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Search indexed NASA NTRS and DOE OSTI research on propulsion, heat transfer, battery materials and energy systems. Follow report and document links to the original sources.

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At least 1,063 records · Page 59
All sourcesNASA NTRSDOE OSTI
DOE OSTI2023

Perfect Crystals: microgravity capillary counterdiffusion crystallization of human manganese superoxide dismutase for neutron crystallography

The NASA mission Perfect Crystals used the microgravity environment on the International Space Station (ISS) to grow crystals of human manganese superoxide dismutase (MnSOD)—an oxidoreductase critical for mitochondrial vitality and human health. The mission’s overarching aim is to perform neutron protein crystallography (NPC) on MnSOD to directly visualize proton positions and derive a chemical understanding of the concerted proton electron transfers performed by the enzyme. Large crystals that are perfect enough to diffract neutrons to sufficient resolution are essential for NPC. This combination, large and perfect, is hard to achieve on Earth due to gravity-induced convective mixing. Capillary counterdiffusion methods were developed that provided a gradient of conditions for crystal growth along with a built-in time delay that prevented premature crystallization before stowage on the ISS. Here, we report a highly successful and versatile crystallization system to grow a plethora of crystals for high-resolution NPC.

37 INORGANIC, ORGANIC, PHYSICAL, AND ANALYTICAL CH↗
DOE OSTI2022

Mapping periplasmic binding protein oligosaccharide recognition with neutron crystallography

Numerous studies have shown how periplasmic binding proteins (PBPs) bind substrates with exquisite specificity, even distinguishing between sugar epimers and anomers, or structurally similar ions. Yet, marked substrate promiscuity is also a feature encoded in some PBPs. Except for three sub-Ångström crystal structures, there are no reports of hydrogen atom positions in the remaining (> 1000) PBP structures. The previous X-ray crystal structure of the maltodextrin periplasmic-binding protein from Thermotoga maritima (tmMBP) complexed with oligosaccharide showed a large network of interconnected water molecules stretching from one end of the substrate binding pocket to the other. These water molecules are positioned to form multiple hydrogen bonds, as well as forming interactions between the protein and substrate. Here we present the neutron crystal structure of tmMBP to a resolution of 2.1 Å. This is the first neutron crystal structure from the PBP superfamily and here we unambiguously identify the nature and orientation of the hydrogen bonding and water-mediated interactions involved in stabilizing a tetrasaccharide in the binding site. More broadly, these results demonstrate the conserved intricate mechanisms that underlie substrate-specificity and affinity in PBPs.

59 BASIC BIOLOGICAL SCIENCES↗
DOE OSTI2026

3D printed water-stable Cd-doped Cs 4 MnBi 2 Cl 12 /polylactic acid perovskite/polymer composites for high-flux X-ray scintillation

Stable and efficient X-ray scintillators are crucial for medical diagnostics, industrial, and defense applications. However, conventional scintillator technologies face a trade-off between stability, optimal performance, and sustainability. Herein, we introduce 3D-printed Cs 4 MnBi 2 Cl 12 (Pero1) and Cs 4 Cd 0.68 Mn 0.32 Bi 2 Cl 12 (Pero2) perovskite microcrystals embedded within a polylactic acid (PLA) polymer composite as X-ray scintillators, combining efficiency, stability, and sustainability. The orange luminescent perovskite powder phosphors exhibited poor water stability, which was successfully addressed through incorporation into PLA via filament extrusion and fused deposition modeling (FDM) 3D printing. The resulting composite films demonstrated remarkable water stability while maintaining uniform orange emission throughout the polymer matrix, as confirmed by 3D topography scanning and X-ray fluorescence mapping. Structural characterization revealed minimal chemical interaction between the perovskite and PLA matrix, with the composites retaining their crystalline properties. The PLA-Pero2 composite exhibited superior optical properties, with a photoluminescence quantum yield of 47%, nearly 17 times higher than that of PLA-Pero1 (2.8%), attributed to the effective suppression of non-radiative decay pathways through Cd 2+ doping. Under hard X-ray irradiation at synchrotron beamlines, both composites exhibited excellent radioluminescence, with emission peaks at 605 nm, a linear response across a wide X-ray flux range, and remarkable radiation stability, showing less than 3% intensity degradation after 600 seconds of continuous high-dose exposure. The PLA-Pero2 composite achieved a spatial resolution of 5 line pairs per millimeter and a contrast ratio of 0.255. These performance metrics, combined with the polymer's biodegradability and scalability through additive manufacturing, position PLA-based composites as a more sustainable alternative to conventional petroleum-based polymer scintillators for next-generation medical imaging, radiation monitoring, and industrial radiography applications.

