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At least 1,063 records · Page 59

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DOE OSTI2025

Editorial: Applications of spectroscopy and chemometrics in nuclear materials analysis

Optical analysis techniques, including spectroscopy and image analysis, have many advantages when applied to the study of nuclear materials. They require small sample sizes, can be performed remotely, and can be proceduralized through consistent practice. Most importantly, they provide a wealth of information by generating multivariate data. For example, ultraviolet–visible–near-infrared absorbance spectroscopy of actinides in aqueous and organic solutions is dependent on the oxidation state, anionic complexation, and temperature. These variables are important for solution-based separation processes, and sensitivity to these factors, combined with online monitoring, can drive the efficiency and control of these processes. The morphology and chemical composition of actinide particles can also provide a vital clue to the mechanisms by which the particles were formed, providing forensic information on the origins of the particles.

11 NUCLEAR FUEL CYCLE AND FUEL MATERIALS↗

NASA NTRS1973

ERTS data user investigation to develop a multistage forest sampling inventory system

The author has identified the following significant results. A unique digital timber volume estimation system was developed for use with the MSS CCT tapes. The system was tested on a 64-square mile area in Northern California's Trinity Alps. The outcome of a systematic experiment, in which several possible combinations of bands 5 and 7 and a contrast measure were tried, showed that an estimated gain in precision of 50% can be obtained in a multistage sampling design. The difference between bands 5 and 7 proved to be of special importance for the estimation of biomass in the form of timber volume. In addition, an interpretation model for high flight U2 photographs was developed. A maximum multiple correlation coefficient of 0.74 was obtained for the regression model, explaining 55% of the variation in timber volume as estimated from aerial photos and ground measurments. An interpretation model for MSS color composites is in the testing stage.

Langley, P. G.↗

NASA NTRS1973

Evaluation of usefulness of Skylab EREP S-190 and S-192 imagery in multistage forest surveys

The author has identified the following significant results. A unique digital timber volume estimation system with digital data for two ERTS-1 MSS bands was tested. The system was tested on a 64-square mile area in Northern California's Trinity Alps. The outcome of a systematic experiment in which possible combinations of the two bands (MSS 5 and 7) were tried, showed than an estimated gain in precision of 50% can be obtained in a multistage sampling design. Especially the difference between the two bands proved to be of major importance for the estimation of biomass in the form of timber volume. Identical tests as the one performed will be conducted with various S-192 bands when the digital data become available.

Langley, P. G.↗

NASA NTRS1980

Artifacts in digital images

Three kinds of artifacts unique to digital images are illustrated, namely aliasing caused by undersampling, interference phenomena caused by improper display of images, and harmonic overtones caused by quantization of amplitudes. Special attention is given to undersampling when the sample size and interval are the same. It is noted that this situation is important because it is typical of solid-state cameras. Quantization of image data of necessity introduces energy at harmonic overtones of the image spectrum. This energy is aliased if the frequency of the overtones is greater than 0.5 cycle/pixel. It cannot be selectively removed from the image through filtering, and the best way to suppress it is to maximize the amplification of the sensor before digital encoding.

Lorre, J. J.↗

NASA NTRS1984

Estimating the Lifetimes of Nickel/Cadmium Cells

Equation based on model of flaw growth. Model assumes cell fails by growth of preexisting flaws. Flaws described by three important quantities: total number of flaws, distribution of flaw sizes and rate of flaw growth. When flaw reaches critical size failure occurs. Flaw concept, in addition to providing ready explanation for reduced lifetime, predicts two important charateristics: statistical variability of lifetime data and dependence of lifetime on volume of sample.

Fedors, R. F.↗

NASA NTRS1984

Wuestite (Fe/1-x/O) - A review of its defect structure and physical properties

Such complexities of the Wustite structure as nonstoichiometry, ferric iron variable site distribution, long and short range ordering, and exsolution, yield complex physical properties. Magnesiowustite, a phase which has been suggested to occur in the earth's lower mantle, is also expected to exhibit many of these complexities. Geophysical models including the properties of (Mg, Fe)O should accordingly take into account the uncertainties associated with the synthesis and measurement of iron-rich oxides. Given the variability of the Fe(1-x)O structure, it is important that future researchers define the structural state and extent of exsolution of their samples.

