCMS both before and after hydrolysis with 6N hydrochloric acid. Establishment of the presence of amino acids would then lead to the next logical step which would be the use of chiral stationary gas chromatography phases to determine the enatiomeic composition of the amino acids present, and thus potentially establish their biotic or abiotic origin. Confirmational analyses for amino acids would include ion-exchange and reversed-phase liquid chromatographic analysis. For analyses of the returned Mars samples for nucleobases and nucleosides, affinity and reversed-phase liquid chromatography would be utilized. This technology coupled with scanning UV detection for identification, presents a powerful tool for nucleobase and nucleoside analysis. Mass spectrometric analysis of these compounds would confirm their presence in samples returned form Mars.

Gehrke, Charles W.↗

NASA NTRS2009

Transport Powder and Liquid Samples by Surface Acoustic Waves

Sample transport is an important requirement for In-situ analysis of samples in NASA planetary exploration missions. Tests have shown that powders or liquid drops on a surface can be transported by surface acoustic waves (SAW) that are generated on the surface using interdigital transducers. The phenomena were investigated experimentally and to generate SAWs interdigital electrodes were deposited on wafers of 128 deg rotated Y-cut LiNbO?. Transporting capability of the SAW device was tested using particles of various sizes and drops of various viscosities liquids. Because of different interaction mechanisms with the SAWs, the powders and the liquid drops were observed to move in opposite directions. In the preliminary tests, a speed of 180 mm/s was achieved for powder transportation. The detailed experimental setup and results are presented in this paper. The transporting mechanism can potentially be applied to miniaturize sample analysis system or " lab-on-chip" devices.

Sample handling↗

NASA NTRS2001

Far-Infrared Extragalactic Surveys: Past, Present, and Future

As much as one third of the luminosity of the local universe is emitted in the far infrared. In order to understand the history of energy release in the universe, it is crucial to characterize this rest-frame far-infrared contribution from the present back to the era of initial galaxy formation. Over the redshift range from 0 to 10, this energy is received in the 80 micrometers to 1 mm spectral region. In the 1980's the Infrared Astronomy Satellite (IRAS) all-sky survey provided the first comprehensive view of the far infrared emission from the local universe. The diffuse background measurements by Cosmic Background Explorer Satellite (COBE) have provided constraints on the integral contributions from the high redshift universe. In the past five years, submillimeter measurements made using the SCUBA instrument have revealed powerful high redshift sources. To develop a clear history of energy release in the universe, we need numbers and redshifts of representative populations of energetically important objects. The near future will bring the Space Infrared Telescope Facility Multiband Imaging Photometer (SIRTF)(MIPS) survey, which will cover about 100 square degrees at wavelengths out to 160 micrometers, providing a large sample of energetically important galaxies out to z of approx.3. In 2005, the Japanese IRIS survey will provide a 160 micrometers full sky survey, which will provide larger samples of the high z galaxy populations and will find intrinsically rare high luminosity objects. The SPIRE instrument on the FIRST facility will extend these surveys to longer wavelengths, providing a view of the universe at higher redshifts in three spectral bands. A concept for an all-sky submillimeter survey is under development, called the Survey of Infrared Cosmic Evolution (SIRCE). With a 2 m cryogenic telescope, it can map the entire sky to the confusion limit in the 100 to 500 micrometers range in six months. This survey will provide photometric redshifts, number counts, and will find the most luminous objects in the universe. In the next decade, the opening of the submillimeter, combined with the near infrared capability of NGST will provide us with a clear picture of energy release in the early universe.

Moseley, Samuel H., Jr.↗

NASA NTRS1988

Martian regolith geochemistry and sampling techniques

Laboratory study of samples of the intermediate and fine-grained regolith, including duricrust peds, is a fundamental prerequisite for understanding the types of physical and chemical weathering processes on Mars. The extraordinary importance of such samples is their relevance to understanding past changes in climate, availability (and possible physical state) of water, eolian forces, the thermal and chemical influences of volcanic and impact processes, and the inventory and fates of Martian volatiles. Fortunately, this regolith material appears to be ubiquitous over the Martian surface, and should be available at many different landing sites. Viking data has been interpreted to indicate a smectite-rich regolith material, implying extensive weathering involving aqueous activity and geochemical alteration. An all-igneous source of the Martian fines has also been proposed. The X-ray fluorescence measurement data set can now be fully explained in terms of a simple two-component model. The first component is silicate, having strong geochemical similarities with Shergottites, but not other SNC meteorites. The second component is salt. Variations in these components could produce silicate and salt-rich beds, the latter being of high potential importance for microenvironments in which liquid water (brines) could exist. It therefore would be desirable to scan the surface of the regolith for such prospects.

