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At least 109 records · Page 6

Metalworking method for composites

Effective fabrication methods for aluminum/boron and aluminum/graphite composites have been investigated. Drawing and rolling were found to be adaptable to Al/B fabrication. Although graphite composites are not amenable to standard metal processing methods, it may be possible to reduce fabrication costs of Al/C through electron-beam heating.

Divecha, A. P.↗

Containerless processing of tungsten

Simultaneous electromagnetic levitation and electron-beam heating allow contaminationless melting of tungsten. Possible application for this technique is production of X-ray targets.

Beser, N.↗

Weldability of three forms of chemically vapor deposited tungsten

Methods were developed for electron-beam welding several forms of chemically vapor-deposited tungsten. Weld ductility was evaluated from the results of ductile-brittle transition-temperature determinations. Welds in tungsten produced from WF6 were considerably more ductile than those associated with WCl6-produced tungsten. The larger grain size of the latter material was largely responsible for this behavior.

Bryant, W. A.↗

Adding through-bolt holes to pin-fin cold plates

Spot-welding technique is less expensive than secondary-brazing and electron-beam methods. With procedure, standard plates can be modified in quantity for various mounting configurations without need for special tooling.

Ruppe, E. P.↗

Effects of high temperature and e-beam irradiation on the stability of refractory thin films

Refractory thin films of Al2O3, ZrO2, MgO, ThO2, and BN have been investigated in situ in an UHV transmission electron microscope. The electron transparent refractory films were prepared by electron-beam evaporation, anodization, RF sputtering, and thinning of bulk crystal materials. The study concentrates on monitoring the thermal and mechanical stability of the films, phase and structural changes, and electron irradiation effects as a function of film-preparation conditions. With increasing temperatures, five different crystallographic phases were observed for both anodized and electron-beam-evaporated alumina films. Zirconia films exhibited two phase transitions upon heating to 1200 C and electron-irradiation-induced crystallization of ZrO2 even at room temperature. MgO, ThO2, and BN films did not undergo any noticeable phase transformation but ruptured due to sintering below 1200 C.

Lee, E. H.↗

Calculation of electrostatic fields in periodic structures of complex shape

A universal algorithm is presented for calculating electrostatic fields in an infinite periodic structure consisting of electrodes of arbitrary shape which are located in mirror-symmetrical manner along the axis of electron-beam propagation. The method is based on the theory of R-functions, and the differential operators which are derived on the basis of the functions. Numerical results are presented and the accuracy of the results is examined.

Kravchenko, V. F.↗

Nondestructive determination of the depth of planar p-n junctions by scanning electron microscopy

A method was developed for measuring nondestructively the depth of planar p-n junctions in simple devices as well as in integrated-circuit structures with the electron-beam induced current (EBIC) by scanning parallel to the junction in a scanning electron microscope (SEM). The results were found to be in good agreement with those obtained by the commonly used destructive method of lapping at an angle to the junction and staining to reveal the junction.

Chi, J.-Y.↗

Adjusting an electron beam for drilling

Reticle contains two concentric circles: inner circle insures beam circularity and outer circle is guide to prevent beam from cutting workpiece clamp. Precise measurement of beam and clamp are required with old reticle. New reticle speeds up electron-beam drilling process by eliminating need to rotate eyepiece to make measurements against reticle scale.

Childress, C. L.↗

Welding multiple plies with an electron beam

Method for electron-beam welding of multi-ply metal sheets eliminates ply separation and minimizes porosity. Method was developed for assembling bellows made of four plies of iron/nickel alloy sheets. Method consists of making successive stitch welds with electron beam until weld seam is completely filled in and all plies have been penetrated.

Kiluk, F. J.↗

Space plasma laboratory - Experiment in simulated ionospheric plasma

Several experiments with simulated ionospheric plasma were performed in the Johnson Space Center's large (17 m diameter x 27 m height) vacuum chamber. Two of these, the RF discharge and the electron-beam plasma discharge, are described here. The RF experiment involved measurement of the loading on a 5 m dipole and a 5 m loop antenna caused by the presence of a plasma. The results indicate that when the RF frequency is near the electron gyro frequency a self-sustained plasma discharge is set up and the real part of the complex antenna impedance increases. The beam-plasma experiment was carried out to study a discharge produced by an electron beam with an energy of about 1 keV when the electron beam was injected parallel to the ambient magnetic field. As the beam current was raised to a critical level, a spontaneous transition occurred whereby a luminous halo was formed around the electron beam indicating a sustained discharge.

Konradi, A.↗

Electron scattering by highly polar molecules. II - LiF

The crossed electron-beam - molecular-beam scattering technique has been used to measure relative values of differential 'elastic' scattering cross sections at electron impact energies of 5.4 and 20 eV for the angular range from 20 to 130 deg. The absolute values of these cross sections have been obtained by normalization to the classical perturbation theory of Dickinson (1977) at a scattering angle of 40 deg. These differential cross sections have then been used to calculate the integral and momentum-transfer cross sections. An energy-loss spectrum at 100 eV electron impact energy and 15 deg scattering angle has also been obtained. Two weak features at the energy losses of 6.74 and 8.82 eV appear. Their energy positions are compared with the recent calculations of Kahn et al. (1974).