Hazen, R. M.↗

NASA NTRS1987

Wafer level reliability for high-performance VLSI design

As very large scale integration architecture requires higher package density, reliability of these devices has approached a critical level. Previous processing techniques allowed a large window for varying reliability. However, as scaling and higher current densities push reliability to its limit, tighter control and instant feedback becomes critical. Several test structures developed to monitor reliability at the wafer level are described. For example, a test structure was developed to monitor metal integrity in seconds as opposed to weeks or months for conventional testing. Another structure monitors mobile ion contamination at critical steps in the process. Thus the reliability jeopardy can be assessed during fabrication preventing defective devices from ever being placed in the field. Most importantly, the reliability can be assessed on each wafer as opposed to an occasional sample.

Root, Bryan J.↗

NASA NTRS1989

Convergent-Filament Nonmechanical Pump

Simple device induces small flow of liquid without help of moving parts, in presence or absence of gravity. Drops of liquid move on filaments from wide end of cone to narrow end. Gradually blend with drops on adjacent filaments to form large drops with menisci. Important use expected to be returning liquid condensate in heat pipes, and collection of samples from clouds or fog.

Collins, Earl R., Jr.↗

NASA NTRS1989

Chemical consequences of the initial diffusional growth of cloud droplets - A clean marine case

A simple microphysical cloud parcel model and a simple representation of the background marine aerosol are used to predict the concentrations and compositions of droplets of various sizes near cloud base. The aerosol consists of an externally-mixed ammonium bisulfate accumulation mode and a sea-salt coarse particle mode. The difference in diffusional growth rates between the small and large droplets as well as the differences in composition between the two aerosol modes result in substantial differences in solute concentration and composition with size of droplets in the parcel. The chemistry of individual droplets is not, in general, representative of the bulk (volume-weighted mean) cloud water sample. These differences, calculated to occur early in the parcel's lifetime, should have important consequences for chemical reactions such as aqueous phase sulfate production.

Twohy, C. H.↗

NASA NTRS1990

Proton irradiation of simple gas mixtures: Influence of irradiation parameters

In order to get information about the influence of irradiation parameters on radiolysis processes of astrophysical interest, methane gas targets were irradiated with 6.5 MeV protons at a pressure of 1 bar and room temperature. Yields of higher hydrocarbons like ethane or propane were found by analysis of irradiated gas samples using gas chromatography. The handling of the proton beam was of great experimental importance for determining the irradiation parameters. In a series of experiments current density of the proton beam and total absorbed energy were shown to have a large influence on the yields of produced hydrocarbons. Mechanistic interpretations of the results are given and conclusions are drawn with regard to the chemistry and the simulation of various astrophysical systems.

Sack, Norbert J.↗

NASA NTRS1990

Containerless processing of undercooled melts

All practical solidification processes involve some level of melt undercooling. Usually in bulk liquids crystallization is initiated at a heterogeneous nucleation site at low undercooling. The realization of appreciable levels of liquid undercooling requires some control over the kinetics of crystal nucleation. One level of control is available in containerless processing where the capability to melt and solidify samples without a container removes a major source of impurities and heterogeneous nucleation sites which can be effective in promoting large undercooling and in studying other potential nucleants. The microgravity environment offers a unique opportunity for containerless processing of large liquid samples with negligible melt disturbance and continuous temperature measurement throughout processing. Perhaps the most important potential for microgravity containerless processing lies in the significant structural control to develop distinct microstructures and metastable phases during solidification at high undercooling.