Clark, B. C.↗

NASA NTRS2010

Searching for Amino Acids in Meteorites and Comet Samples

Chemistry plays an important role in the interdisciplinary field of astrobiology, which strives to understand the origin, distribution, and evolution of life throughout the universe. Chemical techniques are used to search for and characterize the basic ingredients for life, from the elements through simple molecules and up to the more complex compounds that may serve as the ingredients for life. The Astrobiology Analytical Laboratory at NASA Goddard uses state-of-the-art laboratory analytical instrumentation in unconventional ways to examine extraterrestrial materials and tackle some of the big questions in astrobiology. This talk will discuss some of the instrumentation and techniques used for these unique samples, as well as some of our most interesting results. The talk will present two areas of particular interest in our laboratory: (1) the search for chiral excesses in meteoritic amino acids, which may help to explain the origin of homochirality in life on Earth; and (2) the detection of amino acids and amines in material returned by NASA's Stardust mission, which rendevouzed with a cornet and brought back cometary particles to the Earth.

Cook, Jamie Elsila↗

NASA NTRS2024

Current Status of Martian Moons eXploration (MMX) Contamination Control and Curation Activity

Martian Moons eXploration (MMX) is a sample return mission from the Martian moon Phobos. The MMX spacecraft is scheduled to launch in 2026 and return to Earth in 2031. The main science goals of MMX are “to reveal the origin of the Martian moons and make progress in the understanding of planetary system formation and material transport in the solar system, and to observe processes that impact the circumplanetary and surface environments of Mars”. MMX has two sampling systems: coring (C)-sampler and pneumatic (P)-sampler and plans to bring back >10 g of Phobos sample. The retuned sample in the sample capsule will be transferred to the curation facility in ISAS/JAXA for sample curation and subsequent sample analysis. Contamination control of the sample return mission requires special care to prevent terrestrial contamination to the spacecraft, which would ruin the scientific value of the returned sample. Retaining the pristineness of the retuned sample is an important task of the MMX Curation and Sampler Science teams. The basis of the contamination control is (1) to minimize and understand the nature and amount of contaminants, (2) to perform contamination assessment and evaluate the effect of contaminants in the spacecraft on the retuned sample, (3) to employ a contamination knowledge (CK) material coupon in the spacecraft to identify the contaminants in the returned samples. In the MMX contamination control plan, the allowable contamination level for each contaminant is carefully defined. They are mostly set to be 1/1000 of the expected amount of each material in the returned sample and are divided into two main categories: organic and inorganic. The allowable atmospheric leakage rate to the sample container is also defined. The allowable contamination level of the organic materials is based on the composition of carbonaceous chondrites. The target contaminants are amino acids, aliphatic and aromatic hydrocarbons, carboxylic acids, etc. In case of the inorganic materials, the target contaminants are important elements to permit distinguishing the origin of the Martian moon by nucleosynthetic isotope anomalies (Cr, Ti, and Mo) and to reveal the evolution of the Martian moon by chronology (Hf, W, U, Pb, Rb, Sr, Sm, and Nd). The key instrument of contamination control in the sample return mission is the sampler system. The C-sampler has been developed by JAXA and the P-sampler was provided by Honeybee/NASA. In MMX, materials used in the two samplers (C- and P- sampler) were carefully selected to avoid potential contamination from the design stage of the system. The individual parts of the C-sampler FM (Flight Model) were thoroughly cleaned at the curation facility in ISAS/JAXA by the full-course cleaning procedure, which is an ultrasonic cleaning with organic solvents and ultrapure water in several steps. The equivalent level of cleaning was also carried out on the P-Samper FM as well by Honeybee Robotics in the USA. Now, MMX is in the critical phase for contamination control called ATLO: Assembly, Test, and Launch Operations. During the ATLO phase, sampler FM is constantly purged with nitrogen gas and maintained at positive pressure to prevent environmental contamination. The surrounding environments of the sampler FM are also simultaneously monitored using the CK Monitoring Coupon Set, which consists of several witness materials such as a glass petri dish, sapphire glass disk, and carbon adhesive tape (Figure 1). The detailed environmental assessment of each clean room used for the assembly and test of the sampler FM has also been conducted. This assessment includes microbial analysis, which was performed for OSIRIS-REx. Regarding the sample recovery and sample curation, we have started the designing of Sample Container Disassembling Instrument for the sample recovery from the sample container and the MMX curation chamber for sample curation. The curation protocol for the Phobos returned sample has also been discussed by the MMX Sample Analysis Working Team (SAWT). The MMX curation protocol consists of three phases: (1) quick analysis, (2) pre-basic characterization, and (3) basic characterization. (1) is extraction of the sample gas from the sample container and analysis by mass spectrometry, (2) is observation in bulk level, and (3) is observation in grain level and allocation of the sample aliquots. In parallel with the curation protocol, the returned sample undergoes preliminary examination for scientific investigations to achieve science goals. In addition, the CK witness plates made of sapphire glass are on board the sampler system. The CK witness plates will be recovered from the sampler system and analyzed by SAWT for the assessment of in-flight contamination.

