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DOE OSTI2020

Electronically Coupled 2D Polymer/MoS 2 Heterostructures

Emergent quantum phenomena in electronically coupled two-dimensional heterostructures are central to next-generation optical, electronic, and quantum information applications. Tailoring electronic band gaps in coupled heterostructures would permit control of such phenomena and is the subject of significant research interest. Two-dimensional polymers (2DPs) offer a compelling route to tailored band structures through the selection of molecular constituents. However, despite the promise of synthetic flexibility and electronic design, fabrication of 2DPs that form electronically coupled 2D heterostructures remains an outstanding challenge. Here, we report the rational design and optimized synthesis of electronically coupled semiconducting 2DP/2D transition metal dichalcogenide van der Waals heterostructures, demonstrate direct exfoliation of the highly crystalline and oriented 2DP films down to a few nanometers, and present the first thickness-dependent study of 2DP/MoS 2 heterostructures. In this work, control over the 2DP layers reveals enhancement of the 2DP photoluminescence by two orders of magnitude in ultrathin sheets and an unexpected thickness-dependent modulation of the ultrafast excited state dynamics in the 2DP/MoS 2 heterostructure. These results provide fundamental insight into the electronic structure of 2DPs and present a route to tune emergent quantum phenomena in 2DP hybrid van der Waals heterostructures.

37 INORGANIC, ORGANIC, PHYSICAL, AND ANALYTICAL CH↗

DOE OSTI2021

Two-dimensional electronic–vibrational spectroscopy: Exploring the interplay of electrons and nuclei in excited state molecular dynamics

Two-dimensional electronic-vibrational spectroscopy (2DEVS) is an emerging spectroscopic technique which exploits two different frequency ranges for the excitation (visible) and detection (infrared) axes of a 2D spectrum. In contrast to degenerate 2D techniques, such as 2D electronic or 2D infrared spectroscopy, the spectral features of a 2DEV spectrum report cross correlations between fluctuating electronic and vibrational energy gaps rather than autocorrelations as in the degenerate spectroscopies. The center line slope of the spectral features reports on this cross correlation function directly and can reveal specific electronic-vibrational couplings and rapid changes in the electronic structure, for example. The involvement of the two types of transition moments, visible and infrared, makes 2DEVS very sensitive to electronic and vibronic mixing. 2DEV spectra also feature improved spectral resolution, making the method valuable for unraveling the highly congested spectra of molecular complexes. The unique features of 2DEVS are illustrated in this paper with specific examples and their origin described at an intuitive level with references to formal derivations provided. Although early in its development and far from fully explored, 2DEVS has already proven to be a valuable addition to the tool box of ultrafast nonlinear optical spectroscopy and is of promising potential in future efforts to explore the intricate connection between electronic and vibrational nuclear degrees of freedom in energy and charge transport applications.

37 INORGANIC, ORGANIC, PHYSICAL, AND ANALYTICAL CH↗

DOE OSTI2023

Electron-scale current sheets and energy dissipation in 3D kinetic-scale plasma turbulence with low electron beta

ABSTRACT Three-dimensional kinetic-scale turbulence is studied numerically in the regime where electrons are strongly magnetized (the ratio of plasma species pressure to magnetic pressure is βe = 0.1 for electrons and βi = 1 for ions). Such a regime is relevant in the vicinity of the solar corona, the Earth’s magnetosheath, and other astrophysical systems. The simulations, performed using the fluid-kinetic spectral plasma solver (sps) code, demonstrate that the turbulent cascade in such regimes can reach scales smaller than the electron inertial scale, and results in the formation of electron-scale current sheets (ESCS). Statistical analysis of the geometrical properties of the detected ESCS is performed using an algorithm based on the medial axis transform. A typical half-thickness of the current sheets is found to be on the order of electron inertial length or below, while their half-length falls between the electron and ion inertial length. The pressure–strain interaction, used as a measure of energy dissipation, exhibits high intermittency, with the majority of the total energy exchange occurring in current structures occupying approximately 20 per cent of the total volume. Some of the current sheets corresponding to the largest pressure–strain interaction are found to be associated with Alfvénic electron jets and magnetic configurations typical of reconnection. These reconnection candidates represent about 1 per cent of all the current sheets identified.

