Multidisciplinary research activity on the nature and properties of ceramic materials Semiannual status report, 16 Dec. 1967 - 15 Jun. 1968
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Mueller, J. I.↗
SEARCH · Engineering Papers
Results for “Ceramic materials”
Search indexed NASA NTRS and DOE OSTI research on propulsion, heat transfer, battery materials and energy systems. Follow report and document links to the original sources.
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Interdisciplinary research on ceramic materials
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Mueller, J. I.↗
Study of glass preforms for glass fiber optics applications (study of space processing of ceramic materials)
The feasibility, and technical and economic desirability was studied of space processing of glass preforms for optical fiber transmission applications. The results indicate that space processing can produce glass preforms of equal quality at lower cost than earth bound production, and can produce diameter modulation in the glass preform which promotes mode coupling and lowers the dispersion. The glass composition can be modified through the evaporative and diffusion processes, and graded refractive index profiles can be produced. A brief summary of the state of the art in optical fiber transmission is included.
Wang, F. F. Y.↗
Interdisciplinary research and development on the effects of the nature and properties of ceramic materials in the design of advanced structural components
Proposals are presented in supportive and interdisciplinary research from the University of Washington.
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Silicon nitride: A ceramic material with outstanding resistance to thermal shock and corrosion
The known physical, mechanical and chemical properties of reaction-sintered silicon nitride are summarized. This material deserves interest especially because of its unusually good resistance to thermal shock and corrosion at high temperatures. Two types are distinguished: reaction-sintered (porous) and hot-pressed (dense) Si3N4. Only the reaction-sintered material which is being produced today in large scale as crucibles, pipes, nozzles and tiles is considered.
Huebner, K. H.↗
Breakway friction and dynamic friction/wear measurements of various ceramic materials from 25 C (75 F) to 650 C (1200 F)
This report describes the results of a program designed to evaluate the breakaway friction and dynamic friction/wear characteristics of materials having potential for use as load bearing components in a high-performance high-temperature heavy duty diesel engine. Ten candidate materials were selected, six of which were evaluated under all possible material combinations as both stationary as well as moving breakaway specimens. The remaining materials were evaluated either in the static mode against themselves and all other materials, or against themselves only. Experiments were performed at five temperatures up to 650 C (1200 F) and unit pressures of 700 kPa (100 lb/sq in.), 3500 kPa (500 lb/sq in.), and 7000 kPa (1000 lb/sq in.). Experimental results indicate that under dynamic conditions, four of the ten materials exhibited good to excellent friction/wear characteristics in various material combinations. These materials were: titanium carbide, silicon nitride, silicon carbide (reaction sintered), and Refel (SiC).
Boes, D. J.↗
Polymer precursors for SiC ceramic materials
Work on precursor polymers to SiC was performed, concentrating on polymers made from decamethyl cyclohexasilyene units. The initial approach was to synthesize mixed diphenyl decamethyl cyclohexasilane, dephenylate, and polymerize. This produced polymers which had yields of up to 50 percent SiC. (Theoretical yield is 75 percent). The present approach is to make the polymer through the intermediate trans-1,4-diphenyl decamethyl cyclohexasilane. This should produce a crystalline polymer and high strength fibers. These will be thermally decomposed to SiC fibers. This requires new chemistry which is currently being studied.
Litt, Morton H.↗
Fiber reinforced ceramic material
A strong and tough SiC/RBSN composite material is comprised of silicon fibers and a reaction bonded silicon nitride (RBSN) matrix. This composite material may be used at elevated temperatures up to at least 1400 C.
Ramakrishna T Bhatt↗
Tempered glass and thermal shock of ceramic materials
A laboratory experiment is described that shows students the different strengths and fracture toughnesses between tempered and untempered glass. This paper also describes how glass is tempered and the materials science aspects of the process.
Bunnell, L. Roy↗
Free-Roller Versus Fixed-Roller Fixtures in Flexure Testing of Advanced Ceramic Materials
The error associated with strength measurements made with fixed-roller and V-grooved roller figures was studied with a variety of roller and figure material combinations. Both the fixed-roller and the V-grooved fixtures yielded an error in stress of about 4 to 7%. They also exhibited an appreciable amount of load strain hysteresis. Dynamic fatigue testing of 96 wt.% alumina verified the error: the fatigue strength was overestimated by 7 to 9% for the fixed roller configuration. The source of error is exclusively attributed to friction between the rollers and the specimen surface, as verified by previous investigators.
Salem, Jonathan A.↗
Effect of Preloading on Fatigue Strength in Dynamic Fatigue Testing of Ceramic Materials at Elevated Temperatures
Previously derived solutions of fatigue strength as a function of preloading were verified by applying preloads to elevated temperature dynamic fatigue tests of 96 wt% alumina at 1000 C and NC 132 silicon nitride at 1100 C. The technique was found very useful in identification and control of the governing failure mechanism when multiple failure mechanisms, such as slow crack growth, creep and oxidation occurred simultaneously at elevated temperatures.
