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Search indexed NASA NTRS and DOE OSTI research on propulsion, heat transfer, battery materials and energy systems. Follow report and document links to the original sources.

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At least 109 records · Page 6
All sourcesNASA NTRSDOE OSTI
DOE OSTI2024

Carbon Ore-Derived Critical Materials for Clean Energy Technologies

Conference presentation at American Institute of Chemical Engineers (AIChE) Annual Meeting, San Diego, California, October 27–31, 2024. Trends in the manufacture of electric vehicles that use graphite-based LIBs are rising steeply in the United States and globally, but the U.S. domestic supply chains for graphite, the largest component in an LIB by mass, is severely limited and faces complicated geopolitical dynamics with foreign sources. Consequently, the United States has designated graphite as a critical mineral to focus attention and resources to develop technologies to meet the challenge of limited domestic graphite supply chains. Results obtained so far based on the UCOP process have successfully validated the technology at the laboratory scale, with the produced graphite material showing up to 95% degree of graphitization, high carbon purity of ~99.98%, residual ash content of ≤0.02%, negligible moisture, low trace elements, and high electrochemical stability. These results suggest that the emerging UCOP technology is a promising approach to effectively synthesize high-quality graphite from abundant coal and coal waste resources in the United States to create a sustainable domestic critical graphite supply chain. A brief description of the status of UCOP process development and representative results will be presented.

01 COAL, LIGNITE, AND PEAT↗
DOE OSTI2026

Carbon ore, rare earth, and critical minerals (core-cm) assessment of san juan and raton coal basins: what is the future potential of coal in the san juan and raton basins, new mexico and colorado

This report summarizes results from the CORE-CM project in the San Juan and Raton basins of New Mexico and Colorado and ultimately begins to address what is the future of coal in the San Juan and Raton basins. The objective of this project was to determine the nonfuel carbon-based products (CBP), critical minerals, and rare earth elements (REE) potential in coal and related stratigraphic units in the San Juan and Raton basins and adjacent areas. This project delineated favorable geologic terrains and priority areas containing potential CBP, critical minerals, and REE deposits for the DOE mandate, which also is a priority of the NMBGMR and state of New Mexico. This project is important to the state because CBP, critical minerals, and REE resources must be identified before land use decisions are made by government officials. Future mining of CBP, critical minerals, and REE will directly benefit the economy of New Mexico. Furthermore, it is crucial to re-establish a domestic source of critical minerals and REE in the U.S. to help secure the nation’s clean energy future, to reduce the vulnerability of the U.S. to material shortages related to national defense, and to maintain our global technical and economic competitiveness. In addition to these benefits, students at New Mexico Institute of Mining and Technology (NMT) and San

01 COAL, LIGNITE, AND PEAT↗
DOE OSTI2021

Beneficiation of Bastnaesite Ore with New Flotation Collector Ligands

Interest in Rare Earth Elements (REEs) has increased due to their distinct properties and new applications. China currently has a monopoly on rare earth production due to the lack of an economically viable process used outside of China. Bastnaesite, a rare earth fluorocarbonate, is one of the most common minerals containing REEs, which is mostly comprised of cerium and other light REEs. The objective of this research is to find a novel collector for the beneficiation of bastnaesite through froth flotation experiments to increase the grade and recovery of rare earth oxides while rejecting the major gangue minerals. Microflotation and rougher bench flotation studies were evaluated to find optimal collector(s) from 19 possible candidates. Collectors 2, 5, and 8 were the top performing collectors chosen from microflotation experiments. A design of experiment matrix was set up to evaluate the variables, variable interactions, and provide a reference matrix for future optimization studies. Collector 2 was assessed to be the optimal collector. A rougher flotation experiment produced a rare earth oxide grade and recovery of 41% and 78%, respectively with a 91.5% rejection of calcite. Collector 8 and 14 also showed promising results to replace fatty acid. As such, this patent pending technology can serve to provide a pathway for efficient domestic REE production.

