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At least 1,063 records · Page 59
All sourcesNASA NTRSDOE OSTI
DOE OSTI2023

Experimental Assessment of Mammalian Lipidome Complexity Using Multimodal 21 T FTICR Mass Spectrometry Imaging

Herein, we assess the complementarity and complexity of data that can be detected within mammalian lipidome mass spectrometry imaging (MSI) via matrix-assisted laser desorption ionization (MALDI) and nanospray desorption electrospray ionization (nano-DESI). We do so by employing 21 T Fourier transform ion cyclotron resonance mass spectrometry (FTICR-MS) with absorption mode FT processing in both cases, allowing unmatched mass resolving power per unit time (≥613k at m/z 760, 1.536 s transients). While our results demonstrated that molecular coverage and dynamic range capabilities were greater in MALDI analysis, nano-DESI provided superior mass error, and all annotations for both modes had sub-ppm error. Taken together, these experiments highlight the coverage of 1676 lipids and serve as a functional guide for expected lipidome complexity within nano-DESI-MSI and MALDI-MSI. To further assess the lipidome complexity, mass splits (i.e., the difference in mass between neighboring peaks) within single pixels were collated across all pixels from each respective MSI experiment. The spatial localization of these mass splits was powerful in informing whether the observed mass splits were biological or artificial (e.g., matrix related). Mass splits down to 2.4 mDa were observed (i.e., sodium adduct ambiguity) in each experiment, and both modalities highlighted comparable degrees of lipidome complexity. Further, we highlight the persistence of certain mass splits (e.g., 8.9 mDa; double bond ambiguity) independent of ionization biases. Here, we also evaluate the need for ultrahigh mass resolving power for mass splits ≤4.6 mDa (potassium adduct ambiguity) at m/z > 1000, which may only be resolved by advanced FTICR-MS instrumentation.

21T-FTICR-MS↗
DOE OSTI2022

The 2022 magneto-optics roadmap

Abstract Magneto-optical (MO) effects, viz. magnetically induced changes in light intensity or polarization upon reflection from or transmission through a magnetic sample, were discovered over a century and a half ago. Initially they played a crucially relevant role in unveiling the fundamentals of electromagnetism and quantum mechanics. A more broad-based relevance and wide-spread use of MO methods, however, remained quite limited until the 1960s due to a lack of suitable, reliable and easy-to-operate light sources. The advent of Laser technology and the availability of other novel light sources led to an enormous expansion of MO measurement techniques and applications that continues to this day (see section 1). The here-assembled roadmap article is intended to provide a meaningful survey over many of the most relevant recent developments, advances, and emerging research directions in a rather condensed form, so that readers can easily access a significant overview about this very dynamic research field. While light source technology and other experimental developments were crucial in the establishment of today’s magneto-optics, progress also relies on an ever-increasing theoretical understanding of MO effects from a quantum mechanical perspective (see section 2), as well as using electromagnetic theory and modelling approaches (see section 3) to enable quantitatively reliable predictions for ever more complex materials, metamaterials, and device geometries. The latest advances in established MO methodologies and especially the utilization of the MO Kerr effect (MOKE) are presented in sections 4 (MOKE spectroscopy), 5 (higher order MOKE effects), 6 (MOKE microscopy), 8 (high sensitivity MOKE), 9 (generalized MO ellipsometry), and 20 (Cotton–Mouton effect in two-dimensional materials). In addition, MO effects are now being investigated and utilized in spectral ranges, to which they originally seemed completely foreign, as those of synchrotron radiation x-rays (see section 14 on three-dimensional magnetic characterization and section 16 on light beams carrying orbital angular momentum) and, very recently, the terahertz (THz) regime (see section 18 on THz MOKE and section 19 on THz ellipsometry for electron paramagnetic resonance detection). Magneto-optics also demonstrates its strength in a unique way when combined with femtosecond laser pulses (see section 10 on ultrafast MOKE and section 15 on magneto-optics using x-ray free electron lasers), facilitating the very active field of time-resolved MO spectroscopy that enables investigations of phenomena like spin relaxation of non-equilibrium photoexcited carriers, transient modifications of ferromagnetic order, and photo-induced dynamic phase transitions, to name a few. Recent progress in nanoscience and nanotechnology, which is intimately linked to the achieved impressive ability to reliably fabricate materials and functional structures at the nanoscale, now enables the exploitation of strongly enhanced MO effects induced by light–matter interaction at the nanoscale (see section 12 on magnetoplasmonics and section 13 on MO metasurfaces). MO effects are also at the very heart of powerful magnetic characterization techniques like Brillouin light scattering and time-resolved pump-probe measurements for the study of spin waves (see section 7), their interactions with acoustic waves (see section 11), and ultra-sensitive magnetic field sensing applications based on nitrogen-vacancy centres in diamond (see section 17). Despite our best attempt to represent the field of magneto-optics accurately and do justice to all its novel developments and its diversity, the research area is so extensive and active that there remains great latitude in deciding what to include in an article of this sort, which in turn means that some areas might not be adequately represented here. However, we feel that the 20 sections that form this 2022 magneto-optics roadmap article, each written by experts in the field and addressing a specific subject on only two pages, provide an accurate snapshot of where this research field stands today. Correspondingly, it should act as a valuable reference point and guideline for emerging research directions in modern magneto-optics, as well as illustrate the directions this research field might take in the foreseeable future.

