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NASA NTRS2012

Laboratory Studies of Charging Properties of Dust Grains in Astrophysical/Planetary Environments

Dust grains in various astrophysical environments are generally charged electrostatically by photoelectric emissions with UV/X-ray radiation, as well as by electron/ion impact. Knowledge of physical and optical properties of individual dust grains is required for understanding of the physical and dynamical processes in space environments and the role of dust in formation of stellar and planetary systems. In this paper we focus on charging of individual micron/submicron dust grains by processes that include: (a) UV photoelectric emissions involving incident photon energies higher than the work function of the material and b) electron impact, where low energy electrons are scattered or stick to the dust grains, thereby charging the dust grains negatively, and at sufficiently high energies the incident electrons penetrate the grain leading to excitation and emission of electrons referred to as secondary electron emission (SEE). It is well accepted that the charging properties of individual micron/submicron size dust grains are expected to be substantially different from the bulk materials. However, no viable models for calculation of the charging properties of individual micron size dust grains are available at the present time. Therefore, the photoelectric yields, and secondary electron emission yields of micron-size dust grains have to be obtained by experimental methods. Currently, very limited experimental data are available for charging of individual micron-size dust grains. Our experimental results, obtained on individual, micron-size dust grains levitated in an electrodynamic balance facility (at NASA-MSFC), show that: (1) The measured photoelectric yields are substantially higher than the bulk values given in the literature and indicate a particle size dependence with larger particles having order-of-magnitude higher values than for submicron-size grains; (2) dust charging by low energy electron impact is a complex process. Also, our measurements indicate that the electron impact may lead to charging or discharging of dust grains depending upon the grain size, surface potential, electron energy, electron flux, grain composition, and configuration (e.g. Abbas et al, 2010). Laboratory measurements on charging of analogs of the interstellar dust as well as Apollo 11 dust grains conducted at the NASA-MSFC Dusty Plasma Lab. are presented here

Tankosic, D.↗

NASA NTRS1983

Angular distribution for electron excitation of the 4(2)S yields 4(2)P transition in Zn II - Comparison of experiment and theory

Differential electron-scattering cross sections for inelastic excitation of an ion have been measured for the first time. Experiments were carried out in a cross electron-ion beam geometry for the 4(2)S yields 4(2)P transition in Zn II at 75 eV. In addition, differential cross sections were calculated at energies between 15 and 100 eV in a five-state close-coupling approximation in which 4s, 4p, 3d(9)4s(2), 5s, and 4 d states were included. Agreement in shape between theory and experiment at 75 eV is excellent.

Chutjian, A.↗

NASA NTRS1977

Electron impact on atmospheric gases. II - Yield spectra

A concept yield spectrum is introduced and this two-dimensional function is calculated, using a modified discrete energy bin method for 50-eV to 10-keV incident electrons impacting on the gases Ar, H2, H2O, O2, N2, O, CO, CO2, and He. The yield spectrum is amenable to physical interpretation, accurate analytic representation, and convenient application to the determination of all types of yields needed in aeronomical problems.

Green, A. E. S.↗

NASA NTRS2001

Atmospheric Nitrogen Fluorescence Yield

Several existing and planned experiments estimate the energies of ultra-high energy cosmic rays from air showers using the atmospheric nitrogen fluorescence. The nitrogen fluorescence yield from air shower electrons depends on the atmospheric composition. We will discuss the uncertainties in the fluorescence yield form electrons in the real atmosphere and describe a concept for a small balloon payload to measure the atmospheric fluorescence yield as a function of attitude.

Adams, J. H., Jr.↗

NASA NTRS1977

Yield spectra and the continuous-slowing-down approximation

The continuous-slowing-down approximation (CSDA) and the modified discrete-energy-bin (MDEB) method are used to calculate a yield spectra U(E, E sub 0) of electrons with energy E resulting from a primary of energy E sub 0. The results of the two calculations are then compared. The MDEB method is found to produce consistently more ions per energy loss while at the same time producing less excitations of some of the low-lying states when compared with the CSDA. These discrepancies can be explained by studying the contributions from the individual generations of electrons to the yield spectra. An integral equation for the solution of the yield spectra is also presented.

