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At least 1,063 records · Page 59

Transformation enabled nitride magnets absent rare earths and a process of making the same

A process for producing an ordered martensitic iron nitride powder that is suitable for use as a permanent magnetic material is provided. The process includes fabricating an iron alloy powder having a desired composition and uniformity; nitriding the iron alloy powder by contacting the material with a nitrogen source in a fluidized bed reactor to produce a nitride iron powder; transforming the nitride iron powder to a disordered martensitic phase; annealing the disordered martensitic phase to an ordered martensitic phase; and separating the ordered martensitic phase from the iron nitride powder to yield an ordered martensitic iron nitride powder.

Matthiesen, David↗

A magnetic tunnel to shelter hyperpolarized fluids

To shield solutions carrying hyperpolarized nuclear magnetization from rapid relaxation during transfer through low fields, the transfer duct can be threaded through an array of permanent magnets. The advantages are illustrated for solutions containing hyperpolarized {sup 1}H and {sup 13}C nuclei in a variety of molecules.

37 INORGANIC, ORGANIC, PHYSICAL, AND ANALYTICAL CH↗

Structural Characteristics and Phase Evolution of Calcium-Reduced (Sm,Zr)(Fe,Co,Ti) 12 Particles

Magnetic materials are essential for applications in electronics, energy conversion and many other industrial and technological sectors. Among the permanent magnets, rare-earth magnets exhibit the strongest properties and dominate the market shares in related applications. However, due to the increasing cost and unstable supply, the research on reducing the rare-earth elements in magnets attracts significant increasing interest. Rare-earth-lean samarium transition metal (TM) compounds (SmTM 12 or 1:12 for short) have made breakthroughs in 2020 and the (Sm,Zr)(Fe,Co,Ti) 12 monocrystalline particles synthesized by a Ca reduction of elemental oxides at high temperature demonstrated an order of magnitude improvement in coercivity at room temperature. In this study, we made structural analysis of (Sm,Zr)(Fe,Co,Ti) 12 particles to elucidate the impact of synthesis conditions, microstructure and phase transformation on the evolution of magnetic properties.

36 MATERIALS SCIENCE↗

Initial performance of the magnet system in the splitter/combiner section of the Cornell-Brookhaven Energy-Recovery Linac Test Accelerator

The Cornell-Brookhaven Energy-recovery Linac Test Ac- celerator is a four-pass, 150-MeV electron accelerator with a six-cell 1.3 GHz superconducting-RF linear accelerator and a fixed-field alternating-gradient (FFAG) return loop made up of Halbach-style quadrupole magnets. The optics matching between the linear accelerator and the return loop is achieved with a conventional magnet system comprised of 50 dipole magnets and 64 quadrupole magnets in four beamlines at each end of the linac. The 42-, 78-, 114- and 150-MeV electron beams are separated into independent vacuum chambers in order to allow for the path-length ad- justment required by energy recovery. We report on the first beam tests of the initial installation of the splitter/combiner section at the exit of the linac. The vacuum system of the 42-MeV S1 line was installed during the first week of April. Nine dipole and four quadrupole magnets were installed and surveyed into position the following week, and the water cooling system was commissioned. A 6-MeV beam passed through the line on April 11 with no need for adjusting pre-set magnet excitation currents. One week later, time- of-flight measurements were used to calibrate and phase the individual superconducting RF cavities. The S1 magnet settings were then scaled up to achieve 5-cavity, 42-MeV operation through the first nine FFAG permanent-magnet quadrupoles. This initial Fractional Arc Test will conclude on May 18, when the installation of the remaining seven split- ter/combiner lines and the return loop will begin. CBETA operations are scheduled to begin in early 2019.

43 PARTICLE ACCELERATORS↗

A review of Magnetic Suspension and Balance Systems

This paper traces the development of Magnetic Suspension and Balance Systems (MSBSs) for use in wind tunnels. The expression MSBS implies a system that can both suspend a model and also measure the forces and moments acting on the model. This avoids the need for any mechanical support of the model. An MSBS uses electromagnets located outside the test section walls to create magnetic fields inside the test section. Measurement of the electrical current flowing in each of the electromagnets can be used to determine the forces and moments acting on the suspended model. An MSBS is capable of supporting a model with an internal magnetized core subject to gravity, aerodynamic, and inertial loads. The model must have a core made of either a permanent magnet, magnetized soft iron, or a solenoid. The position of the suspended body is inherently unstable. A closed-loop control system which includes a position sensing system has to control the position of the body by controlling the applied magnetic fields. This paper includes a discussion of all the known MSBSs and the outlook for larger systems.

