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At least 1,045 records · Page 58

AlMn Transition Edge Sensors for Advanced ACTPol

Advanced ACTPol (Adv ACT) will use an array of multichroic polarization sensitive AIMn transition edge sensor (TES) bolometers read out through time-division multiplexing. Aluminum doped with a low concentration of manganese can be deposited to a bulk film thickness for a more reliable superconducting critical temperature uniformity compared to thin bilayers. To build the TES, the AlMn alloy is deposited, over Nb wiring, to a specific thickness to set the TES normal resistance. The doping concentration of manganese coarsely defines the TES critical temperature, while a fine tuning is achieved by heating the deposited film to a specific temperature. The TES island is connected to the thermal bath via four silicon-nitride membranes, where their geometry defines the thermal conductance to the temperature of the bath. Lastly, the TES heat capacity is increased by addition of PdAu electrically connected to the AlMn film. Designs and performance characteristics of these AlMn TESs are presented for use in AdvACT.

Advanced ACTPol (AdvACT)↗

Optical Probe of the Superconducting Normal Mixed State in a Magnetic Penetration Thermometer

Using ultraviolet photon pulses, we have probed the internal behavior of a molybdenum-gold Magnetic Penetration Thermometer (MPT) that we designed for x-ray microcalorimetry. In this low-temperature detector, the diamagnetic response of a superconducting MoAu bilayer is used to sense temperature changes in response to absorbed photons. We have previously described an approximate model that explains the high responsivity of the detector to temperature changes as a consequence of a Meissner transition of the molybdenum-gold film in the magnetic field applied by the superconducting circuit used to bias the detector. We compare measurements of MPT heat capacity and thermal conductance, derived from UV photon pulse data, to our model predictions for the thermodynamic properties of the sensor and for the electron cooling obtained by quasiparticle recombination. Our data on electron cooling power is also relevant to the operation of other superconducting detectors, such as Microwave Kinetic Inductance Detectors.

superconductivity↗

Fabrication of X-ray Microcalorimeter Focal Planes Composed of Two Distinct Pixel Types

We develop superconducting transition-edge sensor (TES) microcalorimeter focal planes for versatility in meeting the specifications of X-ray imaging spectrometers, including high count rate, high energy resolution, and large field of view. In particular, a focal plane composed of two subarrays: one of fine pitch, high count-rate devices and the other of slower, larger pixels with similar energy resolution, offers promise for the next generation of astrophysics instruments, such as the X-ray Integral Field Unit Instrument on the European Space Agencys ATHENA mission. We have based the subarrays of our current design on successful pixel designs that have been demonstrated separately. Pixels with an all-gold X-ray absorber on 50 and 75 micron pitch, where the Mo/Au TES sits atop a thick metal heatsinking layer, have shown high resolution and can accommodate high count rates. The demonstrated larger pixels use a silicon nitride membrane for thermal isolation, thinner Au, and an added bismuth layer in a 250-sq micron absorber. To tune the parameters of each subarray requires merging the fabrication processes of the two detector types. We present the fabrication process for dual production of different X-ray absorbers on the same substrate, thick Au on the small pixels and thinner Au with a Bi capping layer on the larger pixels to tune their heat capacities. The process requires multiple electroplating and etching steps, but the absorbers are defined in a single-ion milling step. We demonstrate methods for integrating the heatsinking of the two types of pixel into the same focal plane consistent with the requirements for each subarray, including the limiting of thermal crosstalk. We also discuss fabrication process modifications for tuning the intrinsic transition temperature (T(sub c)) of the bilayers for the different device types through variation of the bilayer thicknesses. The latest results on these 'hybrid' arrays will be presented.

Terms—Arrays↗

Parametric Characterization of TES Detectors Under DC Bias

The X-ray integrated field unit (X-IFU) in European Space Agency's (ESA's) Athena mission will be the first high-resolution X-ray spectrometer in space using a large-format transition-edge sensor microcalorimeter array. Motivated by optimization of detector performance for X-IFU, we have conducted an extensive campaign of parametric characterization on transition-edge sensor (TES) detectors with nominal geometries and physical properties in order to establish sensitivity trends relative to magnetic field, dc bias on detectors, operating temperature, and to improve our understanding of detector behavior relative to its fundamental properties such as thermal conductivity, heat capacity, and transition temperature. These results were used for validation of a simple linear detector model in which a small perturbation can be introduced to one or multiple parameters to estimate the error budget for X-IFU. We will show here results of our parametric characterization of TES detectors and briefly discuss the comparison with the TES model.