36 MATERIALS SCIENCE↗
DOE OSTI2021

Recovery of Rare Earth Oxides from Flotation Concentrates of Bastnaesite Ore by Ultra-Fine Centrifugal Concentration

Historically, the ability to effectively separate carbonate gangue from bastnaesite via flotation has frequently proven to be challenging without sacrificing significant rare earth oxide (REO) grade or recovery. However, in light of the fact that the rare earth bearing minerals often exhibit higher specific gravities than the carbonate gangue, the possibility exists that the use of gravity separation could be used to achieve such a selective separation. This however is complicated by the fact that, in cases such as this study when the liberation size is finer than 50 microns, most traditional gravity separation methods become increasingly challenging. The aim of this study is to determine the applicability of centrifugal concentrators to beneficiate ultra-fine (UF) bastnaesite and calcite bearing flotation concentrates. By using a UF Falcon, it was possible to achieve initial gravity REO recoveries exceeding 90% while rejecting on the order of 25% to 35% of the total calcium from an assortment of rougher and cleaner flotation concentrates. Additionally, when additional stages of cleaner UF Falcon gravity separation were operated in an open circuit configuration, it was possible, from an original fine feed of 35 microns containing 50.5% REO and 5.5% Ca, to upgrade up to approximately 59% REO and 2.0% calcium. While not the goal of this study, these results also support previous limited data to suggest that UF Falcons are potentially capable of treating a wider range of materials than they were originally designed for, including feeds rich in heavy mineral content.

Norgren, Alex↗
DOE OSTI2021

Ultra-Fine Centrifugal Concentration of Bastnaesite Ore

Historically, the ability to effectively separate carbonate gangue from bastnaesite via flotation has frequently proven to be challenging without sacrificing significant rare earth oxide (REO) grade or recovery. However, in light of the fact that the rare earth bearing minerals often exhibit higher specific gravities than the carbonate gangue, the possibility exists that the use of gravity separation could be used to achieve such a selective separation. This however is complicated by the fact that, in cases such as this study when the liberation size is finer than 50 µm, most traditional gravity separation methods become increasingly challenging. The purposes of this study is to determine the applicability of gravity concentrators to beneficiate bastnaesite from deleterious calcite bearing flotation feed material. Via the use of a UF Falcon, it was possible to achieve rougher gravity REO recoveries approaching the upper 80% range while rejecting on the order of 30% of the total calcium. In terms of purely REO recovery, this represents a significant improvement over results obtained via a traditional Falcon in previously reported studies.

36 MATERIALS SCIENCE↗
DOE OSTI2022

On a Unified Core Characterization Methodology to Support the Systematic Assessment of Rare Earth Elements and Critical Minerals Bearing Unconventional Carbon Ores and Sedimentary Strata

A significant gap exists in our understanding and ability to predict the spatial occurrence and extent of rare earth elements (REE) and certain critical minerals (CM) in sedimentary strata. This is largely due to a lack of existing, systematic, and well-distributed REE and CM samples and analyses in United States sedimentary basins. In addition, the type of sampling and characterization performed to date has generally lacked the resolution and approach required to constrain geologic and geographic heterogeneities typical of subsurface, mineral resources. Here, we describe a robust and systematic method for collecting core scale characterization data that can be applied to studies on the contextual and spatial attributes, the geologic history, and lithostratigraphy of sedimentary basins. The methods were developed using drilled cores from coal bearing sedimentary strata in the Powder River Basin, Wyoming (PRB). The goal of this effort is to create a unified core characterization methodology to guide systematic collection of key data to achieve a foundation of spatially and geologically constrained REEs and CMs. This guidance covers a range of measurement types and methods that are each useful either individually or in combination to support characterization and delineation of REE and CM occurrences. The methods herein, whether used in part or in full, establish a framework to guide consistent acquisition of geological, geochemical, and geospatial datasets that are key to assessing and validating REE and CM occurrences from geologic sources to support future exploration, assessment, and techno-economic related models and analyses.