71 CLASSICAL AND QUANTUM MECHANICS, GENERAL PHYSIC↗
NASA NTRS2019

Search for Transient Gravitational-wave Signals Associated with Magnetar Bursts during Advanced LIGO's Second Observing Run

We present the results of a search for short- and intermediate-duration gravitational-wave signals from four magnetar bursts in Advanced LIGO's second observing run. We find no evidence of a signal and set upper bounds on the root sum squared of the total dimensionless strain ( h rss ) from incoming intermediate-duration gravitational waves ranging from 1.1 × 10 −22 at 150 Hz to 4.4 × 10 −22 at 1550 Hz at 50% detection efficiency. From the known distance to the magnetar SGR 1806–20 (8.7 kpc), we can place upper bounds on the isotropic gravitational-wave energy of 3.4 × 10 44 erg at 150 Hz assuming optimal orientation. This represents an improvement of about a factor of 10 in strain sensitivity from the previous search for such signals, conducted during initial LIGO's sixth science run. The short-duration search yielded upper limits of 2.1 × 10 44 erg for short white noise bursts, and 2.3 × 10 47 erg for 100 ms long ringdowns at 1500 Hz, both at 50% detection efficiency.

B. P. Abbott↗
DOE OSTI2021

Discovery and characterization of five new eclipsing AM CVn systems

ABSTRACT AM CVn systems are ultra-compact, hydrogen-depleted, and helium-rich, accreting binaries with degenerate or semidegenerate donors. We report the discovery of five new eclipsing AM CVn systems with orbital periods of 61.5, 55.5, 53.3, 37.4, and 35.4 min. These systems were discovered by searching for deep eclipses in the Zwicky Transient Facility (ZTF) light curves of white dwarfs selected using Gaia parallaxes. We obtained phase-resolved spectroscopy to confirm that all systems are AM CVn binaries, and we obtained high-speed photometry to confirm the eclipse and characterize the systems. The spectra show double-peaked H e lines but also show metals, including K and Zn, elements that have never been detected in AM CVn systems before. By modelling the high-speed photometry, we measured the mass and radius of the donor star, potentially constraining the evolutionary channel that formed these AM CVn systems. We determined that the average mass of the accreting white dwarf is ≈0.8 M⊙, and that the white dwarfs in long-period systems are hotter than predicted by recently updated theoretical models. The donors have a high entropy and are a factor of ≈2 more massive compared to zero-entropy donors at the same orbital period. The large donor radius is most consistent with H e-star progenitors, although the observed spectral features seem to contradict this. The discovery of five new eclipsing AM CVn systems is consistent with the known observed AM CVn space density and estimated ZTF recovery efficiency.