Boyden, Richmond P.↗

Advanced technology lunar telescope

A new type of telescope pointing system designed specifically for space and lunar applications will be discussed, based upon a prototype advanced technology telescope under investigation. The focus here will be the system of hybrid superconductor magnetic bearings (HSMB) used to provide isolation support and steering functions. HSMB's are combinations of high temperature superconductors, permanent magnets, and coils, being passive (requiring no power), noncontact, and essentially frictionless. These also are well suited to long-term unattended operation in the space environment. The characteristics of these subsystems, their expected behavior under space vacuum, and thermal and radiation environments are discussed.

Wilson, Thomas L.↗

Advanced Processing of Functional Magnetic Materials

Functional materials, specifically those which respond to external stimuli such as magnetic and electrical field, are increasingly important for many green energy technologies. Functional magnetic materials are increasingly been investigated from basic and applied sciences perspectives. Probably, the best-known of these are permanent magnets, they are used to supply a magnetic field and are widely applied in motors, generators, data storage, sensors, and actuators. Other examples of functional materials include soft magnets, magnetocalorics, and thermoelectrics.

36 MATERIALS SCIENCE↗

Synthesis of Fe 16 N 2 compound Free-Standing Foils with 20 MGOe Magnetic Energy Product by Nitrogen Ion-Implantation

Rare-earth-free magnets are highly demanded by clean and renewable energy industries because of the supply constraints and environmental issues. A promising permanent magnet should possess high remanent magnetic flux density (Br), large coercivity (Hc) and hence large maximum magnetic energy product ((BH)max). Fe 16 N 2 has been emerging as one of promising candidates because of the redundancy of Fe and N on the earth, its large magnetocrystalline anisotropy (Ku>1.0×107 erg/cc), and large saturation magnetization (4πMs>2.4T). However, there is no report on the formation of Fe 16 N 2 magnet with high Br and large Hc in bulk format before. In this paper, we successfully synthesize freestanding Fe 16 N 2 foils with a coercivity of up to 1910Oe and a magnetic energy product of up to 20 MGOe at room temperature. Nitrogen ion implantation is used as an alternative nitriding approach with the benefit of tunable implantation energy and fluence. An integrated synthesis technique is developed, including a direct foil-substrate bonding step, an ion implantation step and a two-step post-annealing process. With the tunable capability of the ion implantation fluence and energy, a microstructure with grain size 25–30nm is constructed on the FeN foil sample with the implantation fluence of 5×10 17 /cm 2 .

36 MATERIALS SCIENCE↗

Magnetic attachment mechanism

A magnetic attachment mechanism adapted for interfacing with the manipulator arm of a remote manipulator system and comprising a pair of permanent magnets of rare earth material are arranged in a stator-rotor relationship. The rotor magnet is journalled for rotation about its longitudinal axis between pole plates of the stator magnet, each of which includes an adhering surface. In a first rotary position corresponding to the ON condition, each of the poles of the rotor magnet is closely adjacent to a stator magnet pole plate of like polarity whereby the respective magnet fields are additive for producing a strong magnetic field emanating from the adhering surfaces for attracting a ferrous magnetic plate, or the like, affixed to the payload. When the rotor magnet is rotated to a second position corresponding to the OFF condition, each of the poles of the rotor magnet is disposed closely adjacent to a pole plate of unlike polarity whereby the magnetic fields of the magnets are in cancelling relationship at the adhering surfaces, which permits the release of a payload. An actuator for selectively rotating the rotor magnet between the ON and OFF positions is provided for interfacing and connecting the magnetic attachment mechanism with a manipulator arm. For affecting an optimal rigidized attachment the payload is provided with guide means cooperable with guide means on the housing of the mechanism for directing adhering surfaces of the polar plates to the ferrous plate.

Wu, Mitchell B.↗

Single element magnetic suspension actuator

The invention, a single element magnetic suspension actuator with bidirectional force capability along a single axis, includes an electromagnet and a nonmagnetic suspended element. A permanent magnet mounted on the suspended element interacts with a magnetic field established by the electromagnet to produce bidirectional forces in response to a variable force command voltage V (sub FC) applied to the electromagnet. A sensor measures the position of the suspended element on the single axis which is a function of force command voltage V (sub FC).