54 ENVIRONMENTAL SCIENCES↗
NASA NTRS1973

Ratio maps of iron ore deposits Atlantic City district, Wyoming

Preliminary results of a spectral rationing technique are shown for a region at the southern end of the Wind River Range, Wyoming. Digital ratio graymaps and analog ratio images have been produced for the test site, but ground truth is not yet available for thorough interpretation of these products. ERTS analog ratio images were found generally better than either ERTS single-channel images or high altitude aerial photos for the discrimination of vegetation from non-vegetation in the test site region. Some linear geological features smaller than the ERTS spatial resolution are seen as well in ERTS ratio and single-channel images as in high altitude aerial photography. Geochemical information appears to be extractable from ERTS data. Good preliminary quantitative agreement between ERTS-derived ratios and laboratory-derived reflectance ratios of rocks and minerals encourage plans to use lab data as training sets for a simple ratio gating logic approach to automatic recognition maps.

Vincent, R. K.↗
NASA NTRS1973

Relation of ERTS-1 detected geologic structure to known economic ore deposits

A preliminary analysis of ERTS-1 imagery of the Northern Coast Ranges and Sacramento Valley, California, has disclosed a potentially important fracture system which may be one of the controlling factors in the location of known mercury deposits in the Coast Ranges and which appears to be associated with some of the oil and gas fields within the Sacramento Valley. Recognition of this fracture system may prove to be an extremely useful exploration tool, hence careful analysis of subsequent ERTS imagery might delineate areas for field evaluation.

Rich, E. I.↗
NASA NTRS1974

Heat Transfer and Fluid Mechanics Institute, 24th, Oregon State University, Corvallis, Ore., June 12-14, 1974, Proceedings

Recent theoretical and experimental studies in heat transfer and fluid mechanics, including some environmental protection investigations, are presented in a number of papers. Some of the topics covered include condensation heat transfer, a model of turbulent momentum and heat transfer at points of separation and reattachment, an explicit scheme for calculations of confined turbulent flows with heat transfer, heat transfer effects on a delta wing in subsonic flow, fluid mechanics of ocean outfalls, thermal plumes from industrial cooling water, a photochemical air pollution model for the Los Angeles air basin, and a turbulence model of diurnal variations in the planetary boundary layer. Individual items are announced in this issue.

Davis, L. R.↗
NASA NTRS1975

Investigation of LANDSAT imagery on correlations between ore deposits and major shield structures in Finland

The author has identified the following significant results. On the central Baltic Shield, the concept of drainage patterns can be extended to smaller scales in which case many cultural features become involved to the spatial patterns influenced by bedrock structure. Features resulting from agriculture activity and timbering often exaggerate the influence of the bedrock on the image texture.

Tuominen, H. V.↗
NASA NTRS1977

Extraction of trace elements from ores

Trace elements, such as interstitial impurities, can be extracted by low-pressure, relatively low-temperature vaporization from compositions in which they occur.

Ikramuddin, M.↗
NASA NTRS1976

Use of satellite pictures for determining major shield fractures relevant for ore prospecting, northern Finland

The author has identified the following significant results. A combined analysis of LANDSAT 1 imagery, aeromagnetic and other maps, and aerial photos has revealed a dense network of bedrock fractures in northern Finland. They form several fracturing zones, which obviously represent surficial manifestations of major fractures. The fractures follow, in general, the eight main trends of crustal shear characteristics of the Baltic Shield, but show distinct deviations from them in detail. The major fracture zones divide the bedrock into a mosaic of polygonal blocks, which in many cases coincide with the main rock units of the area and are characterized by different patterns of internal fracturing. Known mineralizations show a tendency to concentrate along the fracture zones. Optical filtering of original LANDSAT images might provide a rapid tool for the analysis of major structural trends in extensive areas such as shields or entire continents.

Tuominen, H. V.↗
NASA NTRS1976

Investigation of LANDSAT imagery on correlations between ore deposits and major shield structures in Finland

The author has identified the following significant results. Based on tests, it is obvious that practically all major LANDSAT winter linears found are geologically significant features. Most of them are chains of bogs, lakes, rivers, and cultivated areas covered by ice and/or snow, i.e., unforested linear topographic lows. They need no explanation other than that they are extensive fracture zones of the basement.

Tuominen, H. V.↗