3D Printing↗
DOE OSTI2024

Uncovering the three-dimensional structure of upconverting core–shell nanoparticles with multislice electron ptychography

In photon upconverting core–shell nanoparticles, structure strongly dictates performance. Typical imaging in scanning transmission electron microscopy has sufficient resolution to probe the atomic structure of these nanoparticles, but contrast, dose, and projection limitations make conventional methods insufficient for fully characterizing these structures. Phase retrieval techniques provide a promising alternative imaging mode, and, in particular, multislice electron ptychography can recover depth-dependent information. Here, we study beam-sensitive photon upconverting core–shell nanoparticles with a multislice ptychography approach using a low electron dose to avoid damage. Large strain fields arise in these heterostructures due to the mismatch in lattice parameter between the core and the shell. We reconstruct both a nanoparticle that appears defect-free and one that has a large break in the side and map the distribution of strain in 3D by computing distortion fields from high-resolution potential images of each slice. In the defect-free nanoparticle, we observe twisting of the shell, while in the broken nanoparticle, we measure the 3D position of the crack, the core, and dislocations. These results highlight the advantage of multislice electron ptychography to recover 3D information from a single scan, even under strict electron dose requirements from beam-sensitive samples.

74 ATOMIC AND MOLECULAR PHYSICS↗
DOE OSTI2022

Graph Neural Networks for low-energy event classification & reconstruction in IceCube

IceCube, a cubic-kilometer array of optical sensors built to detect atmospheric and astrophysical neutrinos between 1 GeV and 1 PeV, is deployed 1.45 km to 2.45 km below the surface of the ice sheet at the South Pole. The classification and reconstruction of events from the in-ice detectors play a central role in the analysis of data from IceCube. Reconstructing and classifying events is a challenge due to the irregular detector geometry, inhomogeneous scattering and absorption of light in the ice and, below 100 GeV, the relatively low number of signal photons produced per event. To address this challenge, it is possible to represent IceCube events as point cloud graphs and use a Graph Neural Network (GNN) as the classification and reconstruction method. The GNN is capable of distinguishing neutrino events from cosmic-ray backgrounds, classifying different neutrino event types, and reconstructing the deposited energy, direction and interaction vertex. Based on simulation, we provide a comparison in the 1 GeV–100 GeV energy range to the current state-of-the-art maximum likelihood techniques used in current IceCube analyses, including the effects of known systematic uncertainties. For neutrino event classification, the GNN increases the signal efficiency by 18% at a fixed background rate, compared to current IceCube methods. Alternatively, the GNN offers a reduction of the background (i.e. false positive) rate by over a factor 8 (to below half a percent) at a fixed signal efficiency. For the reconstruction of energy, direction, and interaction vertex, the resolution improves by an average of 13%–20% compared to current maximum likelihood techniques in the energy range of 1 GeV–30 GeV. The GNN, when run on a GPU, is capable of processing IceCube events at a rate nearly double of the median IceCube trigger rate of 2.7 kHz, which opens the possibility of using low energy neutrinos in online searches for transient events.

47 OTHER INSTRUMENTATION↗
DOE OSTI2023

Construction of precision sMDT detector for the ATLAS Muon Spectrometer upgrade

Here, this paper describes the small-diameter monitored drift-tube detector construction at the University of Michigan as a contribution to the ATLAS Muon Spectrometer upgrade for the high-luminosity Large Hadron Collider at CERN. Measurements of the first 30 chambers built at Michigan show that the drift tube wire position accuracy meets the specification of 20 μm. The positions of the platforms for alignment and magnetic field sensors are all installed well within the required precision. The cosmic ray test measurements show single wire tracking resolution of 100 ± 7 μm with an average detection efficiency above 99%. The infrastructure, tooling, techniques, and procedures for chamber production are described in detail. The results from the chamber quality control tests of the first 30 constructed chambers are reported.

47 OTHER INSTRUMENTATION↗
NASA NTRS1972

TIROS-N spacecraft jitter calculations

The TIROS-N television infrared observatory system is discussed. The characteristics of the primary payload sensor are presented. The attitude control system jitter specification for satisfactory performance of the sensor is analyzed. The primary sensor is the advanced very high resolution radiometer. The TIROS-N satellite is an orbital platform carrying a number of earth observation sensors. The requirements for three axis attitude control for proper positioning of the sensors are reported.