X-ray Integral Field↗

In Situ Air Temperature and Humidity Measurements Over Diverse Land Covers in Greenbelt, Maryland, November 2013-November 2015

As our climate changes through time there is an ever-increasing need to quantify how and where it is changing so that mitigation strategies can be implemented. Urban areas have a disproportionate amount of warming due, in part, to the conductive properties of concrete and asphalt surfaces, surface albedo, heat capacity, lack of water, etc. that make up an urban environment. The NASA Climate Adaptation Science Investigation working group at Goddard Space Flight Center in Greenbelt, MD, conducted a study to collect temperature and humidity data at 15 min intervals from 12 sites at the center. These sites represent the major surface types at the center: asphalt, building roof, grass field, forest, and rain garden. The data show a strong distinction in the thermal properties of these surfaces at the center and the difference between the average values for the center compared to a local meteorological station. The data have been submitted to Oak Ridge National Laboratory Distributed Active Archive Center (ORNL-DAAC) for archival in comma separated value (csv) file format (Carroll et al.,2016) and can be found by following this link: http:daac.ornl.govcgi-bindsviewer.pl?ds_id1319.

Carroll, Mark L.↗

Thermophysical Properties of Cold and Vacuum Plasma Sprayed Cu-Cr-X Alloys, NiAl and NiCrAlY Coatings: Electrical and Thermal Conductivity, Thermal Diffusivity, and Total Hemispherical Emissivity - Part 1

This two-part paper reports the thermophysical properties of several cold and vacuum plasma sprayed monolithic Cu and Ni-based alloy coatings. Part I presents the electrical and thermal conductivity, thermal diffusivity, and total hemispherical emissivity data while Part II reports the specific heat capacity data for these coatings. Metallic copper alloys, stoichiometric NiAl and NiCrAlY coatings were fabricated by either the cold sprayed or the vacuum plasma spray deposition processes for thermal property measurements between 77 and 1223 K. The temperature dependencies of the thermal conductivities, thermal diffusivities, electrical conductivities and total hemispherical emissivities of these cold and vacuum sprayed monolithic coatings are reported in this paper. The electrical and thermal conductivity data correlate reasonably well for Cu-8%Cr-1%Al, Cu-23%Cr-5%Al and NiAl in accordance with the Wiedemann-Franz (WF) law although a better fit is obtained using the Smith-Palmer relationship. The Lorentz numbers determined from the WF law are close to the theoretical value.

Raj, S. V.↗

Heat Switches Providing Low-Activation Power and Quick-Switching Time for Use in Adiabatic Demagnetization Refrigerators

An adiabatic demagnetization refrigerator (ADR) is a solid-state cooler capable of achieving sub-Kelvin temperatures. It neither requires moving parts nor a density gradient in a working fluid making it ideal for use in space-based instruments. The flow of energy through the cooler is controlled by heat switches that allow heat transfer when on and isolate portions of the cooler when off. One type of switch uses helium gas as the switching medium. In the off state the gas is adsorbed in a getter thus breaking the thermal path through the switch. To activate the switch, the getter is heated to release helium into the switch body allowing it to complete the thermal path. A getter that has a small heat capacity and low thermal conductance to the body of the switch requires low-activation power. The cooler benefits from this in two ways: shorter recycle times and higher efficiency. We describe such a design here.

