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Results from the First Field Test of a Ruggedized Continuous Holdup Monitor

A first field test of the inexpensive and ruggedized online holdup monitor under development at the US Department of Energy’s Oak Ridge National Laboratory (ORNL) was performed in September of 2023 with highly successful results. ORNL staff collaborated with personnel at the National Fuel Services (NFS) to place two battery-powered detector units at the facility, one on a fuel processing line and the other on a HEPA filter. Both units collected gamma-ray counts per second, temperature, humidity, and battery power data every 5 s seconds over the course of 19 days. Analyzed results from the measurements were discussed with NFS personnel after the units were removed. Vendor feedback on the units was overwhelmingly positive with an expressed desire to deploy finished units at the facility and an open invitation for testing future prototypes.

46 INSTRUMENTATION RELATED TO NUCLEAR SCIENCE AND ↗

Small Scale Field Test Demonstrating CO 2 Sequestration In Arbuckle Saline Aquifer And By CO 2 -Eor At Wellington Field, Sumner County, Kansas

The objectives of this project are to understand the processes that occur when a maximum of 70,000 metric tonnes of CO 2 are injected into two different formations to evaluate the response in different lithofacies and depositional environments. The evaluation will be accomplished through the use of both in situ and indirect MVA (monitoring, verification, and accounting) technologies. The project will optimize for carbon storage accounting for 99% of the CO 2 using lab and field testing and comprehensive characterization and modeling techniques. Site characterization and CO 2 injection should demonstrate state-of-the-art MVA tools and techniques to monitor and visualize the injected CO 2 plume and to refine geomodels developed using nearly continuous core, exhaustive wireline logs, and well tests and a multi-component 3-D seismic survey. Reservoir simulation studies will map the injected CO 2 plume and estimate tonnage of CO 2 stored in solution, as residual gas, and by mineralization and integrate MVA results and reservoir models shall be used to evaluate CO 2 leakage. A rapid-response mitigation plan was developed to minimize CO 2 leakage and provide a comprehensive risk management strategy. The CO 2 was intended to be supplied from a reliable facility and have an adequate delivery and quality of CO 2 . However, several unforeseen circumstances complicated this plan: (1) the initially negotiated CO 2 supply facility went offline and contracts associated with CO 2 supply had to be renegotiated, (2) a UIC Class VI permit proved to be difficult to obtain due to the experimental nature of the project. Both subjects are detailed in separate deliverables attached to this report. The CO 2 enhanced oil recovery (EOR) and geologic storage in Mississippian carbonate reservoir was sucessully deployed. Approximately 20,000 metric tons of CO 2 was injected in the upper part of the Mississippian reservoir to verify CO 2 EOR viability in carbonate reservoirs and evaluate a potential of transitioning to geologic CO 2 storage through EOR. A total of 1,101 truckloads, 19,803 metric tons—an average of 120 tonnes per day—were delivered over the course of injection that lasted from January 9 to June 21, 2016. After cessation of CO 2 injection, the KGS 2-32 well was converted to water injector and continues to operate. CO 2 EOR progression in the field was monitored weekly with fluid level, temperature, and production recording and formation fluid composition sampling. It is important to note that normally, CO 2 EOR pilots are less efficient than commercial operations due to lack of directional and precise well control, lack of surface facilities for CO 2 recycling, and other factors. As a result of this pilot CO 2 injection, the observed incremental average oil production increase was ~68% with only ~18% of injected CO 2 produced back. Decline curve analysis forecasts of additional cumulative oil produced were 32.44M STB to the end of 2027. Wellington Mississippian pilot efficiency by the end of forecast calculations is 11 MCF per barrel of produced oil. Using 32M STB oil production and $1,964,063 cost of CO 2 , CO 2 EOR cost per barrel of oil production is ~$60. Simple but robust monitoring technologies proved to be very efficient in detecting and locating CO 2 . High CO 2 reservoir retentions with low yields within an actively producing field could help to estimate real-world risks of CO 2 geological storage for future projects. The Wellington Field CO 2 EOR was executed in a controlled environment with high efficiency. This case study proves that CO 2 EOR could be successfully applied in Kansas carbonate reservoirs if CO 2 sources and associated infrastructure are available. Recent developments in unconventional resources development in Mid-Continent USA and associated large volume disposal of backflow water and the resulting seismic