Jackman, C. H.↗

NASA NTRS1982

The sputtering of insulating materials by fast heavy ions

In this paper recent experimental results on sputtering of UF4 and H2O (ice) by fast heavy ions are reviewed. Measurements have been made of the dependence of the sputtering yield on the incident ion type, charge state, and energy. In the case of UF4, the energy spectra of neutral sputtered particles have been obtained as well. There is a clear dependence of the sputtering yield on the electronic part of the stopping power, and the yield is strongly affected by the charge state of the incident ion, which shows that in the near-surface region from which sputtered particles arise, the charge state of the incident ion has not reached equilibrium. The shape of the energy spectra observed for UF4 targets is that expected from a thermal distribution rather than that of the collision cascade form typical of ordinary sputtering. A model of the sputtering-track registration process that has arisen from these data is shown to provide a framework of understanding the close relationship of these observations to the 'plasma desorption' of marcromolecules.

Seiberling, L. E.↗

NASA NTRS1998

Recent Results from a Laboratory Study of Charging Mechanisms in a Dusty Plasma

A laboratory investigation has been developed to experimentally study the interaction of micron sized particles with plasmas and electromagnetic radiation. The intent is to investigate under what conditions particles of various compositions and sizes become charged, or discharged, while exposed to an electron beam and UV radiation. This investigation uses a unique laboratory technique known as electrodynamic suspension of particles. Here, a single charged micron size particle is suspended in a quadrupole trap and then subjected to a controlled environment. In this paper, we will discuss recent results from this experiment in which different materials including polystyrene and aluminum oxide, and sizes ranging from 10 microns to 1 micron have been used to determine charge to mass ratios and then subjected to an electron beam and /or UV radiation. In each instance, the particle's charge as well as beam current flux and radiation intensity flux is measured. These results will be compared with initial results using salt crystals. It was found that a negatively charged salt crystal exposed for 30 minutes to a 500 eV electron beam with primary electron beam current of -3.06 x 10(exp -5) picoamps yielded a secondary electron current of 3.23 x 10(exp -5) picoamps. Additionally, the particle was observed to be steadily losing charge over this time interval. By studying the microphysics of one particle, a better understanding of theoretical models and other laboratory results associated with particle charging mechanisms can be achieved.

Venturini, Catherine C.↗

NASA NTRS1969

Primary radical yields in pulse irradiated alkaline aqueous solution

Primary radical yields of hydrated electrons, H atoms, and OH radicals are determined by measuring hydrated electron formation following a 4 microsecond pulse of X rays. The pH dependence of free radical yields beyond pH 12 is determined by observation of the hydrated electrons.

Fielden, E. M.↗

NASA NTRS1983

Sputtering of silicon and its compounds in the electronic stopping region

Silicon, silicon dioxide, and silicon nitride have been sputtered with chlorine ions at 5 MeV and 20 MeV. While the yield from the silicon target was unmeasurably low, the insulating compounds exhibited the enhanced yields observed in other insulating targets. The yield follows the electronic stopping power and seems to be independent of the target's thermal properties. Some of the data suggest that the enhanced sputtering mechanism may be active in extremely thin films (not less than 3 monolayers).

Qiu, Y.↗

NASA NTRS1976

Measurement of the 13 to 100 eV electron impact excitation cross section for the X 1Sigma /+/-g yields a 1Pi-g transition in N2

An inelastic scattering technique was used to measure the electron impact excitation cross section for the X 1Sigma (+)-g yields a 1Pi-g transition in N2 in the energy range 13 to 100 eV. The relative excitation cross section was calculated by integration of the relative differential scattering cross sections at various energies and the relative values of the excitation cross section were put on an absolute scale by comparing the relative cross sections to those for excitation of the X 1Sigma (+)-g yields C 3Pi-u transition and those of the electron impact optical emission cross section for the C 3Pi-u yields B 3Pi-g transition as a secondary standard. The excitation cross section was found to vary from a maximum value of 3.6 x 10 to the -17 cu cm between 15 and 18 eV to 5.2 x 10 to the -18 cu cm at 100 eV.