79 ASTRONOMY AND ASTROPHYSICS↗

DOE OSTI2021

Inverted Geometry Ceramic Insulators in High Voltage DC Electron Guns for Accelerators

A direct current (dc) high voltage photo-emission electron gun operating at 130 kV is utilized at the Jefferson Lab (JLab) Continuous Electron Beam Accelerator Facility to generate spin-polarized electrons for nuclear physics experiments. Over the past decade, JLab has tested and implemented inverted-geometry ceramic insulators in photoguns, connecting the cathode electrode in vacuum to the high voltage power supply using commercial high voltage cables. This contribution reports on tests performed up to 375 kV dc, implementation of inverted insulators in a 300 kV dc photogun generating magnetized electron beams, and describes plans to develop a reliable insulator-cable connector for applying 500 kV dc to a future polarized beam photogun operating reliably and without field emission at 350 kV.

Hernandez-Garcia, C.↗

DOE OSTI2020

Electron-beam-driven chemical processes during liquid phase transmission electron microscopy

Liquid phase (or liquid cell) transmission electron microscopy (LP-TEM) has been established as a powerful tool for observing dynamic processes in liquids at nanometer to atomic length scales. However, the simple act of observation using electrons irreversibly alters the nature of the sample. A clear understanding of electron beam-driven processes during LP-TEM is required to interpret in situ observations and utilize the electron beam as a stimulus to drive nanoscale dynamic processes. In this review, we discuss recent advances toward understanding, quantifying, mitigating, and harnessing electron beam-driven chemical processes occurring during LP-TEM. We will highlight progress in several research areas, including modeling electron beam-induced radiolysis near interfaces, electron beam-induced nanocrystal formation, and radiation damage of soft materials and biomolecules.

Woehl, Taylor J.↗

NASA NTRS1975

Electron plasma oscillations associated with type III radio emissions and solar electrons

Results of an extensive search for electron plasma oscillations associated with type III radio noise bursts are presented which were obtained by analyzing 87 type III bursts detected in plasma-wave and charged-particle measurements carried out by IMP 6, 7, and 8. Only one case is found for which plasma oscillations were associated with electrons of solar origin; at least eight events are identified in which no plasma oscillations were detected even though electrons from solar flares were clearly evident. The type III emissions are compared with similar radiation coming from upstream of earth's bow shock at the harmonic of the local electron plasma frequency, and quantitative calculations of the rate of conversion from plasma oscillatory energy to electromagnetic radiation are performed. The results show that electron plasma oscillations are seldom observed in association with solar electron events and type III radio bursts at 1.0 AU and that neither the type III emissions nor the radiation from upstream of the bow shock can be adequately explained by a current model for the coupling of electron plasma oscillations to electromagnetic radiation. Several possible explanations are considered for this discrepancy between theory and observations.

Gurnett, D. A.↗

NASA NTRS1983

The Mimas ghost revisited: An analysis of the electron flux and electron microsignatures observed in the vicinity of Mimas at Saturn

An analysis of the electron absorption signature observed by the Cosmic Ray System (CRS) on Voyage 2 near the orbit of Mimas is presented. We find that these observations cannot be explained as the absorption signature of Mimas. Combing Pioneer 11 and Voyager 2 measurements of the electron flux at Mimas's orbit (L=3.1), we find an electron spectrum where most of the flux above approx 100 keV is concentrated near 1 to 3 MeV. The expected Mimas absorption signature is calculated from this spectrum neglecting radial diffusion. A lower limit on the diffusion coefficient for MeV electrons is obtained. With a diffusion coefficient this large, both the Voyager 2 and the Pioneer 11 small-scale electron absorption signature observations in Mimas's orbit are enigmatic. Thus we refer to the mechanism for producing these signatures as the Mimas ghost. A cloud of material in orbit with Mimas may account for the observed electron signature if the cloud is at least 1% opaque to electrons across a region extending over a few hundred kilometers.

