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At least 109 records · Page 6
All sourcesNASA NTRSDOE OSTI
DOE OSTI2022

Low temperature catalytic conversion of CH 4 , CO 2 , and C 2 H 4 to value-added C 3 oxygenates and olefins via C 1 -C 2 coupling on Pd-Au/CeO 2

The catalytic conversion of CH 4 and CO 2 in the presence of more reactive co-reactants C 2 H 4 and O 2 on Pd-Au/CeO 2 is achieved at 200 °C and elevated pressures. Propene and acetone were produced from the catalyzed reaction of CH 4 +C 2 H 4 +O 2 ; addition of CO 2 to the reactant stream produced methyl acetate (MAc) but it significantly reduced the C-selectivities of propene and acetone. DRIFTS experiments confirmed the formation of methoxy species from CH 4 +CO 2 at 200 °C, which is an intermediate in the formation of MAc. Here, control experiments with blanks, and with CeO 2 did not show any propene, acetone, or MAc products. The complete oxidation of C 2 H 4 was avoided; the catalyst is stable, and reactant conversions and product yields were sustained for the observed 1200 min time-on-stream, indicating that there is little or no carbon deposition and sintering. This direct coupling of CH 4 and C 2 H 4 intermediates to higher carbon-number products at 200 °C is significant.

37 INORGANIC, ORGANIC, PHYSICAL, AND ANALYTICAL CH↗
DOE OSTI2025

A bipartite bacterial virulence factor targets the complement system and neutrophil activation

Abstract The complement system and neutrophils constitute the two main pillars of the host innate immune defense against infection by bacterial pathogens. Here, we identify T-Mac, a novel virulence factor of the periodontal pathogen Treponema denticola that allows bacteria to evade both defense systems. We show that T-Mac is expressed as a pre-protein that is cleaved into two functional units. The N-terminal fragment has two immunoglobulin-like domains and binds with high affinity to the major neutrophil chemokine receptors FPR1 and CXCR1, blocking N -formyl-Met-Leu-Phe- and IL-8-induced neutrophil chemotaxis and activation. The C-terminal fragment functions as a cysteine protease with a unique proteolytic activity and structure, which degrades several components of the complement system, such as C3 and C3b. Murine infection studies further reveal a critical T-Mac role in tissue damage and inflammation caused by bacterial infection. Collectively, these results disclose a novel innate immunity-evasion strategy, and open avenues for investigating the role of cysteine proteases and immunoglobulin-like domains of gram-positive and -negative bacterial pathogens.

Kurniyati, Kurni↗
DOE OSTI2023

Comprehensive Review of Multi-arm Caliper Data for the Big Hill SPR Site

The Big Hill SPR site has a rich data set consisting of multi-arm caliper (MAC) logs collected from the cavern wells. This data set provides insight into the on-going casing deformation at the Big Hill site. This report summarizes the MAC surveys for each well and presents well longevity estimates where possible. Included in the report is an examination of the well twins for each cavern and a discussion on what may or may not be responsible for the different levels of deformation between some of the well twins. The report also takes a systematic view of the MAC data presenting spatial patterns of casing deformation and deformation orientation in an effort to better understand the underlying causes. The conclusions present a hypothesis suggesting the small-scale variations in casing deformation are attributable to similar scale variations in the character of the salt-caprock interface. These variations do not appear directly related to shear zones or faults.

58 GEOSCIENCES↗
NASA NTRS1982

Development and flight evaluation of an augmented stability active controls concept: Executive summary

A pitch active control system (PACS) was developed and flight tested on a wide body jet transport (L-1011) with a flying horizontal stabilizer. Two dual channel digital computers and the associated software provide command signals to a dual channel series servo which controls the stabilizer power actuators. Input sensor signals to the computer are pitch rate, column trim position, and dynamic pressure. Control laws are given for the PACS and the system architecture is defined. Discussions are given regarding piloted flight simulation and vehicle system simulation and vehicle system simulation tests that are performed to verify control laws and system operation prior to installation on the aircraft. Modifications to the basic aircraft included installation of the PACS, addition of a c.g. management system to provide a c.g. range from 25 to 39% mac, and downrigging of the geared elevator to provide the required nose down control authority for aft c.g. flight test conditions. Three pilots used the Cooper-Harper Rating Scale to judge flying qualities of the aircraft with PACS on and off. The handling qualities with the c.g. at 39% mac (41% stability margin) and PACS operating were judged to be as good as the handling qualities with the c.g. at 25% mac (+15% stability margin) and PACS off.

