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At least 109 records · Page 6

Particle size distributions in Saturn's rings from Voyager 1 radio occultation

Information on Saturn ring particle sizes obtained with the Voyager 1 ring occultation experiment is discussed. The theory underlying the determination of the particle size distribution is presented, including differential extinction and inversion of the scattered signal. Experimental observations and results for the observed spectra, differential cross sections, suprameter and sub- to suprameter size distributions are presented. The size and mass distributions both cut off sharply at about 4-5 m; the mass distribution peaks over the 3-4 m size range for four ring system features at 1.35, 1.51, 2.01, and 2.12 Saturn radii. A power-law type model is consistent with the data over a limited size range of 0.01 to 1 m. The fractional contribution of the suprameter particles to the microwave opacity for the four features appears to be about 1/3, 1/3, 2/3, and 1, respectively, and their cumulative surface mass per unit area are about 11, 16, 41, and 132 g/sq cm if the particles are solid water ice.

Marouf, E. A.↗

Turbulent Concentration of MM-Size Particles in the Protoplanetary Nebula: Scaled-Dependent Multiplier Functions

The initial accretion of primitive bodies (asteroids and TNOs) from freely-floating nebula particles remains problematic. Here we focus on the asteroids where constituent particle (read "chondrule") sizes are observationally known; similar arguments will hold for TNOs, but the constituent particles in those regions will be smaller, or will be fluffy aggregates, and are unobserved. Traditional growth-bysticking models encounter a formidable "meter-size barrier" [1] (or even a mm-cm-size barrier [2]) in turbulent nebulae, while nonturbulent nebulae form large asteroids too quickly to explain long spreads in formation times, or the dearth of melted asteroids [3]. Even if growth by sticking could somehow breach the meter size barrier, other obstacles are encountered through the 1-10km size range [4]. Another clue regarding planetesimal formation is an apparent 100km diameter peak in the pre-depletion, pre-erosion mass distribution of asteroids [5]; scenarios leading directly from independent nebula particulates to this size, which avoid the problematic m-km size range, could be called "leapfrog" scenarios [6-8]. The leapfrog scenario we have studied in detail involves formation of dense clumps of aerodynamically selected, typically mm-size particles in turbulence, which can under certain conditions shrink inexorably on 100-1000 orbit timescales and form 10-100km diameter sandpile planetesimals. The typical sizes of planetesimals and the rate of their formation [7,8] are determined by a statistical model with properties inferred from large numerical simulations of turbulence [9]. Nebula turbulence can be described by its Reynolds number Re = L/eta sup(4/3), where L = ETA alpha sup (1/2) the largest eddy scale, H is the nebula gas vertical scale height, and α the nebula turbulent viscosity parameter, and η is the Kolmogorov or smallest scale in turbulence (typically about 1km), with eddy turnover time tη. In the nebula, Re is far larger than any numerical simulation can handle, so some physical model is needed to extend the results of numerical simulations to nebula conditions.

protoplanetary nebula↗

Particle sizing in rocket motor studies utilizing hologram image processing

A technique of obtaining particle size information from holograms of combustion products is described. The holograms are obtained with a pulsed ruby laser through windows in a combustion chamber. The reconstruction is done with a krypton laser with the real image being viewed through a microscope. The particle size information is measured with a Quantimet 720 image processing system which can discriminate various features and perform measurements of the portions of interest in the image. Various problems that arise in the technique are discussed, especially those that are a consequence of the speckle due to the diffuse illumination used in the recording process.

Netzer, David↗

Mineralogical, optical, geochemical, and particle size properties of four sediment samples for optical physics research

X-ray diffraction and spectroscopy were used to investigate the mineralogical and chemical properties of the Calvert, Ball Old Mine, Ball Martin, and Jordan Sediments. The particle size distribution and index of refraction of each sample were determined. The samples are composed primarily of quartz, kaolinite, and illite. The clay minerals are most abundant in the finer particle size fractions. The chemical properties of the four samples are similar. The Calvert sample is most notably different in that it contains a relatively high amount of iron. The dominant particle size fraction in each sample is silt, with lesser amounts of clay and sand. The indices of refraction of the sediments are the same with the exception of the Calvert sample which has a slightly higher value.