Fleisher, G. M.↗
NASA NTRS1972

ATS ranging and position fixing experiment, phase 3

The experiments to test the concept of position location by range measurements from pairs of satellites in the L-band using ATS-5 are reported. Results of the ranging experiments confirmed that ranging resolution measured in tens or hundreds of feet may be achieved at VHF and L-band within the radio frequency bandwidths used for communications with simple, inexpensive, automatic equipment.

Anderson, R. E.↗
NASA NTRS1978

A precision measurement of the X-ray polarization of the Crab Nebula without pulsar contamination

The linear X-ray polarization of the Crab Nebula has been precisely measured at 2.6 keV and 5.2 keV with the OSO 8 graphite crystal polarimeters. The 1.4 ms time resolution of these instruments permitted the removal of any contribution to the polarization from the pulsar. The nebular polarization is 19.2% plus or minus 1.0% at a position angle of 156.4 plus or minus 1.4 deg at 2.6 keV. At 5.2 keV the corresponding results are 19.5% plus or minus 2.8% at 152.6 plus or minus 4.0 deg.

Weisskopf, M. C.↗
NASA NTRS1981

A CCD tracker for closed-loop instrument pointing at Halley's comet

An optical tracker based on CCD technology has been developed for the closed-loop pointing of the narrow-angle imaging system of the proposed Halley's comet intercept mission at the comet nucleus. The target tracker, needed to assure the accurate pointing of science instruments as the nucleus rapidly passes the spacecraft, is a component of the pointing control system, which also includes a two-axis articulated instrument platform and high-resolution optical encoders to measure platform orientation relative to spacecraft structure. The device was designed on the basis of a CCD imaging array to calculate target centroid position based on the optical intensity of all pixels containing the image, and a processor to perform spacecraft attitude control, pointing control and target tracker control and data processing functions. The tracker has been configured to operate in both target acquisition and tracking modes. Preliminary simulation results and past experiments on similar trackers indicate that excellent tracking performance can be achieved, and a breadboard version of the tracker is currently being fabricated.

Stanton, R. H.↗
NASA NTRS1982

High-resolution imaging with a two-dimensional resistive anode photon counter

A method to achieve high spatial resolution readout of individual photoelectron events using microchannel plates and a resistive anode is presented. A clamped pair of microchannel plates is used, followed by a gap and a clamped triplet of microchannel plates in cascade to achieve a high stable electron gain of 3 x 10 to the 7th. The gain allows the position determination of each photoelectron event with a very high signal-to-noise ratio. A model consisting of a windowless vacuum-ultraviolet image sensor is presented to demonstrate 500 x 500 pixel images of 50 micron FWHM over a 25-mm circular field of view. The detector offers sufficient speed, sensitivity and resolution for a variety of applications, and the mount design is compatible with planar, remotely-processed, proximity-focused photocathodes.

Firmani, C.↗
NASA NTRS1984

Coupled orbiting inertial reference systems and Geopotential Research Mission (GRM) geodesy

Two spacecraft, one following the other with a separation of a few hundred kilometers and orbiting at an altitude of 160 km in a 90-degree polar orbit, are used to detect the minute variations in the earth's gravitational field. Housed in a capacitive cavity located at the centroid of the spacecraft is a free-floating metallic spherical proof-mass, which is the sensor controlling the thrusters that nullify all nongravitational forces on the spacecraft. The proof-mass in each spacecraft is the inertial-guidance reference for its host spacecraft, and the proof-masses are coupled together by a millimeter-wave link. This coupled system detects minute changes in the spacecraft's orbital positions and thus measures the anomalies present in the gravitational field of the earth. To derive a global geodetic model of the gravitational field with an amplitude resolution of 1 milligal and a spatial resolution of 100 km requires that the relative velocity between the proof-mass references be determined to within 1 micron/s.

Keating, T.↗
NASA NTRS1988

Laboratory studies of the infrared spectral propertries of CO in astrophysical ices

The spectral properties of CO in various ices are presented. Included are peak positions, FWHMs, band profiles, and integrated absorbances of the CO fundamental at 2137/cm in different ices under various conditions. The results reveal that good quality moderate-resolution spectra of the interstellar CO feature can be used to unravel the composition, temperature, and thermal history of interstellar and cometary ices containing CO.

Sandford, S. A.↗
NASA NTRS1992

640 x 480 MWIR and LWIR camera system developments

The performance of a 640 x 480 PtSi, 3,5 microns (MWIR), Stirling cooled camera system with a minimum resolvable temperature of 0.03 is considered. A preliminary specification of a full-TV resolution PtSi radiometer was developed using the measured performance characteristics of the Stirling cooled camera. The radiometer is capable of imaging rapid thermal transients from 25 to 250 C with better than 1 percent temperature resolution. This performance is achieved using the electronic exposure control capability of the MOS focal plane array (FPA). A liquid nitrogen cooled camera with an eight-position filter wheel has been developed using the 640 x 480 PtSi FPA. Low thermal mass packaging for the FPA was developed for Joule-Thomson applications.