79 ASTRONOMY AND ASTROPHYSICS↗
DOE OSTI2022

A Flux Balancing Strategy for 10-kV SiC-Based Dual-Active-Bridge Converter

The transformer flux unbalance in dual-active-bridge (DAB) converters is a critical issue due to the electrical parameter and modulation mismatch, and load or control transients. Compared to low voltage DAB converters, the unbalance problem in medium voltage DAB converters may cause more severe problem, and become more difficult to deal with, because of the high operating voltage and insulation requirement. In this paper, a flux balancing strategy for a medium voltage (MV) DAB converter is proposed, including the transformer design with ferrite gap, current harmonic-based unbalance detection, as well as the flux balancing control scheme. With the proposed ferrite gap, nonlinear magnetizing current and its modeling are induced. Then, by analyzing the current harmonics, the flux unbalance level can be detected, and hence controlled. Test results have verified the proposed method in a MV DAB converter.

Gao, Zihan↗
DOE OSTI2025

Analysis of Liquids Using the Submerged Plasma for Isotopic Detection and Elemental Resolution (SPIDER)

We developed a sensor called the Submerged Plasma for Isotopic Detection and Elemental Resolution (SPIDER) probe, which uses an atmospheric pressure glow discharge below the surface of liquids to excite species in the liquid. Through emission spectroscopy of molten salts, liquid metals, and heavy water, we demonstrated the SPIDER probe’s high resolution, accuracy, and versatility. We successfully identified trace concentrations of transition and rare-earth metals in molten salts and detected the isotopic shift of the H β → D β emission line. Our analysis revealed unconventional spectral alkali line shapes, indicating two competing excitation modes: film explosion and droplet vaporization. The film explosion mode, characterized by dense plasma, exhibited self-reversal and broadband continuum emission, while the droplet vaporization mode, associated with diffusive plasma, produced narrow-line emissions. Furthermore, by analyzing circuit transients alongside individual plasma events, we observed that film explosions generate higher currents, likely due to a shorter plasma length as the current preferentially flows through the thin liquid layer. Altogether, our results highlight the SPIDER probe’s efficacy and flexibility, making it well-suited for online material quantification of liquids in extreme environments.

AES↗
NASA NTRS1984

1E 0104.2 + 3153 - A broad absorption-line QSO viewed through a giant elliptical galaxy

The optical identification of the X-ray source 1E 0104.2 + 3153 is complicated by the close projection of a broad absorption-line (BAL) QSO (z = 2.027) 10 arcsec from a giant elliptical galaxy (z = 0.111) at the center of a compact group of galaxies. At only 1.2 de Vaucouleur radii (16 kpc for H sub 0 = 100 km/s Mpc) this QSO-galaxy projection is the closest yet discovered. Based upon current observations, the source of the X-ray emission cannot be conclusively determined. Present in the BAL QSO spectrum are extremely strong Ca II H and K absorption lines due to the intervening galaxy, the first optical detection of the cold interstellar medium in an elliptical galaxy. The strength of these lines (EW = 2 and 1 A) requires observation through several interstellar clouds in the line of sight to the QSO. By its proximity to the central regions of the elliptical galaxy and the relative distances of the galaxy and QSO, this QSO is a particularly good candidate for observing dramatic transient gravitational lensing phenomena due to halo stars in the foreground galaxy.

Stocke, J. T.↗
NASA NTRS1999

Automated Fluid Feature Extraction from Transient Simulations

In the past, feature extraction and identification were interesting concepts, but not required to understand the underlying physics of a steady flow field. This is because the results of the more traditional tools like iso-surfaces, cuts and streamlines were more interactive and easily abstracted so they could be represented to the investigator. These tools worked and properly conveyed the collected information at the expense of much interaction. For unsteady flow-fields, the investigator does not have the luxury of spending time scanning only one "snap-shot" of the simulation. Automated assistance is required in pointing out areas of potential interest contained within the flow. This must not require a heavy compute burden (the visualization should not significantly slow down the solution procedure for co-processing environments like pV3). And methods must be developed to abstract the feature and display it in a manner that physically makes sense. The following is a list of the important physical phenomena found in transient (and steady-state) fluid flow: (1) Shocks, (2) Vortex cores, (3) Regions of recirculation, (4) Boundary layers, (5) Wakes. Three papers and an initial specification for the (The Fluid eXtraction tool kit) FX Programmer's guide were included. The papers, submitted to the AIAA Computational Fluid Dynamics Conference, are entitled : (1) Using Residence Time for the Extraction of Recirculation Regions, (2) Shock Detection from Computational Fluid Dynamics results and (3) On the Velocity Gradient Tensor and Fluid Feature Extraction.