Choi, Sung R.↗
Morphological evolution and transition at nanoscale in BSTO ceramic materials
Considerable efforts have been devoted for the development of low cost ferroelectric and clean energy storage multifunctional materials. Modification in design and production of a low cost material with well proven process provides pathway for high energy density dielectric energy storage. We studied fluorine doped a commercially well-established material system barium strontium titanate with two different concentrations of dopants and studied the morphological transition and its effect on properties. It was observed that sample with higher concentration transitioned much faster into glassy state, followed by growth of fibers which turned into a self-arranged bird nest type shape. The sample with lower concentration changed slowly into glassy state and only few fibers were farmed. Dielectric was highly dependent on processing methods and shows variation with crystallinity of material, temperature and cooling conditions during processing. In the higher concentration range, we observed nano-scale interface breakdown very similar to that of solid-liquid interface breakdown during crystal growth.
dielectric↗
Thermal Conductivity of Some Ceramic Materials at Cryogenic Temperatures
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Ali Ghavami↗
Eccentric loading of microtensile specimens
Ceramic materials have a lower density than most metals and are capable of performing at extremely high temperatures. The utility of these materials is obvious; however, the fracture strength of brittle materials is not easily predicted and often varies greatly. Characteristically, brittle materials lack ductility and do not yield as other materials. Ceramics materials are naturally populated with microscopic cracks due to fabrication techniques. Upon application of a load, stress concentration occurs at the root of these cracks and fracture will eventually occur at some not easily predicted strength. In order to use ceramics in any application some design methodology must exist from which a component can be placed into service. This design methodology is CARES/LIFE (Ceramics Analysis and Reliability Evaluation of Structures) which has been developed and refined at NASA over the last several decades. The CARES/LIFE computer program predicts the probability of failure of a ceramic component over its service life. CARES combines finite element results from a commercial FE (finite element) package such as ANSYS and experimental results to compute the abovementioned probability of failure. Over the course of several tests CARES has had great success in predicting the life of various ceramic components and has been used throughout industry. The latest challenge is to verify that CARES is valid for MEMS (Micro-Electro Mechanical Systems). To investigate a series of microtensile specimens were fractured in the laboratory. From this data, material parameters were determined and used to predict a distribution of strength for other specimens that exhibit a known stress concentration. If the prediction matches the experimental results then these parameters can be applied to a desired component outside of the laboratory. During testing nearly half of the tensile Specimens fractured at a location that was not expected and hence not captured in the FE model. It has been my duty to investigate the nature of this phenomenon in hopes of finding a better correlation between theory and empirical results. To investigate I built complete FE models of all of the tensile specimens using ANSYS. It is suspected that some misalignment naturally occurs during testing and thus additional bending stresses are present in the specimens. I modeled this eccentric loading and ran several FE trials using ANSYS/PDS (a probabilistic design system in ANSYS). My objective this summer has been familiarize myself with the CARES/LIFE program in hopes of using it in conjunction with ANSYS to help verify that CARES is applicable to MEMS-scale (greater that 1 micron, less than 1 millimeter) components.
Trapp, Mark A.↗
Ceramic composites: Enabling aerospace materials
Ceramics and ceramic matrix composites (CMC) have the potential for significant impact on the performance of aerospace propulsion and power systems. In this paper, the potential benefits are discussed in broad qualitative terms and are illustrated by some specific application case studies. The key issues in need of resolution for the potential of ceramics to be realized are discussed.
Levine, S. R.↗
Mechanical behavior of a ceramic matrix composite material
Monolithic ceramic materials have been used in industry for hundreds of years. These materials have proven their usefulness in many applications, yet, their potential for critical structural applications is limited. The existence of an imperfection in a monolithic ceramic on the order of several microns in size may be critical, resulting in catastrophic failure. To overcome this extreme sensitivity to small material imperfections, reinforced ceramic materials were developed. A ceramic matrix which has been reinforced with continuous fibers is not only less sensitive to microscopic flaws, but is also able to sustain significant damage without suffering catastrophic failure. A borosilicate glass reinforced with several layers of plain weave silicon carbide cloth (Nicalon) was studied. The mechanical testing which was performed included both flexural and tensile loading configurations. This testing was done not only to determine the material properties, but also to initiate a controlled amount of damage within each specimen. Several nondestructive testing techniques, including acousto-ultrasonics (AU), were performed on the specimens periodically during testing. The AU signals were monitored through the use of an IBM compatible personal computer with a high speed data acquisition board. Software was written which manipulates the AU signals in both the time and frequency domains, resulting in quantitative measures of the mechanical response of the material. The measured AU parameters are compared to both the mechanical test results and data from other nondestructive methods including ultrasonic C-scans and penetrant enhanced x ray radiography.
Grosskopf, Paul P.↗
Nondestructive evaluation of a ceramic matrix composite material
Monolithic ceramic materials have proven their usefulness in many applications, yet, their potential for critical structural applications is limited because of their sensitivity to small imperfections. To overcome this extreme sensitivity to small imperfections, ceramic matrix composite materials have been developed that have the ability to withstand some distributed damage. A borosilicate glass reinforced with several layers of silicon-carbide fiber mat has been studied. Four-point flexure and tension tests were performed not only to determine some of the material properties, but also to initiate a controlled amount of damage within each specimen. Acousto-ultrasonic (AU) measurements were performed periodically during mechanical testing. This paper will compare the AU results to the mechanical test results and data from other nondestructive methods including acoustic emission monitoring and X-ray radiography. It was found that the AU measurements were sensitive to the damage that had developed within the material.
Grosskopf, Paul P.↗
Film and interstitial formation of metals in plasma-sprayed ceramics
A method is described to electrodeposit noble metals such as platinum and ordinary metals such as copper on and within plasma-sprayed ceramic materials and ceramic fiber materials. Low-density ceramic fiber bodies were vacuum impregnated with plating solution and attached to an electrode. Light micrographs illustrating the density and location of deposited materials are presented and discussed. Voids in the plasma-sprayed ceramic were filled with deposits that vary from spherical to lens-shaped circular and have particle size corresponding to the full range of void size. Multiple coatings of ceramic and metal can be sequenced.
Hendricks, R. C.↗