Vuskovic, L.↗

Radiation energy conversion in space

Topics discussed at the third NASA conference on radiant energy conversion are reviewed. The unconcentrated-photovoltaic-generation version of a solar power satellite is described, noting that it will consist of a 21.3 x 5.3-sq-km silicon-solar-cell array expected to provide 17 Gw of electrical power, with 1 km in diam transmitters oriented to beam 2.45 GHz microwave power to two receiving/rectifying 'rectennas' on earth. The Solares space-energy-system concept, designed for providing a large fraction of the world's energy needs at costs comparable to those of future coal/nuclear alternative, is considered, as are subsystems for improving the economics of the solar power satellite. A concept proposing the use of relativistic-electron-storage rings for electron-beam energy transmission and storage, and a report on the production of a high temperature plasma with concentrated solar radiation are taken into account. Laser-conversion systems, including the direct-solar-pumped space laser, and the telec-powered spacecraft, are discussed.

Billman, K. W.↗

A study of density measurements in hypersonic helium tunnels using an electron beam fluorescence technique

A series of experiments have been conducted at Langley Research Center to determine the feasibility of using electron-beam fluorescence to measure the free-stream static density of gaseous helium flow over a wide range of conditions. These experiments were conducted in the Langley hypersonic helium tunnel facility and its 3-inch prototype. Measurements were made for a range of stagnation pressures and temperatures and produced free-stream number densities of 1.53 x 10 to the 23rd to 1.25 x 10 to the 24th molecules/cu m and static temperatures from 2 K to 80 K. The results showed the collision quenching cross section to be 4.4 x 10 to the -15th sq cm at 1 K and to have a weak temperature dependence of T to the 1/6. With knowledge of these two values, the free-stream number density can be measured quite accurately.

Honaker, W. C.↗

Pulse-shaping circuit for laser excitation

Narrower, impedence-matched pulses initiate stabler electric discharges for gas lasers. Discharges are more efficient, more compact, capable of high repetition rate, and less expensive than conventional electron-beam apparatus, but gas tends to break down and form localized arcs. Pulse-shaping circuit compresses width of high-voltage pulses from relatively-slow rise-time voltage generator and gradually grades circuit impedance from inherent high impedance of generator to low impedence of gas.

Laudenslager, J. B.↗

An analytical approach to evaluation of space radiation effects on materials for long-life missions

An analytical model was developed which quantifies effects on organic composite matrix materials of high energy electrons and of UV as well as interactions between the two radiations. Literature data on polyethylene were used to construct a degradation kinetics scheme corresponding to an Earth orbit at L=3. Analysis of the model showed that steady state concentrations of radicals put limits on accelerated test conditions. These conclusions were validated by an experimental study on polymethylmethacrylate using UV laser excitation. Relationships for balancing electron and UV radiations to equal acceleration factors are derived. Pulse radiolysis using an electron-beam along with time-resolved spectroscopy is shown to be able to separate primary form secondary reactions. Implications of these reactions to changes in engineering material properties are indicated. The use of mechanistic studies is discussed in the context of general test strategies for evaluating materials for space applications.

Moacanin, J.↗

Impacts of Ionizing Radiation on Sulfur Chloride Compounds for Advanced Fuel Cladding Decontamination Processes

Tripling the nation’s nuclear energy capacity is a critical component for significantly increasing energy production and reducing energy costs for American families and businesses. Achieving this vision requires fuel cycle technologies that maximize resource utilization while minimizing radioactive waste generation. Advanced sulfur chloride–based chlorination technologies are being developed to enable efficient recycling of fuel cladding materials, which account for a significant fraction of used nuclear fuel. However, the impacts of ionizing radiation on the longevity and performance of these sulfur chloride compounds are not well established. Here, we will explore the effects of gamma and electron-beam irradiation on the chemical composition of select sulfur chloride reagents, specifically sulfur monochloride (S2Cl2) and thionyl chloride (SOCl2), and the impacts of pre-irradiation on the chlorination yield/chemical dissolution of surrogate aluminum alloy 6061 (AA6061-T6) materials.

38 - RADIATION CHEMISTRY, RADIOCHEMISTRY, AND NUCL↗

Tip-Induced 3D Printing on the Nanoscale with Field Emission Scanning Probes

3D printing down to the nanoscale remains a significant challenge. In this paper, the study explores the use of scanning probes that emit low-energy electrons (<100 eV) coupled with the localized injection and electron-induced decomposition of precursor molecules, for the precise localized deposition of 3D nanostructures. The experiments are performed inside the chamber of a scanning electron microscope (SEM), enabling the use of the in-built gas injector system (GIS) with gaseous naphthalene precursor for carbon deposition, as well as immediate inspection of the deposits by SEM. Substrate materials are planar fused silica with thin conductive coatings and non-planar copper wedges. After investigation of the deposition process parameters, various 2D and 3D carbon deposits are grown. Vertical nanowires several microns in length with a diameter <100 nm are achieved and 3D deposits with a high degree of nanoscale branching are also obtained, presumably due to a charging effect. High aspect ratio carbon nanostructures such as those demonstrated here can be employed as miniaturized electrodes or field emitters. The tip-based approach presented thus paves the way toward 3D nanoscale printing of various materials and functional nanostructures.

3D printing↗