Groom, Nelson J.↗

Transverse-displacement stabilizer for passive magnetic bearing systems

The invention provides a way re-center a rotor's central longitudinal rotational axis with a desired system longitudinal axis. A pair of planar semicircular permanent magnets are pieced together to form a circle. The flux from each magnet is pointed in in opposite directions that are both parallel with the rotational axis. A stationary shorted circular winding the plane of which is perpendicular to the system longitudinal axis and the center of curvature of the circular winding is positioned on the system longitudinal axis. Upon rotation of the rotor, when a transverse displacement of the rotational axis occurs relative to the system longitudinal axis, the winding will experience a time-varying magnetic flux such that an alternating current that is proportional to the displacement will flow in the winding. Such time-varying magnetic flux will provide a force that will bring the rotor back to its centered position about the desired axis.

42 ENGINEERING↗

Borderline Magnetism: How Adding Mg to Paramagnetic Ce Co 3 Makes a 450-K Ferromagnet with Large Magnetic Anisotropy

A recent experimental study [Phys. Rev. Appl. 9, 024023 (2018)] on paramagnetic CeCo 3 finds that magnesium alloying induces a ferromagnetic transition with intrinsic properties large enough for permanent magnet applications. Here we explain these surprising results via a first-principles study of the electronic structure and magnetism of magnesium-alloyed CeCo 3 . We find the origin of this magnesium-induced ferromagnetic transition to be Stoner physics—the substantial increase in the Fermi-level density of states N(E F ) with Mg alloying. Here, our calculations suggest that both Ce and Co atoms are likely to be important for generating large magnetic anisotropy suggesting the viability of Co-3d and Ce-4f interaction for the generation of magnetic anisotropy in magnetic materials. These results offer a route to the discovery of ferromagnetic materials and provide fundamental insight into the magnetic properties of these alloys.

36 MATERIALS SCIENCE↗

Magnetic attachment mechanism

A magnetic attachment mechanism adapted for interfacing with the manipulator arm (11) of a remote manipulator system and comprising a pair of permanent magnets (31,32) of rare earth material which are arranged in a stator-rotor relationship. The rotor magnet (32), is journalled for rotation about its longitudinal axis between pole plates (35,36) of the stator magnet (31), each of which includes an adhering surface (35a,36a). In a first rotary position corresponding to the ON condition, each of the poles of the rotor magnet (32) is closely adjacent a stator magnet pole plate of like polarity whereby the respective magnet fields are additive for producing a strong magnetic field emanating from the adhering surfaces (35a,36a) for attracting a ferrous magnetic plate 20, or the like, affixed to the payload (20 or 50). When the rotor magnet (32) is rotated to a second position corresponding to the OFF condition, each of the poles of the rotor magnet (31) is disposed closely adjacent a pole plate of unlike polarity whereby the magnetic fields of the magnets are in cancelling relationship at the adhering surfaces (35a,36a) which permits the release of a payload. An actuator (51 or 70) for selectively rotating the rotor magnet (32) between the ON and OFF positions is provided for interfacing and connecting the magnetic attachment mechanism with a manipulator arm. For effecting an optimal rigidized attachment the payload is provided with guides (91,92) cooperable with guides (96,16,17) on the housing of the mechanism for directing adhering surfaces (35a,36a) of the polar plates to the ferrous plate (20).

Harwell, William D.↗

Manipulation of Hole Spin Transport in Germanium

Downscaling of the silicon metal-oxide-semiconductor field-effect transistor technology is expected to reach a fundamental limit soon. A paradigm shift in computing is occurring. Spin field-effect transistors are considered a candidate architecture for next-generation microelectronics. Being able to leverage the existing infrastructure for silicon, a spin field-effect transistor technology based on group IV heterostructures will have unparalleled technical and economical advantages. For the same material platform reason, germanium hole quantum dots are also considered a competitive architecture for semiconductor-based quantum technology. In this project, we investigated several approaches to creating hole devices in germanium-based materials as well as injecting hole spins in such structures. We also explored the roles of hole injection in wet chemical etching of germanium. Our main results include the demonstration of germanium metal-oxide-semiconductor field-effect transistors operated at cryogenic temperatures, ohmic current-voltage characteristics in germanium/silicon-germanium heterostructures with ferromagnetic contacts at deep cryogenic temperatures and high magnetic fields, evaluation of the effects of surface preparation on carrier mobility in germanium/silicon- germanium heterostructures, and hole spin polarization through integrated permanent magnets. These results serve as essential components for fabricating next-generation germanium-based devices for microelectronics and quantum systems.

