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Search indexed NASA NTRS and DOE OSTI research on propulsion, heat transfer, battery materials and energy systems. Follow report and document links to the original sources.

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At least 109 records · Page 6
All sourcesNASA NTRSDOE OSTI
NASA NTRS1991

Reconnection voltage as a function of IMF clock angle

Magnetic reconnection between the IMF and the geomagnetic field is thought to play a major role in the transfer of solar wind momentum and energy to the magnetosphere. Both analytic modeling and analysis of geophysical data have shown that this coupling process should be a sensitive function of the clock angle of the IMF. Results are presented from a three-dimensional, MHD, global numerical simulation code for the reconnection voltage between the closed geomagnetic field and the IMF as a function of the IMF clock angle. These results are consistent with a sin(theta/2) functional behavior.

Fedder, J. A.↗
NASA NTRS1960

A Theoretical Study of the Angular Motions of Spinning Bodies in Space

A theoretical study was made of the angular motions of spinning bodies in space. The analysis was based on Euler's dynamic equations which were linearized and solved analytically. The results of the study are directly applicable only to spin-stabilized vehicles with constant moments of inertia and angular displacements not exceeding about 15 degrees. Simple analytical expressions were obtained which relate angular motions to spin-rate and inertia distributions for a given disturbance. Consideration was given to the effects produced by having artificial damping in the system. The study included numerical examples and comparisons of analytical solutions with machine solutions of exact dynamic equations. The analysis indicated that angular motions are sensitive to inertia distribution. In considering a rectangular-pulse pitching moment, it was found that the residual motion was very sensitive to the time at which the moment was removed. Artificial damping due to a perfect proportional control system seemed to be more advantageous to pencil-like configurations than to disk-like configurations.

Suddath, Jerrold H.↗
NASA NTRS1991

Sensitivity-based scaling for correlating structural response from different analytical models

A sensitivity-based linearly varying scale factor is described used to reconcile results from refined models for analysis of the same structure. The improved accuracy of the linear scale factor compared to a constant scale factor as well as the commonly used tangent approximation is demonstrated. A wing box structure is used as an example, with displacements, stresses, and frequencies correlated. The linear scale factor could permit the use of a simplified model in an optimization procedure during preliminary design to approximate the response given by a refined model over a considerable range of design changes.

Chang, Kwan J.↗
NASA NTRS1976

Pulse analysis of acoustic emission signals

A method for the signature analysis of pulses in the frequency domain and the time domain is presented. Fourier spectrum, Fourier transfer function, shock spectrum and shock spectrum ratio are examined in the frequency domain analysis, and pulse shape deconvolution is developed for use in the time domain analysis. To demonstrate the relative sensitivity of each of the methods to small changes in the pulse shape, signatures of computer modeled systems with analytical pulses are presented. Optimization techniques are developed and used to indicate the best design parameters values for deconvolution of the pulse shape. Several experiments are presented that test the pulse signature analysis methods on different acoustic emission sources. These include acoustic emissions associated with: (1) crack propagation, (2) ball dropping on a plate, (3) spark discharge and (4) defective and good ball bearings.

Houghton, J. R.↗
DOE OSTI2022

Hanford Site Composite Analysis: Dose Sensitivity Analyses

This environmental calculation file (ECF) documents the methodologies, assumptions, and results of five analyses that evaluate parameter changes to the revised Hanford Site Composite Analysis (CA) (DOE-RL-2019-52, Composite Analysis for Low-Level Waste Disposal in the Hanford Site Central Plateau). Specifically, this ECF describes the impact on total dose and analyte-specific doses for five sensitivity cases where changes to the following exposure-related parameters were implemented – (1) inventory, (2) recharge rate, (3) external dose conversion factors (DCFs) based on Federal Guidance Report (FGR) No. 15 in (EPA-402-R-19-002, Federal Guidance Report No. 15, External Exposure to Radionuclides in Air, Water, and Soil) instead of FGR No. 12 (EPA 402-R-93-081, Federal Guidance Report No. 12, External Exposure to Radionuclides in Air, Water, and Soil) for groundwater pathway scenario; (4) use of mean instead of 95th percentile intake assumptions for groundwater pathway scenario; and (5) consideration of limited sources based on U.S. Department of Energy (DOE) owned waste sites regulated under DOE O 435.1, Radioactive Waste Management. It should be noted that dose assessments for both base and sensitivity cases are based on the all-pathways representative person groundwater exposure scenario presented in DOE/RL-2022-52, Composite Analysis for Low-Level Waste Disposal in the Hanford Site Central Plateau.