Perepezko, J. H.↗

NASA NTRS1991

On the estimation of climatological Z-R relationships

A statistical framework for climatological Z-R parameter estimation is developed and simulation experiments are conducted to examine sampling properties of the estimators. Both parametric and nonparametric models are considered. For parametric models, it is shown that Z-R parameters can be estimated by maximum likelihood, a procedure with optimal large sample properties. A general nonparametric framework for climatological Z-R estimation is also developed. Nonparametric procedures are attractive because of their flexibility in dealing with certain types of measurement errors common to radar data. Simulation experiments show that even under favorable assumptions on error characteristics of radar and raingages, large datasets are required to obtain accurate Z-R parameter estimates. Another important conclusion is that estimation results are generally quite sensitive to radar and raingage measurement thresholds. For fixed sample size, the simulation results can be used to provide quantitative assessments of the accuracy of Z-R model parameter estimates. These results are particularly useful for error analysis of precipitation products that are derived using climatological Z-R relations. One example is the large-area rainfall estimates derived using the height-area rainfall threshold (HART) technique.

Krajewski, Witold F.↗

NASA NTRS1998

A Satellite Infrared Technique for Diurnal Rainfall Variability Studies

Reliable information on the distribution of precipitation at high temporal resolution (<l hour) is essential for understanding the characteristics of convection in a region. Cloud-top infrared (IR) brightness temperatures from geostationary platforms have a weak physical connection to precipitation, however, their high sampling frequency makes them attractive in studying the temporal evolution of cloudiness and convection. On the other hand, microwave-based (MW) observations from lower sampling-frequency polar-orbiting platforms can provide a better physical connection to precipitating hydrometeors. A recent invention in rainfall estimation from a combination of these two sensors involves adjustment of IR estimates using co-existing MW-based precipitation data on a monthly basis. These techniques use the MW data to remove systematic errors in IR rain estimates, while retaining the high sampling frequency of IR observations (approximately every 15-30 minutes). Perhaps of even greater importance to climate and hydrometeorological applications is the separation of mesoscale convective systems into a portion of rain associated with deep convection (hereafter called convective precipitation), and to precipitation falling from more widespread anvil clouds. This current work focuses on estimation of tropical convective and stratiform rainfall. We attempt to answer fundamental questions, such as : is estimation of convective and stratiform precipitation from IR feasible? If so, how accurate can this be? What is the scale dependence of the IR algorithm's performance? To address these questions, quantitative comparisons are performed between coincident IR- and MW-based instantaneous rainfall estimates at the MW 85 Ghz resolution (-12.5 km). Our data set spans a three-month period (January to March, 1996) of MW and IR observations over northern South America (15N-15S and 35W-80W), which includes the Amazon river basin.

Anagnostou, Emmanouil↗

NASA NTRS2000

Measurements of Cosmogenic Nuclides in and their Significance for Samples Returned from Asteroids

Nuclear interactions of cosmic rays with matter produce cosmogenic nuclides (CNs). Ever since they were first measured nearly 50 years ago, cosmogenic nuclides have been used to infer the irradiation histories of terrestrial and extraterrestrial materials. Here we call for an extension of such measurements to samples returned from an asteroidal surface. The information gained in this way will be important for elucidating the evolution of the asteroidal surface. Additional information is contained in the original extended abstract.

Nishiizumi, K.↗

NASA NTRS2003

Determining Possible Building Blocks of the Earth

Introduction: One of the fundamental questions concerning the formation of the Earth is what is it made out of. The Earth appears to have condensed out of material from the solar nebula. We sample this "primitive" material in the form of chondritic meteorites. One of the most important constraints on possible building blocks for the Earth is the Earth#s oxygen iso-topic composition. Rocks from the Earth and Moon plot along a line (the terrestrial fractionation line) in diagrams of delta(sup 17)O (% relative to Standard Mean Ocean Water or SMOW) versus delta(sup 18)O (% relative to SMOW). Chondritic meteorites fall above and below this line. Distances from this line are given as Delta(sup 17)O (%) (= delta(sup 17)O - 0.52 x delta(sup 18)O).