75 CONDENSED MATTER PHYSICS, SUPERCONDUCTIVITY AND↗

Intense Source of Polarized Hydrogen Atoms

Atoms produced by radio-frequency dissociation of hydrogen molecules sorted according to their hyperfine states in improved polarized hydrogen source. By use of combination of dc magnetic fields, atoms of upper hyperfine ground level selected in numbers greater than those of undesired F = O state. Source built with permanent magnets or electromagnets. Principal utility is source of polarized hydrogen for masers or experimental studies.

Maleki, L.↗

System identification of the Large-Angle Magnetic Suspension Test Facility (LAMSTF)

The Large-Angle Magnetic Suspension Test Facility (LAMSTF), a laboratory-scale research project to demonstrate the magnetic suspension of objects over wide ranges of attitudes, has been developed. This system represents a scaled model of a planned Large-Gap Magnetic Suspension System (LGMSS). The LAMSTF system consists of a planar array of five copper electromagnets which actively suspend a small cylindrical permanent magnet. The cylinder is a rigid body and can be controlled to move in five independent degrees of freedom. Five position variables are sensed indirectly by using infra-red light-emitting diodes and light-receiving phototransistors. The motion of the suspended cylinder is in general nonlinear and hence only the linear, time-invariant perturbed motion about an equilibrium state is considered. One of the main challenges in this project is the control of the suspended element over a wide range of orientations. An accurate dynamic model plans an essential role in controller design. The analytical model of the LAMSTF system includes highly unstable real poles (about 10 Hz) and low-frequency flexible modes (about 0.16 Hz). Projection filters are proposed to identify the state space model from closed-loop test data in time domain. A canonical transformation matrix is also derived to transform the identified state space model into the physical coordinate. The LAMSTF system is stabilized by using a linear quadratic regulator (LQR) feedback controller. The rate information is obtained by calculating the back difference of the sensed position signals. The reference inputs contain five uncorrelated random signals. This control input and the system reponse are recorded as input/output data to identify the system directly from the projection filters. The sampling time is 4 ms and the model is fairly accurate in predicting the step responses for different controllers while the analytical model has a deficiency in the pitch axis.

Huang, Jen-Kuang↗

CaloriSMART: Small-scale test-stand for rapid evaluation of active magnetic regenerator performance

We report operation of a device designed specifically for rapid experimental evaluation of performance of magnetocaloric materials in different magnetic fields using a compact active magnetic regenerator bed with a total volume of approximately 5 mL. Other features of the system include digital control of the rotating-permanent-magnet field source and custom dual-opposed syringe pump that enable precise tuning and coupling of the flow profile and the magnetic field profile. Performance of the device is demonstrated for flow volumes between 1 and 4 mL (utilization from 0.48 to 1.9), maximum magnetic fields of 1.13 and 1.45 T, and applied cooling powers from 0 to 20 W at frequencies from 0.5 to 4 Hz. A regenerator comprised of 25 g of 200 µm spherical Gd powder reached temperature spans of 19.3 K under no applied cooling load and 2.6 K under the maximum applied cooling load of 20 W. The device also achieves a very high specific exergetic cooling power of 73 W L -1 T -1 . Results obtained at two different maximum magnetic fields in the same device suggest a powerful new scaling for regenerator performance: the exergetic power quotient. The exergetic power quotient shows a simple scaling of device cooling performance with the amount of active material and the magnetic field strength. This suggests results from a small device correlate to expected performance of a larger regenerator, making the exergetic power quotient a well-suited parameter for evaluating functionality of active magnetic regenerators employing new magnetocaloric materials.

47 OTHER INSTRUMENTATION↗

Research Update: Plentiful magnetic moments in oxygen deficient SrTiO{sub 3}

Correlated band theory is employed to investigate the magnetic and electronic properties of different arrangements of oxygen di- and tri-vacancy clusters in SrTiO{sub 3}. Hole and electron doping of oxygen deficient SrTiO{sub 3} yields various degrees of magnetization as a result of the interaction between localized magnetic moments at the defect sites. Different kinds of Ti atomic orbital hybridization are described as a function of the doping level and defect geometry. We find that magnetism in SrTiO{sub 3−δ} is sensitive to the arrangement of neighbouring vacancy sites, charge carrier density, and vacancy-vacancy interaction. Permanent magnetic moments in the absence of vacancy doping electrons are observed. Our description of the charged clusters of oxygen vacancies widens the previous descriptions of mono- and multi-vacancies and points out the importance of the controlled formation at the atomic level of defects for the realization of transition metal oxide based devices with a desirable magnetic performance.

36 MATERIALS SCIENCE↗