activity have brought more focus and attention to the Arbuckle Group in southern Kansas. Despite the commercial interest, limited essential information about reservoir properties and structural elements has impeded the management and regulation of disposal, an issue brought to the forefront by recent seismicity in and near areas of large volumes and rates of brine disposal. The Kansas Geological Survey (KGS) collected, compiled, and analyzed available data, including well logs, core data, step rate tests, drill stem tests, 2-D and 3-D seismic data, water level measurements, and others types of data. Several exploratory wells were drilled and core was collected and modern suites of logs were analyzed. Reservoir properties were populated into several site-specific geological models. The geological models illustrate the highly heterogeneous nature of the Arbuckle Group. Vertical and horizontal variability results in several distinct hydro-stratigraphic units that are the result of both depositional and diagenetic processes. During the course of this project, it has been demonstrated that advanced seismic interpretation methods can be used successfully for characterization of the Mississippian reservoir and Arbuckle saline aquifer. Analysis of post-stack 3-D seismic data at the Mississippian reservoir showed the response of a gradational velocity transition. Pre-stack gather analysis showed that porosity zones of the Mississippian and Arbuckle reservoirs exhibit characteristic amplitude versus offset (AVO) response. Simultaneous AVO inversion estimated P- and S-impedances. The 3-D survey gather azimuthal anisotropy analysis (AVAZ) provided information about the fault and fracture network and showed good agreement to the regional stress field and well data. Mississippian reservoir porosity and fracture predictions agreed well with the observed mobility of injected CO 2 in KGS well 2-32. Fluid substitution modeling predicted acoustic impedance reduction in the Mississippian carbonate reservoir introduced by the presence of CO 2 . Seismicity in the United States midcontinent has increased by orders of magnitude over the past decade. Spatiotemporal correlations of seismicity to wastewater injection operations have suggested that injection-related pore fluid pressure increases are inducing the earthquakes. In this investigation, we examine earthquake occurrence in southern Kansas and northern Oklahoma and its relation to the change in pore pressure. The main source of data comes from the Wellington Array in the Wellington oil field, in Sumner County, Kansas, which has monitored for earthquakes in central Sumner County, Kansas, since early 2015. The seismometer array was established to monitor CO 2 injection operations at Wellington Field. Although no seismicity was detected in association with the spring 2016 Mississippian CO 2 injection, the array has recorded more than 2,500 earthquakes in the region and is providing valuable understanding to induced seismicity. A catalog of earthquakes was built from this data and was analyzed for spatial and temporal changes, stress information, and anisotropy information. The region of seismic concern has been shown to be expanding through use of the Wellington earthquake catalog, which has revealed a northward progression of earthquake activity reaching the metropolitan area of Wichita. The stress orientation was also calculated from this earthquake catalog through focal mechanism inversion. The calculated stress orientation was confirmed through comparison to other stress measurements from well data and previous earthquake studies in the region. With this knowledge of the stress orientation, the anisotropy in the basement could be understood. This allowed for the anisotropy measurements to be correlated to pore pressure increases. The increase in pore pressure was monitored through time-lapse shear-wave anisotropy analysis. Since the onset of the observation period in 2010, the orientation of the fast shear wave has rotated 90°, indicating a change associated with critical pore pressure build up. The time delay between fast and slow shear wave arrivals has increased, indicating a corresponding increase in anisotropy induced by pore pressure rise. In-situ near-basement fluid pressure measurements corroborate the continuous pore pressure increase revealed by the shear-wave anisotropy analysis over the earthquake monitoring period. This research is the first to identify a change in pore fluid pressure in the basement using seismological data and it was recently published in the AAAS journal Science Advances (Nolte et al., 2017). The shear-wave splitting analysis is a novel application of the technique, which can be used in other regions to identify an increase in pore pressure. This increasing pore fluid pressure has become more regionally extensive as earthquakes are occurring in southern Kansas, where they previously were absent. These monitoring techniques and analyses provide new insight into mitigating induced seismicity’s impact on society.