Kimball, Mark O.↗

Heat Switches Providing Low-Activation Power and Quick-Switching Time for Use in Cryogenic Multi-Stage Refrigerators

An adiabatic demagnetization refrigerator (ADR) is a solid-state cooler capable of achieving sub-Kelvin temperatures. It neither requires moving parts nor a density gradient in a working fluid making it ideal for use in space-based instruments. The flow of energy through the cooler is controlled by heat switches that allow heat transfer when on and isolate portions of the cooler when off. One type of switch uses helium gas as the switching medium. In the off state the gas is adsorbed in a getter thus breaking the thermal path through the switch. To activate the switch, the getter is heated to release helium into the switch body allowing it to complete the thermal path. A getter that has a small heat capacity and low thermal conductance to the body of the switch requires low-activation power. The cooler benefits from this in two ways: shorter recycle times and higher efficiency. We describe such a design here.

Kimball, Mark O.↗

Effects of Normal Metal Features on Superconducting Transition-Edge Sensors

In transition-edge sensors (TESs), the addition of normal metal stripes on top of the superconducting bilayer, perpendicular to the current direction, is known to globally alter the sensitivity of the resistance R to changes in temperature T and current I. Here, we describe measurements of the dependence of the TES current on magnetic field B, bath temperature and voltage bias in devices with various numbers of stripes. We show that the normal metal features have a profound effect on the appearance of localized regions of very large (T/R) dR/dT. We associate this with changes in the current distribution and corresponding changes in the oscillatory pattern of I (B). 140 μm TESs with no stripes are found to have a relatively smooth resistive transition and sufficiently low noise that the measured energy resolution is 1.6 eV for X-rays of 1.5 keV. The predicted energy resolution at 6 keV is better than 2 eV, once the heat capacity is optimized for these higher energies..

Wakeham, N. A.↗

Molecular Dynamics of ULTEM 9085 for 3D Manufacturing: Spectra, Thermodynamic Properties, and Shear Viscosity.

We present results of a molecular dynamic analysis of welding at the polymer-polymer interface. The analysis is performed for polyetherimide/ polycarbonate polymer blends. The work is motivated by the applications to 3D manufacturing in space. In the first part of the report, we discuss bulk and spectral characteristics of the amorphous polymer blends. The vibrational and infra-red spectra obtained using auto-correlation functions calculations in molecular dynamics are compared with the experimental spectra. The mechanical and thermal properties of the samples including heat capacity, bulk modulus, and thermal expansion coefficients are estimated and compared with experimental values. In the second part of the report, we discuss the result of molecular dynamical modeling of shear viscosity in a fully atomistic model of amorphous polymer blends with flat interface. The key result of the research is the demonstration of shear thinning behavior of the shear viscosity as a function of shear rate which is in good agreement with experimental data.

Luchinsky, Dmitry G.↗

Thermal Expansion from Stochastic Nonlinear Acoustic Fields

The methods of stochastic mechanics are applied to nonlinear acoustic fields generated by random acoustic radiation sources associated with oscillating lattice sites in nonlinear lattices. The assumption of stochastically independent zero-point and temperature-dependent acoustic fields leads to expressions of the thermodynamic internal and Helmholtz free energies per unit mass in terms of modal energies per unit mass that account for the nonlinearity of the propagation modes. The thermodynamic state functions canonically transform to the familiar results of a system of quantized, simple harmonic oscillators in the linear field limit. The thermal expansion coefficient, derived from the Helmholtz free energy per unit mass, is obtained as a sum of the zero-point modal nonlinearity parameters, weighted by temperature-dependent, modal heat capacities. The relationship is fully anharmonic, in contrast to commonly used quasi-harmonic models, and predicts with excellent agreement the experimentally observed null thermal expansion of vitreous silica at the ‘cross-over’ temperature corresponding to the balance between long wavelength modes that contribute negative nonlinearity parameters to the modal sum and short wavelength modes that contribute positive nonlinearity parameters.