Guinn, W. A.↗
NASA NTRS1988

Accuracy study of the Upper Atmosphere Research Satellite (UARS) definitive attitude determination

The Upper Atmosphere Research Satellite (UARS) has two definitive attitude determination requirements: the definitive attitude of the Modular Attitude Control Subsystem (MACS) and the definitive attitude of the gimbaled Solar-Stellar Pointing Platform (SSPP). The onboard computer (OBC) will compute the MACS attitude using a Kalman filter and will transform this attitude solution through the SSPP gimbals to calculate the SSPP attitude. The attitude ground support system (AGSS) will compute the MACS attitude using a batch least-squares differential corrector algorithm and will also transform this solution through the gimbals to obtain the SSPP attitude. This paper reports the results of a prelaunch study to predict the accuracy of the OBC attitude solutions and the accuracy of the AGSS attitude solutions. The OBC and AGSS solution accuracies are then compared to establish the relative quality. The effects of star observability, sensor noise, and sensor misalignment uncertainties on attitude determination accuracy are analyzed for each case.

Snow, Frank↗
NASA NTRS1990

A simulation evaluation of the engine monitoring and control system display

The Engine Monitoring and Control System (E-MACS) display is a new concept for an engine instrument display, the purpose of which is to provide an enhanced means for a pilot to control and monitor aircraft engine performance. It provides graphically-presented information about performance capabilities, current performance, and engine component or subsystem operational conditions relative to nominal conditions. The concept was evaluated by sixteen pilot-subjects against a traditional, state-of-the-art electronic engine display format. The results of this evaluation showed a substantial pilot preference for the E-MACS display relative to the traditional display. The results of the failure detection portion of the evaluation showed a 100 percent detection rate for the E-MACS display relative to a 57 percent rate for the traditional display. From these results, it is concluded that by providing this type of information in the cockpit, a reduction in pilot workload and an enhanced ability for detecting degraded or off-nominal conditions is probable, thus leading to an increase in operational safety.

Abbott, Terence S.↗
NASA NTRS1992

Human exposure limits to hypergolic fuels

Over the past four decades, many studies have been conducted on the toxicities of the rocket propellants hydrazine (HZ) and monomethylhydrazine (MH). Numerous technical challenges have made it difficult to unambiguously interpret the results of these studies, and there is considerable divergence between results obtained by different investigators on the inhalation concentrations (MAC's) for each toxic effect inducible by exposure to hypergolic fuels in spacecraft atmospheres, NASA undertook a critical review of published and unpublished investigations on the toxicities of these compounds. The current state of the art practices for similar studies. While many questions remain unanswered, MAC's were determined using the best available data for a variety of toxic endpoints for potential continuous exposure durations ranging from 1 hour to 180 days. Spacecraft MAC's (SMAC's) were set for each compound based on the most sensitive toxic endpoint at each exposure duration.

Garcia, H. D.↗
NASA NTRS1993

Rapid susceptibility testing of mycobacterium avium complex and mycobacterium tuberculosis isolated from AIDS patients