Finn, T. G.↗

NASA NTRS2015

New Insights on Subsurface Imaging of Carbon Nanotubes in Polymer Composites via Scanning Electron Microscopy

Despite many studies of subsurface imaging of carbon nanotube (CNT)-polymer composites via scanning electron microscopy (SEM), significant controversy exists concerning the imaging depth and contrast mechanisms. We studied CNT-polyimide composites and, by threedimensional reconstructions of captured stereo-pair images, determined that the maximum SEM imaging depth was typically hundreds of nanometers. The contrast mechanisms were investigated over a broad range of beam accelerating voltages from 0.3 to 30 kV, and ascribed to modulation by embedded CNTs of the effective secondary electron (SE) emission yield at the polymer surface. This modulation of the SE yield is due to non-uniform surface potential distribution resulting from current flows due to leakage and electron beam induced current. The importance of an external electric field on SEM subsurface imaging was also demonstrated. The insights gained from this study can be generally applied to SEM nondestructive subsurface imaging of conducting nanostructures embedded in dielectric matrices such as graphene-polymer composites, silicon-based single electron transistors, high resolution SEM overlay metrology or e-beam lithography, and have significant implications in nanotechnology.

Zhao, Minhua↗

NASA NTRS1981

Discrepancies between theoretical and empirical models of the flaring solar chromosphere and their possible resolution

Possible sources of pronounced discrepancy between empirical and theoretical models of the solar chromosphere during flares are discussed. It is noted that a principal source of uncertainty in empirical models is the inhomogeneity of the spectral data on which they are based. With theoretical models, probably the most important source of error is neglect of the radiative coupling of upper and lower chromospheric regions. A new procedure for studying flare energy input is suggested wherein the required input is derived from the empirical model chromosphere. This procedure is applied to the electron-heated case, and it is found that the integral equation defining the flare energy deposition rate can be inverted analytically to yield the injected electron flux energy spectrum from knowledge of the energy balance in the empirical atmosphere. Recent empirical model results are analyzed in this manner, and the calculated injected electron flux spectrum is compared with that needed for hard X-ray bursts in moderately large flares.

Emslie, A. G.↗

NASA NTRS1987

Methods and first results of plasma non-isothermal parameters measurements in meteor trails

There is no reliable experimental evidence so far of either the presence or absence of nonisothermal effects in newly formed meteor trails. Neither is there a common opinion on the most effective mechanism of electron cooling. According to the laboratory experimental data collisions of atomic and molecular particles of all kinds having velocities of 10 to 70/kms often yields 1 eV electrons and not infrequently some have energies reaching several electron volts. These highest energy electrons are referred to as superhot electrons. The method of measurement and the results of these measurements in meteor trails are discussed.

Kostylev, K. K.↗

NASA NTRS1979

Two-potential approach for electron-molecular collisions at intermediate and high energies - Application to e-N2 scatterings

A general theoretical approach is proposed for the calculation of elastic, vibrational, and rotational transitions for electron-molecule scattering at intermediate and high-electron-impact energies. In this formulation, contributions to the scattering process come from the incoherent sum of two dominant potentials: a short-range shielded nuclear Coulomb potential from individual atomic centers, and a permanent/induced long-range potential. Application to e-N2 scattering from 50-500 eV incident electron energies has yielded good agreement with absolutely calibrated experiments. Comparisons with other theoretical approaches are made. The physical picture as well as the general features of electron-molecule scattering process are discussed within the framework of the two-potential approach.

Choi, B. H.↗

NASA NTRS1984

Far Infrared Spectroscopy of (O III) in M82

Emission lines at 52 and 88 micron from O III in the galaxy M82 were observed with the cooled grating spectrometer aboard the Kuiper Airborne Observatory. Raw spectra were corrected for telluric water vapor absorption, instrument response function, and relative detector response by ratioing to a spectrum of Saturn or Mars taken on the same flight. An average electron density Pn regions where oxygen is doubly ionized was derived. The electron density calculated for M 82 is significantly lower than those found in the galaxy using the same method. Results suggest that observations of the galaxy made from a great distance would yield a higher electron density than observed in M82.