Cantrell, John H., Jr.↗

Characterization of Thermal Protection Systems: An Analysis of Optical & Thermal Properties

Thermal Protection System Materials & thermal control coatings were characterized by a variety of methodologies including heat flow meter method (HFM), dynamic scanning calorimetry (DSC), fourier transform infrared spectroscopy (FTIR), and Ultra-Violet & Visible light spectroscopy (UV-VIS). Physical properties were measured to aid in the construction of thermal response models for a number a projects including MEDLI and MEDLI2. Comparing pre-flight predictions with actual flight data can allow for a reduction of margins and improve designs. The models enable design of TPS for flight missions and analysis of flight data to understand aerothermal environments experienced on the mission. This presentation reveals critical information: heat capacity (cp vs T), thermal conductivity ( vs T), and emissivity (E vs T) for Super Lightweight Ablative (SLA), Phenolic Impregnated Carbon Ablative (PICA-D), & Heatshield for Extreme Entry Environment Technology (HEEET). These properties were also measured for various thermal control coatings manufactured by AZ Technology. A portion of this work is incomplete and highlights questions to investigate in the future.

Cole, Brian↗

A survey of thermocouple anomalies: mechanisms, interpretation, and mitigation

Thermocouples (TCs) are a critical diagnostic sensor for high enthalpy environments including thermal protection systems (TPS) for atmospheric re-entry, hypersonic wind tunnels, and arc jet test facilities. They are used for both evaluating facility environmental conditions (enthalpy, heat flux) as well as for measuring in-situ material thermal response under test conditions (thermal conductivity, heat capacity, B’, etc.). Consequently, accurate TC measurements are fundamental for both material and facility verification and validation (V&V). However, a number of TC anomalies have been observed in both ground tests and flight instrumentation. These anomalies are caused via various coupling mechanisms: electrostatic gradients, temperature-dependent electrical shorts, radio pickup, magnetic induction, and pressure-dependent leaks. All of these mechanisms can, if unaddressed, result in obviously compromised results or worse, non-physical measurements which appear reasonable. This work will survey known anomaly mechanisms and discuss ongoing efforts to quantify and mitigate anomaly mechanisms including anomaly modeling, diagnostics, and new TC designs/development.

thermocouple anomalies↗

Electromagnetic Thermocouple (TC) Anomaly Mechanisms During Atmospheric Entry

Thermocouples (TCs) are a critical diagnostic sensor for high enthalpy environments including Thermal Protection Systems (TPS) for atmospheric entry, hypersonic wind tunnels, and arc jet test facilities. They are used for both evaluating facility environmental conditions (enthalpy, and heat flux) as well as for measuring in-situ material thermal response under test conditions (thermal conductivity, heat capacity, etc.). Consequently, accurate TC measurements are fundamental for both material and facility Verification and Validation (V&V). However, a number of electromagnetic TC anomalies have been observed in both ground tests and flight instrumentations. These anomalies are caused via various coupling mechanisms: surface voltage coupling, Hall effect currents, and RF rectification. All of these mechanisms can, if unaddressed, result in obviously compromised results or worse, non-physical measurements which appear reasonable. This talk will provide an overview of each of these anomaly mechanisms and discuss ongoing efforts to quantify and mitigate them.

Magnus Haw↗

A Survey of Thermocouple Anomalies: Mechanisms, Interpretation, and Mitigation

Thermocouples (TCs) are a critical diagnostic sensor for high enthalpy environments including thermal protection systems (TPS) for atmospheric re-entry, hypersonic wind tunnels, and arc jet test facilities. They are used for both evaluating facility environmental conditions (enthalpy, heat flux) as well as for measuring in-situ material thermal response under test conditions (thermal conductivity, heat capacity, B’, etc.). Consequently, accurate TC measurements are fundamental for both material and facility verification and validation (V&V). However, a number of TC anomalies have been observed in both ground tests and flight instrumentation. These anomalies are caused via various coupling mechanisms: electrostatic gradients, temperature-dependent electrical shorts, radio pickup, magnetic induction, and pressure-dependent leaks. All of these mechanisms can, if unaddressed, result in obviously compromised results or worse, non-physical measurements which appear reasonable. This work will survey known anomaly mechanisms and discuss ongoing efforts to quantify and mitigate anomaly mechanisms including anomaly modeling, diagnostics, and new TC designs/development.