In ominous projections issued by both U.S. Public Health Service and the World Health Organization, the epidemic of the Human Immunodeficiency Virus (HIV) infection will continue to rise more rapidly worldwide than predicted earlier. The Acquired Immunodeficiency Syndrome (AIDS) patients are susceptible to diseases called opportunistic infections of which tuberculosis and M. avium Complex (MAC) infection are most common. This has created an urgent need to uncover new drugs for the treatment of these infections. In the seventies, NASA scientists at Goddard Space Flight Center, Greenbelt, Maryland, had adopted a biochemical indicator, adenosine triphosphate (ATP), to detect presence of life in extraterrestrial space. Therefore, we proposed to develop ATP assay technique to determine sensitivity of antibacterial compounds against MAC and M. tuberculosis. The work was initiated in June 1992. In the last report, we described our efforts in developing ATP assay method using MAC. Studies were continued further, and during the period of this report, we established the relationship between colony forming units and ATP levels of these organisms during the growth cycle. Also, we evaluated the effects of standard antimycobacterial drugs using ATP assay technique and compared the results with those obtained with conventional tube dilution proportional method.

Dhople, Arvind M.↗
NASA NTRS1987

Selected spectroscopic and magnetic properties of lanthanide complexes in polyimide XU-218

Polyimide XU-218 films containing approximately 5 wt pct of Eu(III), Gd(III), Tb(III), and Er(III) were prepared, and the effects of complexing each of the metals with the following four ligands were investigated: N-phenylphthalamate (NPPA), 2,4-pentanedionate (AcAc), 1,3-diphenyl 1,3-propanedionate (DBM), and a new hexa-aza-macrocyclic (MAC) ligand. The tris-chelated complexes of the mononegative ligands NPPA, AcAc, and DBM produced transparent, flexible films, which had magnetic and spectral properties very similar to those of the parent lanthanide complexes, while complexes of MAC showed problems due to the presence of lattice water and yielded dark brittle films. AcAc caused little or no effect on the glass transition temperature (Tg), while NPPA and DBM complexes lowered Tg to 269-290 C, and MAC indicated moisture by inflexion at 95-100 C with a true Tg at 320 C. All lanthanide-containing films were paramagnetic.

Stoakley, D. M.↗
NASA NTRS1993

Chemical composition of new Acapulcoites and Lodranites

The bulk compositions of two Antarctic Lodranites, MAC 88177 and FRO 90011, and two Acapulcoites, ALH 81261 and Monument Draw, were determined with instrumental neutron activation analysis. Acapulcoites have essentially chondritic major and trace element abundances but achondritic texture. They consist of entirely recrystallized, fine grained mineral assemblages. Chondrules are extremely rare; one relict radiating pyroxene chondrule was described in Monument Draw (MD). The coarse grained Lodranites also have achondritic textures, but they are different compositionally with depletions in Al, Na, and incompatible elements probably a result of separation of partial, feldspar-rich melt. MAC 88177 is significantly more depleted in incompatible elements than FRO 90011 suggesting a higher degree of partial melting for the MAC-Lodranite. The chemical data support a genetic relationship between Lodranites and Acapulcoites inferred earlier from oxygen isotopes, petrology, and mineral composition.

Zipfel, J.↗
NASA NTRS1995

The classification and complex thermal history of the enstatite chondrites

We have carried out instrumental neutron activation analysis of 11 enstatite chondrites and electron microprobe analyses of 17 enstatite chondrites, most of which were previously little described. We report here the third known EH5 chondrite (LEW 88180) and an unusual EL6 chondrite (LEW 87119), new data on four EL3 chondrites (ALH 85119, EET 90299, PCA 91020, and MAC 88136, which is paired with MAC 88180 and MAC 88184), the second EL5 chondrite (TIL 91714), and an unusual metal-rich and sulfide-poor EL3 chondrite (LEW 87223). The often discussed differences in mineral composition displayed by the EH and EL chondrites are not as marked after the inclusion of the new samples in the database, and the two classes apparently experienced a similar range of equilibrium temperatures. However, texturally the EL chondrites appear to have experienced much higher levels of metamorphic alteration than EH chondrites of similar equilibration temperatures. Most of the petrologic type criteria are not applicable to enstatite chondrites and, unlike the ordinary chondrites, texture and mineralogy reflect different aspects of the meteorite history. We therefore propose that the existing petrologic type scheme not be used for enstatite chondrites. We suggest that while 'textural type' reflects peak metamorphic temperatures, the 'mineralogical type' reflects equilibration during postmetamorphic (probably regolith) processes. Unlike the ordinary chondrites and EH chondrites, EL chondrites experienced an extensive low-temperature metamorphic episode. There are now a large number of enstatite meteorite breccias and impact melts, and apparently surface processes were important in determining the present nature of the enstatite chondrites.