Tower, J. R.↗
NASA NTRS1993

Evidence for precession of the R Aquarii jet

Several models of the R Aqr northeast jet have been proposed which attempt to explain the presence of shock excitation, resulting in a confusing picture of this nearest astrophysical jet. This paper compares observations of the jet in the R Aqr system with the HST's Faint Object Camera (FOC) and radio continuum images acquired with the VLA. The forbidden-O III jet structure is derived from restored FOC imagery, which has been convolved with an elliptical Gaussian of the same size as the restoring beam of the 6-cm VLA maps, allowing image comparison at the same spatial resolution. It is found that, at increasing distances from the central star, the forbidden O III emission knots that comprise the optical jet occur at systematically larger position angles when compared with corresponding features in the radio images. The angular separation of forbidden O III and radio continuum emission can be understood in terms of a shock formed when ejecta in the stream interacts with previously existing circumstellar material and subsequently cools by nebular line emission.

Hollis, J. M.↗
NASA NTRS2012

Advances and Limitations of Atmospheric Boundary Layer Observations with GPS Occultation over Southeast Pacific Ocean

The typical atmospheric boundary layer (ABL) over the southeast (SE) Pacific Ocean is featured with a strong temperature inversion and a sharp moisture gradient across the ABL top. The strong moisture and temperature gradients result in a sharp refractivity gradient that can be precisely detected by the Global Positioning System (GPS) radio occultation (RO) measurements. In this paper, the Constellation Observing System for Meteorology, Ionosphere & Climate (COSMIC) GPS RO soundings, radiosondes and the high-resolution ECMWF analysis over the SE Pacific are analyzed. COSMIC RO is able to detect a wide range of ABL height variations (1-2 kilometer) as observed from the radiosondes. However, the ECMWF analysis systematically underestimates the ABL heights. The sharp refractivity gradient at the ABL top frequently exceeds the critical refraction (e.g., −157 N-unit per kilometer) and becomes the so-called ducting condition, which results in a systematic RO refractivity bias (or called N-bias) inside the ABL. Simulation study based on radiosonde profiles reveals the magnitudes of the N-biases are vertical resolution dependent. The N-bias is also the primary cause of the systematically smaller refractivity gradient (rarely exceeding −110 N-unit per kilometer) at the ABL top from RO measurement. However, the N-bias seems not affect the ABL height detection. Instead, the very large RO bending angle and the sharp refractivity gradient due to ducting allow reliable detection of the ABL height from GPS RO. The seasonal mean climatology of ABL heights derived from a nine-month composite of COSMIC RO soundings over the SE Pacific reveals significant differences from the ECMWF analysis. Both show an increase of ABL height from the shallow stratocumulus near the coast to a much higher trade wind inversion further off the coast. However, COSMIC RO shows an overall deeper ABL and reveals different locations of the minimum and maximum ABL heights as compared to the ECMWF analysis. At low latitudes, despite the decreasing number of COSMIC RO soundings and the lower percentage of soundings that penetrate into the lowest 500-m above the mean-sea-level, there are small sampling errors in the mean ABL height climatology. The difference of ABL height climatology between COSMIC RO and ECMWF analysis over SE Pacific is significant and requires further studies.

COSMIC RO↗
NASA NTRS2018

Remote Recession Measurements of Wire-Seeded PICA Samples in an Arc-Jet Flow

Various methods for remote recession sensing of PICA have been developed and several seeding methods have been tested. The most recent method involved seeding the ablator with wires fed to the sample from the backside with a defined amount of PICA left towards the upstream front of the sample. This seed method mimics the installation of in-depth thermocouples as they are frequently used in ground testing and flight. Arc-jet tests were conducted in the NASA Langley HYMETS facility at a heat flux of 320 W/sq.cm. The emission of the post-shock layer was observed in spectral resolution from the side along an optical axis perpendicular to the arc-jet flow and from the front, looking at the sample surface from an upstream position. Various metallic seed materials with different melting points were used. In addition to the emission spectroscopy measurements, the samples were monitored during the tests through pyrometry and videography. The time resolved response of the seeded material is described and compared to earlier tests with different seeding methods. The combination of seed materials was found to be critical for the selection of emission signatures characteristic for the material recession which can be isolated in the final emission spectra.

Winter, Michael↗