54 ENVIRONMENTAL SCIENCES↗
NASA NTRS1981

Some aspects of analytical chemistry as applied to water quality assurance techniques for reclaimed water: The potential use of X-ray fluorescence spectrometry for automated on-line fast real-time simultaneous multi-component analysis of inorganic pollutants in reclaimed water

The potential use of isotopically excited energy dispersive X-ray fluorescence (XRF) spectrometry for automated on line fast real time (5 to 15 minutes) simultaneous multicomponent (up to 20) trace (1 to 10 parts per billion) analysis of inorganic pollutants in reclaimed water was examined. Three anionic elements (chromium 6, arsenic and selenium) were studied. The inherent lack of sensitivity of XRF spectrometry for these elements mandates use of a preconcentration technique and various methods were examined, including: several direct and indirect evaporation methods; ion exchange membranes; selective and nonselective precipitation; and complexation processes. It is shown tha XRF spectrometry itself is well suited for automated on line quality assurance, and can provide a nondestructive (and thus sample storage and repeat analysis capabilities) and particularly convenient analytical method. Further, the use of an isotopically excited energy dispersive unit (50 mCi Cd-109 source) coupled with a suitable preconcentration process can provide sufficient sensitivity to achieve the current mandated minimum levels of detection without the need for high power X-ray generating tubes.

Ling, A. C.↗
DOE OSTI2020

BioSTEAM-LCA: An Integrated Modeling Framework for Agile Life Cycle Assessment of Biorefineries under Uncertainty

Biorefineries will play a critical role in sustainable bioeconomies, but projections of their environmental impacts vary widely. A core challenge with life cycle assessments (LCAs) of biorefineries is that they are often disconnected from biorefinery design, simulation, and techno-economic analysis (TEA). This lack of integration is a barrier to early stage technology and process evaluations, reducing consistency and transparency across sustainability indicators while limiting our understanding of the relative importance of individual factors (e.g., design decisions, greenhouse gas emission accounting procedures), how these factors interact, and trade-offs or synergies with process economics. In this study, we propose a new agile LCA framework, BioSTEAMLCA, which layers onto BioSTEAM (Biorefinery Simulation and Techno-Economic Analysis Modules, which automates biorefinery design, simulation, and TEA) to characterize the environmental impacts of biorefineries across a landscape of designs, technology performance assumptions, and contexts. Inventory databases and impact assessment methods are integrated to enable flexible user defined LCA system models, and the implications of uncertainties throughout the production system are characterized via Monte Carlo simulation. To demonstrate the capabilities of BioSTEAMLCA, we present a case study for sugarcane ethanol production. Overall, BioSTEAM-LCA enables computationally efficient, agile gate-to-gate LCA to evaluate biorefinery processes, the production of candidate biofuels and bioproducts, and trade-offs among productivity, economics, and environmental impacts under uncertainty.

37 INORGANIC, ORGANIC, PHYSICAL, AND ANALYTICAL CH↗
NASA NTRS1980

IUS solid rocket motor contamination prediction methods

A series of computer codes were developed to predict solid rocket motor produced contamination to spacecraft sensitive surfaces. Subscale and flight test data have confirmed some of the analytical results. Application of the analysis tools to a typical spacecraft has provided early identification of potential spacecraft contamination problems and provided insight into their solution; e.g., flight plan modifications, plume or outgassing shields and/or contamination covers.

Mullen, C. R.↗
NASA NTRS1990

Characterization of the surfaces of platinum/tin oxide based catalysts by Fourier Transform Infrared Spectroscopy (FTIR)

A Pt/SnO2 catalyst has been developed at NASA Langley that is effective for the oxidation of CO at room temperature (1). A mechanism has been proposed to explain the effectiveness of this catalyst (2), but most of the species involved in this mechanism have not been observed under actual catalytic conditions. A number of these species are potentially detectable by Fourier Transform Infrared Spectroscopy (FTIR), e.g., HOSnO sub x, HO sub y PtO sub z, Pt-CO, and SnHCO3. Therefore a preliminary investigation was conducted to determine what might be learned about this particular catalyst by transmission FTIR. The main advantage of FTIR for this work is that the catalyst can be examined under conditions similar to the actual catalytic conditions. This can be of critical importance since some surface species may exist only when the reaction gases are present. Another advantage of the infrared approach is that since vibrations are probed, subtle chemical details may be obtained. The main disadvantage of this approach is that FTIR is not nearly as sensitive as the Ultra High Vacuum (UHV) surface analytical techniques such as Auger, Electron Spectroscopy for Chemical Analysis (ESCA), Electron Energy Loss Spectroscopy (EELS), etc. Another problem is that the assignment of the observed infrared bands may be difficult.