Zhang, Yanhong↗
NASA NTRS2001

Volatility and Wear Characteristics of a Variety of Liquid Lubricants for Space Applications

The vapor pressures and wear characteristics are critical properties for liquid lubricants to assure long-term reliability and performance in space applications. Vapor pressures, obtained using a Knudsen cell technique, and wear properties, obtained using a vacuum four-ball apparatus, were measured for a series of unformulated liquid lubricants. These included two multiply alkylated cyclopentanes (MACs) (X-1000 and X2000), two linear perfluoropolyalkylethers (PFPAEs) (Z-25 and 815Z), and four silahydrocarbons (a tri, a tetra, and two pentas). Vapor pressures were measured at three elevated temperatures (423, 448, and 498 K) and extrapolated to room temperature 298 K. The lowest 298 K vapor pressure of 5.7 x 10(exp -14) Pa was obtained with the PFPAE fluid (815Z) and the highest value with the low molecular weight MAC (X-1000) at 3.6 x 10(exp -7) Pa. In addition, vacuum wear rates were determined for some of the lubricants. The lowest wear rates (approximately 3 x 10(exp -11) cubic mm/mm) were observed for three of the silahydrocarbons while the highest wear rates (approximately 2 x 10(exp -9) cubic mm/mm) were observed with the two PFPAE fluids (Z-25 and 815Z). The MAC (X-2000) yielded a wear rate of about 10(exp -10) cubic mm/mm. The results indicated that the silahydrocarbon class of liquid lubricants offers the better potential for space applications.

Nguyen, QuynhGiao N.↗
NASA NTRS2001

Volatility and Wear Characteristics of a Variety of Liquid Lubricants for Space Applications

The vapor pressures and near characteristics are critical properties for liquid lubricants to assure long-term reliability and performance in space applications. Vapor pressures, obtained using a Knudsen cell technique, and near properties, obtained using a vacuum four-ball apparatus, were measured for a series of unformulated liquid lubricants. These include: two multiple alkylated cyclopentanes (MACs) (X-1000 and X-2000), two linear perfluoropolyalkylethers (PFPAEs) (Z-25 and 815Z), and four silahydrocarbons (a tri-, a tetra-, and two pentas). Vapor pressures were measured at three elevated temperatures (423, 448, and 498 K) and extrapolated to room temperature 298 K. The lowest 298 K vapor pressure of 5.7 x 10(exp -14) Pa, was obtained with the PFPAE fluid (815Z) and the highest value with the low molecular weight MAC (X-1000) at 3.6 x 10(exp -7) Pa. In addition, vacuum near rates were determined for some of the lubricants. The lowest wear rates (approximately 3 x 10(exp -11) cubic mm/mm) were observed for three of the silahydrocarbons while the highest wear rate (approximately 2 x 10(exp-9) cubic mm/mm) were observed with the two PFPAE fluids (Z-25 and 815Z). The MAC (X-2000) yielded a wear rate of about 10(exp -10) cubic mm/mm. The results indicated that the silahydrocarbon class of liquid lubricants offers the better potential for space applications.

Nguyen, Quynhgiao N.↗
NASA NTRS2002

A IAB-Complex Iron Meteorite Containing Low-Ca Clinopyroxene: Northwest Africa 468 and its Relationship to Iodranites and Formation by Impact Melting