Haruna Sugahara↗

NASA NTRS1988

Sampling strategies on Mars: Remote and not-so-remote observations from a surface rover

The mobility and speed of a semi-autonomous Mars rover are of necessity limited by the need to think and stay out of trouble. This consideration makes it essential that the rover's travels be carefully directed to likely targets of interest for sampling and in situ study. Short range remote sensing conducted from the rover, based on existing technology, can provide significant information about the chemistry and mineralogy of surrounding rocks and soils in support of sampling efforts. These observations are of course of direct scientific importance as well. Because of the small number of samples actually to be returned to Earth, it is also important that candidate samples be analyzed aboard the rover so that diversity can be maximized. It is essential to perform certain types of analyses, such as those involving volatiles, prior to the thermal and physical shocks of the return trip to Earth. In addition, whatever measurements can be made of nonreturned samples will be important to enlarge the context of the detailed analyses to be performed later on the few returned samples. Some considerations related to these objectives are discussed.

Singer, R. B.↗

NASA NTRS1978

The lunar highland melt-rock suite

Size can be used as a criterion to select 18 large (larger than 1 cm) samples from among 148 melt-rock fragments of all sizes. This selection provides a suite of large samples which represent the important chemical variants among highland melt rocks; each large sample has enough material for a number of sample-destructive studies, as well as for future reference. Cluster analysis of the total data base of 148 highland melt rocks shows six distinct groups: anorthosite, gabbroic anorthosite, anorthositic gabbro ('highland basalt'), low K Fra Mauro, intermediate-K Fra Mauro, and high-K. Large samples are available for four of the melt-rock groups (gabbroic anorthosite, anorthositic gabbro, low-K Fra Mauro, and intermediate-K Fra Mauro). This sample selection reveals two subgroups of anorthositic gabbro (one anorthite-poor with negative Eu anomaly and one anorthite-rich without Eu anomaly). There is a sharp distinction between those Apollo 16 melt rocks and glasses which have both been classified as 'gabbroic anorthosite'.

Vaniman, D. T.↗

NASA NTRS2005

Stardust@home: A Massively Distributed Public Search for Interstellar Dust in the Stardust Interstellar Dust Collector

In January 2006, the Stardust mission will return the first samples from a solid solar system body beyond the Moon. Stardust was in the news in January 2004, when it encountered comet Wild2 and captured a sample of cometary dust. But Stardust carries an equally important payload: the first samples of contemporary interstellar dust ever collected. Although it is known that interstellar (IS) dust penetrates into the inner solar system [2, 3], to date not even a single contemporary interstellar dust particle has been captured and analyzed in the laboratory. Stardust uses aerogel collectors to capture dust samples. Identification of interstellar dust impacts in the Stardust Interstellar Dust Collector probably cannot be automated, but will require the expertise of the human eye. However, the labor required for visual scanning of the entire collector would exceed the resources of any reasonably-sized research group. We are developing a project to recruit the public in the search for interstellar dust, based in part on the wildly popular SETI@home project, which has five million subscribers. We call the project Stardust@home. Using sophisticated chemical separation techniques, certain types of refractory ancient IS particles (so-called presolar grains) have been isolated from primitive meteorites (e.g., [4] ). Recently, presolar grains have been identified in Interplanetary Dust Particles[6]. Because these grains are not isolated chemically, but are recognized only by their unusual isotopic compositions, they are probably less biased than presolar grains isolated from meteorites. However, it is entirely possible that the typical interstellar dust particle is isotopically solar in composition. The Stardust collection of interstellar dust will be the first truly unbiased one.