Thermocouple Anomalies↗

Fine Optimization of TES Design for the X-IFU Instrument on ATHENA

The X-ray Integral Field Unit (X-IFU) instrument on the Advanced Telescope for High ENergy Astrophysics (ATHENA) is baselined to have 3168 transition-edge sensor (TES) microcalorimeter pixels. These pixels will be DC biased and readout using time division multiplexing. We recently reported a demonstration of the required pixel and readout performance in 252 pixels from a 1 kilo-pixel array (e.g. 2.16 eV resolution for 6.9 keV X-rays). Having achieved the required performance, the 50um square TES design in this demonstration array is considered the baseline pixel design for X-IFU. However, by making small adjustments to the TES design, we may be able to make small but consequential improvements to the instrument performance, while staying within the many constraints of the X-IFU requirements. In this presentation, we will show results from newly fabricated devices with subtle changes from the baseline TES design to further optimize the performance for X-IFU. We will discuss optimizing the TES sheet resistance, normal metal features, X-ray absorber attachment points, TES aspect ratio, and heat capacity. These minor design changes can have significant effects on thermo-electric time constants, thermal fluctuation noise, resistive transition shape and uniformity, and non-linearity of X-ray event pulses. In addition, full characterization of these new TES designs allows greater understanding of the relevant physics within the TES and gives routes for further optimization.

Nick Wakeham↗

Inverse Estimation of Mars 2020 Entry Aeroheating Environments Using MEDLI2 Flight Data

The Mars Entry, Descent, and Landing Instrumentation 2 (MEDLI2) sensor suite collected heating and pressure data during entry into Mars' atmosphere of the Mars 2020 Perseverance rover. MEDLI2 included thermocouples, heat flux sensors, and pressure transducers on both the heatshield and the backshell. This paper covers the inverse estimation of heatshield and backshell surface heating based on the MEDLI2 Instrumented Sensor Plugs (MISPs), a network of thermocouples embedded in thermal protection system plugs across the aeroshell. Monte Carlo analysis was conducted to assess the sensitivity of the surface heat rate and temperature to uncertainties in thermocouple depth and material properties such as density, specific heat capacity, and thermal conductivity. Data from each MISP was also used to estimate the local time of transition from laminar to turbulent flow at each plug location.

Hannah S Alpert↗

LIRA: Probing the Lunar Surface for Resources.

The thermal, compositional and electrical properties of the lunar regolith, such as the triboelectric properties of lunar dust, the volatile content and the thermophysical properties of the polar regolith are essential to understand from a scientific perspective as well as for resource extraction and hazard mitigation. Understanding these properties specifically requires in situ measurement, as these properties are inherent in the ambient environment. With the Lunar In situ Regolith Analyzer (LIRA) we will combine mature surface sensor technologies from previous spacecraft missions (TECP) with new sensors (ClO4- ) and battery capability to achieve a compact in situ analysis package. The surface instrument suite is adapted for lunar conditions from a sensor developed as part of the Microscopy, Electrochemistry, and Conductivity Analyzer (MECA) instrument on the 2007 Mars Phoenix mission, as well as supplemental sensors. • The Thermal and Electrical Conductivity Probe (TECP), flown on MECA/Phoenix, which measures heat capacity, thermal conductivity, electrical resistance, and electrical permittivity between needles inserted into the soil. The TECP also measured atmospheric humidity, a capability that will be retained to search for subsurface H2O ice. The Mars TECP weighed 100-gram and by definition was at TRL 9. The lunar version (LIRA) is TRL 4. • The Perchlorate (ClO4) sensor is based on the fluorescence property of perchlorate (Mg, Fe, Na). We added a light source to excite the perchlorate (ClO4) and a photo diode to collect the emission wavelength. A sun-shade over the photo diode blocks out the ambient light during day light hours. The unifying goal of LIRA is to deliver a complete, integrated experiment suite that investigates properties that must be measured in situ, and provides the capability to power the suite at night or in PSRs, as well as a means to simulate aspects of the diurnal transition by delivering an optical pulse to the surface with intensity comparable to sunlight. We describe the scientific context of LIRA, touching on the electrical state of the near-surface environment, the thermal properties of the undisturbed regolith, and the distribution, geochemistry, and mobility of water. We also address the exploration implications of the work, examining hazards and resources in the context of strategic knowledge gaps (SKGs).

Heather Smith↗