Keiser, Joseph T.↗
NASA NTRS1992

Flow analysis and design optimization methods for nozzle-afterbody of a hypersonic vehicle

This report summarizes the methods developed for the aerodynamic analysis and the shape optimization of the nozzle-afterbody section of a hypersonic vehicle. Initially, exhaust gases were assumed to be air. Internal-external flows around a single scramjet module were analyzed by solving the 3D Navier-Stokes equations. Then, exhaust gases were simulated by a cold mixture of Freon and Ar. Two different models were used to compute these multispecies flows as they mixed with the hypersonic airflow. Surface and off-surface properties were successfully compared with the experimental data. The Aerodynamic Design Optimization with Sensitivity analysis was then developed. Pre- and postoptimization sensitivity coefficients were derived and used in this quasi-analytical method. These coefficients were also used to predict inexpensively the flow field around a changed shape when the flow field of an unchanged shape was given. Starting with totally arbitrary initial afterbody shapes, independent computations were converged to the same optimum shape, which rendered the maximum axial thrust.

Baysal, O.↗
NASA NTRS1997

Microgravity Environment Characterization Program

The Microgravity Science and Applications Division (MSAD), a division within NASA's Office of Life and Microgravity Science and Applications, sponsors a broad range of space-based research in biotechnology, combustion science, fluid physics, fundamental physics, and materials science. To better understand and exploit the orbital environment, MSAD has developed methods and hardware to characterize accelerations on microgravity experiment carriers. MSAD supports research to verify analytically derived acceleration requirements for experiments and provides vibration isolation for sensitive experiments. The Microgravity Measurement and Analysis Project (MMAP), supported by MSAD, incorporates four projects: the Space Acceleration Measurement System (SAMS), the Orbital Acceleration Research Experiment (OARE), the SAMS for International Space Station (SAMS-II), and the Principal Investigator Microgravity Services (PIMS). SAMS was developed to record microgravity accelerations and the OARE was developed to record very low-frequency microgravity accelerations on-board the NASA Orbiters. The SAMS is also used for cooperative investigations on the Russian Mir space station. The SAMS-II is being developed for the same function on-board the International Space Station (ISS). PIMS utilizes microgravity acceleration data to develop a description of each microgravity mission's acceleration environment and to support microgravity investigators in interpreting possible effects of the acceleration environment on their experiments. These elements of the MSAD program will be used to define acceleration requirements for future Orbiter and ISS payloads. This paper describes the MMAP and summarizes the products and services available to principal investigators and other users. This paper also presents some microgravity acceleration characterization results from the last six years of Orbiter microgravity missions.

DeLombard, Richard↗
DOE OSTI2020

Matrix-Assisted Ionization of Molecular Uranium Species

Matrix-assisted ionization (MAI) demonstrates high sensitivity for a variety of organic compounds; however, few studies have reported the application of MAI for the detection and characterization of inorganic analytes. Trace-level uranium analysis is important in the realms of nuclear forensics, nuclear safeguards, and environmental monitoring. Traditional mass spectrometry methods employed in these fields require combinations of extensive laboratory chemistry sample preparation and destructive ionization methods. There has been recent interest in exploring ambient mass spectrometry methods that enable timely sample analysis and higher sensitivity than what is attainable by field-portable radiation detectors. Rapid characterization of uranium at nanogram levels is demonstrated in this study using MAI techniques. Mass spectra were collected on an atmospheric pressure mass spectrometer for solutions of uranyl nitrate, uranyl chloride, uranyl acetate, and uranyl oxalate utilizing 3-nibrobenzonitrile as the ionization matrix. The uranyl complexes investigated were detectable, and the chemical speciation was preserved. Sample analysis was accomplished in a matter of seconds, and limits of detection of 5 ng of uranyl nitrate, 10 ng of uranyl oxalate, 100 ng of uranyl chloride, and 200 ng of uranyl acetate were achieved. The observed gas-phase speciation was similar to negative-ion electrospray ionization of uranyl compounds with notable differences. Six matrix-derived ions were detected in all negative-ion mass spectra, and some of these ions formed adducts with the uranyl analyte. Subsequent analysis of the matrix suggests that these molecules are not matrix contaminants and are instead created during the ionization process.