Haimes, Robert↗
DOE OSTI2024

Overview of the distributed image processing infrastructure to produce the Legacy Survey of Space and Time

The Vera C. Rubin Observatory is preparing to execute the most ambitious astronomical survey ever attempted, the Legacy Survey of Space and Time (LSST). Currently the final phase of construction is under way in the Chilean Andes, with the Observatory’s ten-year science mission scheduled to begin in 2025. Rubin’s 8.4-meter telescope will nightly scan the southern hemisphere collecting imagery in the wavelength range 320–1050 nm covering the entire observable sky every 4 nights using a 3.2 gigapixel camera, the largest imaging device ever built for astronomy. Automated detection and classification of celestial objects will be performed by sophisticated algorithms on high-resolution images to progressively produce an astronomical catalog eventually composed of 20 billion galaxies and 17 billion stars and their associated physical properties. In this article we present an overview of the system currently being constructed to perform data distribution as well as the annual campaigns which reprocess the entire image dataset collected since the beginning of the survey. These processing campaigns will utilize computing and storage resources provided by three Rubin data facilities (one in the US and two in Europe). Each year a Data Release will be produced and disseminated to science collaborations for use in studies comprising four main science pillars: probing dark matter and dark energy, taking inventory of solar system objects, exploring the transient optical sky and mapping the Milky Way. Also presented is the method by which we leverage some of the common tools and best practices used for management of large-scale distributed data processing projects in the high energy physics and astronomy communities. We also demonstrate how these tools and practices are utilized within the Rubin project in order to overcome the specific challenges faced by the Observatory.

79 ASTRONOMY AND ASTROPHYSICS↗
DOE OSTI2023

Optical polarization and spectral properties of the hydrogen-poor superluminous supernovae SN 2021bnw and SN 2021fpl

ABSTRACT New optical photometric, spectroscopic, and imaging polarimetry data are combined with publicly available data to study some of the physical properties of the two hydrogen-poor superluminous supernovae (SLSNe) SN 2021bnw and SN 2021fpl. For each SLSN, the best-fitting parameters obtained from the magnetar model with Modular Open-Source Fitter for Transients do not depart from the range of parameter obtained on other SLSNe discussed in the literature. A spectral analysis with SYN++ shows that SN 2021bnw is a W type, fast evolver, while SN 2021fpl is a 15bn type, slow evolver. The analysis of the polarimetry data obtained on SN 2021fpl at four epochs (+1.8, +20.6, +34.1, and +43.0 d, rest frame) shows >3σ polarization detections in the range of 0.8–1 per cent. A comparison of the spectroscopy data suggests that SN 2021fpl underwent a spectral transition a bit earlier than SN 2015bn, during which, similarly, it could have underwent a polarization transition. The analysis of the polarimetry data obtained on SN 2021bnw does not show any departure from symmetry of the photosphere at an empirical diffusion time-scale of ≈2 (+81.1 d rest frame). This result is consistent with those on the sample of W-type SLSN observed at empirical diffusion time-scale ≤ 1 with that technique, even though it is not clear the effect of limited spectral windows varying from one object to the other. Measurements at higher empirical diffusion time-scale may be needed to see any departure from symmetry as it is discussed in the literature for SN 2017egm.