Northwest Africa 468 (NWA 468) is a new ungrouped, silicate-rich member of the IAB complex of nonmagmatic iron meteorites. The silicates contain relatively coarse (approximately 300 micron-size) grains of low-Ca clinopyroxene with polysynthetic twinning and inclined extinction. Low-Ca clinopyroxene is indicative of quenching from high temperatures (either from protoenstatite in a few seconds or high-temperature clinoenstatite in a few hours). It seems likely that NWA 468 formed by impact melting followed by rapid cooling to less than or equal to 660 C. After the loss of a metal-sulfide melt from the silicates, sulfide was reintroduced, either from impact-mobilized FeS or as an S2 vapor that combined with metallic Fe to produce FeS. The O-isotopic composition (delta O-17 = -1.39 %) indicates that the precursor material of NWA 468 was a metal-rich (e.g., CR) carbonaceous chondrite. Lodranites are similar in bulk chemical and O-isotopic composition to the silicates in NWA 468; the MAC 88177 lodranite (which also contains low-Ca clinopyroxene) is close in bulk chemical composition. Both NWA 468 and MAC 88177 have relatively low abundances of REE (rare earth elements) and plagiophile elements. Siderophiles in the metal-rich areas of NWA 468 are similar to those in the MAC 88177 whole rock; both samples contain low Ir and relatively high Fe, Cu and Se. Most unweathered lodranites contain approximately 20 - 38 wt. % metallic Fe-Ni. These rocks may have formed in an analogous manner to NWA 468 (i.e., by impact melting of metal-rich carbonaceous-chondrite precursors) but with less separation of metal-rich melts from silicates.

Rubin, Alan E.↗
NASA NTRS1994

Issues on Reproducibility/Reliability of Magnetic NDE Methods

One of the critical elements related to the practicality of any NDE technique is its reproducibility under nominally the same inspection conditions. The results of certain test methodologies, however, are not always repeatable and understanding the origin of the irreproducibility is often as critical as obtaining reproducible results. One example is the characterization of residual stress in structural ferromagnets using the magnetoacoustic (MAC) method. Although it has not been widely publicized, the test results of this method are known to be time-dependent. Two distinct types of time dependencies have been observed during testing. The first type has a clearly definable relaxation time, while no such trend has been observed for the second. The purpose of the present study is to systematically investigate the time dependence of the second type, to find out the range and, if possible, the origin of the variation in the test results. For this, MAC curves were obtained under various stress levels and the tests were repeated over time. Particular attention was given to whether noise in the measuring device or a change in the laboratory environment could have been a contributing factor. The steel samples used for the study were cut from C- and U-class railroad wheels. The MAC behavior of these samples was reported previously. Each steel sample was first machined to be a cylindrical rod of 3.175 cm (1.25 in) in diameter and 26.67 cm (10.5 in) in length. The center portion of the samples were further machined to form a pair of flat and parallel surfaces for the launch and reflection of the ultrasonic pulses. Data acquisition involved two major elements; magnetic and acoustic measurements. Throughout the experiment the net magnetic induction, B, was measured by integrating the induction pickup coil output using an integrating fluxmeter. The acoustic measurements employed the phase-locked technique which will be described in the following.

Namkung, M.↗
NASA NTRS2004

Conversion of the Aeronautics Interactive Workstation

This summer I am working in the Educational Programs Office. My task is to convert the Aeronautics Interactive Workstation from a Macintosh (Mac) platform to a Personal Computer (PC) platform. The Aeronautics Interactive Workstation is a workstation in the Aerospace Educational Laboratory (AEL), which is one of the three components of the Science, Engineering, Mathematics, and Aerospace Academy (SEMAA). The AEL is a state-of-the-art, electronically enhanced, computerized classroom that puts cutting-edge technology at the fingertips of participating students. It provides a unique learning experience regarding aerospace technology that features activities equipped with aerospace hardware and software that model real-world challenges. The Aeronautics Interactive Workstation, in particular, offers a variety of activities pertaining to the history of aeronautics. When the Aeronautics Interactive Workstation was first implemented into the AEL it was designed with Macromedia Director 4 for a Mac. Today it is being converted to Macromedia DirectorMX2004 for a PC. Macromedia Director is the proven multimedia tool for building rich content and applications for CDs, DVDs, kiosks, and the Internet. It handles the widest variety of media and offers powerful features for building rich content that delivers red results, integrating interactive audio, video, bitmaps, vectors, text, fonts, and more. Macromedia Director currently offers two programmingkripting languages: Lingo, which is Director's own programmingkripting language and JavaScript. In the workstation, Lingo is used in the programming/scripting since it was the only language in use when the workstation was created. Since the workstation was created with an older version of Macromedia Director it hosted significantly different programming/scripting protocols. In order to successfully accomplish my task, the final product required correction of Xtra and programming/scripting errors. I also had to convert the Mac platform file extensions into compatible file extensions for a PC.