02 PETROLEUM↗

Report on Field Test at INL Cask Farm of Single Detector Fast Neutron Spent Fuel Cask Verification System

Detecting diversion of spent fuel elements in dry storage casks is challenging due to the thick shielding used in cask construction. Measurements on top of the cask to map the underlying arrangement of the fuel elements and looking for anomalous changes over time has proven difficult to achieve using gamma rays due to the high scattering and attenuation from the thick steel structure, weakening information on the present or absence of fuel bundles. Simulations and laboratory experiments suggest that the high-energy neutron flux (>200 keV) measured directly above each fuel bundle is sufficient to produce a position map that enables detection of the present or absence of fuel bundles, and therefore diversion of a spent fuel bundle. A single-detector spent-fuel monitoring technique based on this principle was development at the Lawrence Livermore National Laboratory (LLNL). The INL Cask Farm in the INTEC technical area at Idaho National Laboratory (INL) offers the capability to test this technique on an MC-10 storage cask which has a distribution of full and empty fuel positions. An experimental test plan for the single-detector verification system was developed in consultation with INL personnel to be completed in FY2021. Due to travel advisories related to COVID-19, the experimental test plan was adapted to enable INL personnel to carry out the measurements in consultation with LLNL personnel following shipment of the LLNL system to INL. Field test measurements of the single detector verification system were successfully carried out at the INL cask farm on September 7-9, 2021. This document summarizes results of the field test.

11 NUCLEAR FUEL CYCLE AND FUEL MATERIALS↗

Flow visualization methods for field test verification of CFD analysis of an open gloveport

Anemometer readings alone cannot provide a complete picture of air flow patterns at an open gloveport. Having a means to visualize air flow for field tests in general provides greater insight by indicating direction in addition to the magnitude of the air flow velocities in the region of interest. Furthermore, flow visualization is essential for Computational Fluid Dynamics (CFD) verification, where important modeling assumptions play a significant role in analyzing the chaotic nature of low-velocity air flow. A good example is shown Figure 1, where an unexpected vortex pattern occurred during a field test that could not have been measured relying only on anemometer readings. Here by, observing and measuring the patterns of the smoke flowing into the gloveport allowed the CFD model to be appropriately updated to match the actual flow velocities in both magnitude and direction.

71 CLASSICAL AND QUANTUM MECHANICS, GENERAL PHYSIC↗

Impacts of elevated dissolved CO 2 on a shallow groundwater system: Reactive transport modeling of a controlled-release field test

We report one of the risks that CO 2 geological sequestration imposes on the environment is the impact of potential CO 2 /brine leakage on shallow groundwater. The reliability of reactive transport models predicting the response of groundwater to CO 2 leakage depends on a thorough understanding of the relevant chemical processes and key parameters affecting dissolved CO 2 transport and reaction. Such understanding can be provided by targeted field tests integrated with reactive transport modeling. A controlled-release field experiment was conducted in Mississippi to study the CO 2 -induced geochemical changes in a shallow sandy aquifer at about 50 m depth. The field test involved a dipole system in which the groundwater was pumped from one well, saturated with CO 2 at the pressure corresponding to the hydraulic pressure of the aquifer, and then re-injected into the same aquifer using a second well. Groundwater samples were collected for chemical analyses from four monitoring wells before, during and after the dissolved CO 2 was injected. In this paper, we present reactive transport models used to interpret the observed changes in metal concentrations in these groundwater samples. A reasonable agreement between simulated and measured concentrations indicates that the chemical response in the aquifer can be interpreted using a conceptual model that encompasses two main features: (a) a fast-reacting but limited pool of reactive minerals that responds quickly to changes in pH and causes a pulse-like concentration change, and (b) a slow-reacting but essentially unlimited mineral pool that yields rising metal concentrations upon decreased groundwater velocities after pumping and injection stopped. During the injection, calcite dissolution and Ca-driven cation exchange reactions contribute to a sharp pulse in concentrations of Ca, Ba, Mg, Mn, K, Li, Na and Sr, whereas desorption reactions control a similar increase in Fe concentrations. Finally, after the injection and pumping stops and the groundwater flow rate decreases, the dissolution of relatively slow reacting minerals such as plagioclase drives the rising concentrations of alkali and alkaline earth metals observed at later stages of the test, whereas the dissolution of amorphous iron sulfide causes slowly increasing Fe concentrations.