Bice, K.↗

Particle size distributions and the vertical distribution of suspended matter in the upwelling region off Oregon

Various methods of presenting and mathematically describing particle size distribution are explained and evaluated. The hyperbolic distribution is found to be the most practical but the more complex characteristic vector analysis is the most sensitive to changes in the shape of the particle size distributions. A method for determining onshore-offshore flow patterns from the distribution of particulates was presented. A numerical model of the vertical structure of two size classes of particles was developed. The results show a close similarity to the observed distributions but overestimate the particle concentration by forty percent. This was attributed to ignoring grazing by zooplankton. Sensivity analyses showed the size preference was most responsive to the maximum specific growth rates and nutrient half saturation constants. The verical structure was highly dependent on the eddy diffusivity followed closely by the growth terms.

Kitchen, J. C.↗

Commercial aluminum powders, Part I: Particle size characterization and slow heating rate thermal analysis.

We characterized nine commercial aluminum (Al) powders using several methods to measure particle characteristics and thermal analysis, with the goal to understand how these parameters influence energy release. Although it is well-known that lot-to-lot variations in commercial nanoparticles are common, the Al powders were more heterogeneous than anticipated – both with regards to particle size distributions and impurities. Manufacturer specifications – often quoted in the literature without confirmation – were not always accurate for the specific sample lots we investigated. In several cases, different conclusions could be drawn from individual particle size techniques; a combination of multiple techniques provides a clearer picture of the powder properties. Thorough characterization of Al powders is required prior to interpretation of experimental results from a variety of applications. In particular, previous studies have shown contradictory results on the influence of Al on detonation performance, perhaps partially due to insufficient characterization of the Al powders themselves.

36 MATERIALS SCIENCE↗

Response characteristics of laser diffraction particle size analyzers - Optical sample volume extent and lens effects

The response characteristics of laser diffraction particle sizing instruments were studied theoretically and experimentally. In particular, the extent of optical sample volume and the effects of receiving lens properties were investigated in detail. The experimental work was performed with a particle size analyzer using a calibration reticle containing a two-dimensional array of opaque circular disks on a glass substrate. The calibration slide simulated the forward-scattering characteristics of a Rosin-Rammler droplet size distribution. The reticle was analyzed with collection lenses of 63 mm, 100 mm, and 300 mm focal lengths using scattering inversion software that determined best-fit Rosin-Rammler size distribution parameters. The data differed from the predicted response for the reticle by about 10 percent. A set of calibration factor for the detector elements was determined that corrected for the nonideal response of the instrument. The response of the instrument was also measured as a function of reticle position, and the results confirmed a theoretical optical sample volume model presented here.

Hirleman, E. D.↗

Particle size, number, composition and velocity from solid rocket motors

The damage potentials to the space shuttle orbiter caused by the high velocity particles contained in the exhaust plume of an upper stage is discussed. In particular, the particle size distribution and composition, the velocity of the particles and the expected contribution from shuttle launched upper stages are addressed. Particle size estimates based on historical data are compapred with those derived from upper stage motor performance testing. The particle velocities as determined by the best available plume computational technique are presented. The shuttle is scheduled to launch approximately 135 upper-stages over its lifetime looking at the currently scheduled flights and averaging over a yearly basis yields the contribution of particulates from the uper-stages. On the average, 91,645 llbs of Al2O3 will be ejected on each launch. The analysis to determine how much of this 91,645 lbs will remain in orbit or the decay rate is yet to be accomplished.

Roberts, B. B.↗

Pinhole Calibrator For Particle-Sizing Instrument

Rotating-pinhole calibrator designed for use in calibrating and testing optical instrument measuring sizes of cloud droplets, dust particles, and other small particles suspended in flowing air. Easily attachable to particle-size-measuring instrument and suitable for both quick verification of calibration in field and detailed calibration studies in laboratory. Calibrator used to determine such operating parameters of instrument as optical collection angles, depth of field, profile of laser beam used to measure particles, and response to trajectory of particle. Also used to align instrument. Pinhole reused any number of times without risk of variation in diffraction pattern. Furthermore, size of pinhole chosen precisely and at will.

Hovenac, Edward↗

Wet-chemical synthesis of Li7P3S11 with tailored particle size for solid state electrolytes

The small-size solid-state electrodes (SSEs) with high Li+ conductivity play an important role in reducing the interfacial resistance between electrode materials and SSEs and defects between SSEs. As one of the most conductive sulfide based ionic conductors, scalable synthesis of Li7P3S11 with controllable particle sizes is highly desired but rarely reported. Here, we report a facile wet-chemical synthesis method to prepare Li7P3S11 SSEs with variable sizes for all-solid-state lithium batteries (ASSLBs). By fully dissolving 70Li2S-30P2S5 precursors in ethyl acetate solution, the particle size of Li7P3S11 can be manipulated into as small as ~110 nm and high Li+ conductivity of 1.05 mS cm-1 can be achieved. A systematical mechanistic study of solvent effects suggests that the controlled particle sizes are attributed to the excellent solvability and low binding energy of ethyl acetate solvent toward solutes. Moreover, this generic method can be extended to the facilely synthesis of Li3PS4 nanoparticles with an average size of ~200 nm and high Li+ conductivity of 0.1 mS cm-1.