Riveras, Nykkita L.↗
NASA NTRS2010

An Evaluation of Liquid, Solid, and Grease Lubricants for Space Mechanisms Using a Spiral Orbit Tribometer

We present the findings of the test program performed by The European Space Tribology Laboratory (ESTL) to evaluate the performance (friction and lifetime) of a number of space lubricants under vacuum using a Spiral Orbit Tribometer (SOT). Focus was given to a comparison of various popular space oils, a comparison study between the old and new MAPLUB grease formulations, and the performance of commonly used solid lubricants under various conditions. Tests demonstrated that the lifetimes of hydrocarbon NYE oils 2001 & 2001A outperformed those of the perfluroropolyalkylether (PFPE) oils Fomblin Z25 & Z60, though these pairs displayed similar behavior. This relationship was also generally seen for greases; with the lifetimes of the multiple alkylated cyclopentane (MAC)-based greases being extended in comparison to the PFPE-based greases. Testing on greases also demonstrated similar performance between the old (-a) and new (-b) formulations when considering PFPE-based MAPLUB greases, and indeed for all tested PFPE-based non-MAPLUB greases, but significantly shorter lifetimes for the new formulations when considering MAC-based MAPLUB greases. MAPLUB MAC greases containing molybdenum disulphide (MoS2) thickener were also found to display reduced lifetimes. For solid lubricants, lead displayed significantly extended lifetimes over MoS2, speculated to be caused by redistribution of lead from the ball onto all contact surfaces during the test. Friction coefficients were seen to be some 2.5x higher for lead than for MoS2 under similar conditions, a result that corresponds well with conventional bearing tests. The work described was performed under contract for the European Space Agency as part of the Tribology Applications Program, with all funding for testing and apparatus provided by European Space Agency (ESA).

Buttery, Michael↗
NASA NTRS2006

Lunar Relay Satellite Network for Space Exploration: Architecture, Technologies and Challenges

NASA is planning a series of short and long duration human and robotic missions to explore the Moon and then Mars. A key objective of these missions is to grow, through a series of launches, a system of systems infrastructure with the capability for safe and sustainable autonomous operations at minimum cost while maximizing the exploration capabilities and science return. An incremental implementation process will enable a buildup of the communication, navigation, networking, computing, and informatics architectures to support human exploration missions in the vicinities and on the surfaces of the Moon and Mars. These architectures will support all space and surface nodes, including other orbiters, lander vehicles, humans in spacesuits, robots, rovers, human habitats, and pressurized vehicles. This paper describes the integration of an innovative MAC and networking technology with an equally innovative position-dependent, data routing, network technology. The MAC technology provides the relay spacecraft with the capability to autonomously discover neighbor spacecraft and surface nodes, establish variable-rate links and communicate simultaneously with multiple in-space and surface clients at varying and rapidly changing distances while making optimum use of the available power. The networking technology uses attitude sensors, a time synchronization protocol and occasional orbit-corrections to maintain awareness of its instantaneous position and attitude in space as well as the orbital or surface location of its communication clients. A position-dependent data routing capability is used in the communication relay satellites to handle the movement of data among any of multiple clients (including Earth) that may be simultaneously in view; and if not in view, the relay will temporarily store the data from a client source and download it when the destination client comes into view. The integration of the MAC and data routing networking technologies would enable a relay satellite system to provide end-to-end communication services for robotic and human missions in the vicinity, or on the surface of the Moon with a minimum of Earth-based operational support.

Bhasin, Kul B.↗