58 GEOSCIENCES↗

Field Testing of an In-Situ Neutron Spectrometer for Planetary Exploration: First Results

As part of an ongoing effort to demonstrate the utility of using in-situ neutron spectroscopy to measure water content on planetary surfaces, we have developed a field site for carrying out neutron spectroscopy measurements. Specifically, our objectives in developing the field site are: 1) Demonstrate in-situ neutron measurements in a realistic field test scenario; 2) Demonstrate our ability to accurately model neutron measurements for various conditions and identify measurement factors that need to be controlled and/or accounted for such as detailed stratigraphy; 3) Provide a field test location for future in-situ neutron measurements using a variety of instrument and soil configurations.

Lawrence, D. J.↗

Modeling CO 2 flow in support of a shallow subsurface controlled leakage field test

Here, controlled release of carbon dioxide (CO 2 ) into the soil and atmosphere is performed to test detection and monitoring tools, for which several field laboratories were established by a number of institutions worldwide. Numerical simulations of CO 2 behavior in the shallow subsurface region are other forms of validation and verification of the leakage pathways and destinations. These reports aim to improve monitoring and verification of CO 2 in case of unexpected leakages for public assurance. In this work, we introduce the results of a numerical modeling study conducted to simulate the injection of CO 2 as carried out during a field test in Viamão, southern Brazil, where 20 kg day –1 of CO 2 was pumped for 30 days through a vertical well 3 m below ground in an altered granitic soil. Multiphase flow simulations were performed with the TOUGH2/EOS7CA software for unsaturated porous media, using field data and injection parameters, including sensitivity tests to permeability direction, diffusivity, and boundary conditions. Results with increased horizontal permeabilities are in better agreement with the field observations. In this condition, mass balance calculations indicate approximately 90% of injected CO2 (20 kg day –1 during 30 days) remains in the soil after 180 days from injection start, consistent with the measured flow through the soil–atmosphere interface.

03 NATURAL GAS↗

Performance of Regolith Feed Systems for Analog Field Tests of In-Situ Resource Utilization Oxygen Production Plants in Mauna Kea, Hawaii

This paper focuses on practical aspects of mechanical auger and pneumatic regolith conveying system feeding In-Situ Resource Utilization Oxygen production plants. The subsystems of these feedstock delivery systems include an enclosed auger device, pneumatic venturi educator, jet-lift regolith transfer, innovative electro-cyclone gas-particle separation/filtration systems, and compressors capable of dealing with hot hydrogen and/or methane gas re-circulating in the system. Lessons learned from terrestrial laboratory, reduced gravity and field testing on Mauna Kea Volcano in Hawaii during NASA lunar analog field tests will be discussed and practical design tips will be presented.

Townsend, Ivan I.↗

Near-field testing of the 15-meter model of the hoop column antenna. Volume 3: Near- and far-field plots for the JPL feed

Technical results from near-field testing of the 15-meter model of the hoop column antenna at the Martin Marietta Denver Aerospace facility are discussed. The antenna consists of a deployable central column and a 15 meter hoop, stiffened by cables into a structure with a high tolerance repeatable surface and offset feed location. The surface has been configured to have four offset parabolic apertures, each about 6 meters in diameter, and is made of gold plated molybdenum wire mesh. Pattern measurements were made with feed system radiating at frequencies of 7.73, 11.60, 2.27, 2.225, and 4.26 (all in GHz). This report (Volume 3) gives the detailed patterns measured with the JPL feed (2.225 GHz). Volume 1 covers the testing from an overall viewpoint and contains information of generalized interest for testing large antennas, including the deployment of the antenna in the Martin Facility and the measurements to determine mechanical stability and trueness of the reflector surface, the test program outline, and a synopsis of antenna electromagnetic performance. A detailed listing of the antenna patterns for the LaRC feeds (7.3, 11.60, 2.27, and 4.26 GHz) are given in Volume 2 of this report.