Zhou, Jianbin↗

Understanding the Global Three-Dimensional Distribution of Precipitation Mean Particle Size with the Global Precipitation Measurement Mission

This study addresses the global distribution of precipitation mean particle size using data from the Global Precipitation Measurement (GPM) mission. The mass-weighted mean diameter Dm is a characteristic parameter of the precipitation particle size distribution (PSD), estimated from the GPM Combined Radar–Radiometer Algorithm (CORRA) using data from GPM’s dual-frequency precipitation radar and microwave imager. We examine Dm in individual precipitation systems in different climate regimes and investigate a 6-yr (2014–20) global climatology within 70°N–70°S. The vertical structure of Dm is demonstrated with cases of deep convection, frontal rain and snow, and stratocumulus light rain. The Dm values, detectable by GPM, range from ~0.7 mm in stratocumulus precipitation to >3.5 mm in the ice layers of intense convection. Within the constraint of the 12-dBZ detectability threshold, the smallest annual mean Dm (~0.8 mm) are found in the eastern oceans, and the largest values (~2 mm) occur above the melting levels in convection over land in summer. The standard deviation of the annual mean is generally <0.45 mm below 6 km. Climate regimes are characterized with Dm annual/seasonal variations, its convective/stratiform components, and vertical variabilities (2–10 km). The U.S. Central Plains and Argentina are associated with the largest Dm in a deep layer. Tropical Africa has larger Dm and standard deviation than Amazon. Large convective Dm occurs at high latitudes of Eurasia and North America in summer; the Southern Hemisphere high latitudes have shallower systems with smaller Dm. Oceanic storm tracks in both hemispheres have relatively large Dm, particularly for convective Dm in winter. Relatively small Dm occurs over tropical oceans, including ITCZ, requiring further investigation.

Mei Han↗

Estimation of particle size based on LDV measurements in a de-accelerating flow field

The accuracy of velocity measurements made with a laser velocimeter is strongly dependent upon the response of the seeding particles to the dynamics of the flow field. The smaller the particle the better the response to flow fluctuations and gradients and therefore the more accurate velocity measurement. In direct conflict is the requirement of light scattering efficiency to obtain signals with the laser velocimeter which, in general, is better as the particle size is increased. In low speed flow fields these two requirements on particle size overlap and accurate measurements may be obtained. However in high speed flows, where the velocity gradients may be severe, very small particles are required to maintain sufficient dynamic response characteristics to follow the flow. Therefore if velocity measurements are to be made in these flows, the laser velocimeter must be designed with sufficient sensitivity to obtain signals from these small particles. An insitu determination of the size distribution of kaolin particles (Al2O3, .2 + or - SiO2 . 2H2O) in the 16-foot Transonic Tunnel and the sensitivity characteristics of the laser velocimeter system is described.

Meyers, J. F.↗

A Study of Cirrus Ice Particle Size Distribution Using TC4 Observations

An analysis of two days of in situ observations of ice particle size spectra, in convectively generated cirrus, obtained during NASA s Tropical Composition, Cloud, and Climate Coupling (TC4) mission is presented. The observed spectra are examined for their fit to the exponential, gamma, and lognormal function distributions. Characteristic particle size and concentration density scales are determined using two (for the exponential) or three (for the gamma and lognormal functions) moments of the spectra. It is shown that transformed exponential, gamma, and lognormal distributions should collapse onto standard curves. An examination of the transformed spectra, and of deviations of the transformed spectra from the standard curves, shows that the lognormal function provides a better fit to the observed spectra.

Tian, Lin↗

Effect of particle size on fracture toughness of SiC/Al composite material

Discontinuous SiC/Al composites with SiC particles of different sizes were fabricated in order to study the role of particle size on the fracture process. The fracture process is confined to a very narrow band and takes place within the matrix in composites containing small SiC particle sizes. In the composite reinforced with SiC particles of 20 microns and above fracture of SiC begins to dominate. The matrix is influenced by the high density of dislocations generated at SiC/Al interfaces due to the difference in coefficient of thermal expansion between SiC and the Al matrix. Crack initiation fracture toughness does not depend on SiC particle size. Crack growth fracture toughness increases as the size of the SiC particle increase.

Flom, Y.↗