Astronomy & Astrophysics↗
DOE OSTI2023

High-pressure phase of cold-compressed bulk graphite and graphene nanoplatelets

Here, we have studied the high-pressure vibrational and structural behavior of bulk graphite and graphene nanoplatelets at room temperature by means of high-pressure Raman spectroscopic and x-ray diffraction probes. We have detected a clear pressure-induced structural transition in both materials, evidenced by the appearance of new Bragg peaks and Raman features, deviating from the starting hexagonal graphitic structure. The high-pressure phase is identified as a partially disordered orthorhombic structure, consisting of mixed sp 2 - and sp 3 -type bonding. Our experimental findings serve as direct evidence for the existence of a metastable transient modification in cold compressed carbon, lying between the sp 2 -type graphite and sp 3 -type diamond allotropes.

75 CONDENSED MATTER PHYSICS, SUPERCONDUCTIVITY AND↗
NASA NTRS1991

Comparison of Doppler scintillation and in situ spacecraft plasma measurements of interplanetary disturbances

Results are presented of detailed comparisons between Doppler scintillation and in situ plasma measurements to improve the understanding of Doppler scintillation transients. During a combined observing period of nearly 3 mo in 1981-1982 near solar maximum, 22 transients were observed by the Pioneer Venus Orbiter spacecraft and 23 shocks were observed by Helios 1. It is found that at least 84 percent of the transients are shocks, while at least 90 percent of the shocks are transients. Although the temporal profiles of Doppler scintillation and mass flux density are similar, the magnitudes of the Doppler scintillation transients may not simply reflect those of mass flux density. Only one pronounced solar wind event that was observed in the mass flux density measurements showed no signature in the scintillation data; field and particle measurements by Helios 1 suggest that it is a noncompressive density enhancement and/or a magnetic cloud. It is shown that Doppler scintillation measurements can now be used by themselves to detect and locate interplanetary shocks near the sun with a relatively high degree of certainty.

Woo, Richard↗
NASA NTRS1991

Carbonaceous compounds in comets - Infrared observations

The Comet Halley observations showed that carbon is a major component of the comet nucleus, with mass spectroscopic data giving near-cosmic C/O ratios. Gaseous and solid compounds were also observed with infrared spectroscopy, which gave detections of CO and CO2, probable detections or upper limits of H2CO and CH4, and a tentative detection of OCS. The CH4/CO ratio of less than unity in Comet Halley points to a CO-rich solar nebula; however, the ratio is higher than in interstellar clouds. A broad, complicated emission feature near 3.4 microns is evidence for carbonaceous compounds containing C-H groups in gas or solid phases. Analysis of radiation mechanisms and abundance constraints suggests that thermal emission or transient heating by single photons can account for the 3.4-micron emission feature. The band resembles (but is not identical to) bands of carbonaceous chondrite organic material, synthetic materials, and interstellar carbonaceous bands.

Encrenaz, T.↗
NASA NTRS2007

Diurnal Lightning Distributions as Observed by the Optical Transient Detector (OTD) and the Lightning Imaging Sensor (LIS)

Data obtained from the OTD (April 1995 to March 2000) and LIS (December 1997 to December 2005) satellites (70 and 35 degree inclination low earth orbits, respectively) are used to statistically determine the number of flashes in the diurnal cycle both as a function of local and universal time. Also included are global flash density maps. The data are further subdivided by season, continental versus oceanic, night time versus day time, northern versus southern hemisphere, and other regions of interest. The data include corrections for detection efficiency and instrument view time. The data are compared with both the "Carnegie Curve" and the diurnal global thunderstorm contributions from thunderday statistics from different continents, and are found to agree closely in phase and amplitude with the global thunderday statistics. The analysis also indicates that the southern hemisphere spring (September to November) has larger amplitude than the southern hemisphere fall (March to May). This may be due to differences in the contribution from the Brazilian rain forest during these periods. In general, as highlighted by a difference analysis, more lightning is observed in local springtime than the fall for continental locations, while oceanic regions display an opposite effect. For some areas of the world, the peak of diurnal curve appears to be shifted to later in the evening.