Chenette, D. L.↗

NASA NTRS1983

The Mimas ghost revisited - An analysis of the electron flux and electron microsignatures observed in the vicinity of Mimas at Saturn

An analysis of the electron-absorption signature observed by the cosmic-ray system on Voyager 2 near the orbit of Mimas is presented. It is found that these observations cannot be explained as the absorption signature of Mimas. By combining Pioneer 11 and Voyager 2 measurements of the electron flux at Mimas's orbit (L = 3.1), an electron spectrum is found in which most of the flux above about 100 keV is concentrated near 1 to 3 MeV. This spectral form is qualitatively consistent with the bandpass filter model of Van Allen et al. (1980). The expected Mimas absorption signature is calculated from this spectrum neglecting radial diffusion. Since no Mimas absorption signature was observed in the inbound Voyager 2 data, a lower limit on the diffusion coefficient for MeV electrons at L = 3.1 of D greater than 10 to the -8th sq Saturn radii/sec is obtained. With a diffusion coefficient this large, both the Voyager 2 and the Pioneer 11 small-scale electron-absorption-signature observations in Mimas's orbit are enigmatic. Thus the mechanism for producing these signatures is referred to as the Mimas ghost. A cloud of material in orbit with Mimas may account for the observed electron signature if the cloud is at least 1-percent opaque to electrons across a region extending over a few hundred kilometers.

Chenette, D. L.↗

NASA NTRS1984

Electron-impact-excitation cross sections for electronic levels in neon for incident energies between 25 and 100 eV

Absolute differential cross sections (DCS's) for electron-impact excitation of the lowest forty electronic levels in atomic neon have been determined for incident electron energies of 30 and 50 eV, for the four lowest levels at 25 eV, and two levels at 100 eV. The cross sections for these forty electronic levels are grouped into fifteen features, six of which represent excitation to resolved single electronic levels and the remaining nine which contain the unresolved contributions from two or more electronic levels. These DCS's were extrapolated to 0 deg and 180 deg and integrated to yield absolute integral cross sections as a function of incident electron energy. The results are compared to other experimental and theoretical results.

NASA NTRS1989

Trochoidal analysis of scattered electrons in a merged electron-ion beam geometry

The method and apparatus of this invention provides a plurality of measurements indicative of the absolute cross section for excitation of an ion beam. The ion beam is merged for excitation by specific energies of electrons in an electron beam. Both beams are merged in an evacuated enclosure having a longitudinal magnetic field and a crossed uniform electric field. The ions and electrons interact over a known merged longitudinal length in a merged beam area. After collision, the electron and ion beams are demerged. Forward and backward-scattered electrons are collected and position-detected by a pair of microchannel plate arrays located at opposite ends of said longitudinal beam-merging area. A series of electron and ion primary current measurements are taken at full ion and electron beam strength. Measurements are also taken at greatly reduced beam strength to obtain a beam overlap profile.

Ara Chutjian↗

NASA NTRS1994

Application of electron paramagnetic resonance imaging to the characterization of the Ultem(R) exposed to 1 MeV electrons. Correlation of radical density data to tiger code calculations

A major long-term goal of the Materials Division at the NASA Langley Research Center is the characterization of new high-performance materials that have potential applications in the aircraft industry, and in space. The materials used for space applications are often subjected to a harsh and potentially damaging radiation environment. The present study constitutes the application of a novel technique to obtain reliable data for ascertaining the molecular basis for the resilience and durability of materials that have been exposed to simulated space radiations. The radiations of greatest concern are energetic electrons and protons, as well as galactic cosmic rays. Presently, the effects of such radiation on matter are not understood in their entirety. It is clear however, that electron radiation causes ionization and homolytic bond rupture, resulting in the formation of paramagnetic spin centers in the polymer matrices of the structural materials. Since the detection and structure elucidation of paramagnetic species are most readily accomplished using Electron Paramagnetic Resonance (EPR) Spectroscopy, the NASA LaRC EPR system was brought back on-line during the 1991 ASEE term. The subsequent 1992 ASEE term was devoted to the adaptation of the EPR core system to meet the requirements for EPR Imaging (EPRI), which provides detailed information on the spatial distribution of paramagnetic species in bulk media. The present (1994) ASEE term was devoted to the calibration of this EPR Imaging system, as well as to the application of this technology to study the effects of electron irradiation on Ultem(exp R), a high performance polymer which is a candidate for applications in aerospace. The Ultem was exposed to a dose of 2.4 x 10(exp 9) Rads (1-MeV energy/electron) at the LaRC electron accelerator facility. Subsequently, the exposed specimens were stored in liquid nitrogen, until immediately prior to analyses by EPRI. The intensity and dimensions of the EPR Images that were generated for the irradiated specimens showed that the electrons penetrated the material to a depth of approximately 0.125 inch. These data show a very high degree of correlation to the energy deposition profile as predicted by the Tiger Code, a Monte Carlo code that provides guidelines for the transport of electrons in matter. Subsequent efforts will focus on delineating the transport properties of energetic protons in Ultem(R).