38 RADIATION CHEMISTRY, RADIOCHEMISTRY, AND NUCLEA↗
DOE OSTI2023

HPLC-Parallel accelerator and molecular mass spectrometry analysis of 14 C-labeled amino acids

Accelerator mass spectrometry (AMS) is the method of choice for quantitation of low amounts of 14 C-labeled biomolecules. Despite exquisite sensitivity, an important limitation of AMS is its inability to provide structural information about the analyte. This limitation is not critical when the labeled compounds are well-characterized prior to AMS analysis. However, analyte identity is important in other experiments where, for example, a compound is metabolized and the structures of its metabolites are not known. We previously described a moving wire interface that enables direct AMS measurement of liquid sample in the form of discrete drops or HPLC eluent without the need for individual fraction collection, termed liquid sample-AMS (LS-AMS). Here, we now report the coupling of LS-AMS with a molecular mass spectrometer, providing parallel accelerator and molecular mass spectrometry (PAMMS) detection of analytes separated by liquid chromatography. The repeatability of the method was examined by performing repeated injections of 14 C-labeled tryptophan, and relative standard deviations of the 14 C peak areas were ≤10.57% after applying a normalization factor based on a standard. Five 14 C-labeled amino acids were separated and detected to provide simultaneous quantitative AMS and structural MS data, and AMS results were compared with solid sample-AMS (SS-AMS) data using Bland-Altman plots. To demonstrate the utility of the workflow, yeast cells were grown in a medium with 14 C-labeled tryptophan. The cell extracts were analyzed by PAMMS, and 14 C was detected in tryptophan and its metabolite kynurenine.

38 RADIATION CHEMISTRY, RADIOCHEMISTRY, AND NUCLEA↗
NASA NTRS1989

Solution and sensitivity analysis of a complex transcendental eigenproblem with pairs of real eigenvalues

This paper considers complex transcendental eigenvalue problems where one is interested in pairs of eigenvalues that are restricted to take real values only. Such eigenvalue problems arise in dynamic stability analysis of nonconservative physical systems, i.e., flutter analysis of aeroelastic systems. Some available solution methods are discussed and a new method is presented. Two computational approaches are described for analytical evaluation of the sensitivities of these eigenvalues when they are dependent on other parameters. The algorithms presented are illustrated through examples.

Murthy, Durbha V.↗
NASA NTRS1989

Solution and sensitivity analysis of a complex transcendental eigenproblem with pairs of real eigenvalues

This paper considers complex transcendental eigenvalue problems where one is interested in pairs of eigenvalues that are restricted to take real values only. Such eigenvalue problems arise in dynamic stability analysis of nonconservative physical systems, i.e., flutter analysis of aeroelastic systems. Some available solution methods are discussed and a new method is presented. Two computational approaches are described for analytical evaluation of the sensitivities of these eigenvalues when they are dependent on other parameters. The algorithms presented are illustrated through examples.

Murthy, D. V.↗
NASA NTRS1991

Flow analysis and design optimization methods for nozzle afterbody of a hypersonic vehicle

This report summarizes the methods developed for the aerodynamic analysis and the shape optimization of the nozzle-afterbody section of a hypersonic vehicle. Initially, exhaust gases were assumed to be air. Internal-external flows around a single scramjet module were analyzed by solving the three dimensional Navier-Stokes equations. Then, exhaust gases were simulated by a cold mixture of Freon and Argon. Two different models were used to compute these multispecies flows as they mixed with the hypersonic airflow. Surface and off-surface properties were successfully compared with the experimental data. In the second phase of this project, the Aerodynamic Design Optimization with Sensitivity analysis (ADOS) was developed. Pre and post optimization sensitivity coefficients were derived and used in this quasi-analytical method. These coefficients were also used to predict inexpensively the flow field around a changed shape when the flow field of an unchanged shape was given. Starting with totally arbitrary initial afterbody shapes, independent computations were converged to the same optimum shape, which rendered the maximum axial thrust.

Baysal, Oktay↗
NASA NTRS1992

Recent advances in steady compressible aerodynamic sensitivity analysis

Sensitivity analysis methods are classified as belonging to either of the two broad categories: the discrete (quasi-analytical) approach and the continuous approach. The two approaches differ by the order in which discretization and differentiation of the governing equations and boundary conditions is undertaken. The discussion focuses on the discrete approach. Basic equations are presented, and the major difficulties are reviewed in some detail, as are the proposed solutions. Recent research activity concerned with the continuous approach is also discussed.

Taylor, Arthur C., III↗