Westphal, Andrew J.↗

NASA NTRS2005

XMM-Newton Observations of the DLS Shear-Selected Cluster Survey

The goal of this project continues to be to test the selection effects in cluster surveys by investigating the X-ray properties of the first shear-selected sample of galaxy clusters, the Deep Lens Survey (DLS). Because lensing signal is only sensitive to mass (albeit with projection effects), lensing signal can be used to select a sample that is independent of its X-ray properties. If a lensing-selected sample has very different X-ray properties from an X-ray selected sample, it would have important consequences for evolutionary studies based on existing cluster samples was aimed at refining the lensing-selected sample as part of this continuing study The grant supported a KPNO run to obtain data on another region of the sky to extend the cluster sample, and also the purchase of a disk array for archiving the optical mosaic data (Two terabytes worth) from which the lensing maps are derived As a result of the grant, we have extended the lensing cluster sample to another 4-square degree patch of the sky, adding another three clusters to our sample to be observed While the sample of X-ray observed clusters is too small to derive a firm conclusion yet, our preliminary finding is that the X-ray properties of the observed sample do not differ from those of X-ray selected surveys A paper discussing the first results has been published, and a second paper on the mass differences is still in preparation (with J Hughes as first author)

DellAntonio, Ian↗

NASA NTRS2007

The Abundance and Distribution of Presolar Materials in Cluster IDPS

Presolar grains and remnants of interstellar organic compounds occur in a wide range of primitive solar system materials, including meteorites, interplanetary dust particles (IDPs), and comet Wild-2 samples. Among the most abundant presolar phases are silicate stardust grains and molecular cloud material. However, these materials have also been susceptible to destruction and alteration during parent body and nebular processing. In addition to their importance as direct samples of remote and ancient astrophysical environments, presolar materials thus provide a measure of how well different primitive bodies have preserved the original solar system starting materials. The matrix normalized abundances of presolar silicate grains in meteorites range from 20 ppm in Semarkona and Bishunpur to 170 ppm for Acfer 094. The lower abundances of presolar silicates in Bishunpur and Semarkona has been ascribed to the destruction of presolar silicates during aqueous processes. Presolar silicates appear to be significantly more abundant in anhydrous IDPs, possibly because these materials did not experience parent body hydrothermal alteration. Among IDPs the estimated abundances of presolar silicates vary by more than an order of magnitude, from 480 to 5500 ppm. The wide disparity in the abundances of presolar silicates of IDPs may be a consequence of the relatively small total area analyzed in those studies and the fine grain sizes of the IDPs. Alternatively, there may be a wide range in presolar silicate abundances between different IDPs. This view is supported by the observation that 15N-rich IDPs have higher presolar silicate abundances than those with isotopically normal N.

Messenger, Scott↗

NASA NTRS2007

The Abundance and Distribution of Presolar Materials in Cluster IDPS

Messenger, Scott↗

NASA NTRS2010

Lunar and Meteorite Sample Education Disk Program - Space Rocks for Classrooms, Museums, Science Centers, and Libraries

NASA is eager for students and the public to experience lunar Apollo samples and meteorites first hand. Lunar rocks and soil, embedded in Lucite disks, are available for educators to use in their classrooms, museums, science centers, and public libraries for education activities and display. The sample education disks are valuable tools for engaging students in the exploration of the Solar System. Scientific research conducted on the Apollo rocks reveals the early history of our Earth-Moon system and meteorites reveal much of the history of the early solar system. The rocks help educators make the connections to this ancient history of our planet and solar system and the basic processes accretion, differentiation, impact and volcanism. With these samples, educators in museums, science centers, libraries, and classrooms can help students and the public understand the key questions pursued by many NASA planetary missions. The Office of the Curator at Johnson Space Center is in the process of reorganizing and renewing the Lunar and Meteorite Sample Education Disk Program to increase reach, security and accountability. The new program expands the reach of these exciting extraterrestrial rocks through increased access to training and educator borrowing. One of the expanded opportunities is that trained certified educators from science centers, museums, and libraries may now borrow the extraterrestrial rock samples. Previously the loan program was only open to classroom educators so the expansion will increase the public access to the samples and allow educators to make the critical connections to the exciting exploration missions taking place in our solar system. Each Lunar Disk contains three lunar rocks and three regolith soils embedded in Lucite. The anorthosite sample is a part of the magma ocean formed on the surface of Moon in the early melting period, the basalt is part of the extensive lunar mare lava flows, and the breccias sample is an important example of the violent impact history of the Moon. The disks also include two regolith soils and orange glass from a pyroclastic deposit. Each Meteorite Disk contains two ordinary chondrites, one carbonaceous chondrite, one iron, one stony iron, and one achondrite. These samples will help educators share the early history of the solar system with students and the public. Educators may borrow either lunar or meteorite disks and the accompanying education materials through the Johnson Space Center Curatorial Office. In trainings provided by the NASA Aerospace Education Services Program specialists, educators certified to borrow the disk learn about education resources, the proper use of the samples, and the special security for care and shipping of the disks. The Lunar and Meteorite Sample Education Disk Program will take NASA exploration to more people. Getting Space Rocks out to the public and inspiring the public about new space exploration is the focus of the NASA disk loan program.

Allen, Jaclyn↗