Duffy, P.↗

NASA NTRS2008

Andreyivanovite: A Second New Phosphide from the Kaidun Meteorite

Andreyivanovite (ideally FeCrP) is another new phosphide species from the Kaidun meteorite, which fell in South Yemen in 1980. Kaidun is a unique breccia containing an unprecedented variety of fragments of different chondritic as well as achondritic lithologies. Andreyivanovite was found as individual grains and linear arrays of grains with a maximum dimension of 8 m within two masses of Fe-rich serpentine. In one sample it is associated with Fe-Ni-Cr sulfides and florenskyite (FeTiP). Andreyivanovite is creamy white in reflected light, and its luster is metallic. The average of nine electron microprobe analyses yielded the formula Fe(Cr0.587 Fe0.150 V0.109 Ti0.081 Ni0.060 Co0.002)P. Examination of single grains of andreyivanovite using Laue patterns collected by in-situ synchrotron X-ray diffraction (XRD), and by electron backscattered diffraction revealed that it is isostructural with florenskyite; we were unable to find single crystals of sufficient quality to perform a complete structure analysis. Andreyivanovite crystallizes in the space group Pnma, and has the anti-PbCl2 structure. Previously-determined cell constants of synthetic material [a = 5.833(1), b = 3.569(1), c = 6.658(1) A] were consistent with our XRD work. We used the XPOW program to calculate a powder XRD pattern; the 5 most intense reflections are d = 2.247 (I = 100), 2.074 (81), 2.258 (46), 1.785 (43), and 1.885 A (34). Andreyivanovite is the second new phosphide to be described from the Kaidun meteorite. Andreyivanovite could have formed as a result of cooling and crystallization of a melted precursor consisting mainly of Fe-Ni metal enriched in P, Ti, and Cr. Serpentine associated with andreyivanovite would then have formed during aqueous alteration on the parent asteroid. It is also possible that the andreyivanovite could have formed during aqueous alteration, however, artificial FeTiP has been synthesized only during melting experiments, at low oxygen fugacity, and there is no evidence that a hydrothermal genesis is reasonable.

Zolensky, Michael↗

NASA NTRS2010

Investigation of a Gallium MPD Thruster with an Ablating Cathode

Arc impedance, exhaust velocity, and plasma probe measurements are presented. The thruster is driven by a 50 microsecond pulse from a 6.2 milliohm pulse forming network, and gallium is supplied to the discharge by evaporation of the cathode. The arc voltage is found to vary linearly with the discharge current with an arc impedance of 6.5 milliohms. Electrostatic probes yield an exhaust velocity that is invariant with the discharge current and has a peak value of 20 kilometers per second, which is in reasonable agreement with the value (16 plus or minus 1 kilometer per second) calculated from the mass bit and discharge current data. Triple probe measurements yield on axis electron temperatures in the range of 0.8-3.8 eV, electron densities in the range of 1.6 x 10(exp 21) to 2.1 x 10(exp 22) per cubic meter, and a divergence half angle of 16 degrees. Measurements within the interelectrode region yield a peak magnetic field of 0.8 T, and the observed radial trends are consistent with an azimuthally symmetric current distribution. A cathode power balance model is coupled with an ablative heat conduction model predicting mass bit values that are within 20% of the experimental values.

Thomas, Robert E.↗

NASA NTRS1994

Unusual satellite-electron signature within the Uranian magnetosphere and its implications regarding whistler electron loss processes

It has been reported that during the outbound (nightside) portion of the Voyager 2 encounter with the Uranian magnetosphere, intense whistler mode emissions were observed near the magnetic equator (lambda(sub m) approx. 16 deg) and at L shell values between approx. 5.5 and approx. 9 R(sub U). Comprehensive calculations of whistler-driven pitch angle diffusion, in previous work, have yielded strong diffusion electron lifetimes of approx. 1 hour for 20 to 40 keV electrons. In this paper we report on an unusual and sharply defined charged particle feature that: (1) involved electrons between 22 and 35 keV, (2) was observed during the time period of the intense whistler mode observations, (3) was aligned very accurately and sharply with the minimum L shell position (L approx. 7.5) of the satellite Ariel, and (4) has an appearance that suggests that electrons were removed only at and beyond Ariel's minimum-L. On the basis of our conclusion that the signature was caused by electron interactions with either Ariel or materials distributed along Ariel's orbit, the signature could not have been generated for at least 10 hours prior to its observation. Thus the calculated whistler loss times are in apparent conflict with the signature observation. A scenario of events is proposed to explain the data that involves substormlike electron acceleration on the Uranian nightside and a subsequent sculpting of the electron spatial distributions via interactions with Ariel or materials distributed along Ariel's orbit. The possibility exists that the accurate alignment of the sharp electron feature with Ariel's minimum-L, and the absorptionlike character of the feature, are accidental, and that the feature is caused by dynamical processes (e.g., substorms). In this case the dynamical processes must be quite dissimilar to those occurring in the Earth's magnetosphere.

Mauk, B. H.↗