Suleman, Naushadalli K.↗

NASA NTRS2003

Electron Bremsstrahlung Hard X-Ray Spectra, Electron Distributions and Energetics in the 2002 July 23 Solar Flare

We present and analyze the first high-resolution hard X-ray spectra from a solar flare observed in both X-ray/gamma-ray continuum and gamma-ray lines. The 2002 July 23 flare was observed by the Ramaty High Energy Solar Spectroscopic Imager (RHESSI). The spatially integrated photon flux spectra are well fitted between 10 and 300 keV by the combination of an isothermal component and a double power law. The flare plasma temperature peaks at 40 MK around the time of peak hard X-ray emission and remains above 20 MK 37 min later. We derive the evolution of the nonthermal mean electron flux distribution by directly fitting the RHESSI X-ray spectra with the thin-target bremsstrahlung from a double power-law electron distribution with a low-energy cutoff. We also derive the evolution of the electron flux distribution on the assumption that the emission is thick-target bremsstrahlung. We find that the injected nonthermal electrons are well described throughout the flare by this double power-law distribution with a low-energy cutoff that is typically between 20 - 40 keV. Using our thick-target results, we compare the energy contained in the nonthermal electrons with the energy content of the thermal flare plasma observed by RHESSI and GOES. We find that the minimum total energy deposited into the flare plasma by nonthermal electrons, 2.6 x 10(exp 31) erg, is on the order of and possibly less than the energy in the thermal plasma. However, these fits do not rule out the possibility that the energy in nonthermal electrons exceeds the energy in the thermal plasma. This work was supported in part by the RHESSI Project and the NASA Sun-Earth Connection program.

Holman, G. D.↗

NASA NTRS2003

Electron Bremsstrahlung Hard X-Ray Spectra, Electron Distributions and Energetics in the 2002 July 23 Solar Flare

We present and analyze the first high-resolution hard X-ray spectra from a solar flare observed in both X-ray/gamma-ray continuum and gamma-ray lines. The 2002 July 23 flare was observed by the Ramaty High Energy Solar Spectroscopic Imager (RHESSI). The spatially integrated photon flux spectra are well fitted between 10 and 300 keV by the combination of an isothermal component and a double power law. The flare plasma temperature peaks at 40 MK around the time of peak hard X-ray emission and remains above 20 MK 37 min later. We derive the evolution of the nonthermal mean electron flux distribution by directly fitting the RHESSI X-ray spectra with the thin-target bremsstrahlung from a double power-law electron distribution with a low-energy cutoff. We also derive the evolution of the electron flux distribution on the assumption that the emission is thick-target bremsstrahlung. We find that the injected nonthermal electrons are well described throughout the flare by this double power-law distribution with a low-energy cutoff that is typically between 20-40 keV. Using our thick-target results, we compare the energy contained in the nonthermal electrons with the energy content of the thermal flare plasma observed by RHESSI and GOES. We find that the minimum total energy deposited into the flare plasma by nonthermal electrons, 2.6 x 10(exp 31)erg, is on the order of and possibly less than the energy in the thermal plasma. However, these fits do not rule out the possibility that the energy in nonthermal electrons exceeds the energy in the thermal plasma.