Hoover, J.↗

Near-field testing of the 15-meter model of the hoop column antenna. Volume 2: Near- and far-field plots for the LaRC feeds

The technical results from near-field testing of the 15-meter model of the hoop column antenna at the Martin Marietta Denver Aerospace facility are described. The antenna consists of a deployable central column and a 15-meter hoop, stiffened by cable into a structure with a high tolerance repeatable surface and offset feed location. The surface has been configured to have four offset parabolic apertures, each about 6 meters in diameter, and is made of gold plated molybdenum wire mesh. Pattern measurements were made with feed systems radiating at frequencies of 7.73, 11.60, 2.27, 2.225, and 4.26 (all in GHz). This report (Volume II) gives the detailed patterns measured with the LaRC feeds (7.73, 11.60, 2.27, and 4.26 GHz). Volume I covers the testing from an overall viewpoint and contains information of generalized interest for testing large antennas, including the deployment of the antenna in the Martin Facility and the measurements to determine mechanical stability and trueness of the reflector surface, the test program outline, and a synopsis of antenna electromagnetic performance. A detailed listing of the antenna patterns are provided for the 2.225 Ghz feed in Volume III of this report.

Hoover, J.↗

Cosmological backreaction for a test field observer in a chaotic inflationary model

In an inhomogeneous universe, an observer associated with a particular matter field does not necessarily measure the same cosmological evolution as an observer in a homogeneous and isotropic universe. Here we consider, in the context of a chaotic inflationary background model, a class of observers associated with a ''clock field'' for which we use a light test field. We compute the effective expansion rate and fluid equation of state in a gauge invariant way, taking into account the quantum fluctuations of the long wavelength modes, and working up to second order in perturbation theory and in the slow-roll approximation. We find that the effective expansion rate is smaller than what would be measured in the absence of fluctuations. Within the stochastic approach we study the bounds for which the approximations we make are consistent.

79 ASTRONOMY AND ASTROPHYSICS↗

ALFA Field Testing of a Dual Sonar System for Detecting Woody Debris

Field testing of a dual sonar system for detecting woody debris in natural settings was conducted at the Tanana River Test Site (TRTS) in Nenana, AK between 8/26 and 9/23, 2015. The TRTS is approximately 65 miles south of Fairbanks and is well suited for testing hydrokinetic energy generation technologies and environmental monitoring technologies such as the dual sonar system used here in realistic settings.

16 TIDAL AND WAVE POWER↗

Analyses of Field Test Data at the Atucha-1 Spent Fuel Pools

A field test was conducted at the Atucha-1 spent nuclear fuel pools to validate a software package for gross defect detection that is used in conjunction with the inspection tool, Spent Fuel Neutron Counter (SFNC). A set of measurements was taken with the SFNC and the software predictions were compared with these data and analyzed. The data spanned a wide range of cooling times and a set of burnup levels leading to count rates from the several hundreds to around twenty per second. The current calibration in the software using linear fitting required the use of multiple calibration factors to cover the entire range of count rates recorded. The solution to this was to use power regression data fitting to normalize the predicted response and derive one calibration factor that can be applied to the entire set of data. The resulting comparisons between the predicted and measured responses were generally good and provided a quantitative method of detecting missing fuel in virtually all situations. Since the current version of the software uses the linear calibration method, it would need to be updated with the new power regression method to make it more user-friendly for real time verification and fieldable for the range of responses that will be encountered.

98 NUCLEAR DISARMAMENT, SAFEGUARDS, AND PHYSICAL P↗

Goldstone field test activities: Target search

In March of this year prototype SETI equipment was installed at DSS13, the 26 meter research and development antenna at NASA's Goldstone complex of satellite tracking dishes. The SETI equipment will remain at this site at least through the end of the summer so that the hardware and software developed for signal detection and recognition can be fully tested in a dynamic observatory environment. The field tests are expected to help understand which strategies for observing and which signal recognition algorithms perform best in the presence of strong man-made interfering signals (RFI) and natural astronomical sources.