Bailey, Jeff C.↗
DOE OSTI2024

Nuclear reactor radiation and temperature effects on piezoelectric surface acoustic wave devices

Surface acoustic wave (SAW) resonators were characterized in-situ in a nuclear reactor environment at high temperature. Devices based on lithium niobate (LiNbO 3 ), aluminum nitride (sc-AlN), and thin-film aluminum nitride on sapphire substrate (AlN/sapphire) were tested up to 400 °C temperature and 1.9 × 10 12 n/cm 2 s neutron flux. Shifts in device resonant frequency were detected in response to temperature and neutron flux. Devices undergo a frequency change when exposed to neutron flux. At 300 °C, AlN/sapphire produced the strongest neutron flux response about 1.02 ppm at 1.27 × 10 12 n/cm 2 s neutron flux (5.7 × 10 4 rad-Si/hr neutron dose rate), compared to 0.30 ppm for LiNbO 3 and 0.17 ppm for sc-AlN. While the transient kinetics in response to step change in neutron flux support the defect-accumulation mechanism, the concurrent measurement of device temperature using resistive temperature sensor suggests additional heating caused by absorption of gamma rays can also play a role. These results make SAW devices attractive candidates for sensor applications in extreme environments.

Aluminum nitride↗
DOE OSTI2025

Bringing weak transitions to light

Abstract Weak transitions between quantum states are of fundamental importance for a broad range of phenomena from analytical biochemistry to precision physics, but generally challenge experimental detection. Due to their small cross sections scaling with the absolute square of their transition matrix elements, spectroscopic measurements often fail in particular in the presence of competing background processes. Here we introduce a general concept to break this scaling law and enhance the transition probability by exploiting a stronger laser-coupled pathway to the same excited state. We demonstrate the concept experimentally by attosecond transient absorption spectroscopy in helium atoms. The quasi-forbidden transitions from the ground state 1s 2 to the weakly coupled doubly excited 2p3dandsp 2,4− states are boosted by an order of magnitude. Enhancing single-photon-suppressed transitions can find widespread applicability, from spectral diagnostics of complex molecules in life and chemical sciences to precision spectroscopy of weak transitions in metastable atomic nuclei in the search for new physics.

Science & Technology - Other Topics↗
NASA NTRS1973

Cardiac R-wave detector with automatic sensitivity control

An electronic circuit that automatically changes its sensitivity was developed for detecting the bioelectric signal resulting from activation of the heart's ventricles. Regulation of sensitivity was accomplished with two feedback channels that maintain the sensitivity level between an upper and a lower limit. These limits are proportional to the R-wave amplitude. Tests on an experimental circuit demonstrated a capability to reject unwanted signal noise, illustrated difficulties encountered without sensitivity control, and presented closed loop transients which occurred for step changes in R-wave amplitude.

Gebben, V. D.↗
NASA NTRS2004

Global Lightning Activity

Our knowledge of the global distribution of lightning has improved dramatically since the advent of spacebased lightning observations. Of major importance was the 1995 launch of the Optical Transient Detector (OTD), followed in 1997 by the launch of the Lightning Imaging Sensor (LIS). Together, these instruments have generated a continuous eight-year record of global lightning activity. These lightning observations have provided a new global perspective on total lightning activity. For the first time, total lightning activity (cloud-to-ground and intra-cloud) has been observed over large regions with high detection efficiency and accurate geographic location. This has produced new insights into lightning distributions, times of occurrence and variability. It has produced a revised global flash rate estimate (44 flashes per second) and has lead to a new realization of the significance of total lightning activity in severe weather. Accurate flash rate estimates are now available over large areas of the earth (+/- 72 deg. latitude). Ocean-land contrasts as a function of season are clearly reveled, as are orographic effects and seasonal and interannual variability. The space-based observations indicate that air mass thunderstorms, not large storm system dominate global activity. The ability of LIS and OTD to detect total lightning has lead to improved insight into the correlation between lightning and storm development. The relationship between updraft development and lightning activity is now well established and presents an opportunity for providing a new mechanism for remotely monitoring storm development. In this concept, lightning would serve as a surrogate for updraft velocity. It is anticipated that this capability could lead to significantly improved severe weather warning times and reduced false warning rates. This talk will summarize our space-based lightning measurements, will discuss how lightning observations can be used to monitor severe weather, and present a concept for continuous geostationary-based lightning observations.

Christian, Hugh J.↗