Burbine, T. H.↗

NASA NTRS1997

Vibrational force alters mRNA expression in osteoblasts

Serum-deprived mouse osteoblastic (MC3T3E1) cells were subjected to a vibrational force modeled by NASA to simulate a space shuttle launch (7.83 G rms). The mRNA levels for eight genes were investigated to determine the effect of vibrational force on mRNA expression. The mRNA levels of two growth-related protooncogenes, c-fos and c-myc, were up-regulated significantly within 30 min after vibration, whereas those of osteocalcin as well as transforming growth factor-beta1 were decreased significantly within 3 h after vibration. No changes were detected in the levels of beta-actin, histone H4, or cytoplasmic phospholipase A2 after vibration. No basal levels of cyclooxygenase-2 expression were detected. In addition, the extracellular concentrations of prostaglandin E2 (PGE2), a potent autocrine/paracrine growth factor in bone, were not significantly altered after vibration most likely due to the serum deprivation state of the osteoblasts. In comparison with the gravitational launch profile, vibrational-induced changes in gene expression were greater both in magnitude and number of genes activated. Taken together, these data suggest that the changes in mRNA expression are due to a direct mechanical effect of the vibrational force on the osteoblast cells and not to changes in the local PGE2 concentrations. The finding that launch forces induce gene expression is of utmost importance since many of the biological experiments do not dampen vibrational loads on experimental samples. This lack of dampening of vibrational forces may partially explain why 1-G onboard controls sometimes do not reflect 1-G ground controls. These data may also suggest that scientists use extra ground controls that are exposed to launch forces, have these forces dampened on launched samples, or use facilities such as Biorack that provide an onboard 1-G centrufuge in order to control for space shuttle launch forces.

NASA Discipline Cell Biology↗

NASA NTRS2008

Using Optically Stimulated Electron Emission as an Inspection Method to Monitor Surface Contamination

During redesign of the Space Shuttle reusable solid rocket motor (RSRM), NASA amended the contract with ATK Launch Systems (then Morton Thiokol Inc.) with Change Order 966 to implement a contamination control and cleanliness verification method. The change order required: (1) A quantitative inspection method (2) A written record of actual contamination levels versus a known reject level (3) A method that is more sensitive than existing methods of visual and black light inspection. Black light inspection is only useful for inspection of contaminants that fluoresce near the 365 nm spectral line and is not useful for inspection of most silicones that will not produce strong fluorescence. Black light inspection conducted by a qualified inspector under controlled light is capable of detecting Conoco HD-2 grease in gross amounts and is very subjective due to operator sensitivity. Optically stimulated electron emission (OSEE), developed at the Materials and Process Laboratory at Marshall Space Flight Center (MSFC), was selected to satisfy Change Order 966. OSEE offers several important advantages over existing laboratory methods with similar sensitivity, e.g., spectroscopy and nonvolatile residue sampling, which provide turn around time, real time capability, and full coverage inspection capability. Laboratory methods require sample gathering and in-lab analysis, which sometimes takes several days to get results. This is not practical in a production environment. In addition, these methods do not offer full coverage inspection of the large components

Lingbloom, Mike S.↗

DOE OSTI2021

Visualization of shocked material instabilities using a fast-framing camera and XFEL four-pulse train

Many questions regarding dynamic materials could be answered by using time-resolved ultra-fast imaging techniques to characterize the physical and chemical behavior of materials in extreme conditions and their evolution on the nanosecond scale. In this work, we perform multi-frame phase-contrast imaging (PCI) of micro-voids in low density polymers under laser-driven shock compression. At the Matter in Extreme Conditions (MEC) Instrument at the Linac Coherent Light Source (LCLS), we used a train of four x-ray free electron laser (XFEL) pulses to probe the evolution of the samples. To visualize the void and shock wave interaction, here, we deployed the Icarus V2 detector to record up to four XFEL pulses, separated by 1-3 nanoseconds. In this work, we image elastic waves interacting with the micro-voids at a pressure of several GPa. Monitoring how the material’s heterogeneities, like micro-voids, dictate its response to a compressive wave is important for benchmarking the performances of inertial confinement fusion energy materials. For the first time in a single sample, we have combined an ultrafast x-ray framing camera and four XFEL pulse train to create an ultrafast movie of micro-void evolution under laser-driven shock compression. Eventually, we hope this technique will resolve the material density as it evolves dynamically under laser shock compression.

fusion↗