Tarter, J.↗

Laboratory and Field Testing of Commercially Available Detectors for the Identification of Chemicals of Interest in the Nuclear Fuel Cycle for the Detection of Undeclared Activities

Traditionally, IAEA inspectors have focused on the detection of nuclear indicators as part of infield inspection activities. The ability to rapidly detect and identify chemical as well as nuclear signatures can increase the ability of IAEA inspectors to detect undeclared activities at a site. Identification of chemical indicators have been limited to use in the analysis of environmental samples. Although IAEA analytical laboratories are highly effective, environmental sample processing does not allow for immediate or real-time results to an IAEA inspector at a facility. During a complementary access inspection, under the Additional Protocol, the use of fieldable technologies that can quickly provide accurate information on chemicals that may be indicative of undeclared activities can increase the ability of IAEA to effectively and efficiently complete their mission. The Complementary Access Working Group (CAWG) is a multi-laboratory team with members from Brookhaven National Laboratory, Idaho National Laboratory, Los Alamos National Laboratory, and Sandia National Laboratory. The team identified chemicals at each stage of the nuclear fuel cycle that may provide IAEA inspectors with indications that proliferation activities may be occurring. The group eliminated all indicators related to equipment, technology and training, developing a list of by-products/effluents, non-nuclear materials, nuclear materials, and other observables. These proliferation indicators were prioritized based on detectability from a conduct of operations (CONOPS) perspective of a CA inspection (for example, whether an inspector actually can access the S&O or whether it is in process with no physical access), and the IAEA’s interest in the detection technology in conjunction with radiation detectors. The list was consolidated to general categories (nuclear materials from a chemical detection technique, inorganic chemicals, organic chemicals, halogens, and miscellaneous materials). The team then identified commercial off the shelf (COTS) chemical detectors that may detect the chemicals of interest. Three chemical detectors were selected and tested both in laboratory settings and in field operations settings at Idaho National Laboratory. The instruments selected are: Thermo Scientific TruDefender FT (FTIR), Thermo Scientific FirstDefender RM (Raman), and Bruker Tracer III SD (XRF). Functional specifications, operability, and chemical detectability, selectivity, and limits of detection were determined. Results from the laboratory and field tests will be presented. This work is supported by the Next Generation Safeguards Initiative, Office of Nonproliferation and International Security, National Nuclear Security Administration.

38 RADIATION CHEMISTRY, RADIOCHEMISTRY, AND NUCLEA↗

Load Composition Analysis in Support of the NERC Load Modeling Task Force. 2019-2020 Field Test of the Composite Load Model

In 2015, NERC’s reliability standards were revised to require the use of dynamic load models in transmission planning studies. To comply with the standards, planners must use load models that explicitly represent the dynamic behavior of the different constituents of load at each load bus within their transmission planning models. The most important of these constituents are motor-driven and power electronics-based loads. Collectively, these representations are known as composite load models. In anticipation of the compliance date for the new standards, NERC’s Load Modeling Task Force (LMTF), in 2019, initiated a field test of composite load models involving the regional reliability planning entities. In support of the field test, DOE and BPA researchers developed region-specific composite load models that could be assigned to each non-industrial load bus in the planning models for each of the North American interconnections. Separate models were developed for each hour of a summer peak day, a winter peak day, and a spring light-load day. This report is the technical documentation for the load composition analysis that was conducted to develop these non-industrial composite load models.

24 POWER TRANSMISSION AND DISTRIBUTION↗

Detecting forest structure and biomass with C-band multipolarization radar - Physical model and field tests

The ability of C-band radar (4.75 GHz) to discriminate features of forest structure, including biomass, is tested using a truck-mounted scatterometer for field tests on a 1.5-3.0 m pygmy forest of cypress (Cupressus pygmaea) and pine (Pinus contorta ssp, Bolanderi) near Mendocino, CA. In all, 31 structural variables of the forest are quantified at seven sites. Also measured was the backscatter from a life-sized physical model of the pygmy forest, composed of nine wooden trees with 'leafy branches' of sponge-wrapped dowels. This model enabled independent testing of the effects of stem, branch, and leafy branch biomass, branch angle, and moisture content on radar backscatter. Field results suggested that surface area of leaves played a greater role in leaf scattering properties than leaf biomass per se. Tree leaf area index was strongly correlated with vertically polarized power backscatter (r = 0.94; P less than 0.01). Field results suggested that the scattering role of leaf water is enhanced as leaf surface area per unit leaf mass increases; i.e., as the moist scattering surfaces become more dispersed. Fog condensate caused a measurable rise in forest backscatter, both from surface and internal rises in water content. Tree branch mass per unit area was highly correlated with cross-polarized backscatter in the field (r = 0.93; P less than 0.01), a result also seen in the physical model.

Westman, Walter E.↗