Holman, Gordon D.↗

NASA NTRS2009

Non-ambipolar radio-frequency plasma electron source and systems and methods for generating electron beams

An electron generating device extracts electrons, through an electron sheath, from plasma produced using RF fields. The electron sheath is located near a grounded ring at one end of a negatively biased conducting surface, which is normally a cylinder. Extracted electrons pass through the grounded ring in the presence of a steady state axial magnetic field. Sufficiently large magnetic fields and/or RF power into the plasma allow for helicon plasma generation. The ion loss area is sufficiently large compared to the electron loss area to allow for total non-ambipolar extraction of all electrons leaving the plasma. Voids in the negatively-biased conducting surface allow the time-varying magnetic fields provided by the antenna to inductively couple to the plasma within the conducting surface. The conducting surface acts as a Faraday shield, which reduces any time-varying electric fields from entering the conductive surface, i.e. blocks capacitive coupling between the antenna and the plasma.

Hershkowitz, Noah↗

NASA NTRS2011

Non-ambipolar radio-frequency plasma electron source and systems and methods for generating electron beams

Hershkowitz, Noah↗

NASA NTRS2011

Miniature, low-power X-ray tube using a microchannel electron generator electron source

Embodiments of the invention provide a novel, low-power X-ray tube and X-ray generating system. Embodiments of the invention use a multichannel electron generator as the electron source, thereby increasing reliability and decreasing power consumption of the X-ray tube. Unlike tubes using a conventional filament that must be heated by a current power source, embodiments of the invention require only a voltage power source, use very little current, and have no cooling requirements. The microchannel electron generator comprises one or more microchannel plates (MCPs), Each MCP comprises a honeycomb assembly of a plurality of annular components, which may be stacked to increase electron intensity. The multichannel electron generator used enables directional control of electron flow. In addition, the multichannel electron generator used is more robust than conventional filaments, making the resulting X-ray tube very shock and vibration resistant.

Elam, Wm. Timothy↗

NASA NTRS2005

Effect of electron-nuclear spin interactions for electron-spin qubits localized in InGaAs self-assembled quantum dots

The effect of electron-nuclear spin interactions on qubit operations is investigated for a qubit represented by the spin of an electron localized in an InGaAs self-assembled quantum dot. The localized electron wave function is evaluated within the atomistic tight-binding model. The electron Zeeman splitting induced by the electron-nuclear spin interaction is estimated in the presence of an inhomogeneous environment characterized by a random nuclear spin configuration, by the dot-size distribution, alloy disorder, and interface disorder. Due to these inhomogeneities, the electron Zeeman splitting varies from one qubit to another by the order of 10(-6), 10(-6), 10(-7), and 10(-9) eV, respectively. Such fluctuations cause errors in exchange operations due to the inequality of the Zeeman splitting between two qubits. However, the error can be made lower than the quantum error threshold if an exchange energy larger than 10(-4) eV is used for the operation. This result shows that the electron-nuclear spin interaction does not hinder quantum-dot based quantum computer architectures from being scalable even in the presence of inhomogeneous environments.

Whaley, K. Birgitta↗

NASA NTRS2023

Thermal Electron Heat Fluxes Associated with Precipitated Auroral Electrons During the Saint Patrick's Days 2013 and 2015 Geomagnetic Storms

The Rice Convection Model-Equilibrium (RCM-E) and SuperThermal Electron Transport (STET) are combined to investigate electron heat flux formation in the region of the diffuse aurora for the geomagnetic storms of 17 March 2013 and 17 March 2015. The primary electron precipitation into the atmosphere resulting from wave particle scattering in the magnetosphere are simulated by the magnetically and electrically RCM-E during these two geomagnetic storms. The primary precipitating electron fluxes are modified by the STET model by taking into account atmospheric backscatter processes. The modified electron energy fluxes and their mean energies are coupled to the STET code to calculate electron thermal fluxes associated with diffuse aurora on a global scale. We use the simulated heat flux to estimate electron temperatures at the upper ionospheric altitudes and compare them with corresponding observations from the Defense Meteorological Satellite Program satellite.

George V. Khazanov↗